#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/91/2209157.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209157_Fobs loop_ _publ_author_name 'Che, Guang-Bo' 'Liu, Chun-Bo' _publ_section_title ; A new Mn^II^ coordination polymer with a double-chain structure ; _journal_coeditor_code EZ2004 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1453 _journal_page_last m1455 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.328 _cell_angle_gamma 90.000 _cell_length_a 15.3900 _cell_length_b 15.9350 _cell_length_c 18.8390 _exptl_crystal_F_000 2104.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file ez2004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yjmn1shelxl in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 906.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11792.89 11304.83 185.28 o 6 0 0 12682.68 12022.56 181.61 o 8 0 0 1310.09 1252.38 84.92 o 10 0 0 958.57 966.40 87.66 o 12 0 0 836.57 1021.07 101.18 o 14 0 0 3980.00 4097.26 182.29 o 16 0 0 29.30 187.59 224.99 o 18 0 0 552.63 905.73 736.32 o 3 1 0 24713.59 22872.85 606.54 o 5 1 0 13100.57 12311.25 133.20 o 7 1 0 2973.82 3063.20 72.70 o 9 1 0 8171.33 8923.81 127.49 o 11 1 0 2304.35 2301.52 94.65 o 13 1 0 1912.78 2177.32 98.69 o 15 1 0 82.61 54.54 38.70 o 17 1 0 996.60 1050.44 143.29 o 2 2 0 21887.02 21030.58 195.69 o 4 2 0 7725.25 8536.47 98.38 o 6 2 0 717.40 1004.37 34.26 o 8 2 0 579.10 703.76 34.01 o 10 2 0 921.11 958.25 48.52 o 12 2 0 10.88 35.13 35.46 o 14 2 0 103.71 83.62 36.48 o 16 2 0 7.09 67.52 102.57 o 18 2 0 11.43 -24.90 95.95 o 1 3 0 2238.61 2220.37 66.54 o 3 3 0 15070.54 14910.86 137.61 o 5 3 0 2762.36 2538.21 50.62 o 7 3 0 5702.70 5806.69 94.21 o 9 3 0 2134.01 2307.15 76.24 o 11 3 0 1998.74 2027.25 89.56 o 13 3 0 376.41 347.10 45.55 o 15 3 0 98.76 79.54 33.55 o 17 3 0 467.80 440.18 162.40 o 0 4 0 25953.10 26750.49 413.16 o 2 4 0 1397.34 1102.96 53.30 o 4 4 0 208.77 123.76 23.33 o 6 4 0 42810.19 43246.61 608.15 o 8 4 0 19857.55 20233.55 199.04 o 10 4 0 2460.77 2527.43 64.10 o 12 4 0 3254.75 3380.08 121.46 o 14 4 0 3504.18 3135.50 168.61 o 16 4 0 207.76 135.44 96.04 o 18 4 0 139.66 104.70 125.62 o 1 5 0 12581.33 12659.68 119.34 o 3 5 0 3129.27 3872.29 66.61 o 5 5 0 21654.75 22999.84 237.86 o 7 5 0 17008.33 17805.13 177.13 o 9 5 0 501.10 512.95 43.87 o 11 5 0 330.76 309.80 40.29 o 13 5 0 17.44 23.42 27.06 o 15 5 0 946.26 992.84 126.12 o 17 5 0 