#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/91/2209128.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209128_Fobs loop_ _publ_author_name 'You, Zhong-Lu' _publ_section_title ; Aqua{2-[2-(2-hydroxyethylamino)ethyliminomethyl]-4-nitrophenolato}copper(II) perchlorate ; _journal_coeditor_code CI2063 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1216 _journal_page_last m1218 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.488 _cell_angle_gamma 90.000 _cell_length_a 19.5519 _cell_length_b 11.8592 _cell_length_c 14.6578 _exptl_crystal_F_000 1768.00 _reflns_d_resolution_high 0.8110 _[local]_cod_data_source_file ci2063Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CI2063 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 888.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 40525.92 47480.16 532.79 o 4 0 0 4.62 -5.61 8.31 o 6 0 0 31611.18 35226.59 406.05 o 8 0 0 4942.58 3936.11 124.11 o 10 0 0 3168.65 2863.51 79.36 o 12 0 0 8.86 99.20 23.35 o 14 0 0 3272.53 3322.89 120.60 o 16 0 0 1013.22 852.41 78.09 o 18 0 0 3754.07 3861.27 328.64 o 20 0 0 351.13 319.05 63.64 o 22 0 0 29.60 -70.94 65.55 o 1 1 0 13581.00 15011.55 124.40 o 3 1 0 4751.61 5332.21 52.21 o 5 1 0 11072.69 11455.45 148.71 o 7 1 0 72.59 65.09 11.11 o 9 1 0 35496.67 35439.17 447.54 o 11 1 0 10.35 37.75 13.40 o 13 1 0 2792.23 2902.72 63.26 o 15 1 0 3333.40 3800.15 110.42 o 17 1 0 428.77 332.97 44.22 o 19 1 0 287.48 412.55 49.46 o 21 1 0 70.65 144.84 44.72 o 23 1 0 664.77 615.40 109.55 o 0 2 0 40729.88 41323.34 466.58 o 2 2 0 13017.37 12790.45 111.86 o 4 2 0 9419.16 8489.21 94.73 o 6 2 0 443.48 233.68 13.86 o 8 2 0 2510.65 2157.75 40.24 o 10 2 0 196.44 160.79 17.30 o 12 2 0 211.98 290.50 23.34 o 14 2 0 6272.22 6069.29 205.49 o 16 2 0 671.49 624.26 50.44 o 18 2 0 424.79 419.20 58.97 o 20 2 0 222.75 199.98 47.14 o 22 2 0 10.13 40.37 36.27 o 1 3 0 31.93 79.56 9.45 o 3 3 0 3317.36 4471.44 86.54 o 5 3 0 4528.57 4250.29 57.16 o 7 3 0 13166.31 12563.19 162.78 o 9 3 0 173.02 368.49 28.81 o 11 3 0 307.22 336.84 24.36 o 13 3 0 67.51 146.45 40.24 o 15 3 0 212.46 189.27 54.30 o 17 3 0 3109.06 2872.54 88.70 o 19 3 0 1.31 -4.21 35.23 o 21 3 0 388.30 453.64 78.56 o 0 4 0 44792.13 49954.25 569.00 o 2 4 0 12894.80 12599.30 218.58 o 4 4 0 4889.13 4798.76 117.47 o 6 4 0 13158.19 10941.96 173.56 o 8 4 0 12978.26 13571.11 213.11 o 10 4 0 2462.25 1808.19 44.14 o 12 4 0 