#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/90/2209051.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209051_Fobs loop_ _publ_author_name 'Yang, E.' 'Zheng, Yi' 'Chen, Gu-Yong' _publ_section_title ; catena-Poly[[(di-2-pyridylamine-\k^2^N,N')copper(II)]-\m-benzene-1,4-dicarboxylato-\k^4^O,O':O'',O'''] ; _journal_coeditor_code XU2023 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1079 _journal_page_last m1080 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.066 _cell_angle_gamma 90.000 _cell_length_a 7.6403 _cell_length_b 21.1030 _cell_length_c 9.8015 _exptl_crystal_F_000 811.81 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file xu2023Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 257.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 66522.42 65371.85 892.24 o 3 0 0 352.57 400.01 11.72 o 4 0 0 21299.62 21998.22 228.92 o 5 0 0 61.99 73.24 29.00 o 6 0 0 841.50 846.69 27.74 o 7 0 0 129.74 175.90 28.15 o 8 0 0 839.13 807.73 58.21 o 9 0 0 0.97 41.91 23.28 o 2 1 0 365.18 435.76 7.62 o 3 1 0 11936.33 12834.83 66.70 o 4 1 0 64.22 65.93 4.85 o 5 1 0 1159.71 1113.53 41.82 o 6 1 0 4.79 19.22 5.40 o 7 1 0 52.19 35.78 9.23 o 8 1 0 66.96 52.01 16.90 o 9 1 0 313.37 387.99 33.19 o 1 2 0 803.12 875.38 11.79 o 2 2 0 14369.77 15143.27 64.81 o 3 2 0 21.60 20.94 4.60 o 4 2 0 268.18 368.32 9.66 o 5 2 0 356.59 359.71 11.18 o 6 2 0 35.34 46.90 5.67 o 7 2 0 77.10 61.04 12.90 o 8 2 0 51.74 51.79 16.79 o 9 2 0 13.01 19.68 11.79 o 1 3 0 19560.06 19453.90 101.54 o 2 3 0 3647.49 4035.62 21.02 o 3 3 0 3733.07 3387.17 23.39 o 4 3 0 1943.06 2323.82 25.20 o 5 3 0 2048.63 2086.94 24.35 o 6 3 0 251.39 217.29 10.43 o 7 3 0 1994.35 2079.65 46.31 o 8 3 0 9.15 21.02 11.65 o 9 3 0 104.43 64.10 17.01 o 0 4 0 9979.57 9979.52 187.65 o 1 4 0 2420.71 2725.07 16.21 o 2 4 0 2609.65 2089.57 15.57 o 3 4 0 7.92 33.78 7.91 o 4 4 0 14362.78 14501.67 129.68 o 5 4 0 5.94 12.05 2.65 o 6 4 0 711.91 626.08 26.39 o 7 4 0 400.43 387.05 20.22 o 8 4 0 2011.63 2195.82 78.35 o 9 4 0 76.81 62.50 19.10 o 1 5 0 6854.16 6886.06 36.15 o 2 5 0 254.69 260.94 7.86 o 3 5 0 2209.89 2177.07 20.98 o 4 5 0 691.73 752.75 16.15 o 5 5 0 1602.79 1665.94 40.48 o 6 5 0 962.58 907.05 19.52 o 7 5 0 1408.92 1411.17 52.49 o 8 5 0 1.59 