#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:22:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181012 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/92/2209207.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209207_Fobs loop_ _publ_author_name 'Shen, Li' 'Wang, Feng-Wu' 'Cheng, Ai-Bin' 'Yang, Song' _publ_section_title ; 2,2'-(Piperazine-1,4-diium-1,4-diyl)diacetate dihydrate ; _journal_coeditor_code HK2023 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2242 _journal_page_last o2244 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.5060 _cell_length_b 11.3440 _cell_length_c 14.5870 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8105 _cod_data_source_file hk2023Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5801.13 6212.59 45.64 o 4 0 0 35.95 42.90 6.25 o 6 0 0 2357.61 2258.19 49.16 o 8 0 0 271.37 239.37 21.36 o 2 1 0 1208.26 1210.71 84.60 o 4 1 0 586.50 597.43 23.95 o 6 1 0 392.80 397.30 15.24 o 0 2 0 788.20 902.00 8.90 o 2 2 0 9891.65 10536.13 1257.40 o 4 2 0 76.42 71.13 10.85 o 6 2 0 207.19 195.18 11.16 o 2 3 0 549.27 505.37 52.84 o 4 3 0 54.64 60.30 5.97 o 6 3 0 331.60 303.86 35.56 o 0 4 0 3053.10 2974.45 22.15 o 2 4 0 1092.90 1114.49 123.60 o 4 4 0 2.42 -0.23 4.24 o 6 4 0 346.34 317.44 18.20 o 2 5 0 8.94 11.39 3.15 o 4 5 0 2.35 4.31 3.91 o 6 5 0 3.49 5.23 5.46 o 0 6 0 203.31 189.25 7.06 o 2 6 0 22.94 16.79 7.82 o 4 6 0 626.84 571.11 55.40 o 6 6 0 8.26 10.42 5.37 o 2 7 0 41.18 43.13 5.20 o 4 7 0 200.11 201.88 24.44 o 6 7 0 0.07 -7.09 7.09 o 0 8 0 283.96 276.17 9.98 o 2 8 0 156.67 158.74 13.73 o 4 8 0 180.32 177.52 19.08 o 6 8 0 95.02 126.69 9.89 o 2 9 0 738.51 725.01 31.92 o 4 9 0 207.65 208.92 36.00 o 6 9 0 101.38 119.61 11.49 o 0 10 0 379.19 384.16 13.49 o 2 10 0 240.98 233.63 11.45 o 4 10 0 73.48 67.82 8.38 o 2 11 0 81.79 74.85 16.71 o 4 11 0 1.41 0.82 8.57 o 0 12 0 166.65 156.65 10.43 o 2 12 0 69.54 82.32 21.44 o 4 12 0 8.95 12.43 5.68 o 2 13 0 64.96 61.88 9.51 o 1 1 1 1374.50 1275.62 117.35 o 2 1 1 29.96 34.66 9.29 o 3 1 1 450.44 454.75 11.05 o 4 1 1 42.15 44.27 4.97 o 5 1 1 32.53 24.61 14.40 o 6 1 1 118.67 107.88 8.87 o 7 1 1 5.21 -0.98 5.56 o 0 2 1 1544.05 1259.20 98.44 o 1 2 1 3936.89 