#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:23:16 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181014 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209402.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209402_Fobs loop_ _publ_author_name 'Wang, Shou-Wu' 'Ge, Hai-Yan' 'Yang, Jian-Hu' 'Li, Bao-Long' 'Zhang, Yong' _publ_section_title ; Poly[[bis(benzimidazole)manganese(II)]-di-\m-1,5-dicyanamido] ; _journal_coeditor_code BT2089 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1646 _journal_page_last m1648 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.839 _cell_angle_gamma 90.000 _cell_length_a 9.2994 _cell_length_b 9.9531 _cell_length_c 9.9585 _exptl_crystal_F_000 430.00 _reflns_d_resolution_high 0.8304 _cod_data_source_file bt2089Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _051210b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1747.19 1716.81 11.26 o 4 0 0 902.66 853.66 9.25 o 6 0 0 345.66 334.38 5.63 o 8 0 0 256.08 258.50 15.53 o 10 0 0 103.51 118.36 6.73 o 1 1 0 447.06 434.27 5.36 o 2 1 0 2990.05 2950.79 12.86 o 3 1 0 1292.76 1160.24 6.41 o 4 1 0 43.52 39.99 1.30 o 5 1 0 3991.59 4027.42 22.59 o 6 1 0 218.85 216.39 3.25 o 7 1 0 727.02 701.41 7.33 o 8 1 0 116.89 110.57 3.44 o 9 1 0 28.38 26.78 2.35 o 10 1 0 67.67 59.45 3.50 o 0 2 0 3449.66 3226.72 24.88 o 1 2 0 2681.88 2606.79 15.79 o 2 2 0 1977.74 2050.04 9.65 o 3 2 0 88.85 94.86 1.64 o 4 2 0 173.18 139.96 2.16 o 5 2 0 44.44 54.99 1.61 o 6 2 0 1371.63 1305.37 11.35 o 7 2 0 58.04 58.90 1.97 o 8 2 0 1261.14 1348.86 16.22 o 9 2 0 533.38 537.34 9.57 o 10 2 0 583.89 604.61 10.03 o 1 3 0 1670.64 1601.83 8.60 o 2 3 0 118.11 112.92 1.73 o 3 3 0 85.74 48.16 1.35 o 4 3 0 352.71 377.82 3.57 o 5 3 0 2002.95 1969.64 15.03 o 6 3 0 3.86 2.70 0.80 o 7 3 0 110.57 98.73 3.59 o 8 3 0 360.35 348.55 6.96 o 9 3 0 346.04 335.15 6.86 o 10 3 0 57.40 56.05 3.50 o 0 4 0 7072.49 6870.78 55.35 o 1 4 0 621.96 672.28 4.99 o 2 4 0 116.11 101.78 1.78 o 3 4 0 179.14 195.27 2.56 o 4 4 0 957.29 996.61 6.58 o 5 4 0 23.15 22.46 1.23 o 6 4 0 1787.19 1772.54 14.68 o 7 4 0 111.78 101.51 3.25 o 8 4 0 210.06 205.46 5.39 o 9 4 0 1.72 1.67 1.21 o 10 4 0 0.94 2.07 1.57 o 1 5 0 2923.34 2966.65 15.56 o 2 5 0 6.86 10.31 0.90 o 