24.41 15.03 o 9 5 0 195.25 155.74 26.23 o 0 6 0 530.11 616.17 27.31 o 1 6 0 21.17 24.06 4.25 o 2 6 0 1217.00 1236.66 23.22 o 3 6 0 1047.82 1153.39 19.09 o 4 6 0 301.07 287.61 11.37 o 5 6 0 43.97 33.38 5.30 o 6 6 0 1996.04 2082.74 32.82 o 7 6 0 4.68 7.05 5.53 o 8 6 0 195.33 186.33 19.92 o 9 6 0 3.72 17.32 10.76 o 1 7 0 4537.08 4300.98 31.12 o 2 7 0 11.96 23.25 2.91 o 3 7 0 5696.47 5580.01 47.13 o 4 7 0 22.04 27.43 5.81 o 5 7 0 2286.61 2427.19 33.74 o 6 7 0 388.17 341.85 15.76 o 7 7 0 1939.34 1992.23 52.43 o 8 7 0 5.52 4.31 8.25 o 9 7 0 757.37 827.84 76.41 o 0 8 0 22109.62 23059.54 156.97 o 1 8 0 1021.86 1095.98 13.88 o 2 8 0 7776.36 7655.23 42.91 o 3 8 0 473.54 478.02 15.45 o 4 8 0 7949.96 8282.09 65.68 o 5 8 0 504.26 499.82 13.29 o 6 8 0 1156.46 1186.59 31.95 o 7 8 0 16.21 19.50 6.81 o 8 8 0 1080.90 1184.41 77.46 o 9 8 0 78.95 74.72 31.96 o 1 9 0 2309.19 2317.75 26.23 o 2 9 0 500.99 637.25 11.53 o 3 9 0 1062.78 1078.09 16.83 o 4 9 0 12.79 5.66 4.33 o 5 9 0 3.81 8.36 4.56 o 6 9 0 25.96 24.63 7.27 o 7 9 0 1.33 13.11 3.55 o 8 9 0 147.04 142.65 18.23 o 9 9 0 7.70 33.87 27.73 o 0 10 0 415.13 315.53 14.49 o 1 10 0 142.73 139.61 7.45 o 2 10 0 2042.21 2019.81 17.20 o 3 10 0 418.40 391.83 10.90 o 4 10 0 1367.24 1336.47 15.33 o 5 10 0 493.23 500.28 20.56 o 6 10 0 1362.76 1524.80 39.63 o 7 10 0 265.68 278.09 26.51 o 8 10 0 49.07 40.23 10.22 o 9 10 0 46.58 44.87 31.33 o 1 11 0 9549.92 9996.24 64.97 o 2 11 0 2057.07 2288.14 74.08 o 3 11 0 4836.81 4785.79 43.22 o 4 11 0 535.46 541.13 17.92 o 5 11 0 1497.59 1496.53 26.27 o 6 11 0 600.21 497.13 32.04 o 7 11 0 832.41 878.29 35.58 o 8 11 0 0.66 13.83 8.81 o 9 11 0 168.55 259.08 50.17 o 0 12 0 5826.18 5685.14 87.63 o 1 12 0 0.94 11.00 27.92 o 2 12 0 796.96 639.13 9.90 o 3 12 0 217.75 170.59 6.25 o 4 12 0 3087.88 3104.61 33.77 o 5 12 0 6.46 9.33 5.96 o 6 12 0 477.88 489.82 27.58 o 7 12 0 62.06 79.95 18.97 o 8 12 0 121.37 148.36 20.96 o 1 13 0 2287.12 2556.48 32.15 o 2 13 0 68.60 75.46 13.55 o 3 13 0 592.14 593.43 21.03 o 4 13 0 56.77 33.85 8.47 o 5 13 0 62.57 55.67 10.86 o 6 13 0 2.54 6.46 9.85 o 7 13 0 36.62 17.01 9.56 o 8 13 0 44.44 36.32 13.86 o 0 14 0 793.83 661.69 31.62 o 1 14 0 1.94 11.45 4.34 o 2 14 0 3279.22 3481.74 42.10 o 3 14 0 435.33 403.09 16.96 o 4 