3791.24 506.19 o 2 2 1 1066.96 1130.92 94.93 o 3 2 1 353.39 337.73 23.28 o 4 2 1 29.84 29.86 4.20 o 5 2 1 8.44 14.00 4.46 o 6 2 1 106.16 121.28 10.43 o 7 2 1 20.27 15.21 10.26 o 1 3 1 7716.03 7282.40 731.83 o 2 3 1 1370.79 1377.27 182.92 o 3 3 1 108.81 104.52 7.10 o 4 3 1 469.35 470.54 13.12 o 5 3 1 0.74 -4.10 4.10 o 6 3 1 31.89 32.62 6.67 o 7 3 1 652.42 683.37 21.93 o 0 4 1 133.79 130.21 5.11 o 1 4 1 204.88 209.55 26.02 o 2 4 1 142.13 158.02 27.25 o 3 4 1 164.33 171.47 12.35 o 4 4 1 12.64 15.03 3.74 o 5 4 1 472.09 454.74 32.76 o 6 4 1 52.04 43.08 7.56 o 7 4 1 110.02 117.54 9.94 o 1 5 1 1668.13 1585.56 117.07 o 2 5 1 16.34 21.63 3.78 o 3 5 1 77.70 82.09 7.11 o 4 5 1 41.45 42.60 8.49 o 5 5 1 699.03 668.97 43.25 o 6 5 1 10.80 14.01 5.80 o 7 5 1 123.16 119.39 23.94 o 0 6 1 1645.22 1602.89 31.03 o 1 6 1 30.51 31.10 3.86 o 2 6 1 1338.07 1345.73 136.43 o 3 6 1 20.00 21.70 3.90 o 4 6 1 122.30 121.44 9.58 o 5 6 1 19.75 18.18 7.95 o 6 6 1 141.26 162.30 15.72 o 7 6 1 9.25 16.45 12.97 o 1 7 1 416.81 354.63 46.83 o 2 7 1 46.87 44.67 5.90 o 3 7 1 70.28 72.85 14.47 o 4 7 1 2.08 2.36 4.30 o 5 7 1 42.39 39.35 9.57 o 6 7 1 12.96 5.34 6.52 o 0 8 1 1226.10 1242.31 20.67 o 1 8 1 236.29 241.53 18.56 o 2 8 1 78.60 75.61 6.20 o 3 8 1 147.46 133.40 10.89 o 4 8 1 8.77 7.98 4.85 o 5 8 1 24.96 22.03 6.02 o 6 8 1 35.84 40.65 18.78 o 1 9 1 125.38 133.01 13.48 o 2 9 1 0.74 2.62 4.14 o 3 9 1 11.36 4.98 5.10 o 4 9 1 42.84 39.72 10.45 o 5 9 1 89.82 111.40 10.82 o 6 9 1 15.66 23.19 8.06 o 0 10 1 100.66 91.46 7.76 o 1 10 1 25.03 23.51 5.70 o 2 10 1 41.52 47.39 16.78 o 3 10 1 216.96 206.96 33.31 o 4 10 1 35.64 32.93 6.68 o 5 10 1 6.19 1.65 9.42 o 1 11 1 164.13 165.64 10.26 o 2 11 1 36.48 32.62 6.23 o 3 11 1 44.65 48.95 18.59 o 4 11 1 25.55 37.19 11.01 o 0 12 1 113.45 92.41 9.91 o 1 12 1 2.27 -1.46 5.46 o 2 12 1 0.07 4.04 4.95 o 3 12 1 149.22 137.94 15.89 o 4 12 1 13.60 18.29 6.52 o 1 13 1 14.48 19.06 12.35 o 2 13 1 61.19 53.02 8.09 o 0 0 2 10102.72 9700.46 197.77 o 1 0 2 739.15 687.50 12.05 o 2 0 2 643.59 695.33 15.19 o 3 0 2 1845.52 1972.76 31.06 o 4 0 2 226.08 217.12 12.93 o 5 0 2 269.42 242.98 14.79 o 6 0 2 179.24 165.78 15.48 o 7 0 2 94.68 104.19 13.19 o 1 1 2 1672.68 1779.02 