3 5 0 808.77 786.50 5.74 o 4 5 0 5.01 3.56 0.75 o 5 5 0 596.94 555.24 6.89 o 6 5 0 0.08 0.99 0.83 o 7 5 0 6.84 10.95 2.80 o 8 5 0 2.19 3.92 1.23 o 9 5 0 114.23 115.08 4.46 o 0 6 0 2229.22 2209.21 19.68 o 1 6 0 23.29 24.83 1.17 o 2 6 0 768.93 748.26 6.41 o 3 6 0 45.48 48.85 1.65 o 4 6 0 500.75 514.96 5.45 o 5 6 0 161.83 154.88 3.42 o 6 6 0 679.72 687.81 7.92 o 7 6 0 5.49 5.63 1.12 o 8 6 0 180.35 171.89 5.32 o 9 6 0 42.32 44.65 3.86 o 1 7 0 306.06 299.04 3.93 o 2 7 0 219.66 225.80 3.44 o 3 7 0 516.69 516.57 5.96 o 4 7 0 30.38 31.42 1.78 o 5 7 0 248.90 223.66 4.53 o 6 7 0 0.35 2.43 0.96 o 7 7 0 222.77 214.42 5.66 o 8 7 0 59.20 51.86 3.26 o 0 8 0 262.70 249.98 6.24 o 1 8 0 61.18 60.89 2.00 o 2 8 0 6.94 7.33 1.17 o 3 8 0 89.31 79.80 3.00 o 4 8 0 24.92 25.55 1.88 o 5 8 0 55.88 64.20 3.35 o 6 8 0 963.37 1022.80 11.69 o 7 8 0 143.14 153.87 5.05 o 8 8 0 327.56 338.55 12.62 o 1 9 0 383.56 391.47 6.87 o 2 9 0 0.62 2.83 1.20 o 3 9 0 546.94 573.52 9.20 o 4 9 0 86.24 88.33 3.73 o 5 9 0 342.13 339.31 7.55 o 6 9 0 96.01 101.49 4.21 o 7 9 0 58.66 48.52 3.46 o 0 10 0 410.88 417.61 11.55 o 1 10 0 16.10 15.50 1.73 o 2 10 0 1511.20 1593.33 14.30 o 3 10 0 0.41 1.88 1.29 o 4 10 0 29.62 31.16 2.64 o 5 10 0 34.65 39.46 3.05 o 1 11 0 30.60 26.79 2.60 o 2 11 0 21.72 23.18 2.10 o 3 11 0 108.09 104.22 4.42 o 4 11 0 9.53 9.42 1.52 o -9 0 1 403.72 401.22 11.00 o -7 0 1 827.57 783.78 10.98 o -5 0 1 1884.89 1847.30 13.30 o -3 0 1 3255.51 3080.49 26.29 o 1 0 1 841.35 810.71 5.59 o 3 0 1 399.78 349.73 4.29 o 5 0 1 57.58 34.17 1.98 o 7 0 1 116.68 108.48 3.63 o 9 0 1 508.20 515.64 20.71 o -10 1 1 188.47 190.67 5.43 o -9 1 1 98.06 95.98 3.78 o -8 1 1 1271.92 1290.38 14.34 o -7 1 1 11.25 11.65 1.19 o -6 1 1 494.80 462.37 4.75 o -5 1 1 1144.73 1241.03 7.21 o -4 1 1 1209.45 1125.44 7.22 o -3 1 1 2739.67 2677.00 18.37 o -2 1 1 454.80 424.60 2.81 o -1 1 1 163.33 157.72 1.32 o 1 1 1 404.77 393.74 2.54 o 2 1 1 96.44 119.26 1.64 o 3 1 1 1686.07 1727.52 8.78 o 4 1 1 1492.17 1445.14 9.02 o 5 1 1 676.59 706.00 5.70 o 6 1 1 3468.97 3526.25 21.09 o 7 1 1 7.08 5.96 0.84 o 8 1 1 2.64 1.95 0.78 o 9 1 1 43.90 42.77 3.57 o 10 1 1 581.83 603.22 10.09 o -10 2 1 5.07 5.30 1.64 o -9 2 1 39.63 41.07 2.52 o -8 2 1 0.00 1.17 0.88 o -7 2 1 194.16 