14 0 451.68 423.94 27.00 o 5 14 0 7.21 6.66 7.79 o 6 14 0 1512.92 1572.87 57.63 o 7 14 0 51.27 32.90 12.40 o 8 14 0 610.15 602.75 36.48 o 1 15 0 680.21 602.00 22.88 o 2 15 0 7.54 5.28 4.00 o 3 15 0 3244.34 3293.10 46.75 o 4 15 0 0.73 3.86 7.12 o 5 15 0 3016.42 3140.08 83.88 o 6 15 0 146.72 126.27 16.06 o 7 15 0 1485.02 1515.86 57.19 o 8 15 0 47.69 33.41 13.34 o 0 16 0 27.86 30.32 19.05 o 1 16 0 31.51 25.68 5.45 o 2 16 0 20.93 18.58 4.96 o 3 16 0 1.06 2.90 4.84 o 4 16 0 38.86 26.99 12.40 o 5 16 0 379.64 332.46 21.52 o 6 16 0 329.52 396.37 34.09 o 7 16 0 33.55 31.69 9.37 o 8 16 0 401.24 482.58 126.37 o 1 17 0 5.51 18.03 4.02 o 2 17 0 27.26 23.10 8.17 o 3 17 0 49.03 44.54 8.24 o 4 17 0 116.78 98.14 16.50 o 5 17 0 185.60 198.24 21.54 o 6 17 0 23.27 27.15 7.77 o 7 17 0 120.24 87.49 14.13 o 0 18 0 16.51 14.75 7.28 o 1 18 0 135.17 139.21 12.76 o 2 18 0 399.31 335.07 16.47 o 3 18 0 697.06 674.21 21.44 o 4 18 0 65.19 59.56 19.28 o 5 18 0 673.49 668.16 31.14 o 6 18 0 222.70 270.19 32.66 o 7 18 0 94.41 55.45 11.78 o 1 19 0 1524.71 1492.47 30.31 o 2 19 0 1251.12 1227.90 30.86 o 3 19 0 1119.31 1077.91 34.02 o 4 19 0 67.83 70.21 13.06 o 5 19 0 412.40 419.96 31.13 o 6 19 0 171.15 152.22 19.92 o 7 19 0 530.82 579.32 42.37 o 0 20 0 533.74 505.02 37.40 o 1 20 0 776.51 786.41 23.51 o 2 20 0 1671.41 1714.32 43.58 o 3 20 0 38.56 26.93 9.69 o 4 20 0 170.96 188.23 18.84 o 5 20 0 46.27 24.95 8.96 o 6 20 0 207.66 218.46 31.48 o 1 21 0 81.75 89.31 13.26 o 2 21 0 59.24 51.40 9.79 o 3 21 0 2.50 11.39 7.29 o 4 21 0 151.46 119.79 13.78 o 5 21 0 3.64 0.95 12.25 o 6 21 0 80.53 87.55 20.50 o 0 22 0 1646.21 1682.57 73.92 o 1 22 0 164.86 170.79 16.75 o 2 22 0 625.81 680.79 23.53 o 3 22 0 10.51 19.33 4.26 o 4 22 0 755.52 841.32 36.36 o 5 22 0 0.91 8.74 11.19 o 1 23 0 615.72 652.27 28.86 o 2 23 0 29.26 27.07 8.65 o 3 23 0 629.32 656.11 33.06 o 4 23 0 4.10 17.67 8.65 o 5 23 0 314.91 416.86 34.16 o 0 24 0 0.71 53.33 26.14 o 1 24 0 88.27 29.41 9.75 o 2 24 0 26.20 18.44 6.72 o 3 24 0 139.77 115.37 22.15 o 4 24 0 3.00 13.68 9.32 o 1 25 0 460.53 400.08 24.64 o 2 25 0 0.12 13.33 7.01 o 3 25 0 123.83 146.54 27.97 o 4 25 0 0.40 22.01 17.87 o 0 26 0 77.32 52.67 274.43 o 1 26 0 12.92 22.83 8.04 o 2 26 0 21.89 30.64 8.74 o 3 26 0 0.20 18.97 