136.38 o 2 1 2 618.81 756.50 59.42 o 3 1 2 78.70 83.05 6.04 o 4 1 2 777.47 798.64 23.34 o 5 1 2 73.55 74.95 7.42 o 6 1 2 109.63 102.67 8.52 o 7 1 2 471.61 417.42 17.53 o 0 2 2 3061.96 2590.00 222.11 o 1 2 2 21.22 28.37 2.82 o 2 2 2 920.16 927.12 103.37 o 3 2 2 66.22 70.08 5.17 o 4 2 2 101.35 98.73 6.83 o 5 2 2 152.78 149.35 8.70 o 6 2 2 1.76 2.00 4.85 o 7 2 2 36.34 28.66 12.33 o 1 3 2 7418.98 7514.37 718.24 o 2 3 2 4860.12 5045.28 580.32 o 3 3 2 47.19 47.91 4.19 o 4 3 2 916.97 933.54 90.78 o 5 3 2 934.04 889.83 61.82 o 6 3 2 2.85 9.60 4.35 o 7 3 2 28.24 43.77 7.01 o 0 4 2 5515.34 5535.13 302.69 o 1 4 2 1525.63 1439.33 135.51 o 2 4 2 24.21 24.60 3.25 o 3 4 2 25.05 27.42 6.97 o 4 4 2 121.41 102.63 10.47 o 5 4 2 137.88 132.34 15.60 o 6 4 2 203.71 196.40 33.62 o 7 4 2 11.76 6.79 7.68 o 1 5 2 594.02 554.25 52.71 o 2 5 2 763.21 744.57 65.45 o 3 5 2 250.41 259.42 24.19 o 4 5 2 929.21 887.95 63.15 o 5 5 2 6.70 11.11 4.84 o 6 5 2 126.52 110.96 9.40 o 7 5 2 8.16 8.44 7.07 o 0 6 2 775.66 736.95 36.93 o 1 6 2 805.66 837.41 81.70 o 2 6 2 654.25 626.15 50.95 o 3 6 2 17.15 10.30 4.72 o 4 6 2 403.80 401.59 36.89 o 5 6 2 15.30 14.82 11.76 o 6 6 2 0.49 10.88 4.98 o 7 6 2 28.40 31.06 7.50 o 1 7 2 123.45 122.24 19.80 o 2 7 2 14.06 14.15 6.48 o 3 7 2 13.10 9.29 11.67 o 4 7 2 34.89 31.66 5.87 o 5 7 2 41.86 41.11 7.86 o 6 7 2 15.26 11.34 7.03 o 0 8 2 196.61 181.19 8.64 o 1 8 2 19.71 18.46 4.47 o 2 8 2 5.55 5.29 4.04 o 3 8 2 290.57 260.77 16.10 o 4 8 2 71.89 67.29 8.75 o 5 8 2 22.60 26.32 14.80 o 6 8 2 48.19 53.37 16.09 o 1 9 2 211.25 189.32 12.14 o 2 9 2 204.17 185.27 15.62 o 3 9 2 122.84 129.47 8.80 o 4 9 2 14.05 22.19 5.52 o 5 9 2 0.83 0.27 5.04 o 6 9 2 43.81 50.85 8.48 o 0 10 2 45.66 49.39 5.80 o 1 10 2 73.20 69.97 7.21 o 2 10 2 62.59 66.96 22.41 o 3 10 2 0.01 6.56 4.10 o 4 10 2 50.65 61.89 8.02 o 5 10 2 55.71 55.35 12.06 o 1 11 2 62.85 53.62 6.69 o 2 11 2 32.78 40.46 6.10 o 3 11 2 16.52 19.00 11.54 o 4 11 2 16.17 14.70 5.59 o 0 12 2 381.13 412.46 21.52 o 1 12 2 14.00 5.25 6.47 o 2 12 2 23.99 21.47 6.67 o 3 12 2 50.45 44.82 9.19 o 4 12 2 19.68 28.19 11.00 o 1 13 2 67.59 69.31 14.77 o 2 13 2 3.29 -1.77 5.21 o 1 1 3 2456.09 2604.48 233.01 o 2 1 3 197.11 228.30 19.44 