11.96 157.57 22.10 o 14 4 0 2472.60 2343.47 64.99 o 16 4 0 1642.74 1548.87 67.49 o 18 4 0 850.23 1016.77 98.49 o 20 4 0 1.40 42.22 34.27 o 22 4 0 70.73 206.39 44.31 o 1 5 0 54517.18 53072.25 471.38 o 3 5 0 4432.99 5424.05 69.49 o 5 5 0 8319.31 8130.04 94.61 o 7 5 0 27107.89 27034.35 276.41 o 9 5 0 14981.99 12554.14 138.46 o 11 5 0 987.27 1331.93 45.89 o 13 5 0 35.75 -38.63 20.84 o 15 5 0 4036.63 4090.86 103.12 o 17 5 0 2360.65 2306.42 109.08 o 19 5 0 526.02 565.44 65.27 o 21 5 0 2.28 30.11 35.06 o 0 6 0 7728.68 5530.97 102.70 o 2 6 0 322.52 390.69 20.16 o 4 6 0 912.11 1753.66 40.72 o 6 6 0 4878.36 3378.35 59.72 o 8 6 0 2470.85 2833.03 56.93 o 10 6 0 479.13 291.16 26.05 o 12 6 0 1156.14 1053.37 41.36 o 14 6 0 30.54 74.38 26.99 o 16 6 0 667.38 602.41 65.29 o 18 6 0 2264.73 2458.91 105.21 o 20 6 0 49.35 164.50 42.22 o 1 7 0 2781.34 3218.56 53.61 o 3 7 0 17.14 295.20 35.10 o 5 7 0 367.44 522.16 38.35 o 7 7 0 289.68 303.65 25.12 o 9 7 0 3.98 -11.66 16.52 o 11 7 0 4190.94 3571.46 95.84 o 13 7 0 12.38 49.28 23.17 o 15 7 0 421.65 456.72 79.92 o 17 7 0 36.20 21.08 64.65 o 19 7 0 7.26 63.86 47.51 o 0 8 0 429.74 572.65 93.38 o 2 8 0 1735.25 1847.80 68.65 o 4 8 0 789.79 1158.92 68.69 o 6 8 0 838.56 867.63 55.02 o 8 8 0 3380.89 3185.27 74.85 o 10 8 0 32.48 64.32 24.43 o 12 8 0 565.59 594.33 59.87 o 14 8 0 781.29 713.42 65.83 o 16 8 0 695.65 905.08 96.11 o 18 8 0 247.12 378.12 64.69 o 1 9 0 3050.83 2990.31 85.82 o 3 9 0 1338.65 1215.53 60.48 o 5 9 0 2862.05 2701.44 113.65 o 7 9 0 4125.17 3594.40 93.42 o 9 9 0 1757.31 1661.40 66.76 o 11 9 0 443.27 511.53 45.63 o 13 9 0 194.50 236.65 62.42 o 15 9 0 371.70 466.92 110.44 o 17 9 0 1846.12 1943.10 158.93 o 0 10 0 3479.42 3351.20 134.79 o 2 10 0 1254.46 1212.82 63.45 o 4 10 0 0.34 23.50 30.54 o 6 10 0 1065.34 1099.22 63.28 o 8 10 0 4474.51 3823.49 102.20 o 10 10 0 1386.91 1265.65 82.16 o 12 10 0 269.90 170.46 59.83 o 14 10 0 236.35 235.52 55.87 o 16 10 0 607.79 562.10 101.47 o 1 11 0 729.52 831.44 61.61 o 3 11 0 269.20 272.01 44.78 o 5 11 0 45.75 161.89 38.52 o 7 11 0 186.62 151.36 39.40 o 9 11 0 134.79 144.87 37.03 o 11 11 0 14.69 -40.37 46.60 o 13 11 0 1.17 134.91 49.20 o 15 11 0 45.44 116.73 73.63 o 0 12 0 22.76 -5.06 85.30 o 2 12 0 242.26 216.67 45.55 o 4 12 0 318.94 407.35 68.04 o 6 12 0 65.96 59.84 34.43 o 8 12 0 87.27 161.31 38.49 o 10 12 0 131.69 229.10 47.23 o 12 12 0 6.82 75.87 58.45 o 1 13 0 417.27 