#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:22:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181013 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/93/2209328.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209328_Fobs loop_ _publ_author_name 'Banu, Afroza' 'Golzar Hossain, G. M.' _publ_section_title ; A new polymorph of sulfanilic acid monohydrate ; _journal_coeditor_code TK2027 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2252 _journal_page_last o2253 _journal_volume 62 _journal_year 2006 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1630 _cell_length_b 6.9607 _cell_length_c 18.3251 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.8027 _cod_data_source_file tk2027Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2654.44 2669.12 52.56 o 4 0 0 587.00 629.72 19.12 o 6 0 0 28.86 33.60 4.94 o 1 1 0 4803.52 4700.34 56.54 o 2 1 0 504.62 546.17 17.59 o 3 1 0 585.59 629.34 18.92 o 4 1 0 98.11 102.67 5.35 o 5 1 0 36.22 5.60 14.31 o 6 1 0 33.47 32.56 5.19 o 0 2 0 21285.86 18698.87 132.50 o 1 2 0 801.39 765.45 21.49 o 2 2 0 3.28 10.04 2.32 o 3 2 0 49.36 48.37 3.86 o 4 2 0 1166.96 1156.18 38.62 o 5 2 0 75.27 104.29 6.80 o 6 2 0 152.07 144.28 10.37 o 7 2 0 1.98 4.56 16.47 o 1 3 0 222.13 209.53 6.22 o 2 3 0 190.76 208.79 6.55 o 3 3 0 0.00 4.27 7.96 o 4 3 0 28.21 1.37 11.12 o 5 3 0 21.41 29.70 4.40 o 6 3 0 5.37 1.78 14.19 o 7 3 0 48.63 37.92 7.47 o 0 4 0 1923.69 2005.63 44.10 o 1 4 0 1525.30 1469.92 39.04 o 2 4 0 9.03 10.62 3.07 o 3 4 0 20.19 23.31 3.90 o 4 4 0 562.46 570.52 15.89 o 5 4 0 94.77 94.75 8.09 o 6 4 0 56.33 55.96 7.43 o 1 5 0 197.05 185.35 7.43 o 2 5 0 420.29 398.82 12.40 o 3 5 0 132.08 130.30 7.55 o 4 5 0 27.36 3.40 14.85 o 5 5 0 44.76 30.74 7.01 o 6 5 0 0.86 2.45 19.75 o 0 6 0 811.91 875.46 24.18 o 1 6 0 934.29 884.26 27.13 o 2 6 0 19.41 6.39 16.26 o 3 6 0 3.97 12.65 3.77 o 4 6 0 83.39 83.09 8.09 o 1 7 0 8.87 14.77 4.98 o 2 7 0 112.22 115.61 9.50 o 4 7 0 0.07 1.78 14.10 o 0 8 0 14.96 4.44 6.14 o 1 8 0 38.54 34.89 7.05 o 1 0 1 4070.10 3843.61 233.41 o 2 0 1 32.54 23.98 2.65 o 3 0 1 64.79 76.31 3.24 o 4 0 1 625.62 732.12 15.79 o 5 0 1 83.00 99.32 4.81 o 6 0 1 9.28 7.26 4.19 o 7 0 1 36.14 28.75 6.84 o 0 1 1 23.47 22.74 1.04 o 1 1 1 4663.43 4599.66 40.89 o 2 1 1 1914.74 2087.67 34.92 o 3 1 1 1632.14 1879.53 46.36 o 4 1 1 293.56 312.30 13.59 o 5 1 1 128.15 145.10 5.16 o 6 1 1 1.07 1.64 8.95 o 7 1 1 6.50 13.32 20.33 o 0 2 1 687.83 661.68 13.13 o 1 2 1 1297.95 1204.85 41.32 o 2 2 1 527.31 554.42 11.78 o 3 2 1 125.88 114.61 4.31 o 4 2 1 229.69 242.13 5.94 o 5 2 1 495.72 482.58 9.44 o 6 2 1 0.84 0.62 4.98 o 7 2 1 41.67 40.03 5.16 o 0 3 1 9.82 11.71 1.67 o 1 3 1 359.78 375.59 7.53 o 2 3 1 1082.47 1066.71 31.36 o 3 3 1 705.60 747.69 17.05 o 4 3 1 234.82 266.03 6.48 o 5 3 1 138.60 140.23 5.76 o 6 3 1 4.39 2.95 5.52 o 7 3 1 12.10 13.44 6.72 o 0 4 1 5.31 3.69 2.42 o 1 4 1 931.83 972.20 22.45 o 2 4 1 40.04 40.58 4.46 o 3 4 1 218.03 221.63 16.12 o 4 4 1 98.50 96.29 10.37 o 5 4 1 194.60 194.04 7.26 o 6 4 1 14.73 8.89 3.78 o 0 5 1 33.91 40.47 2.99 o 1 5 1 470.62 461.34 24.83 o 2 5 1 515.34 542.41 10.99 o 3 5 1 51.43 50.64 3.91 o 4 5 1 86.45 98.08 6.45 o 5 5 1 4.33 1.58 12.78 o 6 5 1 3.14 1.78 14.39 o 0 6 1 283.92 276.60 7.28 o 1 6 1 369.51 346.67 10.35 