298.10 364.13 131.63 o 0 6 0 51092.78 49948.61 592.96 o 4 6 0 2184.27 1824.20 67.75 o 6 6 0 9819.40 11240.31 151.19 o 8 6 0 270.71 274.70 45.46 o 10 6 0 56.04 32.78 38.22 o 12 6 0 634.86 348.31 81.64 o 14 6 0 2818.07 2861.10 246.00 o 16 6 0 493.43 526.04 110.07 o 18 6 0 0.47 -98.11 151.23 o 1 7 0 18412.53 18634.62 177.04 o 3 7 0 0.25 19.53 38.43 o 5 7 0 2430.36 2144.57 70.07 o 7 7 0 1962.89 1810.84 75.85 o 9 7 0 979.22 996.11 93.86 o 11 7 0 3327.40 3363.23 119.66 o 13 7 0 1825.90 1696.16 128.64 o 15 7 0 217.82 66.96 105.75 o 17 7 0 75.09 144.74 109.52 o 0 8 0 8901.49 6507.04 119.62 o 2 8 0 898.69 1191.65 54.72 o 4 8 0 127.93 159.91 42.17 o 6 8 0 2323.68 2068.17 74.99 o 8 8 0 4124.24 4253.20 71.84 o 10 8 0 1088.37 1244.42 243.73 o 12 8 0 1380.62 1385.35 95.13 o 14 8 0 1665.95 1852.95 151.94 o 16 8 0 520.91 454.58 115.25 o 1 9 0 22.33 -18.06 48.81 o 3 9 0 4.42 10.95 36.98 o 5 9 0 1006.98 1164.70 76.93 o 7 9 0 1430.20 1418.35 74.39 o 9 9 0 3.80 8.85 29.25 o 11 9 0 222.52 151.51 67.64 o 13 9 0 28.00 -25.49 82.82 o 15 9 0 855.04 867.27 98.39 o 0 10 0 2718.41 2389.41 102.88 o 2 10 0 2004.71 2211.58 70.85 o 4 10 0 2022.60 2027.77 83.92 o 6 10 0 18.80 32.47 63.61 o 8 10 0 4106.05 4269.28 123.99 o 10 10 0 380.89 410.47 59.10 o 12 10 0 37.14 124.02 105.94 o 14 10 0 192.94 297.52 92.64 o 16 10 0 11.83 64.28 122.72 o 1 11 0 11095.37 10533.67 115.80 o 3 11 0 665.34 675.32 71.25 o 5 11 0 6718.45 6891.59 114.69 o 7 11 0 9456.94 9082.39 180.84 o 9 11 0 31.38 32.53 47.44 o 11 11 0 420.70 543.18 97.86 o 13 11 0 674.47 771.90 82.23 o 15 11 0 168.89 159.27 77.10 o 0 12 0 634.98 851.88 122.72 o 2 12 0 26.79 73.62 56.28 o 4 12 0 829.42 886.76 83.34 o 6 12 0 10973.88 10450.38 148.89 o 8 12 0 326.45 307.80 59.56 o 10 12 0 346.04 395.64 57.50 o 12 12 0 1502.26 1581.38 200.56 o 14 12 0 361.40 371.37 92.56 o 1 13 0 1500.75 1655.77 104.20 o 3 13 0 34.13 -17.73 86.95 o 5 13 0 95.42 64.28 74.75 o 7 13 0 494.08 451.34 57.57 o 9 13 0 1050.57 1078.32 134.96 o 11 13 0 301.33 382.44 75.82 o 13 13 0 3.93 -27.24 80.94 o 0 14 0 7983.92 7517.50 187.64 o 2 14 0 32.79 63.68 61.51 o 4 14 0 1127.58 1318.55 86.28 o 6 14 0 105.15 81.89 60.36 o 8 14 0 2758.27 2902.59 92.35 o 10 14 0 70.02 68.98 51.01 o 12 14 0 1311.37 1320.26 176.29 o 1 15 0 9130.45 9048.50 124.92 o 3 15 0 172.79 227.69 74.91 o 5 15 0 678.22 1009.54 129.81 o 7 15 0 4210.45 4017.36 124.83 o 9 15 0 2.78 -44.03 51.39 o 11 15 0 