#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/93/2209384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209384_Fobs loop_ _publ_author_name 'Nellas, Ricky B.' 'Fronczek, Frank R.' 'Newkome, George R.' 'Watkins, Steven F.' 'Xia, Yuanjiao' _publ_section_title ; [6,6'-Bis(chloromethyl)-2,2'-bipyridyl]dichlorocobalt(II) ; _journal_coeditor_code BH2020 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1522 _journal_page_last m1523 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.847 _cell_angle_gamma 90.000 _cell_length_a 7.4783 _cell_length_b 15.7270 _cell_length_c 12.6520 _exptl_crystal_F_000 764.00 _reflns_d_resolution_high 0.6398 _[local]_cod_data_source_file bh2020Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sfwnellas in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5799.41 5324.31 76.81 o 2 0 0 71710.53 71186.34 948.64 o 3 0 0 11495.25 11048.70 137.83 o 4 0 0 751.56 769.04 14.38 o 5 0 0 4287.63 4262.13 59.48 o 6 0 0 1938.80 1950.50 40.19 o 7 0 0 456.28 446.31 12.36 o 8 0 0 319.83 310.33 11.41 o 9 0 0 162.71 192.53 44.15 o 10 0 0 138.80 127.89 50.70 o 11 0 0 344.14 221.59 66.76 o 1 1 0 10895.54 10739.11 104.55 o 2 1 0 6342.92 6397.31 57.31 o 3 1 0 632.44 608.79 9.62 o 4 1 0 21115.72 21417.41 187.30 o 5 1 0 114.89 121.74 3.06 o 6 1 0 1971.14 1934.91 22.90 o 7 1 0 1791.33 1786.89 27.22 o 8 1 0 822.63 791.73 46.81 o 9 1 0 672.54 646.85 38.58 o 10 1 0 54.23 31.26 24.54 o 11 1 0 9.76 -47.21 47.21 o 0 2 0 361.11 339.46 9.47 o 1 2 0 239.11 234.51 3.51 o 2 2 0 23569.82 24319.83 218.55 o 3 2 0 310.56 308.08 4.82 o 4 2 0 7943.46 8372.02 77.39 o 5 2 0 337.94 330.85 11.25 o 6 2 0 30.30 42.24 2.99 o 7 2 0 14.87 14.07 2.56 o 8 2 0 813.23 861.32 29.98 o 9 2 0 171.66 142.00 26.35 o 10 2 0 302.10 318.34 61.47 o 11 2 0 26.56 -73.08 73.08 o 1 3 0 1578.95 1618.28 34.04 o 2 3 0 8523.80 8942.27 84.65 o 3 3 0 43.18 31.25 1.84 o 4 3 0 4793.67 5164.94 51.26 o 5 3 0 3153.87 3120.16 33.16 o 6 3 0 535.75 542.39 8.55 o 7 3 0 1545.84 1557.57 29.88 o 8 3 0 1.76 3.57 16.32 o 9 3 0 266.07 281.27 19.65 o 10 3 0 252.68 204.47 61.37 o 0 4 0 7988.40 7977.14 139.39 o 1 4 0 1545.54 1591.24 19.20 o 2 4 0 114.50 88.43 2.50 o 3 4 0 6013.73 6006.24 59.51 o 4 4 0 8846.73 9540.88 97.84 o 5 4 0 847.30 841.85 11.99 