o 2 6 1 139.23 126.41 5.67 o 3 6 1 67.34 66.97 4.70 o 4 6 1 28.53 20.59 10.93 o 5 6 1 37.58 42.33 13.65 o 0 7 1 3.32 2.20 17.42 o 1 7 1 81.40 73.20 5.60 o 2 7 1 150.06 156.50 7.20 o 3 7 1 14.37 11.41 4.94 o 4 7 1 19.45 22.67 4.19 o 0 8 1 39.52 39.61 6.68 o 1 8 1 42.56 36.15 16.63 o 2 8 1 44.90 40.76 5.41 o 0 0 2 10.45 8.30 0.73 o 1 0 2 1036.91 971.70 30.95 o 2 0 2 127.90 126.59 2.87 o 3 0 2 2978.63 3186.44 118.52 o 4 0 2 4.04 0.53 2.66 o 5 0 2 3.22 0.35 2.32 o 6 0 2 0.00 0.79 3.96 o 7 0 2 7.13 2.42 13.22 o 0 1 2 2435.77 2487.63 27.41 o 1 1 2 586.67 661.93 32.94 o 2 1 2 1146.74 1107.11 18.54 o 3 1 2 74.29 90.45 3.15 o 4 1 2 437.62 401.18 8.67 o 5 1 2 1.74 4.81 2.95 o 6 1 2 128.42 125.79 8.88 o 7 1 2 25.62 19.33 4.50 o 0 2 2 3203.70 3293.90 41.99 o 1 2 2 5277.32 5410.15 54.66 o 2 2 2 246.94 298.43 19.23 o 3 2 2 251.08 287.53 6.31 o 4 2 2 74.41 74.96 3.60 o 5 2 2 16.88 15.97 2.89 o 6 2 2 44.29 32.06 12.55 o 7 2 2 30.48 37.99 5.70 o 0 3 2 36.98 22.77 2.36 o 1 3 2 517.45 548.36 10.37 o 2 3 2 622.02 672.54 13.48 o 3 3 2 91.50 89.90 3.74 o 4 3 2 626.30 623.19 18.13 o 5 3 2 42.88 47.44 3.95 o 6 3 2 176.77 161.29 7.83 o 7 3 2 48.39 49.95 6.64 o 0 4 2 168.33 190.75 11.41 o 1 4 2 798.71 869.95 20.12 o 2 4 2 16.53 17.88 2.40 o 3 4 2 226.61 254.92 10.47 o 4 4 2 77.60 73.32 4.98 o 5 4 2 4.17 0.72 3.91 o 6 4 2 34.68 36.15 15.58 o 0 5 2 997.63 992.12 20.79 o 1 5 2 62.71 68.58 3.66 o 2 5 2 764.88 799.99 17.37 o 3 5 2 27.66 22.55 3.30 o 4 5 2 79.18 86.18 4.87 o 5 5 2 2.26 2.24 17.96 o 6 5 2 30.24 33.67 7.82 o 0 6 2 211.95 208.40 6.71 o 1 6 2 6.47 11.38 3.61 o 2 6 2 100.44 108.33 7.51 o 3 6 2 260.01 242.11 9.00 o 4 6 2 28.49 30.83 4.34 o 5 6 2 0.38 12.24 5.06 o 0 7 2 219.70 220.70 7.49 o 1 7 2 61.46 62.35 6.41 o 2 7 2 227.15 238.89 8.70 o 3 7 2 66.48 67.23 5.16 o 4 7 2 11.75 15.14 8.13 o 0 8 2 31.88 27.72 4.44 o 1 8 2 7.92 7.34 6.22 o 2 8 2 13.30 13.56 7.36 o 1 0 3 1939.24 1989.70 27.00 o 2 0 3 1408.48 1474.80 29.58 o 3 0 3 132.98 119.11 4.83 o 4 0 3 653.42 653.32 22.98 o 5 0 3 0.92 1.41 11.28 o 6 0 3 0.98 1.87 14.85 o 7 0 3 24.34 14.99 6.95 o 0 1 3 0.15 0.26 1.39 o 1 1 3 2403.03 2415.37 32.73 o 2 1 3 95.94 100.08 2.71 o 3 1 3 303.42 251.09 5.44 o 4 1 3 36.64 43.37 2.90 o 5 1 3 202.98 181.15 5.70 o 6 1 3 128.01 115.06 8.69 o 7 1 3 37.53 42.93 6.72 o 0 2 3 747.60 712.10 33.33 o 1 2 3 311.41 350.02 6.96 o 2 2 3 480.92 529.55 16.24 o 3 2 3 35.64 33.60 2.53 o 4 2 3 82.06 69.80 3.58 o 5 2 3 50.51 39.39 3.84 o 6 2 3 14.60 17.96 3.53 o 7 2 3 39.71 34.50 17.65 o 0 3 3 171.82 170.65 4.04 o 1 3 3 16.58 25.76 2.39 o 2 3 3 159.61 166.05 4.16 o 3 3 3 560.04 534.19 10.45 o 4 3 3 219.04 228.23 6.22 o 5 3 3 550.16 503.24 10.70 o 6 3 3 28.81 25.86 4.53 o 7 3 3 60.41 67.09 6.88 o 0 4 3 10.64 12.57 2.53 o 1 4 3 177.29 192.41 10.99 o 2 4 3 155.51 150.04 4.47 o 3 4 3 48.00 51.52 3.37 o 4 4 3 55.95 55.50 4.29 o 5 4 3 9.09 10.98 2.81 o 6 4 3 11.16 2.70 21.61 o 0 5 3 153.28 153.32 4.87 o 1 5 3 545.57 559.75 14.85 o 2 5 3 60.93 54.73 5.16 o 3 5 3 331.37 341.02 8.36 o 4 5 3 50.19 50.21 4.65 o 5 5 3 112.13 100.48 5.93 o 6 5 3 8.20 6.59 3.94 o 0 6 3 23.58 19.89 3.48 o 1 6 3 206.10 217.95 6.85 o 2 6 3 16.88 19.57 2.99 o 3 6 3 154.97 162.35 6.83 o 4 6 3 17.45 26.83 4.81 o 5 6 3 27.56 25.84 10.00 o 0 7 3 46.17 46.99 4.75 o 1 7 3 97.37 