1139.88 1155.83 82.44 o 0 16 0 10605.30 10416.99 298.03 o 2 16 0 718.06 638.23 69.70 o 4 16 0 667.90 697.92 131.44 o 6 16 0 761.69 924.81 104.33 o 8 16 0 150.92 102.81 67.46 o 10 16 0 655.73 373.23 127.04 o 1 17 0 17.56 29.01 64.93 o 3 17 0 377.37 500.86 91.09 o 5 17 0 115.06 306.70 117.74 o 7 17 0 163.53 270.50 81.47 o 9 17 0 0.03 -21.59 58.72 o 0 18 0 926.62 946.72 113.95 o 2 18 0 730.28 760.52 147.89 o 4 18 0 31.58 38.53 69.52 o 6 18 0 804.00 888.60 98.45 o 8 18 0 541.32 548.09 77.68 o 1 19 0 1848.23 2046.45 105.85 o 3 19 0 121.50 211.54 80.83 o 5 19 0 237.07 202.30 92.58 o 7 19 0 1051.40 968.44 106.24 o 0 20 0 5.76 -161.31 161.31 o 2 20 0 277.81 352.26 87.31 o 4 20 0 44.58 36.49 78.40 o -19 1 1 18.78 110.37 131.00 o -17 1 1 1288.32 1524.93 112.43 o -15 1 1 561.86 558.88 55.30 o -13 1 1 116.62 106.28 72.77 o -11 1 1 9.62 70.80 71.93 o -9 1 1 1018.42 1201.78 53.89 o -7 1 1 7268.73 7242.07 101.52 o -5 1 1 3039.49 3113.19 80.52 o -3 1 1 2926.83 2638.09 61.38 o 3 1 1 28964.47 25878.45 214.51 o 5 1 1 2202.40 2607.79 55.80 o 7 1 1 6858.26 6386.12 88.57 o 9 1 1 492.39 571.48 62.67 o 11 1 1 395.79 334.73 61.43 o 13 1 1 1778.64 1892.75 100.60 o 15 1 1 117.79 135.76 43.21 o 17 1 1 925.03 1115.72 150.03 o -18 2 1 514.59 475.41 114.92 o -16 2 1 2407.81 2489.20 206.67 o -14 2 1 489.40 482.04 63.24 o -12 2 1 5330.85 5200.20 199.28 o -10 2 1 8014.77 8182.28 276.12 o -8 2 1 1011.18 1330.11 103.21 o -6 2 1 16227.86 15033.90 202.65 o -4 2 1 30029.42 31333.66 326.00 o -2 2 1 3359.19 3702.01 75.62 o 2 2 1 49213.56 48826.43 559.23 o 4 2 1 1650.08 1699.33 44.53 o 6 2 1 14119.69 13400.61 154.36 o 8 2 1 25633.61 26090.22 259.73 o 10 2 1 2081.28 2183.80 50.66 o 12 2 1 2039.93 2208.74 64.68 o 14 2 1 4588.99 4329.57 246.49 o 16 2 1 443.55 375.24 46.47 o 18 2 1 470.75 463.60 178.24 o -17 3 1 373.69 473.51 93.05 o -15 3 1 366.61 310.42 80.83 o -13 3 1 763.62 643.70 47.82 o -11 3 1 1245.08 1150.48 41.55 o -9 3 1 3580.35 3995.71 55.19 o -7 3 1 4599.95 4602.38 67.59 o -5 3 1 6000.64 5808.98 64.18 o -3 3 1 583.81 230.89 32.09 o -1 3 1 1438.83 1571.67 35.91 o 1 3 1 154243.06 175652.30 1571.58 o 3 3 1 16763.84 16222.59 143.57 o 5 3 1 2392.82 2476.62 51.12 o 7 3 1 4972.35 5236.65 71.29 o 9 3 1 3993.59 3898.06 86.88 o 11 3 1 385.70 377.93 53.14 o 13 3 1 1421.30 1442.66 83.50 o 15 3 1 193.19 200.33 56.51 o 17 3 1 74.71 88.99 93.74 o -18 4 1 254.66 226.64 109.35 o -16 4 1 150.53 75.81 