o 6 4 0 5345.49 5569.52 68.92 o 7 4 0 223.00 215.61 9.38 o 8 4 0 1707.21 1744.40 45.21 o 9 4 0 6.20 3.17 12.78 o 10 4 0 673.24 671.02 75.75 o 1 5 0 6904.39 6788.52 78.00 o 2 5 0 731.63 759.90 12.53 o 3 5 0 6501.38 6398.09 72.69 o 4 5 0 8182.88 7999.81 86.92 o 5 5 0 34.05 36.53 3.40 o 6 5 0 14.48 16.46 2.95 o 7 5 0 723.39 754.06 17.86 o 8 5 0 1950.39 1818.88 136.28 o 9 5 0 51.81 35.31 14.82 o 10 5 0 147.39 117.13 44.36 o 0 6 0 18156.50 18477.93 281.55 o 1 6 0 12.33 15.81 2.99 o 2 6 0 187.61 246.69 5.37 o 3 6 0 991.31 972.32 13.59 o 4 6 0 1181.96 1124.11 15.68 o 5 6 0 9.82 11.46 3.50 o 6 6 0 1545.47 1580.00 24.21 o 7 6 0 16.39 25.19 8.04 o 8 6 0 180.95 153.66 14.51 o 9 6 0 368.79 371.28 126.80 o 10 6 0 45.37 -2.11 31.79 o 1 7 0 776.77 792.20 12.25 o 2 7 0 6084.14 6232.69 79.84 o 3 7 0 68.59 73.94 10.67 o 4 7 0 622.83 611.56 10.05 o 5 7 0 406.59 414.88 8.84 o 6 7 0 1.62 3.12 4.70 o 7 7 0 104.31 101.24 4.92 o 8 7 0 2.96 -2.02 46.05 o 9 7 0 94.14 105.51 20.07 o 10 7 0 1849.49 1702.21 91.22 o 0 8 0 90.52 197.33 12.73 o 1 8 0 2913.41 2955.70 36.23 o 2 8 0 1209.93 1319.24 36.59 o 3 8 0 866.56 849.62 13.20 o 4 8 0 150.00 138.20 7.34 o 5 8 0 142.83 138.01 8.08 o 6 8 0 5100.82 5154.12 193.87 o 7 8 0 402.16 362.13 10.91 o 8 8 0 356.95 386.06 90.95 o 9 8 0 349.16 351.62 23.13 o 10 8 0 49.00 6.23 29.47 o 1 9 0 203.52 179.47 12.09 o 2 9 0 5611.74 5800.52 69.92 o 3 9 0 1088.00 1076.76 16.91 o 4 9 0 385.80 413.59 11.25 o 5 9 0 648.12 678.80 13.73 o 6 9 0 479.37 450.09 37.66 o 7 9 0 716.06 679.00 24.56 o 8 9 0 0.33 2.23 114.27 o 9 9 0 39.25 56.82 18.16 o 10 9 0 338.35 297.85 34.75 o 0 10 0 167.98 186.31 8.18 o 1 10 0 2275.05 2265.82 28.19 o 2 10 0 80.22 86.72 5.12 o 3 10 0 1.46 -0.04 6.81 o 4 10 0 855.08 878.48 16.19 o 5 10 0 1696.48 1640.73 32.94 o 6 10 0 210.36 209.88 9.26 o 7 10 0 26.61 43.84 8.84 o 8 10 0 14.66 2.11 15.95 o 9 10 0 38.99 21.02 21.12 o 10 10 0 133.61 106.78 24.19 o 1 11 0 8457.41 8493.00 132.31 o 2 11 0 1551.34 1428.92 56.79 o 3 11 0 339.21 301.68 20.92 o 4 11 0 1805.19 1805.04 29.12 o 5 11 0 572.91 540.91 25.78 o 6 11 0 373.12 406.53 14.47 o 7 11 0 484.34 453.54 21.60 o 8 11 0 277.70 319.50 30.21 o 9 11 0 246.05 239.33 23.13 o 10 11 0 26.03 19.01 45.31 o 0 12 0 1078.10 1035.96 31.57 o 1 12 0 84.61 84.71 