9.06 o 1 27 0 71.76 48.44 13.81 o -9 1 1 278.37 279.52 31.36 o -8 1 1 334.43 310.41 32.77 o -7 1 1 313.17 298.77 39.58 o -6 1 1 506.32 483.25 14.36 o -5 1 1 609.21 538.68 16.31 o -4 1 1 2651.55 2821.68 29.16 o -3 1 1 987.74 967.23 18.24 o -2 1 1 179.33 123.81 6.57 o -1 1 1 3735.74 3869.19 23.62 o 1 1 1 2176.25 2131.59 11.93 o 2 1 1 34003.70 33717.03 306.73 o 3 1 1 2498.50 2485.46 17.47 o 4 1 1 23961.23 25688.79 163.54 o 5 1 1 387.59 364.74 12.41 o 6 1 1 3550.80 3606.66 52.04 o 7 1 1 579.05 561.19 31.24 o 8 1 1 1276.84 1274.15 54.26 o 9 1 1 147.37 91.41 26.67 o -9 2 1 47.64 70.84 30.69 o -8 2 1 529.97 551.45 31.58 o -7 2 1 160.11 134.01 15.73 o -6 2 1 716.06 688.53 16.39 o -5 2 1 1527.17 1510.04 23.64 o -4 2 1 5872.14 6014.30 48.31 o -3 2 1 1537.07 1353.69 22.99 o -2 2 1 18.20 52.24 4.82 o -1 2 1 15191.38 14901.14 92.69 o 1 2 1 6739.97 6591.55 32.74 o 2 2 1 6962.65 8153.28 41.42 o 3 2 1 7961.22 7812.81 37.31 o 4 2 1 216.13 153.15 6.74 o 5 2 1 3805.83 3862.94 46.99 o 6 2 1 563.10 569.70 22.53 o 7 2 1 3832.68 3826.15 81.61 o 8 2 1 313.30 216.82 27.73 o 9 2 1 425.39 424.98 35.96 o -9 3 1 115.34 159.77 26.40 o -8 3 1 125.18 111.22 17.05 o -7 3 1 4.91 4.04 10.82 o -6 3 1 207.12 192.75 10.95 o -5 3 1 918.45 947.63 14.64 o -4 3 1 6039.17 6726.22 61.47 o -3 3 1 1952.30 2023.58 18.08 o -2 3 1 2288.51 2245.91 16.54 o -1 3 1 2615.28 2603.82 31.10 o 0 3 1 98.55 85.21 2.79 o 1 3 1 2805.87 3296.47 21.46 o 2 3 1 3778.14 4545.58 26.43 o 3 3 1 90.46 68.19 3.17 o 4 3 1 176.50 132.59 4.66 o 5 3 1 54.51 59.95 5.30 o 6 3 1 4.03 7.75 4.83 o 7 3 1 37.00 34.51 15.81 o 8 3 1 1042.24 1116.81 50.11 o 9 3 1 9.52 -3.79 10.27 o -9 4 1 15.71 2.56 9.76 o -8 4 1 40.46 36.06 9.09 o -7 4 1 147.81 131.09 10.65 o -6 4 1 17.15 21.07 5.43 o -5 4 1 10.73 9.97 4.31 o -4 4 1 4.05 -1.99 6.77 o -3 4 1 9.36 1.71 3.83 o -2 4 1 76.66 111.39 4.27 o -1 4 1 796.55 832.73 12.03 o 0 4 1 14670.90 15902.15 117.14 o 1 4 1 627.60 726.70 12.64 o 2 4 1 336.15 418.04 9.17 o 3 4 1 2873.92 3210.08 24.57 o 4 4 1 48.12 47.28 4.02 o 5 4 1 18.56 15.92 2.97 o 6 4 1 1366.71 1320.40 28.79 o 7 4 1 27.63 13.89 8.97 o 8 4 1 42.28 28.28 12.94 o 9 4 1 50.87 15.15 11.73 o -9 5 1 52.79 49.80 14.60 o -8 5 1 442.88 425.29 42.25 o -7 5 1 1225.19 1195.83 31.83 o -6 5 1 