#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/91/2209159.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2209159_Fobs
loop_
_publ_author_name
'Xu, Yan'
'Cheng, Li-Ying'
'Zhou, Guang-Peng'
'Wang, Yan-Li'
_publ_section_title
;
 Lead germanium oxide
;
_journal_coeditor_code           FI2002
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i135
_journal_page_last               i137
_journal_volume                  62
_journal_year                    2006
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-P 3*'
_symmetry_space_group_name_H-M   'R -3 :R'
_cell_angle_alpha                113.456
_cell_angle_beta                 113.456
_cell_angle_gamma                113.456
_cell_length_a                   9.3282
_cell_length_b                   9.3282
_cell_length_c                   9.3282
_exptl_crystal_F_000             828.00
_reflns_d_resolution_high        0.8261
_[local]_cod_data_source_file    fi2002Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' cly10b in R-3'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            518.35
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'z, x, y'
'y, z, x'
'-x, -y, -z'
'-z, -x, -y'
'-y, -z, -x'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 0 1 23328.29 19596.67 525.84 o
0 0 1 3785.68 4757.19 111.83 o
-1 1 1 18904.69 18249.81 612.36 o
0 1 1 48144.21 50847.41 1245.14 o
1 1 1 46458.60 46172.22 1806.55 o
-2 -1 2 58028.61 63179.77 1490.36 o
-1 -1 2 2109.99 1378.82 63.90 o
0 -1 2 2866.20 2218.32 73.61 o
1 -1 2 2855.30 3333.19 122.76 o
-2 0 2 10750.48 8056.64 250.49 o
-1 0 2 2709.29 2280.84 65.03 o
0 0 2 7389.46 7875.82 200.82 o
1 0 2 2370.20 2108.71 72.89 o
-2 1 2 105.46 160.43 27.15 o
-1 1 2 173995.52 202609.63 5914.65 o
0 1 2 40249.51 45395.27 1118.41 o
1 1 2 24047.17 23700.61 585.19 o
-2 2 2 37895.86 35750.69 1076.52 o
-1 2 2 64.43 43.17 27.47 o
0 2 2 46007.99 47909.73 1279.81 o
1 2 2 3.01 15.88 32.88 o
2 2 2 13002.68 12612.16 1089.40 o
-3 -2 3 26681.60 26443.64 732.33 o
-2 -2 3 965.71 1225.25 52.83 o
-1 -2 3 8030.12 6755.88 191.15 o
0 -2 3 16628.45 16057.34 353.90 o
1 -2 3 15908.84 14321.83 487.82 o
2 -2 3 21805.75 21787.50 732.08 o
-3 -1 3 82.10 44.51 22.90 o
-2 -1 3 268682.84 252653.38 8044.78 o
-1 -1 3 28754.20 30317.21 731.41 o
0 -1 3 5480.90 5630.10 171.25 o
1 -1 3 1373.41 1354.61 63.78 o
2 -1 3 26488.84 25764.24 771.77 o
-3 0 3 22801.64 20276.07 479.42 o
-2 0 3 4910.44 5012.60 116.45 o
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0 0 3 5824.04 5101.87 150.56 o
1 0 3 13247.03 12910.50 340.11 o
2 0 3 5523.55 6142.36 217.20 o
-3 1 3 4072.54 4061.15 115.87 o
-2 1 3 2032.47 2060.18 80.23 o
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0 1 3 38108.32 40123.64 1076.86 o
1 1 3 1634.98 1769.42 83.83 o
2 1 3 21521.92 22646.51 1044.84 o
-3 2 3 11090.18 10818.66 351.91 o
-2 2 3 6137.68 5592.81 195.00 o
-1 2 3 16979.15 17941.07 547.75 o