o 3 1 3 304.57 295.00 9.03 o 4 1 3 266.58 281.86 23.13 o 5 1 3 52.56 70.09 19.71 o 6 1 3 664.63 607.29 44.47 o 7 1 3 129.57 124.42 11.27 o 0 2 3 10283.04 9354.37 854.94 o 1 2 3 468.91 430.85 37.15 o 2 2 3 155.98 124.44 22.31 o 3 2 3 451.66 493.39 13.94 o 4 2 3 123.70 131.06 7.19 o 5 2 3 228.46 214.54 14.66 o 6 2 3 135.56 127.11 9.26 o 7 2 3 10.74 13.93 5.55 o 1 3 3 3723.99 3771.08 411.94 o 2 3 3 22.57 19.82 3.44 o 3 3 3 805.08 820.64 40.10 o 4 3 3 13.10 5.19 8.33 o 5 3 3 171.51 164.74 10.40 o 6 3 3 0.17 -2.64 3.47 o 7 3 3 2.20 4.31 6.36 o 0 4 3 64.60 70.63 4.07 o 1 4 3 22.62 21.14 2.90 o 2 4 3 372.13 321.25 21.39 o 3 4 3 6.66 11.98 3.77 o 4 4 3 163.34 171.60 21.94 o 5 4 3 104.63 116.57 11.65 o 6 4 3 4.90 -1.30 4.24 o 7 4 3 2.66 0.59 5.45 o 1 5 3 268.52 245.08 8.43 o 2 5 3 1292.31 1255.59 90.04 o 3 5 3 29.43 27.68 4.61 o 4 5 3 529.81 527.18 49.79 o 5 5 3 17.48 31.31 7.39 o 6 5 3 7.12 6.59 5.40 o 7 5 3 87.50 97.38 9.30 o 0 6 3 415.47 373.77 38.75 o 1 6 3 820.91 815.59 80.95 o 2 6 3 515.04 550.90 65.35 o 3 6 3 411.57 389.19 18.35 o 4 6 3 43.96 33.27 5.75 o 5 6 3 271.53 255.27 29.02 o 6 6 3 63.38 58.91 7.62 o 7 6 3 3.90 3.53 12.25 o 1 7 3 0.22 -0.72 4.86 o 2 7 3 224.90 262.46 31.78 o 3 7 3 0.89 0.04 3.33 o 4 7 3 13.57 13.97 4.69 o 5 7 3 162.01 163.57 10.80 o 6 7 3 45.79 48.44 8.00 o 0 8 3 244.86 223.34 17.49 o 1 8 3 52.68 54.88 5.33 o 2 8 3 71.21 83.62 6.52 o 3 8 3 985.11 1007.87 97.44 o 4 8 3 13.05 11.08 6.88 o 5 8 3 22.81 17.60 5.95 o 6 8 3 0.16 8.01 5.57 o 1 9 3 0.63 -4.19 4.19 o 2 9 3 97.65 99.85 20.40 o 3 9 3 107.89 100.27 10.63 o 4 9 3 0.02 -4.17 4.17 o 5 9 3 68.59 56.70 7.55 o 6 9 3 34.91 50.56 13.46 o 0 10 3 7.11 9.20 4.54 o 1 10 3 3.95 14.46 9.96 o 2 10 3 39.19 45.40 5.86 o 3 10 3 108.69 121.72 15.96 o 4 10 3 55.04 53.78 7.68 o 5 10 3 160.75 165.48 31.88 o 1 11 3 40.10 36.47 6.57 o 2 11 3 9.46 14.12 4.94 o 3 11 3 45.41 48.75 7.55 o 4 11 3 2.10 0.72 5.09 o 0 12 3 111.78 107.71 9.38 o 1 12 3 62.42 67.44 8.47 o 2 12 3 7.04 5.19 6.04 o 3 12 3 24.20 29.44 8.12 o 1 13 3 0.28 0.20 5.21 o 2 13 3 102.60 109.48 10.25 o 0 0 4 2226.81 1990.75 25.10 o 1 0 4 2131.77 2185.20 27.09 o 2 0 4 898.28 958.28 20.02 o 3 0 4 7599.56 8098.33 70.35 o 4 0 4 70.05 