86.02 5.98 o 2 7 3 84.64 91.91 5.79 o 3 7 3 133.07 143.39 7.78 o 4 7 3 27.30 25.01 5.85 o 0 8 3 24.59 22.67 4.66 o 1 8 3 70.83 65.63 6.07 o 2 8 3 46.42 44.33 5.79 o 0 0 4 2602.17 2534.84 37.25 o 1 0 4 0.01 6.32 2.26 o 2 0 4 3.96 24.84 4.07 o 3 0 4 899.48 939.37 25.70 o 4 0 4 1065.58 1126.19 21.50 o 5 0 4 99.39 87.71 8.15 o 6 0 4 56.76 45.48 4.26 o 7 0 4 15.33 17.21 5.98 o 0 1 4 1113.61 1086.92 18.73 o 1 1 4 220.85 238.93 4.81 o 2 1 4 1028.82 1084.31 24.72 o 3 1 4 746.56 732.14 21.20 o 4 1 4 199.59 198.46 5.29 o 5 1 4 223.63 241.89 7.11 o 6 1 4 4.07 0.54 4.40 o 7 1 4 92.34 93.59 6.57 o 0 2 4 2528.82 2297.81 64.61 o 1 2 4 1034.46 1047.15 18.21 o 2 2 4 128.45 112.80 3.46 o 3 2 4 278.73 291.85 6.03 o 4 2 4 1532.16 1497.97 31.93 o 5 2 4 40.57 34.35 16.07 o 6 2 4 99.50 89.11 6.14 o 7 2 4 0.02 2.03 11.47 o 0 3 4 481.67 532.01 12.19 o 1 3 4 313.53 309.15 6.61 o 2 3 4 64.28 71.39 6.41 o 3 3 4 230.84 229.49 5.57 o 4 3 4 498.20 455.00 10.46 o 5 3 4 12.09 21.83 3.36 o 6 3 4 56.21 58.60 5.31 o 7 3 4 34.29 31.82 10.18 o 0 4 4 2031.93 2049.03 32.79 o 1 4 4 161.56 182.31 8.86 o 2 4 4 207.15 200.69 5.87 o 3 4 4 83.19 81.56 7.40 o 4 4 4 712.68 737.19 14.66 o 5 4 4 49.08 37.31 9.71 o 6 4 4 51.11 51.94 5.44 o 0 5 4 48.75 43.95 2.90 o 1 5 4 122.33 118.85 4.56 o 2 5 4 44.36 40.33 3.88 o 3 5 4 57.81 55.79 3.87 o 4 5 4 150.59 143.91 10.47 o 5 5 4 21.41 7.46 5.74 o 6 5 4 40.74 33.68 7.05 o 0 6 4 679.59 683.44 14.64 o 1 6 4 49.42 50.34 4.19 o 2 6 4 66.53 57.62 4.50 o 3 6 4 77.75 72.12 4.94 o 4 6 4 238.64 247.19 8.49 o 5 6 4 29.60 25.38 4.96 o 0 7 4 0.60 1.87 4.52 o 1 7 4 14.82 11.48 3.80 o 2 7 4 13.26 8.78 4.83 o 3 7 4 61.39 51.92 5.99 o 4 7 4 33.83 34.64 4.54 o 0 8 4 143.02 152.19 8.27 o 1 8 4 40.55 40.71 5.16 o 2 8 4 45.91 56.94 6.93 o 1 0 5 10299.92 9239.67 69.28 o 2 0 5 43.09 45.46 2.15 o 3 0 5 493.83 484.07 16.14 o 4 0 5 0.48 4.31 7.82 o 5 0 5 1042.95 1005.00 21.87 o 6 0 5 136.29 123.73 15.93 o 7 0 5 1.21 8.10 5.24 o 0 1 5 49.05 59.64 1.97 o 1 1 5 307.77 269.46 7.32 o 2 1 5 12.56 16.08 1.61 o 3 1 5 67.86 85.97 10.39 o 4 1 5 16.71 12.74 6.20 o 5 1 5 385.96 362.37 9.40 o 6 1 5 90.53 107.01 7.22 o 7 1 5 24.58 24.01 8.90 o 0 2 5 104.01 118.07 5.08 o 1 2 5 640.33 581.49 11.78 o 2 2 5 543.12 590.97 13.07 o 3 2 5 327.11 337.86 7.92 o 4 2 5 164.75 183.61 5.38 o 5 2 5 1326.93 1404.36 28.58 o 6 2 5 78.77 88.89 5.60 o 7 2 5 34.53 41.94 5.66 o 0 3 5 341.18 353.96 7.30 o 1 3 5 1055.84 1135.34 57.23 o 2 3 5 196.04 233.25 5.19 o 3 3 5 59.92 67.36 3.40 o 4 3 5 8.89 9.35 4.67 o 5 3 5 78.43 80.03 4.85 o 6 3 5 142.08 138.68 6.76 o 7 3 5 54.38 48.66 8.79 o 0 4 5 230.34 212.06 5.09 o 1 4 5 257.71 248.14 5.69 o 2 4 5 82.88 90.31 3.92 o 3 4 5 239.54 227.37 6.10 o 4 4 5 179.23 195.36 6.58 o 5 4 5 557.26 509.19 12.11 o 6 4 5 87.94 80.61 6.51 o 0 5 5 28.86 29.24 3.98 o 1 5 5 96.41 93.97 4.19 o 2 5 5 17.98 13.30 3.28 o 3 5 5 31.88 36.29 3.56 o 4 5 5 23.98 18.37 4.38 o 5 5 5 77.07 77.07 5.59 o 6 5 5 31.18 36.84 19.87 o 0 6 5 397.00 361.41 8.74 o 1 6 5 263.50 278.97 7.71 o 2 6 5 111.91 126.72 7.84 o 3 6 5 61.25 62.80 7.61 o 4 6 5 79.77 84.46 5.84 o 5 6 5 68.04 81.56 6.24 o 0 7 5 33.62 34.64 4.01 o 1 7 5 20.26 23.23 12.78 o 2 7 5 4.05 1.45 11.66 o 3 7 5 24.49 33.16 11.70 o 4 7 5 3.01 14.02 5.14 o 0 8 5 13.79 8.78 5.86 o 1 8 5 16.28 17.50 