1155.85 1254.92 45.33 o -5 5 1 1003.85 959.00 20.60 o -4 5 1 2053.40 1932.19 30.00 o -3 5 1 3099.84 2868.16 29.57 o -2 5 1 1867.01 1712.54 12.08 o -1 5 1 1492.16 1367.98 20.89 o 0 5 1 3674.54 3732.21 26.16 o 1 5 1 5314.67 5372.20 39.56 o 2 5 1 14.21 68.47 5.36 o 3 5 1 850.88 745.65 13.97 o 4 5 1 711.46 546.63 14.08 o 5 5 1 522.69 527.25 18.22 o 6 5 1 3211.77 3365.87 52.71 o 7 5 1 237.42 231.64 16.59 o 8 5 1 1329.57 1404.08 65.63 o 9 5 1 51.99 48.90 13.34 o -9 6 1 186.84 197.28 46.78 o -8 6 1 1167.90 1143.36 38.26 o -7 6 1 1498.93 1501.76 43.05 o -6 6 1 62.70 70.43 9.40 o -5 6 1 3186.81 3514.89 52.40 o -4 6 1 1634.07 1536.98 40.27 o -3 6 1 7997.58 8589.11 57.45 o -2 6 1 90.60 190.65 8.03 o -1 6 1 7671.07 7609.00 47.04 o 0 6 1 4239.20 4241.83 29.50 o 1 6 1 15.38 32.29 3.76 o 2 6 1 686.65 563.00 16.28 o 3 6 1 8620.31 9207.19 54.18 o 4 6 1 2291.79 2377.31 26.96 o 5 6 1 307.50 279.68 11.46 o 6 6 1 234.01 207.86 14.14 o 7 6 1 2646.18 2625.29 65.12 o 8 6 1 270.39 296.73 27.50 o 9 6 1 977.87 860.65 77.05 o -9 7 1 94.37 102.66 34.71 o -8 7 1 18.16 21.83 7.20 o -7 7 1 13.11 18.77 5.23 o -6 7 1 489.40 550.27 22.89 o -5 7 1 12.29 7.92 6.83 o -4 7 1 489.19 465.97 13.63 o -3 7 1 230.23 308.20 9.59 o -2 7 1 8.23 16.66 2.45 o -1 7 1 80.39 45.45 5.74 o 0 7 1 1314.70 1364.44 22.54 o 1 7 1 145.57 98.55 5.37 o 2 7 1 983.46 1255.70 19.85 o 3 7 1 347.57 369.72 13.89 o 4 7 1 224.09 184.32 8.06 o 5 7 1 1.52 9.51 3.09 o 6 7 1 273.82 257.55 17.26 o 7 7 1 113.81 113.17 11.44 o 8 7 1 487.68 468.85 25.69 o 9 7 1 9.79 10.16 12.91 o -9 8 1 138.69 66.68 29.00 o -8 8 1 3.78 2.41 5.25 o -7 8 1 190.81 194.17 14.69 o -6 8 1 1237.11 1281.79 29.60 o -5 8 1 2082.04 2167.21 31.83 o -4 8 1 25.40 36.44 6.17 o -3 8 1 541.87 568.85 10.79 o -2 8 1 126.11 104.16 6.46 o -1 8 1 2826.69 3074.68 20.73 o 0 8 1 349.79 411.74 13.62 o 1 8 1 2574.34 2606.57 22.78 o 2 8 1 89.03 74.27 5.67 o 3 8 1 102.19 61.82 5.03 o 4 8 1 139.46 115.05 6.70 o 5 8 1 392.62 370.22 15.04 o 6 8 1 147.54 159.48 13.03 o 7 8 1 2.16 10.68 6.24 o 8 8 1 77.16 43.69 9.87 o 9 8 1 12.71 20.32 18.42 o -9 9 1 165.67 131.24 46.57 o -8 9 1 210.30 216.03 25.57 o -7 9 1 1529.78 1493.45 53.91 o -6 9 1 48.90 43.14 7.58 o -5 9 1 783.48 774.02 24.28 o -4 9 1 1158.06 1096.67 19.11 o -3 9 1 