500.15 56.64 o 3 13 0 79.16 291.74 59.75 o 5 13 0 1.87 76.25 43.70 o 7 13 0 133.04 215.33 41.11 o 9 13 0 264.11 432.92 61.52 o 0 14 0 433.17 566.79 82.47 o 2 14 0 277.73 322.77 45.59 o 4 14 0 0.35 54.68 60.53 o 6 14 0 44.21 120.38 36.92 o -23 1 1 37.22 112.99 65.80 o -21 1 1 339.48 436.79 57.46 o -19 1 1 621.39 558.73 52.94 o -17 1 1 1355.14 1136.15 58.73 o -15 1 1 650.11 506.68 58.45 o -13 1 1 4015.59 4234.19 102.60 o -11 1 1 3479.63 3052.51 58.90 o -9 1 1 11792.29 13555.35 174.41 o -7 1 1 181.34 98.25 10.91 o -5 1 1 344.41 118.09 9.21 o -3 1 1 55978.59 69555.98 806.03 o -1 1 1 19465.50 21834.27 192.34 o 1 1 1 8123.40 9749.55 84.08 o 3 1 1 20182.08 20487.17 375.66 o 5 1 1 259.18 341.36 12.73 o 7 1 1 635.95 876.95 27.19 o 9 1 1 729.49 1195.00 41.63 o 11 1 1 13402.07 13069.41 134.98 o 13 1 1 420.37 337.70 36.95 o 15 1 1 1034.49 986.52 56.91 o 17 1 1 183.00 206.44 40.43 o 19 1 1 29.46 78.88 35.32 o 21 1 1 814.08 916.31 65.36 o -22 2 1 451.45 687.96 95.06 o -20 2 1 1156.41 1103.07 105.72 o -18 2 1 2262.87 2038.52 88.78 o -16 2 1 1937.12 1750.17 67.31 o -14 2 1 348.24 409.80 28.74 o -12 2 1 10913.71 10484.50 228.56 o -10 2 1 24210.51 25628.91 230.43 o -8 2 1 41562.30 45448.84 373.11 o -6 2 1 1271.60 1177.84 36.21 o -4 2 1 5667.17 4801.81 102.06 o -2 2 1 435.35 521.34 30.37 o 0 2 1 44615.61 54497.46 463.17 o 2 2 1 38457.22 45566.01 361.11 o 4 2 1 544.11 695.33 18.32 o 6 2 1 7322.41 5883.96 68.80 o 8 2 1 6867.17 7167.15 82.45 o 10 2 1 4242.00 4172.50 72.32 o 12 2 1 5104.62 4680.07 134.21 o 14 2 1 7023.86 6051.20 120.06 o 16 2 1 5289.92 5207.46 118.13 o 18 2 1 348.82 329.77 48.47 o 20 2 1 781.46 714.31 59.08 o 22 2 1 250.85 321.02 62.54 o -21 3 1 830.59 1062.22 153.86 o -19 3 1 566.53 507.18 65.57 o -17 3 1 2994.39 2915.14 87.50 o -15 3 1 2846.17 2732.96 97.12 o -13 3 1 953.18 934.62 36.77 o -11 3 1 13229.39 14729.45 160.43 o -9 3 1 29496.04 24745.39 223.46 o -7 3 1 33.25 93.09 13.51 o -5 3 1 7766.55 9431.32 95.55 o -3 3 1 84135.69 87609.13 768.52 o -1 3 1 2713.76 2190.91 91.50 o 1 3 1 4431.28 3035.93 39.71 o 3 3 1 16423.11 13385.61 124.07 o 5 3 1 7466.05 9607.70 98.82 o 7 3 1 9274.73 8252.09 123.41 o 9 3 1 6011.83 5477.07 73.88 o 11 3 1 4102.77 3868.25 68.06 o 13 3 1 2211.30 2010.03 69.13 o 15 3 1 8152.53 8019.34 149.09 o 17 3 1 376.28 454.90 49.84 o 19 3 1 417.40 469.72 51.99 o 21 3 1 610.42 812.18 74.52 o -22 4 1 150.71 276.17 47.89 o -20 4 1 154.35 