9.08 o 2 8 5 9.58 16.39 5.06 o 0 0 6 4152.30 4158.15 49.13 o 1 0 6 1331.73 1424.94 35.72 o 2 0 6 25.72 20.41 2.74 o 3 0 6 167.69 184.90 4.83 o 4 0 6 28.26 18.50 3.32 o 5 0 6 12.84 5.03 10.13 o 6 0 6 83.01 77.95 5.69 o 7 0 6 20.55 19.66 6.43 o 0 1 6 2348.79 2116.49 35.87 o 1 1 6 124.81 133.73 3.31 o 2 1 6 852.13 817.58 18.23 o 3 1 6 231.52 242.07 5.53 o 4 1 6 777.82 768.32 47.91 o 5 1 6 88.72 77.86 4.47 o 6 1 6 117.61 117.36 6.56 o 7 1 6 15.71 2.67 15.00 o 0 2 6 141.96 111.77 6.74 o 1 2 6 791.78 852.17 18.04 o 2 2 6 43.83 41.19 2.60 o 3 2 6 304.49 314.86 0.82 o 4 2 6 184.86 193.09 12.88 o 5 2 6 31.00 34.61 3.59 o 6 2 6 200.69 197.40 8.28 o 7 2 6 25.97 21.44 9.04 o 0 3 6 993.08 911.44 27.32 o 1 3 6 525.28 523.45 10.70 o 2 3 6 501.82 536.28 12.36 o 3 3 6 316.24 331.00 7.43 o 4 3 6 655.20 614.46 12.96 o 5 3 6 86.07 97.63 6.37 o 6 3 6 92.54 96.32 6.01 o 0 4 6 127.80 128.82 4.09 o 1 4 6 141.66 148.38 8.82 o 2 4 6 139.42 136.27 6.53 o 3 4 6 111.83 102.84 4.65 o 4 4 6 87.99 86.88 4.99 o 5 4 6 24.76 23.39 12.34 o 6 4 6 54.52 60.63 5.81 o 0 5 6 94.08 101.95 4.21 o 1 5 6 103.59 97.19 4.27 o 2 5 6 167.78 171.07 5.78 o 3 5 6 224.00 221.58 7.03 o 4 5 6 267.71 282.52 8.96 o 5 5 6 5.74 2.91 5.71 o 0 6 6 89.81 86.67 4.93 o 1 6 6 138.84 128.49 5.67 o 2 6 6 58.59 56.73 4.23 o 3 6 6 10.39 10.44 6.12 o 4 6 6 3.96 3.75 3.39 o 5 6 6 7.74 3.83 13.43 o 0 7 6 6.72 5.84 10.15 o 1 7 6 31.29 35.23 4.58 o 2 7 6 42.16 41.93 4.36 o 3 7 6 104.87 87.44 6.51 o 4 7 6 104.37 108.60 8.01 o 0 8 6 1.75 8.04 7.16 o 1 8 6 10.76 7.14 6.51 o 2 8 6 18.35 20.82 8.86 o 1 0 7 4146.67 4192.63 54.16 o 2 0 7 44.47 43.20 5.35 o 3 0 7 162.28 178.33 4.73 o 4 0 7 131.28 130.53 7.05 o 5 0 7 395.24 390.39 9.09 o 6 0 7 36.63 38.14 6.45 o 7 0 7 7.35 22.33 12.63 o 0 1 7 154.62 164.61 7.09 o 1 1 7 1534.46 1470.48 23.60 o 2 1 7 1120.33 1124.75 22.29 o 3 1 7 798.75 798.56 17.23 o 4 1 7 5.44 4.98 2.70 o 5 1 7 424.75 438.27 13.57 o 6 1 7 23.07 20.22 9.71 o 7 1 7 51.92 57.97 6.26 o 0 2 7 150.05 146.41 3.70 o 1 2 7 105.42 108.27 3.84 o 2 2 7 284.08 330.88 7.01 o 3 2 7 203.19 209.97 11.14 o 4 2 7 37.52 37.43 3.16 o 5 2 7 46.84 43.29 4.06 o 6 2 7 8.61 0.92 5.04 o 7 2 7 8.96 9.95 4.26 o 0 3 7 59.05 62.73 2.88 o 1 3 7 375.64 386.69 8.25 o 2 3 7 104.57 99.01 4.65 o 3 3 7 548.05 550.26 33.85 o 4 3 7 41.63 43.88 3.84 o 5 3 7 299.08 295.05 8.69 o 6 3 7 13.46 19.86 4.46 o 0 4 7 19.80 17.52 2.19 o 1 4 7 77.39 94.41 3.82 o 2 4 7 20.57 21.45 2.37 o 3 4 7 69.98 65.59 4.00 o 4 4 7 93.80 86.02 5.01 o 5 4 7 11.43 7.93 4.03 o 6 4 7 5.47 10.51 5.63 o 0 5 7 57.59 60.90 5.91 o 1 5 7 316.21 322.88 7.38 o 2 5 7 175.36 174.12 6.32 o 3 5 7 267.32 275.09 7.90 o 4 5 7 20.90 29.83 5.43 o 5 5 7 111.70 118.07 6.89 o 0 6 7 119.58 103.10 5.10 o 1 6 7 43.67 43.57 4.00 o 2 6 7 12.01 6.65 3.42 o 3 6 7 17.30 15.70 3.92 o 4 6 7 105.60 87.62 6.63 o 5 6 7 5.18 2.90 23.31 o 0 7 7 14.30 13.43 3.89 o 1 7 7 54.37 52.88 4.95 o 2 7 7 41.17 50.21 22.94 o 3 7 7 78.52 85.64 6.25 o 0 0 8 170.01 157.15 3.67 o 1 0 8 365.19 375.04 11.66 o 2 0 8 442.18 450.60 9.69 o 3 0 8 254.58 252.81 7.30 o 4 0 8 1546.36 1523.11 48.58 o 5 0 8 138.06 140.43 5.69 o 6 0 8 101.40 105.72 6.24 o 7 0 8 11.44 5.00 5.59 o 0 1 8 3615.67 3587.08 55.95 o 1 1 8 2089.84 2099.79 40.93 o 2 1 8 131.84 114.63 3.62 o 3 1 8 137.16 131.60 