85.47 o -14 4 1 63.05 63.75 69.06 o -12 4 1 1201.71 1089.02 108.81 o -10 4 1 8.40 2.83 21.32 o -8 4 1 402.00 374.97 29.17 o -6 4 1 49.75 43.20 21.09 o -4 4 1 4916.36 5131.63 71.81 o -2 4 1 977.33 714.80 54.11 o 0 4 1 37685.24 39827.77 317.28 o 2 4 1 5022.98 4848.36 76.18 o 4 4 1 4266.83 4920.19 64.06 o 6 4 1 2183.04 2709.76 49.20 o 8 4 1 6107.29 6199.49 126.52 o 10 4 1 959.01 899.89 53.15 o 12 4 1 613.64 608.77 85.48 o 14 4 1 153.44 147.60 40.72 o 16 4 1 386.88 421.22 100.25 o 18 4 1 38.42 95.71 119.98 o -17 5 1 27.09 -27.37 80.41 o -15 5 1 127.65 140.61 77.83 o -13 5 1 746.38 786.29 79.71 o -11 5 1 2180.74 2269.93 111.22 o -9 5 1 2149.62 2010.06 108.86 o -7 5 1 5254.91 5222.10 103.49 o -5 5 1 7889.07 7653.80 110.56 o -3 5 1 11.81 122.97 34.95 o -1 5 1 1084.15 1280.18 58.94 o 1 5 1 1090.30 1400.29 47.33 o 3 5 1 11929.27 11327.21 102.47 o 5 5 1 3402.74 3248.82 74.23 o 7 5 1 5553.18 4923.85 117.38 o 9 5 1 1049.56 952.81 93.63 o 11 5 1 4974.88 4939.64 156.04 o 13 5 1 236.73 202.08 27.76 o 15 5 1 32.86 27.19 27.85 o 17 5 1 315.95 325.66 106.82 o -18 6 1 118.44 132.05 65.29 o -16 6 1 449.41 515.27 96.66 o -14 6 1 120.68 92.79 79.50 o -12 6 1 3286.86 3315.67 118.44 o -10 6 1 3069.95 2809.70 112.68 o -8 6 1 1345.21 1148.15 80.94 o -6 6 1 29799.46 31466.68 438.89 o -4 6 1 467.36 365.88 37.94 o -2 6 1 1008.67 1026.59 52.53 o 0 6 1 1553.05 1205.85 67.81 o 2 6 1 2104.04 2052.17 55.27 o 4 6 1 2213.11 2240.35 48.17 o 6 6 1 21358.91 21813.72 178.97 o 8 6 1 8463.21 8605.95 109.65 o 10 6 1 952.14 1000.45 42.78 o 12 6 1 1514.33 1404.39 68.32 o 14 6 1 37.31 3.17 35.43 o 16 6 1 942.02 1171.78 131.91 o -17 7 1 891.36 725.60 212.27 o -15 7 1 32.78 -30.79 72.84 o -13 7 1 273.95 250.89 75.16 o -11 7 1 67.54 73.56 91.47 o -9 7 1 678.99 676.84 83.72 o -7 7 1 613.95 795.11 57.28 o -5 7 1 5722.70 5956.40 177.97 o -3 7 1 101.97 256.35 52.67 o -1 7 1 2459.71 2017.08 49.59 o 1 7 1 13023.53 14397.54 158.21 o 3 7 1 1560.36 2033.76 57.43 o 7 7 1 2900.15 3008.55 61.67 o 9 7 1 319.37 279.07 52.09 o 11 7 1 2011.06 2019.87 87.72 o 13 7 1 3857.17 3841.08 187.00 o 15 7 1 4107.89 4198.85 164.58 o 17 7 1 321.37 686.57 154.94 o -16 8 1 29.50 77.61 83.87 o -14 8 1 685.18 657.66 89.09 o -12 8 1 272.72 241.21 85.77 o -10 8 1 479.39 499.76 98.20 o -8 8 1 626.17 628.98 46.32 o -6 8 1 1403.38 1613.72 83.75 o -4 8 1 107.71 29.37 31.28 o -2 8 1 534.36 600.66 48.96 o 0 8 1 6534.89 7920.92 88.97 