212.43 43.45 o -18 4 1 1291.84 1297.28 84.50 o -16 4 1 6.46 -16.16 26.53 o -14 4 1 1803.19 1865.30 58.63 o -12 4 1 3946.67 3635.01 89.55 o -10 4 1 389.56 629.30 30.02 o -8 4 1 7748.03 7148.04 88.25 o -6 4 1 697.70 1039.82 43.90 o -4 4 1 5363.12 4916.94 67.33 o -2 4 1 4947.42 5431.95 62.80 o 0 4 1 157.37 119.25 8.90 o 2 4 1 37141.16 36950.09 306.30 o 4 4 1 3807.97 4429.87 59.48 o 6 4 1 9858.70 8378.50 95.73 o 8 4 1 4565.35 6498.97 102.09 o 10 4 1 1230.73 741.87 33.49 o 12 4 1 7966.30 7054.29 111.85 o 14 4 1 1003.13 923.85 62.70 o 16 4 1 3.94 8.77 31.51 o 18 4 1 49.11 87.33 37.46 o 20 4 1 148.51 276.45 72.78 o -21 5 1 144.19 190.48 43.78 o -19 5 1 1.17 66.05 40.62 o -17 5 1 341.32 359.26 57.71 o -15 5 1 27.29 108.69 27.33 o -13 5 1 3.64 17.43 19.00 o -11 5 1 226.21 109.67 20.24 o -9 5 1 2748.32 2028.85 46.95 o -7 5 1 267.88 236.06 39.94 o -5 5 1 7379.51 6036.19 77.06 o -3 5 1 7367.99 10463.88 128.50 o -1 5 1 2022.36 1056.14 67.90 o 1 5 1 348.68 286.65 58.96 o 3 5 1 6359.49 6031.02 75.80 o 5 5 1 232.34 316.12 20.78 o 7 5 1 1720.51 1968.00 50.73 o 9 5 1 377.40 560.30 30.15 o 11 5 1 314.81 328.35 32.01 o 13 5 1 707.96 892.52 47.70 o 15 5 1 110.99 142.49 36.24 o 17 5 1 3.15 99.88 35.93 o 19 5 1 381.52 515.00 62.83 o 21 5 1 0.83 122.72 39.02 o -20 6 1 867.91 997.99 81.74 o -18 6 1 480.69 587.88 70.54 o -16 6 1 53.34 149.68 43.27 o -14 6 1 1333.73 1378.39 53.69 o -12 6 1 1857.35 1828.11 57.75 o -10 6 1 2253.25 1792.50 53.01 o -8 6 1 6.99 122.76 18.87 o -6 6 1 3087.83 3520.00 107.08 o -4 6 1 8829.52 6635.97 83.27 o -2 6 1 3077.11 2692.93 87.28 o 0 6 1 1029.52 1308.93 41.36 o 2 6 1 2639.91 2185.05 69.73 o 4 6 1 5677.16 4452.41 67.93 o 6 6 1 6706.61 6368.96 95.38 o 8 6 1 2826.44 2654.97 79.31 o 10 6 1 415.56 481.89 30.59 o 12 6 1 665.34 614.08 42.26 o 14 6 1 1941.40 2042.83 75.27 o 16 6 1 184.67 271.17 44.31 o 18 6 1 2.54 103.59 42.77 o 20 6 1 168.74 275.93 50.09 o -19 7 1 1313.87 1381.79 99.29 o -17 7 1 1553.20 1469.50 128.85 o -15 7 1 4.39 46.51 39.99 o -13 7 1 56.13 25.73 34.57 o -11 7 1 817.63 849.04 51.30 o -9 7 1 6878.98 6156.73 102.33 o -7 7 1 1154.96 1187.16 45.54 o -5 7 1 9851.40 8432.20 197.17 o -3 7 1 16068.17 15530.26 178.88 o -1 7 1 8748.29 7293.99 105.26 o 1 7 1 887.39 857.43 34.15 o 3 7 1 4525.08 4003.99 64.46 o 5 7 1 7831.86 8182.29 104.78 o 7 7 1 6058.06 5026.40 105.68 o 9 7 1 1647.20 1715.38 49.33 o 11 7 1 153.53 244.54 33.33 o 13 