4.30 o 4 1 8 408.34 381.17 17.26 o 5 1 8 22.07 22.99 3.68 o 6 1 8 4.79 6.07 5.66 o 7 1 8 8.54 6.18 6.99 o 0 2 8 814.45 758.09 16.51 o 1 2 8 32.70 36.92 4.79 o 2 2 8 301.75 319.36 6.10 o 3 2 8 8.03 6.60 3.28 o 4 2 8 508.42 511.30 19.48 o 5 2 8 78.87 68.04 6.18 o 6 2 8 95.27 103.57 6.06 o 0 3 8 284.25 272.37 5.56 o 1 3 8 53.81 60.45 2.90 o 2 3 8 15.22 17.62 2.32 o 3 3 8 345.03 335.50 10.29 o 4 3 8 471.20 472.12 20.33 o 5 3 8 71.38 67.49 5.50 o 6 3 8 28.20 34.04 8.96 o 0 4 8 235.70 256.67 5.98 o 1 4 8 96.88 104.84 4.14 o 2 4 8 80.04 79.87 6.47 o 3 4 8 199.22 195.05 6.45 o 4 4 8 178.10 183.60 6.73 o 5 4 8 53.08 60.89 5.15 o 6 4 8 69.45 65.10 25.30 o 0 5 8 678.40 664.54 14.80 o 1 5 8 125.32 132.74 9.23 o 2 5 8 190.45 173.81 6.24 o 3 5 8 39.21 27.20 7.30 o 4 5 8 66.67 63.76 5.16 o 5 5 8 18.67 17.18 9.23 o 0 6 8 28.11 33.99 15.43 o 1 6 8 37.50 32.02 4.90 o 2 6 8 61.41 64.49 7.11 o 3 6 8 112.63 132.02 6.60 o 4 6 8 140.04 148.52 7.86 o 0 7 8 157.40 131.88 6.42 o 1 7 8 48.87 46.18 4.73 o 2 7 8 24.38 22.65 4.33 o 3 7 8 36.15 36.67 9.60 o 0 8 8 34.93 24.84 5.84 o 1 8 8 13.83 21.07 6.70 o 1 0 9 713.76 702.59 15.41 o 2 0 9 494.47 537.67 10.37 o 3 0 9 489.32 479.63 21.36 o 4 0 9 514.69 493.71 10.27 o 5 0 9 245.78 242.08 9.48 o 6 0 9 1.56 0.88 4.36 o 7 0 9 70.40 79.99 6.61 o 0 1 9 27.87 28.69 5.04 o 1 1 9 42.77 49.42 2.57 o 2 1 9 82.57 77.62 3.32 o 3 1 9 18.04 3.39 7.70 o 4 1 9 631.74 617.04 21.57 o 5 1 9 142.32 149.87 6.35 o 6 1 9 14.62 19.54 5.10 o 0 2 9 350.11 359.56 14.95 o 1 2 9 2077.05 2052.84 32.65 o 2 2 9 514.50 511.03 10.44 o 3 2 9 601.16 591.55 18.27 o 4 2 9 34.14 30.94 5.72 o 5 2 9 211.89 193.72 10.83 o 0 3 9 504.34 522.22 1.49 o 1 3 9 218.16 220.34 5.52 o 2 3 9 40.66 41.46 3.96 o 3 3 9 198.29 201.91 8.69 o 4 3 9 148.22 124.85 5.75 o 5 3 9 27.39 18.91 9.17 o 6 3 9 4.31 6.91 4.57 o 0 4 9 42.16 38.32 3.17 o 1 4 9 1035.64 1045.39 45.80 o 2 4 9 263.69 268.29 6.67 o 3 4 9 281.09 283.77 7.68 o 4 4 9 11.21 15.14 4.96 o 5 4 9 111.31 106.03 6.42 o 6 4 9 10.22 9.83 18.42 o 0 5 9 15.42 13.26 7.05 o 1 5 9 122.92 107.95 4.93 o 2 5 9 0.36 0.50 2.82 o 3 5 9 134.03 122.04 5.93 o 4 5 9 13.32 22.50 3.91 o 5 5 9 98.83 93.82 7.01 o 0 6 9 16.94 21.11 3.20 o 1 6 9 104.66 101.54 5.46 o 2 6 9 202.23 197.36 7.91 o 3 6 9 104.89 111.56 6.27 o 4 6 9 23.75 22.40 7.56 o 0 7 9 2.66 7.59 2.87 o 1 7 9 26.33 30.73 4.13 o 2 7 9 6.81 14.15 5.23 o 3 7 9 22.54 27.17 6.31 o 0 0 10 2822.01 2673.65 70.69 o 1 0 10 4.01 0.71 2.55 o 2 0 10 626.99 616.98 14.06 o 3 0 10 19.46 25.02 2.54 o 4 0 10 7.12 4.78 3.14 o 5 0 10 29.36 23.13 3.90 o 6 0 10 57.27 36.71 20.70 o 0 1 10 1526.47 1533.98 53.08 o 1 1 10 11.12 10.99 2.95 o 2 1 10 143.61 157.61 8.36 o 3 1 10 424.83 429.96 9.23 o 4 1 10 713.07 732.57 15.69 o 5 1 10 33.92 33.32 6.14 o 6 1 10 150.56 157.58 7.42 o 0 2 10 637.05 601.49 12.67 o 1 2 10 237.04 249.96 5.80 o 2 2 10 232.30 224.46 5.51 o 3 2 10 228.14 217.43 5.98 o 4 2 10 21.28 17.86 3.12 o 5 2 10 16.94 11.16 3.78 o 6 2 10 90.15 88.56 11.91 o 0 3 10 3380.99 3594.35 89.73 o 1 3 10 239.67 235.09 5.76 o 2 3 10 198.07 191.10 5.47 o 3 3 10 294.11 277.73 7.03 o 4 3 10 109.56 116.44 5.50 o 5 3 10 29.53 32.75 5.58 o 6 3 10 22.41 16.22 8.01 o 0 4 10 373.79 367.84 7.60 o 1 4 10 103.72 111.43 4.69 o 2 4 10 280.03 272.60 6.91 o 3 4 10 20.26 22.35 