5136.26 5162.21 41.43 o -2 9 1 6201.11 6784.77 61.91 o -1 9 1 4381.63 4522.45 25.67 o 0 9 1 14388.25 15306.20 75.23 o 1 9 1 4605.75 4718.03 35.65 o 2 9 1 13749.52 14316.33 121.38 o 3 9 1 1355.84 1323.09 19.79 o 4 9 1 5292.03 5658.60 49.87 o 5 9 1 523.19 518.78 19.34 o 6 9 1 2244.20 2361.32 43.67 o 7 9 1 33.12 20.01 5.29 o 8 9 1 588.98 532.48 36.36 o 9 9 1 53.42 44.45 24.98 o -9 10 1 2.03 15.03 15.24 o -8 10 1 425.13 480.57 51.01 o -7 10 1 40.28 27.71 16.42 o -6 10 1 943.19 911.66 20.79 o -5 10 1 375.89 352.23 17.07 o -4 10 1 4655.13 4821.88 60.22 o -3 10 1 21.33 67.94 6.57 o -2 10 1 1841.22 1797.04 25.08 o -1 10 1 2249.89 2000.18 19.01 o 0 10 1 4957.67 4905.79 44.08 o 1 10 1 1812.84 1643.89 20.29 o 2 10 1 98.73 29.37 9.49 o 3 10 1 4833.08 4903.02 46.48 o 4 10 1 425.10 406.26 15.65 o 5 10 1 1358.05 1382.24 25.88 o 6 10 1 13.86 14.09 6.62 o 7 10 1 911.45 953.56 37.90 o 8 10 1 80.44 43.75 17.59 o 9 10 1 64.17 77.26 31.54 o -9 11 1 9.86 24.55 23.28 o -8 11 1 33.61 25.76 14.73 o -7 11 1 66.78 60.11 14.79 o -6 11 1 83.58 78.40 10.77 o -5 11 1 1.99 3.21 4.68 o -4 11 1 149.47 137.24 9.90 o -3 11 1 35.07 41.94 5.10 o -2 11 1 120.77 103.13 10.74 o -1 11 1 661.85 676.61 11.21 o 0 11 1 355.53 339.31 12.23 o 1 11 1 101.03 130.96 7.36 o 2 11 1 1.91 6.85 3.23 o 3 11 1 19.47 21.25 5.39 o 4 11 1 252.67 268.53 12.18 o 5 11 1 309.22 291.72 14.46 o 6 11 1 3.35 17.25 8.07 o 7 11 1 55.10 48.85 22.76 o 8 11 1 178.09 179.64 28.08 o -8 12 1 202.88 195.70 24.62 o -7 12 1 5.07 6.88 9.74 o -6 12 1 776.05 847.08 33.08 o -5 12 1 133.78 155.89 15.12 o -4 12 1 98.50 141.77 19.05 o -3 12 1 27.83 32.42 7.45 o -2 12 1 547.95 551.49 18.65 o -1 12 1 683.10 684.02 10.08 o 0 12 1 115.36 92.16 9.22 o 1 12 1 1925.18 1873.36 26.98 o 2 12 1 699.61 698.19 18.04 o 3 12 1 1405.02 1408.36 23.23 o 4 12 1 578.00 543.71 18.38 o 5 12 1 736.56 797.12 24.53 o 6 12 1 157.99 153.93 20.24 o 7 12 1 95.69 89.10 11.56 o 8 12 1 30.65 28.97 28.89 o -8 13 1 236.44 248.80 32.19 o -7 13 1 1269.69 1290.49 51.69 o -6 13 1 67.81 78.99 14.26 o -5 13 1 1091.67 1088.52 27.97 o -4 13 1 619.85 575.05 43.57 o -3 13 1 2659.76 2661.77 42.54 o -2 13 1 767.38 714.76 23.20 o -1 13 1 180.93 82.99 4.29 o 0 13 1 2843.40 2768.42 31.65 o 1 13 1 4081.87 4121.32 42.51 o 2 13 