182.14 3.29 o -6 2 1 77.67 79.12 2.00 o -5 2 1 2374.32 2479.97 12.61 o -4 2 1 183.59 192.35 2.63 o -3 2 1 2.66 6.96 0.60 o -2 2 1 423.16 399.07 2.88 o -1 2 1 2722.53 2710.75 21.10 o 0 2 1 0.00 2.57 0.63 o 1 2 1 7172.20 6853.93 35.39 o 2 2 1 49.70 41.40 1.07 o 3 2 1 301.17 254.08 2.70 o 4 2 1 225.30 250.17 2.84 o 5 2 1 2439.68 2529.90 13.69 o 6 2 1 34.56 36.32 1.54 o 7 2 1 241.07 235.40 4.15 o 8 2 1 33.04 32.18 2.74 o 9 2 1 305.42 289.77 6.98 o 10 2 1 16.33 14.46 3.01 o -10 3 1 5.76 9.32 1.79 o -9 3 1 0.36 4.11 1.44 o -8 3 1 977.77 1017.72 13.26 o -7 3 1 39.23 37.47 1.90 o -6 3 1 47.33 36.58 1.60 o -5 3 1 277.94 310.04 3.44 o -4 3 1 716.40 690.25 4.90 o -3 3 1 697.05 761.54 5.98 o -2 3 1 3682.04 3457.25 21.36 o -1 3 1 234.05 242.15 2.26 o 0 3 1 4039.55 3862.12 22.18 o 1 3 1 11.18 12.16 0.71 o 2 3 1 435.14 384.03 3.37 o 3 3 1 231.55 229.41 2.70 o 4 3 1 569.67 541.51 4.47 o 5 3 1 183.85 191.95 2.94 o 6 3 1 1137.92 1119.26 12.66 o 7 3 1 209.86 200.70 4.01 o 8 3 1 40.35 35.46 2.48 o 9 3 1 1.71 0.46 1.70 o 10 3 1 107.76 120.13 4.80 o -10 4 1 4.41 5.31 1.33 o -9 4 1 120.53 126.09 4.55 o -8 4 1 18.47 15.40 1.73 o -7 4 1 291.66 306.39 4.95 o -6 4 1 160.64 155.44 3.14 o -5 4 1 1005.18 1008.31 7.85 o -4 4 1 633.08 726.74 5.66 o -3 4 1 755.54 698.47 4.92 o -2 4 1 311.35 324.31 3.21 o -1 4 1 2986.34 3017.39 16.13 o 0 4 1 1181.10 1217.77 7.63 o 1 4 1 2219.71 2210.85 12.45 o 2 4 1 25.89 35.65 1.36 o 3 4 1 1190.63 1111.54 6.78 o 4 4 1 17.16 19.82 1.12 o 5 4 1 994.02 970.00 8.29 o 6 4 1 22.67 17.23 1.25 o 7 4 1 36.47 37.10 2.25 o 8 4 1 0.43 0.30 1.36 o 9 4 1 561.39 567.45 9.09 o -10 5 1 64.00 67.84 3.82 o -9 5 1 2.46 3.19 1.08 o -8 5 1 981.36 959.76 16.15 o -7 5 1 2.98 5.09 1.22 o -6 5 1 493.47 482.97 6.17 o -5 5 1 228.16 219.84 3.32 o -4 5 1 301.61 275.53 3.52 o -3 5 1 419.96 443.85 4.69 o -2 5 1 1725.89 1655.93 9.27 o -1 5 1 117.77 125.85 2.05 o 0 5 1 1129.73 1060.02 7.17 o 1 5 1 65.77 76.75 1.67 o 2 5 1 120.21 95.85 1.91 o 3 5 1 0.53 2.01 0.58 o 4 5 1 1513.86 1545.05 11.48 o 5 5 1 396.95 404.16 5.05 o 6 5 1 1609.48 1610.50 15.81 o 7 5 1 141.87 134.72 4.44 o 8 5 1 169.91 159.31 4.89 o 9 5 1 24.46 29.48 2.64 o -9 6 1 203.55 194.18 5.74 o -8 6 1 77.57 74.59 3.54 o -7 6 1 798.54 815.11 11.32 o -6 6 1 178.68 