66.72 8.22 o 5 0 4 118.23 123.41 12.14 o 6 0 4 56.22 60.00 9.91 o 7 0 4 16.26 12.31 8.88 o 1 1 4 489.71 494.11 28.68 o 2 1 4 199.17 214.76 7.23 o 3 1 4 324.09 337.93 9.98 o 4 1 4 387.76 382.50 12.34 o 5 1 4 23.24 8.49 5.70 o 6 1 4 23.18 20.50 5.68 o 7 1 4 19.45 21.98 6.45 o 0 2 4 67.57 61.13 3.61 o 1 2 4 1968.23 1971.33 160.68 o 2 2 4 525.18 564.86 49.32 o 3 2 4 2092.70 2187.99 181.47 o 4 2 4 92.82 88.32 6.48 o 5 2 4 1333.31 1338.87 64.94 o 6 2 4 0.74 1.44 4.57 o 7 2 4 42.81 43.37 8.57 o 1 3 4 699.52 670.00 61.35 o 2 3 4 1987.06 2055.58 203.32 o 3 3 4 370.27 385.93 14.70 o 4 3 4 178.91 157.69 8.76 o 5 3 4 116.54 111.41 10.42 o 6 3 4 67.31 66.25 8.68 o 7 3 4 17.30 28.67 10.33 o 0 4 4 1065.60 1114.01 52.23 o 1 4 4 128.27 126.94 14.87 o 2 4 4 1198.31 1259.09 144.55 o 3 4 4 0.03 -3.04 3.04 o 4 4 4 251.75 247.41 10.38 o 5 4 4 20.70 20.42 5.53 o 6 4 4 32.10 14.44 9.04 o 7 4 4 0.58 -1.13 5.06 o 1 5 4 1440.83 1528.97 160.68 o 2 5 4 273.29 257.27 23.16 o 3 5 4 2.45 -1.00 3.96 o 4 5 4 238.54 244.63 22.08 o 5 5 4 15.56 5.81 4.98 o 6 5 4 18.20 19.26 6.93 o 7 5 4 0.00 -4.04 5.92 o 0 6 4 61.15 60.71 4.67 o 1 6 4 755.57 727.70 58.78 o 2 6 4 1321.77 1335.88 182.67 o 3 6 4 303.61 322.70 23.92 o 4 6 4 238.39 257.52 22.17 o 5 6 4 5.43 9.16 5.85 o 6 6 4 11.53 8.25 5.25 o 7 6 4 38.95 41.72 8.14 o 1 7 4 7.20 9.95 3.55 o 2 7 4 417.86 427.90 57.85 o 3 7 4 0.53 6.86 4.57 o 4 7 4 713.23 675.34 85.40 o 5 7 4 42.62 47.85 9.00 o 6 7 4 21.23 25.00 7.05 o 0 8 4 536.59 525.87 50.07 o 1 8 4 137.26 135.11 10.31 o 2 8 4 60.37 51.46 6.00 o 3 8 4 0.29 3.39 5.02 o 4 8 4 0.04 -2.68 3.91 o 5 8 4 0.32 -0.21 5.51 o 6 8 4 45.96 48.02 15.00 o 1 9 4 122.32 117.52 9.05 o 2 9 4 89.99 107.30 18.56 o 3 9 4 101.73 97.33 16.44 o 4 9 4 30.30 14.89 6.23 o 5 9 4 46.02 63.96 13.94 o 0 10 4 232.74 242.12 26.06 o 1 10 4 8.78 11.77 5.19 o 2 10 4 68.57 70.13 8.38 o 3 10 4 11.35 16.25 6.12 o 4 10 4 5.96 10.04 5.85 o 5 10 4 22.76 26.23 7.42 o 1 11 4 48.10 50.75 8.43 o 2 11 4 92.57 99.08 15.21 o 3 11 4 48.37 55.45 7.37 o 4 11 4 41.61 50.43 7.79 o 0 12 4 271.67 285.83 13.55 o 1 12 4 9.40 10.61 5.40 o 2 12 4 2.78 7.95 10.77 o 3 12 4 30.82 36.88 9.99 o 1 13 4 3.91 -6.83 7.23 o 2 13 4 14.50 16.22 7.64 o 1 1 5 