8.01 o 2 12 0 3288.83 3197.75 50.27 o 3 12 0 1256.05 1267.76 26.05 o 4 12 0 316.87 282.34 10.40 o 5 12 0 2869.60 2927.03 50.99 o 6 12 0 2476.54 2498.81 57.33 o 7 12 0 4.42 0.00 14.94 o 8 12 0 1424.67 1436.86 66.58 o 9 12 0 149.99 127.89 25.03 o 1 13 0 970.28 1006.11 24.00 o 2 13 0 2742.32 2782.64 70.21 o 3 13 0 2.63 1.44 7.29 o 4 13 0 1030.12 977.75 19.37 o 5 13 0 878.52 878.41 24.38 o 6 13 0 419.45 415.97 18.74 o 7 13 0 312.43 292.76 19.74 o 8 13 0 149.83 161.48 28.94 o 9 13 0 441.83 406.03 32.75 o 0 14 0 181.74 205.43 26.88 o 1 14 0 322.29 305.46 19.44 o 2 14 0 2080.31 2098.40 41.98 o 3 14 0 482.79 472.95 16.31 o 4 14 0 649.64 617.43 19.76 o 5 14 0 89.04 74.97 10.93 o 6 14 0 41.51 43.32 12.66 o 7 14 0 110.59 114.27 14.48 o 8 14 0 156.13 183.66 30.00 o 9 14 0 4.16 -7.50 33.90 o 1 15 0 426.89 425.13 18.06 o 2 15 0 123.84 71.42 11.23 o 3 15 0 683.16 638.75 18.94 o 4 15 0 1075.77 1075.96 62.51 o 5 15 0 67.66 84.39 13.46 o 6 15 0 123.82 95.35 14.54 o 7 15 0 27.39 1.43 14.17 o 8 15 0 9.04 20.07 32.63 o 0 16 0 5732.39 5724.59 146.17 o 1 16 0 209.66 222.74 17.43 o 2 16 0 2179.17 2221.89 48.46 o 3 16 0 726.20 744.57 25.10 o 4 16 0 841.30 842.23 24.45 o 5 16 0 3009.84 3116.06 73.14 o 6 16 0 2.04 2.81 12.13 o 7 16 0 16.66 36.27 18.36 o 8 16 0 716.42 567.61 52.61 o 1 17 0 3507.01 3391.62 94.72 o 2 17 0 562.94 572.41 23.11 o 3 17 0 349.84 365.86 18.45 o 4 17 0 972.75 937.32 59.44 o 5 17 0 59.31 89.12 18.48 o 6 17 0 188.55 153.54 19.08 o 7 17 0 4.30 12.38 20.01 o 8 17 0 13.31 10.56 28.51 o 0 18 0 76.55 69.46 18.45 o 1 18 0 101.91 100.59 25.45 o 2 18 0 16.41 25.46 14.00 o 3 18 0 289.90 278.61 18.48 o 4 18 0 86.16 84.16 13.14 o 5 18 0 1039.76 997.51 37.01 o 6 18 0 42.61 19.82 18.01 o 7 18 0 51.49 3.17 24.40 o 1 19 0 950.10 1029.43 43.75 o 2 19 0 0.41 4.20 14.55 o 3 19 0 24.69 46.06 15.32 o 4 19 0 0.14 -13.67 24.77 o 5 19 0 122.50 87.89 28.99 o 6 19 0 82.72 72.24 20.37 o 7 19 0 120.55 136.13 43.20 o 0 20 0 3.57 -14.92 26.47 o 1 20 0 1.07 -10.15 15.67 o 2 20 0 2.95 -0.16 16.97 o 3 20 0 19.43 -12.22 16.38 o 4 20 0 174.08 172.34 23.40 o 5 20 0 23.40 17.33 19.36 o 6 20 0 424.33 305.85 32.72 o 1 21 0 207.07 186.25 22.28 o 2 21 0 136.75 132.77 21.07 o 3 21 0 46.45 52.97 24.13 o 4 21 0 299.50 337.08 42.78 o 5 21 0 59.71 49.70 