160.76 3.83 o -5 6 1 717.37 705.96 7.74 o -4 6 1 247.53 248.20 3.55 o -3 6 1 290.50 288.49 3.68 o -2 6 1 591.67 666.53 5.89 o -1 6 1 58.69 49.43 1.85 o 0 6 1 390.91 402.45 3.99 o 1 6 1 424.95 442.01 4.26 o 2 6 1 3.82 8.83 0.86 o 3 6 1 175.23 160.85 2.84 o 4 6 1 63.39 51.44 1.79 o 5 6 1 347.52 329.44 4.79 o 6 6 1 93.32 90.14 3.94 o 7 6 1 147.74 146.18 4.81 o 8 6 1 27.70 23.68 2.36 o 9 6 1 183.65 178.77 6.57 o -8 7 1 142.42 159.61 5.07 o -7 7 1 14.47 10.06 1.25 o -6 7 1 190.64 201.44 4.57 o -5 7 1 62.54 60.47 2.58 o -4 7 1 76.14 72.16 2.39 o -3 7 1 32.78 30.64 1.48 o -2 7 1 1817.67 1872.98 13.79 o -1 7 1 33.84 34.29 1.50 o 0 7 1 1256.01 1356.19 9.90 o 1 7 1 83.02 86.42 2.17 o 2 7 1 57.71 54.54 1.88 o 3 7 1 9.45 7.56 0.89 o 4 7 1 401.79 398.57 5.27 o 5 7 1 4.16 4.07 1.33 o 6 7 1 92.12 92.18 3.87 o 7 7 1 70.79 72.20 3.55 o 8 7 1 92.51 96.98 4.24 o -8 8 1 0.23 0.96 1.17 o -7 8 1 608.63 637.82 9.52 o -6 8 1 104.72 106.41 3.55 o -5 8 1 76.72 72.13 2.88 o -4 8 1 4.64 6.33 1.00 o -3 8 1 663.47 684.91 9.31 o -2 8 1 246.31 237.95 4.41 o -1 8 1 77.16 72.86 2.28 o 0 8 1 14.17 16.20 1.22 o 1 8 1 679.17 682.27 9.30 o 2 8 1 0.66 3.32 0.89 o 3 8 1 2444.97 2475.88 20.27 o 4 8 1 205.22 205.77 5.33 o 5 8 1 572.30 597.68 11.45 o 6 8 1 12.40 12.41 1.97 o 7 8 1 212.04 213.04 6.05 o -7 9 1 172.21 167.90 5.81 o -6 9 1 78.17 70.09 3.86 o -5 9 1 48.83 47.38 3.40 o -4 9 1 35.61 35.66 2.21 o -3 9 1 181.68 180.19 4.47 o -2 9 1 1968.30 2020.59 25.23 o -1 9 1 123.54 122.71 3.60 o 0 9 1 932.69 951.11 10.77 o 1 9 1 432.73 437.18 8.32 o 2 9 1 134.99 134.41 4.29 o 3 9 1 13.27 12.95 1.77 o 4 9 1 429.92 441.62 8.60 o 5 9 1 0.00 1.92 0.75 o 6 9 1 54.66 57.75 3.41 o -6 10 1 185.73 177.85 5.92 o -5 10 1 342.59 348.85 7.46 o -4 10 1 465.48 479.66 9.19 o -3 10 1 107.59 100.32 4.20 o -2 10 1 116.42 113.79 4.10 o -1 10 1 175.85 180.80 5.21 o 0 10 1 0.00 0.55 0.94 o 1 10 1 160.15 159.90 5.24 o 2 10 1 320.25 317.58 6.62 o 3 10 1 92.60 93.52 4.72 o 4 10 1 50.86 54.26 3.28 o 5 10 1 127.02 130.18 4.90 o -4 11 1 1.37 1.54 1.08 o -3 11 1 7.27 7.36 2.28 o -2 11 1 287.26 292.27 6.84 o -1 11 1 180.40 176.71 5.35 o 0 11 1 9.86 12.76 1.66 o 1 11 1 11.77 8.30 1.75 o 2 11 1 33.41 34.26 3.16 o 3 11 1 36.14 33.06 2.84 o -10 0 2 10.43 10.19 1.91 