7 1 96.31 50.39 24.96 o 15 7 1 2015.55 1963.27 77.25 o 17 7 1 1012.82 1259.00 102.20 o 19 7 1 182.91 164.70 54.06 o -18 8 1 2015.00 1817.96 151.75 o -16 8 1 487.54 344.96 69.83 o -14 8 1 306.37 353.34 54.22 o -12 8 1 248.06 323.90 33.51 o -10 8 1 884.84 900.02 46.67 o -8 8 1 3448.32 3461.88 87.60 o -6 8 1 691.83 830.69 42.58 o -4 8 1 10746.55 9274.41 193.61 o -2 8 1 12524.67 10613.94 202.17 o 0 8 1 4211.20 4225.04 173.45 o 2 8 1 2441.89 2766.67 79.85 o 4 8 1 2223.62 1666.64 64.10 o 6 8 1 5278.27 5121.41 181.67 o 8 8 1 1978.04 1933.04 59.09 o 10 8 1 163.52 94.41 25.68 o 12 8 1 1843.99 1787.73 69.52 o 14 8 1 397.87 378.85 53.66 o 16 8 1 401.99 488.65 120.77 o 18 8 1 107.62 186.66 50.50 o -17 9 1 55.88 222.68 89.79 o -15 9 1 33.13 95.37 47.78 o -13 9 1 20.43 -2.38 46.93 o -11 9 1 34.23 -3.47 24.97 o -9 9 1 2027.26 1910.31 70.19 o -7 9 1 119.13 267.03 37.99 o -5 9 1 81.22 421.66 45.04 o -3 9 1 836.76 1120.30 61.73 o -1 9 1 493.15 512.03 45.15 o 1 9 1 722.61 894.40 54.65 o 3 9 1 105.18 138.52 34.35 o 5 9 1 813.91 667.32 50.13 o 7 9 1 1339.66 1247.92 61.12 o 9 9 1 98.36 206.14 36.44 o 11 9 1 1071.85 1151.67 72.37 o 13 9 1 22.34 32.24 33.88 o 15 9 1 305.11 207.42 81.71 o 17 9 1 81.82 258.60 81.71 o -16 10 1 53.40 216.69 51.14 o -14 10 1 421.09 640.88 83.87 o -12 10 1 1.72 67.84 34.89 o -10 10 1 3.98 26.26 38.29 o -8 10 1 497.08 667.95 76.69 o -6 10 1 51.79 90.42 34.39 o -4 10 1 1190.37 1105.01 64.02 o -2 10 1 166.01 259.35 42.12 o 0 10 1 74.69 100.10 36.44 o 2 10 1 35.58 115.59 35.22 o 4 10 1 2293.02 2285.04 80.99 o 6 10 1 1051.54 747.13 56.51 o 8 10 1 2977.58 2777.84 87.97 o 10 10 1 44.99 129.00 31.14 o 12 10 1 8.17 155.10 43.02 o 14 10 1 53.54 64.65 69.14 o 16 10 1 26.55 282.85 79.02 o -15 11 1 19.02 93.73 103.26 o -13 11 1 157.64 143.63 131.55 o -11 11 1 1166.77 1156.76 77.15 o -9 11 1 344.48 450.80 59.79 o -7 11 1 102.18 86.65 38.88 o -5 11 1 1979.19 1855.84 79.06 o -3 11 1 757.70 758.80 68.04 o -1 11 1 1854.01 1787.57 77.16 o 1 11 1 44.27 114.77 37.52 o 3 11 1 463.93 500.10 52.86 o 5 11 1 447.18 432.88 50.38 o 7 11 1 210.53 124.93 35.95 o 9 11 1 146.71 132.84 36.24 o 11 11 1 0.54 92.69 38.79 o 13 11 1 600.77 765.52 110.00 o -12 12 1 500.03 539.70 79.81 o -10 12 1 1936.02 1701.31 91.61 o -8 12 1 570.57 555.17 66.46 o -6 12 1 18.51 92.93 35.38 o -4 12 1 834.42 1045.50 69.40 o -2 12 1 2539.61 2437.60 90.62 o 0 12 1 1163.87 1056.94 71.73 o 2 12 