24.40 o 0 22 0 6.20 -29.45 48.16 o 1 22 0 152.03 185.82 21.81 o 2 22 0 16.81 23.80 18.91 o 3 22 0 84.62 102.77 35.15 o 4 22 0 61.19 104.39 27.47 o 5 22 0 379.81 306.84 52.39 o 1 23 0 237.30 261.91 33.85 o 2 23 0 53.50 57.04 23.16 o 3 23 0 293.66 312.20 40.89 o 0 24 0 270.79 207.71 44.94 o 1 24 0 314.73 273.07 41.09 o 2 24 0 119.97 60.03 55.50 o -11 1 1 224.80 283.37 73.30 o -10 1 1 61.96 9.28 32.29 o -9 1 1 2.10 5.05 17.85 o -8 1 1 839.93 896.05 22.70 o -7 1 1 495.73 474.28 15.53 o -6 1 1 35.69 42.12 3.22 o -5 1 1 129.23 122.08 9.40 o -4 1 1 287.43 296.74 5.11 o -3 1 1 811.64 825.60 8.49 o -2 1 1 607.80 583.60 7.83 o -1 1 1 8449.20 8252.96 74.16 o 1 1 1 9415.27 9422.66 92.78 o 2 1 1 5432.57 6000.80 66.16 o 3 1 1 4071.94 4235.61 38.98 o 4 1 1 3946.16 3645.51 36.15 o 5 1 1 277.67 290.85 5.04 o 6 1 1 2052.96 2049.82 32.23 o 7 1 1 738.09 777.12 28.05 o 8 1 1 32.47 24.51 21.24 o 9 1 1 283.73 332.17 39.94 o 10 1 1 100.29 39.85 28.20 o -11 2 1 543.12 497.10 79.76 o -10 2 1 609.19 797.77 78.91 o -9 2 1 96.14 95.90 28.41 o -8 2 1 692.88 773.24 23.01 o -7 2 1 38.53 42.67 3.25 o -6 2 1 156.81 170.30 5.30 o -5 2 1 1196.17 1210.67 13.50 o -4 2 1 6784.03 6736.35 98.98 o -3 2 1 10182.81 10037.42 91.37 o -2 2 1 14871.82 15221.82 140.26 o -1 2 1 13674.24 13569.83 144.28 o 0 2 1 5919.21 6069.50 65.23 o 1 2 1 715.07 713.52 9.15 o 2 2 1 3695.11 3645.33 35.46 o 3 2 1 4020.04 4068.69 39.58 o 4 2 1 537.22 616.76 6.87 o 5 2 1 1286.69 1312.10 18.32 o 6 2 1 193.15 205.08 15.16 o 7 2 1 128.87 126.96 20.17 o 8 2 1 2347.40 2293.72 59.01 o 9 2 1 127.47 129.07 33.80 o 10 2 1 1401.46 1504.03 100.82 o -11 3 1 146.00 148.49 46.68 o -10 3 1 1.84 -22.18 37.07 o -9 3 1 278.20 231.23 65.91 o -8 3 1 1460.24 1494.25 34.34 o -7 3 1 2015.87 2140.30 27.40 o -6 3 1 60.10 59.41 5.81 o -5 3 1 949.44 994.47 12.30 o -4 3 1 1132.41 959.70 15.12 o -3 3 1 363.15 375.81 8.19 o -2 3 1 13143.17 13571.48 136.20 o -1 3 1 359.39 387.60 5.85 o 0 3 1 975.13 972.00 11.50 o 1 3 1 417.52 405.06 5.57 o 2 3 1 3372.91 3392.53 37.27 o 3 3 1 241.84 222.10 3.44 o 4 3 1 18187.22 18449.87 170.10 o 5 3 1 13.65 16.66 2.66 o 6 3 1 5747.19 5946.13 85.38 o 7 3 1 3075.20 3074.83 55.40 o 8 3 1 33.05 32.47 36.07 o 9 3 1 857.91 783.21 60.01 o 10 3 1 15.26 59.35 40.03 o -11 4 1 