6.35 o 4 4 10 22.28 23.31 5.77 o 5 4 10 5.66 6.02 5.81 o 0 5 10 268.37 265.52 7.42 o 1 5 10 26.87 24.49 3.39 o 2 5 10 74.02 82.24 13.50 o 3 5 10 117.65 104.65 5.93 o 4 5 10 102.08 119.11 6.10 o 5 5 10 108.37 111.93 18.40 o 0 6 10 208.13 215.32 8.10 o 1 6 10 96.24 82.71 5.90 o 2 6 10 231.61 252.99 8.85 o 4 6 10 32.87 36.87 5.41 o 0 7 10 51.97 62.01 5.92 o 1 7 10 52.75 52.12 5.28 o 2 7 10 30.52 32.75 5.11 o 3 7 10 8.73 2.07 16.51 o 1 0 11 161.50 160.48 4.47 o 2 0 11 202.04 217.51 5.34 o 3 0 11 142.24 130.76 4.65 o 4 0 11 13.99 7.43 4.27 o 5 0 11 14.23 14.78 6.78 o 6 0 11 4.72 2.32 18.71 o 0 1 11 57.66 62.72 5.60 o 1 1 11 349.89 321.73 6.67 o 2 1 11 166.29 161.31 4.74 o 3 1 11 251.78 242.36 6.12 o 4 1 11 62.55 61.91 4.25 o 5 1 11 281.93 265.60 13.69 o 6 1 11 7.96 10.18 5.55 o 0 2 11 102.31 97.79 3.76 o 1 2 11 31.99 29.61 5.10 o 2 2 11 104.66 101.25 3.96 o 3 2 11 12.95 2.82 12.20 o 4 2 11 156.52 159.65 6.14 o 5 2 11 90.39 74.65 5.51 o 6 2 11 1.01 2.25 12.61 o 0 3 11 6.28 5.07 3.42 o 1 3 11 1155.43 1150.88 3.08 o 2 3 11 27.47 29.76 2.98 o 3 3 11 210.19 212.07 11.59 o 4 3 11 124.84 132.11 5.98 o 5 3 11 110.01 105.84 6.11 o 6 3 11 5.58 12.15 5.64 o 0 4 11 0.89 0.41 3.32 o 1 4 11 47.01 42.91 3.24 o 2 4 11 138.35 141.05 5.73 o 3 4 11 0.33 6.80 3.44 o 4 4 11 58.28 53.54 4.85 o 5 4 11 40.24 43.60 5.25 o 0 5 11 0.77 1.70 13.52 o 1 5 11 412.26 430.76 9.65 o 2 5 11 58.74 60.05 6.28 o 3 5 11 91.19 85.50 7.22 o 4 5 11 54.71 64.37 5.55 o 5 5 11 88.67 98.51 7.78 o 0 6 11 42.32 38.75 7.70 o 1 6 11 16.69 5.50 11.68 o 2 6 11 8.09 4.19 5.72 o 3 6 11 16.57 2.26 12.84 o 4 6 11 4.14 4.40 5.14 o 0 7 11 51.17 47.58 8.84 o 1 7 11 252.24 271.81 10.09 o 2 7 11 25.18 17.93 9.06 o 0 0 12 156.73 190.97 5.26 o 1 0 12 4.04 1.18 2.63 o 2 0 12 40.17 49.60 6.93 o 3 0 12 6.05 4.25 7.65 o 4 0 12 21.55 18.26 3.31 o 5 0 12 18.35 12.44 5.89 o 6 0 12 28.84 32.32 4.80 o 0 1 12 1299.21 1279.08 29.46 o 1 1 12 138.13 151.33 4.72 o 2 1 12 144.13 131.71 4.72 o 3 1 12 226.61 221.28 8.38 o 4 1 12 531.18 526.78 11.02 o 5 1 12 7.95 5.69 4.38 o 6 1 12 42.34 49.80 10.41 o 0 2 12 852.58 794.20 25.84 o 1 2 12 45.49 46.79 2.96 o 2 2 12 170.15 158.28 8.07 o 3 2 12 51.51 47.32 3.93 o 4 2 12 4.25 8.24 4.04 o 5 2 12 27.52 34.33 8.71 o 6 2 12 8.29 2.71 15.36 o 0 3 12 1567.33 1499.74 32.83 o 1 3 12 118.05 110.79 4.50 o 2 3 12 254.93 251.78 6.69 o 3 3 12 426.90 434.58 9.68 o 4 3 12 214.49 216.00 16.01 o 5 3 12 18.46 11.65 5.78 o 0 4 12 394.16 381.51 15.45 o 1 4 12 22.58 18.34 3.44 o 2 4 12 180.14 193.34 10.52 o 3 4 12 21.58 26.24 5.33 o 4 4 12 6.10 9.62 4.98 o 5 4 12 22.02 17.67 4.95 o 0 5 12 409.72 396.68 9.55 o 1 5 12 98.25 94.06 5.89 o 2 5 12 40.87 46.14 4.52 o 3 5 12 80.12 70.75 5.76 o 4 5 12 120.68 122.74 15.83 o 0 6 12 8.41 8.89 5.03 o 1 6 12 10.20 9.26 5.52 o 2 6 12 87.77 91.70 8.71 o 3 6 12 0.35 0.71 5.68 o 0 7 12 92.62 115.10 6.79 o 1 7 12 38.58 36.02 5.12 o 2 7 12 6.86 7.73 6.20 o 1 0 13 696.15 623.90 13.25 o 2 0 13 10.31 6.80 2.48 o 3 0 13 746.98 730.95 15.78 o 4 0 13 4.02 1.49 4.31 o 5 0 13 413.78 420.63 22.07 o 6 0 13 3.11 1.78 6.10 o 0 1 13 50.51 52.53 3.69 o 1 1 13 442.98 474.45 10.32 o 2 1 13 59.11 57.05 3.78 o 3 1 13 77.67 81.07 4.52 o 4 1 13 30.28 19.46 5.39 o 5 1 13 64.73 65.54 7.05 o 6 1 13 2.58 2.95 23.52 o 0 2 13 32.06 28.72 