1 7.83 -21.02 51.30 o 4 12 1 595.92 673.44 60.62 o 6 12 1 384.96 526.01 55.28 o 8 12 1 890.70 831.77 62.59 o 10 12 1 7.70 1.39 36.37 o 12 12 1 69.38 287.61 87.55 o -9 13 1 201.09 170.20 50.60 o -7 13 1 232.69 154.68 51.18 o -5 13 1 83.75 133.93 52.58 o -3 13 1 947.51 1129.88 74.80 o -1 13 1 1156.74 1287.16 74.59 o 1 13 1 80.62 165.40 40.40 o 3 13 1 143.52 266.29 50.03 o 5 13 1 413.23 406.98 57.28 o 7 13 1 184.05 208.55 45.88 o 9 13 1 3.92 69.99 184.07 o -6 14 1 45.31 62.34 44.67 o -4 14 1 39.47 106.81 37.20 o -2 14 1 58.01 115.12 36.53 o 0 14 1 33.24 149.37 56.25 o 2 14 1 61.46 155.22 42.84 o 4 14 1 78.39 100.20 41.61 o 6 14 1 0.37 89.77 46.13 o -22 0 2 1097.90 1038.00 159.83 o -20 0 2 2347.81 1981.71 172.40 o -18 0 2 3889.71 4061.02 193.50 o -16 0 2 457.21 608.29 65.27 o -14 0 2 1220.94 1108.29 52.62 o -12 0 2 21545.02 23182.55 305.18 o -10 0 2 5963.11 6522.77 112.51 o -8 0 2 4015.10 3907.91 74.50 o -6 0 2 98370.79 108811.95 1187.47 o -4 0 2 7536.52 9481.92 146.85 o -2 0 2 25351.92 29605.77 365.17 o 0 0 2 11676.86 14695.13 186.71 o 2 0 2 43499.69 56984.59 781.19 o 4 0 2 718.91 945.74 40.50 o 6 0 2 9719.59 9846.64 181.79 o 8 0 2 266.16 245.84 35.56 o 10 0 2 3407.55 2992.20 101.76 o 12 0 2 24311.68 23684.24 628.55 o 14 0 2 11.96 -9.56 35.49 o 16 0 2 854.34 1009.62 88.56 o 18 0 2 3772.95 3779.11 151.44 o 20 0 2 1669.11 1692.29 107.44 o 22 0 2 381.60 690.86 150.40 o -23 1 2 203.10 192.62 78.12 o -21 1 2 1693.06 1612.76 116.81 o -19 1 2 326.34 347.52 68.15 o -17 1 2 2294.21 2251.06 93.19 o -15 1 2 4580.03 4512.29 74.92 o -13 1 2 4133.96 4256.19 68.11 o -11 1 2 17465.66 17578.83 170.40 o -9 1 2 504.67 502.17 24.86 o -7 1 2 21354.93 22617.67 195.12 o -5 1 2 1469.94 1710.31 26.70 o -3 1 2 154467.75 180177.86 1538.17 o -1 1 2 302.41 409.64 10.94 o 1 1 2 2625.70 2965.60 33.79 o 3 1 2 231812.34 280550.25 2676.25 o 5 1 2 62.58 83.41 11.13 o 7 1 2 4867.05 4990.46 70.33 o 9 1 2 1701.97 1864.91 43.44 o 11 1 2 5090.55 4429.36 93.64 o 13 1 2 4222.99 4097.74 95.52 o 15 1 2 559.48 586.83 51.06 o 17 1 2 1186.20 1006.17 65.44 o 19 1 2 650.03 669.48 59.39 o 21 1 2 1308.69 1437.95 74.70 o -22 2 2 46.26 45.57 46.12 o -20 2 2 45.20 54.95 38.26 o -18 2 2 271.91 170.11 46.19 o -16 2 2 22.17 29.05 32.92 o -14 2 2 71.68 100.18 24.30 o -12 2 2 7938.85 7852.13 113.52 o -10 2 2 10448.54 9927.27 121.07 o -8 2 2 10104.82 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