62.06 -11.62 39.08 o -10 4 1 272.89 223.49 62.21 o -9 4 1 5.61 21.47 91.62 o -8 4 1 3.65 7.76 3.85 o -7 4 1 812.76 800.83 26.79 o -6 4 1 6599.92 6842.65 82.42 o -5 4 1 1084.11 1077.41 20.35 o -4 4 1 361.66 411.92 15.21 o -3 4 1 3483.71 3572.53 36.50 o -2 4 1 0.57 5.76 2.20 o -1 4 1 9568.50 9509.99 105.74 o 0 4 1 12928.55 13231.85 139.16 o 1 4 1 6993.31 6738.59 78.68 o 2 4 1 434.01 399.01 5.49 o 3 4 1 8890.93 8595.95 93.95 o 4 4 1 1178.87 1124.99 13.87 o 5 4 1 1087.45 1045.33 53.28 o 6 4 1 192.41 182.71 6.49 o 7 4 1 5.88 11.56 7.01 o 8 4 1 982.81 1058.77 35.93 o 9 4 1 269.67 266.16 32.85 o 10 4 1 391.31 494.22 67.92 o -11 5 1 33.77 -5.28 48.69 o -10 5 1 956.38 1092.80 98.90 o -9 5 1 162.33 173.41 22.02 o -8 5 1 6.62 6.55 4.56 o -7 5 1 2258.06 2234.07 43.21 o -6 5 1 308.34 319.79 31.06 o -5 5 1 4450.57 4562.00 51.22 o -4 5 1 293.32 348.21 7.82 o -3 5 1 144.91 171.02 12.15 o -2 5 1 12286.17 11981.01 127.59 o -1 5 1 2.66 7.92 3.70 o 0 5 1 1875.38 1870.45 21.88 o 1 5 1 3295.80 3309.67 38.38 o 2 5 1 1970.73 1963.81 40.46 o 3 5 1 5796.26 5764.46 86.65 o 4 5 1 21.08 36.20 2.50 o 5 5 1 8.08 10.26 1.76 o 6 5 1 2440.66 2590.85 66.65 o 7 5 1 2.69 -3.17 12.14 o 8 5 1 2028.78 2017.88 135.96 o 9 5 1 2.84 5.28 10.67 o 10 5 1 17.33 14.68 53.86 o -10 6 1 33.56 50.69 55.02 o -9 6 1 1018.33 939.28 98.06 o -8 6 1 140.65 129.87 8.82 o -7 6 1 35.20 30.65 4.30 o -6 6 1 1668.57 1672.14 24.10 o -5 6 1 253.64 237.34 5.89 o -4 6 1 215.73 203.15 4.87 o -3 6 1 7701.87 7687.69 79.39 o -2 6 1 608.69 564.74 12.31 o -1 6 1 13522.94 13335.33 144.45 o 0 6 1 3898.82 3880.72 45.95 o 1 6 1 205.62 225.86 6.34 o 2 6 1 21669.52 22369.82 227.11 o 3 6 1 2219.94 2184.44 23.65 o 4 6 1 6232.52 6483.28 83.46 o 5 6 1 2122.75 2158.65 28.80 o 6 6 1 47.36 46.57 7.23 o 7 6 1 2266.72 2247.74 49.49 o 8 6 1 386.53 355.18 30.58 o 9 6 1 5.34 25.35 14.68 o 10 6 1 967.34 941.49 57.90 o -10 7 1 21.11 49.74 23.34 o -9 7 1 95.76 109.86 351.79 o -8 7 1 292.71 254.35 17.22 o -7 7 1 2900.87 2932.46 56.45 o -6 7 1 2973.95 2994.82 41.93 o -5 7 1 2026.78 2008.90 47.92 o -4 7 1 6566.99 6420.89 89.03 o -3 7 1 1065.79 1099.35 13.96 o -2 7 1 12656.36 12523.50 234.27 o -1 7 1 1207.50 1265.93 18.80 o 0 7 1 16157.02 16402.96 198.79 o 1 7 1 4440.75 4445.73 56.79 o 2 7 1 6603.07 6851.71 