0 2 3 26370.12 26733.77 808.86 o
1 2 3 36926.17 37110.27 1649.01 o
2 2 3 49.24 0.00 113.78 o
-3 3 3 64077.37 66254.13 1809.94 o
-2 3 3 12336.72 12312.44 389.29 o
-1 3 3 1573.06 1800.31 119.14 o
0 3 3 16394.45 15698.02 757.08 o
1 3 3 2012.00 2198.46 251.47 o
2 3 3 218.95 0.00 132.29 o
-4 -3 4 7549.53 7772.54 250.15 o
-3 -3 4 98456.95 101306.04 3023.96 o
-2 -3 4 9222.30 8676.21 438.07 o
-1 -3 4 1987.88 2379.03 109.57 o
0 -3 4 1423.61 1682.97 73.09 o
1 -3 4 4333.85 4463.63 150.62 o
2 -3 4 44.23 70.84 37.93 o
3 -3 4 18272.55 18609.28 749.32 o
-4 -2 4 978.05 1057.41 80.28 o
-3 -2 4 20372.53 19215.13 474.84 o
-2 -2 4 17176.32 17028.39 416.17 o
-1 -2 4 17362.77 17587.56 412.50 o
0 -2 4 121700.44 131405.50 3269.32 o
1 -2 4 17663.14 18540.06 522.81 o
2 -2 4 21295.28 21005.18 718.17 o
3 -2 4 3239.44 3251.50 208.51 o
-4 -1 4 4528.62 4364.82 124.23 o
-3 -1 4 18768.08 19284.24 473.62 o
-2 -1 4 69.88 70.30 29.32 o
-1 -1 4 36125.90 35537.88 914.27 o
0 -1 4 23175.89 24308.93 622.88 o
1 -1 4 63081.55 66033.59 1922.91 o
2 -1 4 680.80 668.29 124.15 o
3 -1 4 12591.62 12466.11 550.48 o
-4 0 4 561.89 797.67 61.98 o
-3 0 4 31642.41 28369.99 1113.92 o
-2 0 4 10056.32 9641.66 267.81 o
-1 0 4 15924.52 15619.09 418.94 o
0 0 4 36357.51 35971.07 1188.76 o
1 0 4 222.38 156.18 55.06 o
2 0 4 7548.16 7901.60 383.53 o
3 0 4 350.81 184.84 129.55 o
-4 1 4 72665.28 68158.94 2451.26 o
-3 1 4 62.63 89.92 51.12 o
-2 1 4 902.86 1170.92 67.25 o
-1 1 4 19802.34 19520.70 690.73 o
0 1 4 2212.04 2143.79 145.21 o
1 1 4 10000.51 10418.54 542.93 o
2 1 4 18140.03 18548.40 894.69 o
3 1 4 8516.22 9067.14 532.34 o
-4 2 4 34684.15 34266.18 832.65 o
-3 2 4 6304.86 5846.18 191.11 o
-2 2 4 7774.83 7731.65 243.45 o
-1 2 4 14770.83 14962.54 474.49 o
0 2 4 14538.42 14540.90 710.70 o
1 2 4 1928.04 2117.45 222.15 o
2 2 4 7130.61 7146.16 454.36 o
-4 3 4 65.32 141.93 62.48 o
-3 3 4 49413.89 49471.77 1487.22 o
-2 3 4 702.01 762.49 127.85 o
-1 3 4 15599.09 14512.95 622.69 o
0 3 4 957.45 802.72 158.70 o
1 3 4 37169.78 38752.25 1760.76 o
-4 4 4 2446.10 2317.67 171.44 o
-3 4 4 19974.42 19804.50 808.23 o
-2 4 4 33431.99 32018.37 1265.03 o
-1 4 4 1986.45 2397.28 207.94 o
0 4 4 460.19 577.81 172.21 o
-5 -4 5 43.79 74.30 182.36 o
-4 -4 5 5078.01 5466.96 256.32 o
-3 -4 5 4032.46 3388.82 185.71 o
-2 -4 5 471.54 357.82 49.46 o
-1 -4 5 123425.63 136572.27 3227.23 o
0 -4 5 7832.32 8039.94 263.22 o
1 -4 5 15198.35 16079.09 468.71 o
2 -4 5 445.87 531.27 58.18 o
3 -4 5 25685.89 25843.60 1022.26 o
4 -4 5 7981.52 8310.71 400.35 o
-5 -3 5 4727.44 4751.29 318.57 o
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-1 -3 5 30971.88 31250.11 867.27 o
0 -3 5 68897.01 71682.44 1812.29 o
1 -3 5 10951.78 10479.15 319.23 o
2 -3 5 6370.44 6671.76 278.47 o
3 -3 5 6384.06 6604.09 334.49 o
4 -3 5 5051.62 5593.17 315.48 o
-5 -2 5 6230.54 6125.64 469.32 o
-4 -2 5 71583.54 68990.48 1659.18 o
-3 -2 5 2481.23 2688.62 116.62 o