1589.98 1648.19 97.85 o 2 1 5 430.01 439.03 28.42 o 3 1 5 406.27 447.41 11.88 o 4 1 5 113.29 125.75 9.44 o 5 1 5 367.61 345.64 13.22 o 6 1 5 182.11 199.92 11.43 o 7 1 5 16.86 21.04 6.24 o 0 2 5 70.52 66.35 4.06 o 1 2 5 55.38 56.38 8.94 o 2 2 5 785.88 943.77 85.28 o 3 2 5 194.08 194.54 10.67 o 4 2 5 296.17 304.44 11.20 o 5 2 5 1.06 4.25 4.77 o 6 2 5 47.62 47.25 7.25 o 7 2 5 6.16 4.46 4.98 o 1 3 5 0.48 -0.92 2.22 o 2 3 5 255.35 266.57 14.18 o 3 3 5 29.68 28.04 4.15 o 4 3 5 299.97 317.73 24.77 o 5 3 5 94.05 100.45 8.23 o 6 3 5 12.52 2.87 5.96 o 7 3 5 3.20 4.20 5.99 o 0 4 5 214.65 210.01 18.48 o 1 4 5 3.74 5.69 6.55 o 2 4 5 152.77 169.42 23.38 o 3 4 5 339.01 371.82 14.56 o 4 4 5 457.75 467.13 55.63 o 5 4 5 106.44 89.63 18.00 o 6 4 5 20.19 9.28 6.91 o 7 4 5 16.36 16.77 6.13 o 1 5 5 40.81 54.55 11.21 o 2 5 5 1822.64 1913.98 223.70 o 3 5 5 77.82 79.38 6.79 o 4 5 5 38.03 41.72 7.08 o 5 5 5 17.20 19.82 5.08 o 6 5 5 21.50 30.47 7.31 o 7 5 5 0.21 -1.70 4.54 o 0 6 5 24.06 23.18 3.34 o 1 6 5 0.00 -1.98 3.03 o 2 6 5 156.10 158.43 25.56 o 3 6 5 156.93 180.01 18.32 o 4 6 5 35.09 38.72 6.69 o 5 6 5 4.72 12.03 5.15 o 6 6 5 1.00 4.65 5.35 o 1 7 5 22.77 24.55 4.04 o 2 7 5 59.34 53.92 10.51 o 3 7 5 160.72 146.35 25.98 o 4 7 5 171.39 188.51 17.58 o 5 7 5 32.50 30.29 7.07 o 6 7 5 28.19 22.80 6.73 o 0 8 5 111.15 97.14 7.45 o 1 8 5 243.23 235.82 23.32 o 2 8 5 20.24 26.95 15.45 o 3 8 5 92.53 91.08 8.76 o 4 8 5 150.74 140.31 26.96 o 5 8 5 156.34 157.81 20.91 o 6 8 5 44.43 47.37 7.46 o 1 9 5 38.80 41.11 8.51 o 2 9 5 175.66 175.96 30.10 o 3 9 5 54.20 51.58 6.91 o 4 9 5 88.31 93.10 8.30 o 5 9 5 160.22 151.25 11.17 o 0 10 5 211.81 200.08 10.73 o 1 10 5 80.88 84.31 17.32 o 2 10 5 3.33 2.62 4.62 o 3 10 5 198.76 223.31 16.23 o 4 10 5 24.22 19.04 6.60 o 5 10 5 57.52 39.65 9.52 o 1 11 5 180.65 201.34 11.90 o 2 11 5 164.89 160.40 11.13 o 3 11 5 0.17 1.42 6.90 o 4 11 5 74.42 77.84 9.25 o 0 12 5 99.82 114.23 9.83 o 1 12 5 19.34 16.06 6.44 o 2 12 5 19.56 23.95 6.68 o 3 12 5 5.74 -3.53 9.22 o 1 13 5 92.21 93.18 9.83 o 0 0 6 5013.10 5043.69 49.99 o 1 0 6 80.55 77.02 7.04 o 2 0 6 0.03 9.04 4.07 o 3 0 6 1988.08 2146.37 37.66 o 4 0 6 329.62 355.72 17.61 o 5 0 6 226.61 189.04 15.85 o 6 0 