77.67 o 3 7 1 9560.46 9492.25 96.67 o 4 7 1 114.56 104.58 4.65 o 5 7 1 53.24 59.14 4.70 o 6 7 1 1861.89 1839.55 44.68 o 7 7 1 987.30 943.07 28.04 o 8 7 1 0.59 12.97 68.12 o 9 7 1 61.56 69.70 16.79 o 10 7 1 270.45 211.02 39.61 o -10 8 1 941.64 859.60 51.46 o -9 8 1 298.40 271.45 23.55 o -8 8 1 379.07 395.15 28.26 o -7 8 1 455.59 456.19 16.17 o -6 8 1 110.70 122.46 6.61 o -5 8 1 107.37 96.80 4.44 o -4 8 1 830.36 865.85 13.04 o -3 8 1 853.15 898.06 13.60 o -2 8 1 1270.61 1406.30 18.73 o -1 8 1 3130.89 3137.96 42.50 o 0 8 1 546.16 457.84 9.30 o 1 8 1 212.70 188.16 5.04 o 2 8 1 176.27 147.05 5.08 o 3 8 1 324.56 297.94 7.13 o 4 8 1 0.75 8.90 3.70 o 5 8 1 134.55 139.93 13.15 o 6 8 1 306.74 293.95 10.62 o 7 8 1 97.36 89.71 13.39 o 8 8 1 28.45 39.76 78.73 o 9 8 1 93.07 101.49 19.01 o 10 8 1 7.22 25.35 28.51 o -10 9 1 1.44 53.02 18.90 o -9 9 1 184.27 186.30 21.33 o -8 9 1 418.99 468.65 36.87 o -7 9 1 89.18 96.51 12.71 o -6 9 1 81.13 71.91 6.79 o -5 9 1 452.77 436.92 9.77 o -4 9 1 731.05 738.35 13.99 o -3 9 1 215.28 227.50 7.09 o -2 9 1 12711.56 12971.19 147.50 o -1 9 1 1479.64 1513.65 21.26 o 0 9 1 2882.51 2924.52 39.82 o 1 9 1 3134.60 3090.65 61.67 o 2 9 1 896.26 877.17 14.23 o 3 9 1 8.59 12.59 4.03 o 4 9 1 233.65 252.94 7.05 o 5 9 1 61.09 41.73 4.84 o 6 9 1 24.70 33.53 4.87 o 7 9 1 12.67 16.15 23.29 o 8 9 1 1026.30 934.34 190.56 o 9 9 1 373.09 304.62 26.09 o 10 9 1 21.18 -29.46 37.07 o -10 10 1 10.37 29.46 28.62 o -9 10 1 705.23 807.00 38.77 o -8 10 1 258.78 217.32 27.46 o -7 10 1 2.60 2.66 9.39 o -6 10 1 4610.12 4681.32 102.59 o -5 10 1 909.16 927.91 22.83 o -4 10 1 123.33 141.20 9.77 o -3 10 1 1733.84 1769.68 31.47 o -2 10 1 521.13 402.23 9.39 o -1 10 1 795.34 834.56 13.52 o 0 10 1 36.67 17.81 7.45 o 1 10 1 389.45 360.87 8.26 o 2 10 1 6136.60 6083.77 75.46 o 3 10 1 1556.77 1492.06 27.60 o 4 10 1 2803.22 2792.03 37.61 o 5 10 1 3426.90 3503.40 127.39 o 6 10 1 287.98 284.58 44.79 o 7 10 1 1364.85 1377.46 41.26 o 8 10 1 106.10 147.74 22.07 o 9 10 1 101.23 130.85 25.24 o 10 10 1 102.79 239.31 68.33 o -10 11 1 992.42 777.83 52.62 o -9 11 1 109.33 99.49 20.07 o -8 11 1 11.33 25.35 22.28 o -7 11 1 1308.52 1267.03 35.15 o -6 11 1 0.57 -0.63 7.28 o -5 11 1 1516.30 1547.84 27.63 o -4 11 1 5.02 13.87 6.33 o -3 11 1 