1 3980.81 4022.35 39.66 o 3 13 1 829.79 818.93 22.33 o 4 13 1 2068.79 2079.65 48.33 o 5 13 1 495.07 489.79 32.89 o 6 13 1 1558.25 1498.83 54.91 o 7 13 1 246.03 274.71 23.41 o 8 13 1 176.07 152.99 26.28 o -8 14 1 189.83 191.68 25.51 o -7 14 1 19.38 34.95 9.55 o -6 14 1 557.26 642.14 32.09 o -5 14 1 1370.69 1433.92 34.98 o -4 14 1 260.53 274.20 20.88 o -3 14 1 1030.87 1055.65 23.27 o -2 14 1 622.16 632.96 22.30 o -1 14 1 2556.83 2598.26 28.69 o 0 14 1 834.31 768.40 16.75 o 1 14 1 1122.33 1093.85 19.24 o 2 14 1 47.75 39.26 5.90 o 3 14 1 902.89 888.38 20.61 o 4 14 1 2837.48 2987.50 64.41 o 5 14 1 559.92 533.81 31.53 o 6 14 1 525.94 526.79 28.91 o 7 14 1 559.34 556.33 37.55 o 8 14 1 385.71 371.77 60.22 o -8 15 1 17.28 5.66 10.07 o -7 15 1 1.41 12.18 7.87 o -6 15 1 47.50 57.31 15.11 o -5 15 1 155.16 172.19 14.65 o -4 15 1 58.54 55.01 12.42 o -3 15 1 0.17 0.12 6.51 o -2 15 1 290.05 279.67 13.32 o -1 15 1 44.86 34.47 18.97 o 0 15 1 171.94 169.71 10.18 o 1 15 1 90.33 71.61 10.73 o 2 15 1 1224.49 1193.32 31.28 o 3 15 1 239.00 239.60 20.38 o 4 15 1 175.68 187.22 22.12 o 5 15 1 624.59 584.70 29.42 o 6 15 1 115.02 117.80 18.77 o 7 15 1 24.86 33.22 13.01 o 8 15 1 3.41 23.82 9.35 o -8 16 1 381.11 418.63 36.73 o -7 16 1 141.95 160.26 22.67 o -6 16 1 721.32 738.67 37.04 o -5 16 1 81.77 74.34 12.82 o -4 16 1 858.82 873.75 25.68 o -3 16 1 1200.83 1289.49 45.31 o -2 16 1 667.29 663.35 19.95 o -1 16 1 3414.63 3592.47 43.22 o 0 16 1 366.88 343.01 12.32 o 1 16 1 756.74 765.60 18.52 o 2 16 1 2531.56 2660.00 38.57 o 3 16 1 612.42 584.35 24.96 o 4 16 1 233.12 246.02 21.29 o 5 16 1 111.19 111.24 17.92 o 6 16 1 580.33 561.65 40.69 o 7 16 1 422.43 445.74 41.30 o -7 17 1 1007.19 1117.63 55.54 o -6 17 1 367.59 369.16 27.89 o -5 17 1 94.23 107.54 12.37 o -4 17 1 691.50 699.86 24.60 o -3 17 1 1660.29 1699.28 39.38 o -2 17 1 260.92 247.87 17.01 o -1 17 1 41.12 38.16 6.81 o 0 17 1 75.82 70.51 7.27 o 1 17 1 552.97 539.45 22.31 o 2 17 1 791.30 808.82 26.15 o 3 17 1 162.31 162.01 13.65 o 4 17 1 56.00 65.10 10.50 o 5 17 1 1107.19 1113.70 57.80 o 6 17 1 278.94 280.91 23.91 o 7 17 1 119.25 141.25 27.87 o -7 18 1 223.24 289.32 25.41 o -6 18 1 592.71 628.29 33.28 o -5 18 1 1.41 13.66 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