o 2 8 1 2464.77 2952.74 64.72 o 4 8 1 2171.91 2042.71 80.97 o 6 8 1 449.83 472.41 61.87 o 8 8 1 12.54 11.23 36.16 o 10 8 1 343.36 336.34 73.34 o 12 8 1 614.55 451.54 95.38 o 14 8 1 820.92 694.88 98.99 o 16 8 1 69.57 89.49 90.48 o -17 9 1 792.92 656.19 94.35 o -15 9 1 162.77 275.14 98.14 o -13 9 1 391.98 331.92 99.34 o -11 9 1 3108.68 3199.85 125.75 o -9 9 1 317.26 318.75 38.89 o -7 9 1 455.62 441.26 56.51 o -5 9 1 10574.56 10716.52 120.83 o -3 9 1 2154.21 2221.82 59.97 o -1 9 1 5069.73 5070.28 79.95 o 1 9 1 11865.88 12988.14 148.36 o 3 9 1 1377.03 1139.42 59.52 o 5 9 1 372.82 252.82 51.08 o 7 9 1 9195.96 9276.88 152.72 o 9 9 1 335.89 307.96 73.34 o 11 9 1 322.87 363.28 123.44 o 13 9 1 1629.42 1774.30 99.00 o 15 9 1 272.74 238.54 85.42 o -16 10 1 420.76 276.53 94.60 o -14 10 1 158.82 183.11 128.56 o -12 10 1 879.00 868.97 91.26 o -10 10 1 2954.55 2783.56 67.60 o -8 10 1 21.94 -7.35 52.57 o -6 10 1 3969.87 4155.24 113.26 o -4 10 1 1500.65 1360.00 75.29 o -2 10 1 27.70 -0.65 31.48 o 0 10 1 6798.28 6185.73 102.09 o 2 10 1 1190.74 1438.73 57.09 o 4 10 1 139.34 200.01 63.63 o 6 10 1 3707.78 3767.92 108.81 o 8 10 1 40.36 62.18 44.23 o 10 10 1 1972.42 2030.53 133.27 o 12 10 1 1108.52 1221.93 91.04 o 14 10 1 205.78 105.45 88.40 o 16 10 1 0.22 -99.34 216.22 o -15 11 1 375.86 411.41 86.14 o -13 11 1 122.40 93.84 72.99 o -11 11 1 4.13 -4.49 67.45 o -9 11 1 384.58 292.73 60.85 o -7 11 1 31.30 2.69 51.37 o -5 11 1 429.11 530.29 68.78 o -3 11 1 30.92 54.88 40.39 o -1 11 1 65.32 117.22 50.01 o 1 11 1 2003.81 1966.73 79.34 o 3 11 1 98.73 129.71 62.75 o 5 11 1 301.10 260.85 55.07 o 7 11 1 88.04 121.06 66.83 o 9 11 1 6151.05 5850.39 114.00 o 11 11 1 679.49 845.90 80.67 o 13 11 1 60.13 49.67 70.25 o 15 11 1 3.58 82.86 138.38 o -14 12 1 128.02 140.13 80.94 o -12 12 1 525.44 451.88 77.60 o -10 12 1 146.64 162.60 56.25 o -8 12 1 2892.50 2945.37 107.15 o -6 12 1 314.96 548.97 112.08 o -4 12 1 2431.34 2335.28 117.93 o -2 12 1 1270.21 1157.47 62.91 o 0 12 1 23776.09 23215.54 241.83 o 2 12 1 721.76 755.36 59.28 o 4 12 1 393.69 389.99 58.76 o 6 12 1 921.58 993.94 64.68 o 8 12 1 1199.14 1075.37 99.30 o 10 12 1 718.88 731.57 58.57 o 12 12 1 447.53 390.73 80.08 o 14 12 1 48.54 29.21 104.48 o -13 13 1 1221.95 1193.47 98.79 o -11 13 1 3801.89 3307.12 89.90 o -9 13 1 2124.69 2275.76 161.95 o -7 13 1 756.10 776.91 88.49 o -5 13 1 10457.55 10547.74 167.57 o -3 13 1 1333.40 1144.09 