127.92 121.01 8.19 o -2 11 1 4338.75 4172.49 62.47 o -1 11 1 186.55 173.65 6.94 o 0 11 1 1053.70 1029.18 16.03 o 1 11 1 2507.26 2472.86 56.68 o 2 11 1 436.36 419.11 14.00 o 3 11 1 3294.42 3289.40 52.20 o 4 11 1 31.05 24.08 5.97 o 5 11 1 29.81 21.20 6.86 o 6 11 1 715.53 753.09 22.57 o 7 11 1 202.05 191.76 12.31 o 8 11 1 460.03 453.15 34.65 o 9 11 1 141.71 114.28 24.29 o -9 12 1 3.93 -1.06 22.39 o -8 12 1 8.00 13.73 19.96 o -7 12 1 706.53 704.78 35.29 o -6 12 1 551.77 588.69 17.73 o -5 12 1 0.67 5.17 9.45 o -4 12 1 12.89 24.18 6.72 o -3 12 1 1686.11 1742.00 29.70 o -2 12 1 4.28 9.20 6.13 o -1 12 1 6838.26 6832.66 100.95 o 0 12 1 237.49 223.64 9.23 o 1 12 1 191.81 170.74 9.03 o 2 12 1 1049.12 1064.39 22.49 o 3 12 1 438.55 415.71 12.61 o 4 12 1 59.23 78.70 7.12 o 5 12 1 427.48 428.62 19.54 o 6 12 1 162.17 114.76 11.65 o 7 12 1 340.39 324.75 42.88 o 8 12 1 48.91 29.47 22.18 o 9 12 1 14.60 40.13 25.56 o -9 13 1 342.00 335.99 41.72 o -8 13 1 337.95 326.48 36.44 o -7 13 1 56.97 43.79 11.52 o -6 13 1 505.82 507.15 26.25 o -5 13 1 4.20 11.11 8.07 o -4 13 1 91.01 81.96 8.42 o -3 13 1 1333.21 1314.36 28.88 o -2 13 1 149.21 148.04 15.42 o -1 13 1 1537.59 1447.17 30.56 o 0 13 1 65.54 62.15 17.06 o 1 13 1 534.98 532.06 23.14 o 2 13 1 4.44 9.37 7.38 o 3 13 1 1951.74 1929.22 36.38 o 4 13 1 153.08 174.69 19.12 o 5 13 1 15.34 20.67 8.83 o 6 13 1 146.68 156.97 12.85 o 7 13 1 9.65 7.92 16.84 o 8 13 1 7.01 43.09 29.46 o 9 13 1 572.04 438.06 34.02 o -9 14 1 618.70 511.70 47.01 o -8 14 1 128.08 156.51 24.40 o -7 14 1 392.07 384.95 21.59 o -6 14 1 392.85 366.24 27.99 o -5 14 1 1972.59 1991.02 45.00 o -4 14 1 135.48 107.22 9.02 o -3 14 1 440.33 456.89 27.68 o -2 14 1 109.34 105.06 10.10 o -1 14 1 535.51 498.05 17.93 o 0 14 1 162.45 148.00 12.57 o 1 14 1 446.55 425.25 16.39 o 2 14 1 5.52 11.10 9.00 o 3 14 1 553.21 563.86 43.58 o 4 14 1 64.96 63.53 10.56 o 5 14 1 3189.25 3097.58 70.52 o 6 14 1 319.87 339.91 18.98 o 7 14 1 2.36 26.40 28.41 o 8 14 1 1058.39 1008.53 55.79 o 9 14 1 55.14 6.23 35.59 o -9 15 1 411.71 435.38 56.93 o -8 15 1 4.99 28.41 28.41 o -7 15 1 5.28 27.60 31.68 o -6 15 1 100.61 88.44 13.77 o -5 15 1 2.66 14.91 12.62 o -4 15 1 19.00 42.84 10.42 o -3 15 1 340.70 343.83 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