-2 -2 5 2036.79 1853.87 60.81 o
-1 -2 5 244.82 243.97 34.90 o
0 -2 5 13437.86 12830.75 376.55 o
1 -2 5 13637.24 12948.25 425.35 o
2 -2 5 7279.08 7211.08 349.66 o
3 -2 5 23389.87 24026.78 976.33 o
4 -2 5 1266.83 1195.42 165.71 o
-5 -1 5 14546.65 14281.13 507.95 o
-4 -1 5 4296.01 4790.05 147.01 o
-3 -1 5 529.25 621.75 61.09 o
-2 -1 5 5161.65 5217.06 190.08 o
-1 -1 5 588.39 744.09 73.21 o
0 -1 5 21341.63 21802.08 680.67 o
1 -1 5 18463.29 18378.76 750.62 o
2 -1 5 19046.52 20015.48 824.99 o
3 -1 5 598.53 732.99 140.24 o
4 -1 5 1.02 26.59 139.58 o
-5 0 5 14052.36 17187.74 557.39 o
-4 0 5 241.32 175.52 51.67 o
-3 0 5 105734.19 105348.96 2581.62 o
-2 0 5 53608.84 54864.86 1540.23 o
-1 0 5 17349.42 16987.30 560.20 o
0 0 5 56.39 152.25 86.59 o
1 0 5 27060.35 28049.90 1116.73 o
2 0 5 12354.04 12761.82 655.48 o
3 0 5 385.22 321.84 153.06 o
-5 1 5 11071.34 10490.09 568.51 o
-4 1 5 30588.84 28960.12 843.11 o
-3 1 5 386.18 227.68 63.80 o
-2 1 5 47160.51 46540.65 1574.54 o
-1 1 5 9256.02 9896.95 369.74 o
0 1 5 11872.96 11432.09 579.31 o
1 1 5 210.15 242.69 129.24 o
2 1 5 2527.67 2766.35 273.05 o
-5 2 5 1266.71 1374.54 113.23 o
-4 2 5 8273.10 8632.32 341.51 o
-3 2 5 28809.22 28076.10 977.72 o
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-1 2 5 7652.57 7696.67 372.02 o
0 2 5 581.61 586.32 151.68 o
1 2 5 1345.04 1458.37 212.43 o
-5 3 5 573.37 603.57 119.96 o
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0 3 5 11782.16 10857.57 598.77 o
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-3 5 5 7396.61 7826.94 413.06 o
-6 -5 6 5047.11 5536.75 552.24 o
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-3 -5 6 1294.45 1257.08 133.08 o
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-1 -5 6 6413.40 7326.77 277.79 o
0 -5 6 6272.42 6208.42 377.24 o
1 -5 6 48979.46 51572.86 1672.78 o
2 -5 6 3005.31 3312.92 291.94 o
3 -5 6 11012.16 12133.67 638.93 o
4 -5 6 4348.41 5121.49 482.75 o
5 -5 6 19124.23 19036.14 1205.06 o
-6 -4 6 2347.91 2155.65 342.73 o
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-3 -4 6 61.87 0.00 73.62 o
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3 -4 6 746.88 874.75 162.74 o
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-1 2 6 9774.84 9267.42 511.29 o
0 2 6 850.80 1104.79 187.55 o
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-2 3 6 223.08 206.00 109.22 o
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-3 4 6 3228.20 3621.00 258.98 o
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-4 5 6 4669.88 4669.89 419.02 o
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-3 -6 7 17766.43 16962.25 726.65 o
-2 -6 7 427.77 403.46 133.74 o
-1 -6 7 8202.15 10861.88 445.81 o
0 -6 7 37442.13 40120.05 1267.74 o
1 -6 7 36596.94 36549.43 1267.35 o
2 -6 7 5868.93 5148.84 847.52 o
3 -6 7 508.98 167.14 478.09 o
4 -6 7 5034.35 4927.32 534.43 o
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