120.56 o -1 13 1 398.56 416.72 65.58 o 1 13 1 72.97 67.30 48.94 o 3 13 1 268.98 195.86 85.06 o 5 13 1 869.12 818.25 68.47 o 7 13 1 3359.92 3436.42 140.94 o 9 13 1 2751.56 2602.85 95.70 o 11 13 1 807.48 798.32 80.64 o 13 13 1 1087.66 892.77 125.49 o -14 14 1 42.63 158.53 79.51 o -12 14 1 10.05 25.54 83.50 o -10 14 1 1204.03 1166.92 69.03 o -8 14 1 1342.80 1456.31 166.17 o -6 14 1 4728.62 4723.58 132.78 o -4 14 1 7354.51 7162.35 186.82 o -2 14 1 112.30 164.38 60.59 o 0 14 1 11286.72 11011.12 161.98 o 2 14 1 1626.42 1737.34 94.50 o 4 14 1 769.26 810.29 79.92 o 6 14 1 8.66 41.06 58.00 o 8 14 1 501.12 491.28 65.05 o 10 14 1 369.07 356.55 57.41 o 12 14 1 612.49 486.78 116.90 o -13 15 1 0.70 54.91 87.71 o -11 15 1 145.74 96.40 90.25 o -9 15 1 232.96 159.50 80.00 o -7 15 1 50.50 71.36 94.92 o -5 15 1 5.24 73.74 67.31 o -3 15 1 256.00 700.76 209.04 o -1 15 1 1406.44 1828.05 82.27 o 1 15 1 691.01 865.36 64.51 o 3 15 1 2510.69 2419.64 132.41 o 5 15 1 250.10 225.15 73.07 o 7 15 1 140.95 85.47 64.00 o 9 15 1 51.70 27.80 54.49 o 11 15 1 7.82 -55.10 96.07 o -12 16 1 712.20 888.65 101.94 o -10 16 1 88.51 32.72 69.82 o -8 16 1 341.81 298.43 141.49 o -6 16 1 342.83 379.81 80.83 o -4 16 1 2.68 48.09 74.91 o -2 16 1 56.98 173.89 76.71 o 0 16 1 674.11 813.70 138.74 o 2 16 1 1258.35 1203.03 103.93 o 4 16 1 7.47 44.96 73.75 o 6 16 1 2070.15 2026.36 145.08 o 8 16 1 251.01 315.71 83.62 o 10 16 1 8.28 9.30 47.73 o -9 17 1 192.73 159.86 84.87 o -7 17 1 1561.87 1374.89 102.19 o -5 17 1 604.66 733.40 99.53 o -3 17 1 552.82 625.26 95.60 o -1 17 1 312.01 444.18 69.88 o 1 17 1 3098.83 3279.90 116.59 o 3 17 1 1508.64 1819.47 160.26 o 5 17 1 1336.88 1379.95 96.98 o 7 17 1 1137.92 990.87 91.10 o 9 17 1 169.85 156.59 73.44 o -8 18 1 215.90 192.80 97.66 o -6 18 1 34.28 41.68 86.59 o -4 18 1 3.62 33.07 72.53 o -2 18 1 359.43 333.68 89.90 o 0 18 1 529.78 654.92 75.24 o 2 18 1 549.39 450.84 94.30 o 4 18 1 127.06 76.70 82.77 o 6 18 1 117.68 68.20 76.49 o 8 18 1 456.74 354.58 91.01 o -7 19 1 849.91 1119.82 111.05 o -5 19 1 87.37 143.72 90.24 o -3 19 1 1.23 -85.59 85.59 o -1 19 1 543.34 745.60 89.03 o 1 19 1 3.00 -30.97 61.97 o 3 19 1 341.23 427.61 99.98 o 5 19 1 80.85 103.55 90.84 o 7 19 1 291.96 260.20 72.72 o -4 20 1 563.35 742.63 104.79 o -2 20 1 224.91 176.76 94.32 o 0 20 1 664.90 872.14 106.48 o 2 20 1 171.36 321.11 100.34 o 4 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