2.80 o 1 2 13 1344.55 1352.47 31.65 o 2 2 13 13.83 12.74 3.57 o 3 2 13 283.20 266.33 7.61 o 4 2 13 2.80 5.49 2.92 o 5 2 13 88.86 88.22 6.26 o 6 2 13 15.20 20.69 4.19 o 0 3 13 159.88 183.05 5.69 o 1 3 13 47.68 54.39 6.39 o 2 3 13 234.93 227.18 11.24 o 3 3 13 76.92 68.96 4.56 o 4 3 13 216.78 213.50 8.42 o 5 3 13 49.38 51.07 5.20 o 0 4 13 200.81 219.16 6.86 o 1 4 13 421.27 420.11 9.63 o 2 4 13 251.95 243.71 14.44 o 3 4 13 88.51 90.62 5.52 o 4 4 13 32.96 34.26 4.98 o 5 4 13 47.58 48.74 5.88 o 0 5 13 166.06 173.34 6.93 o 1 5 13 12.56 6.97 5.27 o 2 5 13 27.94 24.56 4.28 o 3 5 13 10.54 7.63 5.31 o 4 5 13 21.44 22.44 6.68 o 0 6 13 10.53 3.32 5.68 o 1 6 13 54.84 65.58 10.12 o 2 6 13 102.00 106.48 8.13 o 3 6 13 69.14 76.14 6.56 o 0 7 13 11.48 6.56 16.19 o 1 7 13 23.75 26.61 5.54 o 0 0 14 29.56 29.71 2.77 o 1 0 14 8.35 11.69 7.16 o 2 0 14 507.91 513.56 11.42 o 3 0 14 22.19 21.86 4.85 o 4 0 14 809.29 766.31 16.02 o 5 0 14 1.59 0.50 4.15 o 6 0 14 124.94 155.91 8.40 o 0 1 14 985.61 917.94 18.10 o 1 1 14 664.59 713.25 15.18 o 2 1 14 43.69 49.63 8.75 o 3 1 14 29.71 30.70 3.20 o 4 1 14 220.83 210.05 10.91 o 5 1 14 40.34 40.03 4.44 o 6 1 14 5.00 9.54 6.14 o 0 2 14 450.66 426.85 8.90 o 1 2 14 166.91 159.48 5.94 o 2 2 14 896.09 913.64 27.17 o 3 2 14 160.75 165.73 9.44 o 4 2 14 379.51 369.26 10.53 o 5 2 14 10.93 7.07 6.08 o 0 3 14 869.51 828.63 18.48 o 1 3 14 162.41 159.80 5.94 o 2 3 14 23.50 25.43 4.77 o 3 3 14 154.26 144.63 7.72 o 4 3 14 64.63 63.00 5.57 o 5 3 14 7.55 15.39 7.67 o 0 4 14 227.59 219.47 7.22 o 1 4 14 75.98 66.44 5.08 o 2 4 14 313.99 321.08 9.05 o 3 4 14 249.83 246.20 8.92 o 4 4 14 105.13 118.65 7.03 o 0 5 14 88.54 101.01 6.22 o 1 5 14 92.19 82.78 5.82 o 2 5 14 67.89 70.80 5.49 o 3 5 14 48.38 49.18 9.21 o 4 5 14 50.54 53.19 5.83 o 0 6 14 0.22 1.13 5.73 o 1 6 14 14.65 11.86 5.60 o 2 6 14 23.59 24.70 5.32 o 1 0 15 60.30 48.85 3.53 o 2 0 15 0.61 2.38 8.29 o 3 0 15 155.83 158.63 6.41 o 4 0 15 12.38 17.80 9.15 o 5 0 15 88.66 87.56 6.01 o 0 1 15 82.85 79.80 4.43 o 1 1 15 592.69 541.54 53.12 o 2 1 15 205.22 199.54 6.42 o 3 1 15 79.01 92.97 5.27 o 4 1 15 0.06 3.90 14.10 o 5 1 15 417.59 419.14 12.18 o 0 2 15 117.42 94.23 4.96 o 1 2 15 48.07 45.52 4.83 o 2 2 15 174.00 170.05 6.30 o 3 2 15 69.34 67.88 4.79 o 4 2 15 9.07 5.10 5.23 o 5 2 15 47.18 46.38 5.85 o 0 3 15 558.40 505.27 10.15 o 1 3 15 851.72 832.25 17.70 o 2 3 15 41.96 44.78 4.92 o 3 3 15 38.75 44.81 5.97 o 4 3 15 28.12 29.22 4.76 o 5 3 15 108.04 107.36 15.89 o 0 4 15 53.00 37.14 17.17 o 1 4 15 95.82 91.49 5.29 o 2 4 15 11.62 1.95 15.60 o 3 4 15 47.66 51.32 4.62 o 4 4 15 6.18 0.75 6.02 o 0 5 15 153.40 164.01 7.39 o 1 5 15 63.83 73.79 9.96 o 2 5 15 14.19 15.94 3.69 o 3 5 15 59.02 56.87 11.57 o 0 6 15 36.64 44.22 7.51 o 1 6 15 57.12 60.36 7.43 o 2 6 15 13.30 8.36 7.24 o 0 0 16 7.46 6.36 3.84 o 1 0 16 53.60 60.69 4.32 o 2 0 16 182.25 153.27 6.12 o 3 0 16 52.04 46.65 4.34 o 4 0 16 34.58 37.55 19.23 o 5 0 16 2.91 1.18 5.77 o 0 1 16 411.53 426.65 10.25 o 1 1 16 250.28 236.13 7.14 o 2 1 16 18.83 19.78 3.46 o 3 1 16 36.45 35.75 3.68 o 4 1 16 266.46 273.28 8.73 o 5 1 16 17.93 17.12 6.67 o 0 2 16 5.51 4.18 8.95 o 1 2 16 24.15 20.87 5.83 o 2 2 16 116.02 101.33 5.38 o 3 2 16 53.35 44.85 5.12 o 4 2 16 6.48 2.03 16.14 o 5 2 16 1.74 7.92 4.77 o 0 3 16 855.87 