6 67.01 63.38 11.25 o 7 0 6 27.06 18.27 10.76 o 1 1 6 309.15 290.95 8.54 o 2 1 6 14.28 18.41 4.11 o 3 1 6 63.93 63.82 6.24 o 4 1 6 126.44 147.60 8.29 o 5 1 6 7.70 13.18 4.96 o 6 1 6 45.49 29.39 6.72 o 7 1 6 2.36 -4.32 4.32 o 0 2 6 3053.99 2948.83 75.73 o 1 2 6 319.15 322.20 10.89 o 2 2 6 2868.70 3175.45 162.97 o 3 2 6 92.37 84.16 12.18 o 4 2 6 287.68 288.80 24.85 o 5 2 6 38.90 33.13 6.39 o 6 2 6 154.66 156.19 15.69 o 7 2 6 11.06 13.52 16.32 o 1 3 6 1414.85 1439.15 90.21 o 2 3 6 385.52 391.96 21.21 o 3 3 6 291.97 319.27 24.52 o 4 3 6 35.24 44.06 6.82 o 5 3 6 33.47 38.81 5.97 o 6 3 6 1.97 7.31 5.40 o 7 3 6 2.82 1.31 5.72 o 0 4 6 277.47 288.16 14.60 o 1 4 6 131.06 135.84 6.76 o 2 4 6 86.92 94.01 13.09 o 3 4 6 335.77 328.70 20.24 o 4 4 6 15.95 11.07 4.74 o 5 4 6 311.63 305.25 27.81 o 6 4 6 11.86 -0.03 5.99 o 7 4 6 0.28 2.21 10.01 o 1 5 6 396.68 370.52 35.22 o 2 5 6 9.71 11.29 3.43 o 3 5 6 94.39 97.61 13.05 o 4 5 6 136.76 121.17 8.43 o 5 5 6 11.68 12.23 6.85 o 6 5 6 109.22 90.86 9.82 o 7 5 6 132.19 136.04 18.24 o 0 6 6 0.02 -0.02 3.46 o 1 6 6 436.36 461.83 26.78 o 2 6 6 269.44 279.10 10.73 o 3 6 6 709.25 656.88 71.16 o 4 6 6 6.37 11.83 4.76 o 5 6 6 0.23 -1.31 4.40 o 6 6 6 94.64 112.50 9.75 o 1 7 6 74.74 86.16 6.71 o 2 7 6 323.21 322.01 28.05 o 3 7 6 73.62 76.86 7.66 o 4 7 6 147.80 141.21 12.76 o 5 7 6 61.32 53.21 7.44 o 6 7 6 12.56 13.19 6.25 o 0 8 6 545.33 540.21 42.85 o 1 8 6 98.87 109.83 10.54 o 2 8 6 10.31 4.61 5.88 o 3 8 6 277.14 284.12 49.77 o 4 8 6 0.82 0.33 6.52 o 5 8 6 51.13 61.65 15.83 o 6 8 6 36.56 45.69 11.51 o 1 9 6 311.41 304.92 29.45 o 2 9 6 0.32 -6.67 9.75 o 3 9 6 20.66 21.75 6.60 o 4 9 6 42.03 56.76 13.17 o 5 9 6 56.08 64.67 8.41 o 0 10 6 38.87 40.08 9.33 o 1 10 6 216.97 224.51 21.41 o 2 10 6 248.83 246.61 22.64 o 3 10 6 5.01 6.81 5.48 o 4 10 6 27.96 24.04 6.48 o 1 11 6 2.04 8.21 4.57 o 2 11 6 293.67 327.32 51.68 o 3 11 6 1.69 -3.46 8.62 o 4 11 6 230.80 227.53 14.51 o 0 12 6 19.56 12.40 10.42 o 1 12 6 21.41 19.52 6.11 o 2 12 6 2.79 0.35 4.56 o 3 12 6 147.78 171.37 23.36 o 1 13 6 23.81 28.43 8.08 o 1 1 7 434.88 489.81 11.83 o 2 1 7 1433.60 1506.23 91.45 o 3 1 7 36.12 37.60 5.69 o 4 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