820.09 18.82 o 1 3 16 97.75 99.76 5.46 o 2 3 16 105.87 102.55 6.12 o 3 3 16 56.81 53.90 4.92 o 4 3 16 114.37 127.72 7.45 o 0 4 16 27.78 28.56 4.71 o 1 4 16 6.49 4.46 3.47 o 2 4 16 34.68 28.71 4.25 o 3 4 16 52.50 55.82 8.03 o 4 4 16 0.75 3.05 5.60 o 0 5 16 110.52 117.96 8.28 o 1 5 16 24.69 35.21 4.53 o 2 5 16 71.57 75.03 5.93 o 3 5 16 18.59 24.80 4.69 o 0 6 16 1.05 2.53 14.34 o 1 6 16 12.44 3.62 5.41 o 1 0 17 19.14 18.77 2.88 o 2 0 17 23.70 18.89 8.73 o 3 0 17 106.11 89.94 5.92 o 4 0 17 11.21 7.09 6.14 o 5 0 17 238.32 253.64 17.40 o 0 1 17 1.89 2.75 3.87 o 1 1 17 42.37 45.25 4.40 o 2 1 17 75.97 81.64 4.91 o 3 1 17 134.71 119.27 6.69 o 4 1 17 21.77 15.31 4.64 o 5 1 17 136.79 131.67 8.24 o 0 2 17 12.68 14.69 4.92 o 1 2 17 94.30 90.31 6.37 o 2 2 17 22.86 31.19 8.75 o 3 2 17 134.75 122.50 6.94 o 4 2 17 33.05 9.32 15.39 o 0 3 17 19.09 5.40 11.44 o 1 3 17 318.79 318.21 9.46 o 2 3 17 43.09 43.96 4.30 o 3 3 17 49.63 48.76 5.05 o 4 3 17 9.33 7.43 5.68 o 0 4 17 48.81 61.73 4.41 o 1 4 17 103.82 99.15 5.95 o 2 4 17 5.14 11.49 5.43 o 3 4 17 120.62 123.05 7.96 o 0 5 17 2.39 1.48 4.62 o 1 5 17 55.81 54.96 6.43 o 2 5 17 34.23 35.24 4.97 o 0 0 18 328.50 346.13 9.61 o 1 0 18 12.07 6.54 4.52 o 2 0 18 205.76 199.44 7.95 o 3 0 18 47.76 47.28 4.97 o 4 0 18 513.83 488.77 13.55 o 0 1 18 1.91 6.02 3.61 o 1 1 18 26.04 22.13 11.22 o 2 1 18 48.91 39.70 5.58 o 3 1 18 13.35 13.52 6.12 o 4 1 18 1.94 3.86 6.03 o 0 2 18 642.77 611.34 21.53 o 1 2 18 9.68 11.81 3.71 o 2 2 18 217.82 199.93 17.15 o 3 2 18 2.16 9.25 4.98 o 4 2 18 220.69 211.56 14.19 o 0 3 18 4.94 2.49 20.04 o 1 3 18 7.25 5.09 4.52 o 2 3 18 51.35 57.13 4.55 o 3 3 18 81.96 91.46 11.08 o 0 4 18 205.70 221.89 8.93 o 1 4 18 84.52 95.94 11.80 o 2 4 18 98.04 93.26 6.95 o 3 4 18 76.70 73.34 6.48 o 0 5 18 14.40 10.45 4.22 o 1 5 18 24.91 12.45 16.82 o 1 0 19 64.78 77.14 5.62 o 2 0 19 9.38 14.72 7.84 o 3 0 19 223.10 219.12 8.64 o 4 0 19 55.90 81.62 6.43 o 0 1 19 1.69 0.58 3.77 o 1 1 19 178.32 172.91 7.55 o 2 1 19 11.99 12.03 5.10 o 3 1 19 182.88 203.33 9.79 o 4 1 19 47.86 61.45 5.82 o 0 2 19 61.42 62.73 5.26 o 1 2 19 372.34 384.73 11.21 o 2 2 19 47.22 45.18 4.84 o 3 2 19 171.12 192.02 8.44 o 0 3 19 1.79 4.92 4.24 o 1 3 19 51.58 48.51 5.70 o 2 3 19 51.44 50.98 5.21 o 3 3 19 109.73 122.04 7.47 o 0 4 19 26.15 18.66 4.36 o 1 4 19 116.90 114.81 7.26 o 2 4 19 71.68 64.58 6.13 o 0 0 20 25.84 22.95 3.92 o 1 0 20 17.32 4.19 15.14 o 2 0 20 6.59 8.75 16.43 o 3 0 20 0.42 0.71 5.77 o 0 1 20 374.58 368.06 10.74 o 1 1 20 4.27 6.60 4.52 o 2 1 20 112.86 110.37 8.46 o 3 1 20 11.31 2.28 18.13 o 0 2 20 19.27 23.40 4.30 o 1 2 20 3.03 2.20 17.63 o 2 2 20 18.12 19.97 6.47 o 3 2 20 22.34 18.57 4.78 o 0 3 20 400.22 410.81 13.65 o 1 3 20 76.80 71.17 6.19 o 2 3 20 117.67 126.09 12.44 o 0 4 20 23.57 34.59 18.36 o 1 4 20 1.69 3.26 5.34 o 1 0 21 251.26 282.67 9.86 o 2 0 21 0.02 1.48 5.32 o 3 0 21 20.31 22.28 7.26 o 0 1 21 0.01 1.14 5.75 o 1 1 21 241.75 259.31 16.70 o 2 1 21 4.23 2.90 23.11 o 0 2 21 0.01 5.31 5.31 o 1 2 21 54.01 50.81 5.72 o 2 2 21 73.21 66.83 5.88 o 0 3 21 24.14 28.62 5.04 o 1 3 21 283.23 295.43 10.75 o 0 0 22 672.27 801.06 17.36 o 1 0 22 0.11 1.21 6.04 o 2 0 22 75.18 90.99 6.98 o 0 1 22 1.11 1.78 5.14 o 1 1 22 17.41 16.48 6.08 o 0 2 22 552.21 576.49 30.45 o 1 2 22 35.63 43.24 5.69 o