o -8 0 2 747.10 767.51 9.78 o -6 0 2 26.13 30.37 1.73 o -4 0 2 3812.18 3729.19 27.34 o -2 0 2 18195.64 16298.12 218.11 o 0 0 2 6240.93 6602.10 74.72 o 2 0 2 5003.49 4848.69 44.66 o 4 0 2 1365.65 1287.67 10.24 o 6 0 2 1408.30 1526.55 18.16 o 8 0 2 84.11 78.71 5.59 o 10 0 2 342.59 357.63 11.78 o -11 1 2 23.52 18.34 2.30 o -10 1 2 135.25 130.74 4.68 o -9 1 2 1001.87 1053.97 12.78 o -8 1 2 136.00 134.31 3.23 o -7 1 2 993.81 1031.58 9.44 o -6 1 2 647.40 651.20 6.04 o -5 1 2 100.88 82.34 1.67 o -4 1 2 156.32 151.86 1.99 o -3 1 2 934.30 847.85 4.82 o -2 1 2 60.24 70.22 1.75 o -1 1 2 2.91 6.82 1.04 o 0 1 2 2198.04 2206.85 11.36 o 1 1 2 14569.22 14626.38 168.49 o 2 1 2 1418.27 1440.35 7.24 o 3 1 2 2260.63 2318.05 14.93 o 4 1 2 12.02 16.46 1.00 o 5 1 2 863.35 859.51 6.92 o 6 1 2 2.06 3.51 0.76 o 7 1 2 258.03 258.83 4.55 o 8 1 2 4.46 5.66 1.78 o 9 1 2 19.51 22.81 2.28 o 10 1 2 0.05 1.80 1.81 o -10 2 2 831.73 850.26 10.93 o -9 2 2 82.04 86.53 3.13 o -8 2 2 2016.27 2082.80 19.86 o -7 2 2 340.76 332.08 4.40 o -6 2 2 525.06 492.36 4.84 o -5 2 2 70.59 65.09 1.59 o -4 2 2 2494.96 2508.76 13.82 o -3 2 2 113.18 120.21 1.55 o -2 2 2 4894.39 4732.89 23.20 o -1 2 2 2330.35 2392.41 10.54 o 0 2 2 7872.75 8116.91 87.84 o 1 2 2 4552.44 4601.54 22.36 o 2 2 2 297.05 256.92 2.44 o 3 2 2 1.39 1.99 0.44 o 4 2 2 270.01 213.86 2.77 o 5 2 2 257.16 261.84 3.49 o 6 2 2 596.65 596.69 6.50 o 7 2 2 229.75 227.02 4.26 o 8 2 2 428.63 420.66 7.86 o 9 2 2 18.77 17.45 2.24 o -10 3 2 145.92 155.28 4.89 o -9 3 2 276.19 286.13 5.81 o -8 3 2 104.75 96.70 3.79 o -7 3 2 634.96 624.82 6.96 o -6 3 2 55.95 48.76 1.84 o -5 3 2 1070.99 1089.22 6.78 o -4 3 2 492.58 567.02 4.23 o -3 3 2 971.30 885.12 5.92 o -2 3 2 169.01 172.50 1.92 o -1 3 2 501.27 440.01 3.20 o 0 3 2 1677.18 1780.57 10.81 o 1 3 2 857.20 783.09 4.87 o 2 3 2 834.18 847.17 6.16 o 3 3 2 5.64 14.58 0.88 o 4 3 2 40.41 47.96 1.53 o 5 3 2 452.55 446.94 4.78 o 6 3 2 217.01 199.20 3.52 o 7 3 2 423.85 408.92 6.11 o 8 3 2 27.59 22.92 2.27 o 9 3 2 936.95 966.36 11.80 o -10 4 2 305.22 324.97 7.26 o -9 4 2 26.15 27.10 2.18 o -8 4 2 549.71 556.23 11.34 o -7 4 2 9.19 8.47 1.13 o -6 4 2 52.57 52.39 1.72 o -5 4 2 229.09 247.29 3.27 o -4 4 2 1159.29 1119.88 10.52 o -3 4 2 35.40 37.62 1.14 o -2 4 2 1874.52 1828.96 10.65 o -1 4 2 13.12 15.59 0.77 o 0 4 2 377.46 373.35 3.61 o 1 4 2 450.66 472.05 4.04 o 2 4 2 4595.38 4858.84 26.37 o 3 4 2 42.17 35.70 1.29 o 4 4 2 1193.95 1179.18 8.68 o 5 4 2 63.45 62.67 1.96 o 6 4 2 583.58 608.63 8.53 o 7 4 2 15.90 15.66 1.64 o 8 4 2 4.22 2.54 0.94 o 9 4 2 259.35 252.99 6.40 o -10 5 2 31.38 29.53 3.37 o -9 5 2 25.84 29.08 2.25 o -8 5 2 225.81 208.20 5.67 o -7 5 2 375.62 361.91 5.44 o -6 5 2 117.79 118.07 2.84 o -5 5 2 504.91 503.25 5.16 o -4 5 2 85.04 79.59 1.93 o -3 5 2 2357.94 2383.29 14.89 o -2 5 2 50.97 58.22 1.50 o -1 5 2 2810.20 2897.85 13.10 o 0 5 2 10.17 14.22 0.89 o 1 5 2 1754.18 1781.04 9.33 o 2 5 2 0.97 1.97 0.47 o 3 5 2 559.78 516.04 5.08 o 4 5 2 2.03 1.20 0.58 o 5 5 2 423.58 417.21 5.36 o 6 5 2 59.75 55.19 2.59 o 7 5 2 331.06 330.27 7.11 o 8 5 2 104.44 100.49 4.24 o 9 5 2 156.04 149.62 5.28 o -9 6 2 14.18 15.22 1.93 o -8 6 2 327.64 334.48 6.61 o -7 6 2 48.08 42.47 2.22 o -6 6 2 4.06 7.18 1.12 o -5 6 2 4.95 4.94 0.94 o -4 6 2 164.01 150.43 2.72 o -3 6 2 68.87 67.60 1.83 o -2 6 2 1604.14 1608.51 10.86 o -1 6 2 87.58 89.07 2.03 o 0 6 2 271.15 261.06 3.35 o 1 6 2 11.66 18.35 1.04 o 2 6 2 1436.79 1462.82 10.27 o 3 6 2 223.67 242.74 3.55 o 4 6 2 2239.66 2268.28 20.83 o 5 6 2 0.05 2.09 1.08 o 6 6 2 36.49 38.57 3.00 o 7 6 2 22.61 25.81 3.04 o 8 6 2 33.95 33.35 3.17 o -9 7 2 160.27 154.86 5.39 o -8 7 2 76.97 86.13 3.72 o -7 7 2 686.84 670.38 9.09 o -6 7 2 298.33 297.28 5.35 o -5 7 2 106.85 104.98 3.17 o -4 7 2 154.40 158.87 3.50 o -3 7 2 631.86 619.35 6.65 o -2 7 2 0.12 2.07 0.55 o -1 7 2 227.58 216.43 3.30 o 0 7 2 26.57 25.42 1.32 o 1 7 2 93.51 91.35 2.19 o 2 7 2 22.66 21.58 1.26 o 3 7 2 272.16 260.19 3.98 o 4 7 2 300.56 284.02 5.25 o 5 7 2 48.43 54.35 2.99 o 6 7 2 2.30 2.50 0.96 o 7 7 2 678.16 724.85 10.23 o 8 7 2 9.55 9.71 1.59 o -8 8 2 489.16 502.84 11.52 o -7 8 2 0.03 1.16 1.08 o -6 8 2 495.36 503.09 7.93 o -5 8 2 7.81 9.43 1.24 o -4 8 2 592.54 586.85 7.07 o -3 8 2 0.00 1.81 0.59 o -2 8 2 279.37 272.06 4.70 o -1 8 2 38.52 36.93 1.84 o 0 8 2 90.39 93.15 2.70 o 1 8 2 4.39 5.91 0.91 o 2 8 2 8.60 7.19 0.99 o 3 8 2 12.10 11.96 1.28 o 4 8 2 681.05 671.76 10.03 o 5 8 2 82.33 81.67 3.66 o 6 8 2 103.08 104.90 4.16 o 7 8 2 0.02 3.02 4.01 o -7 9 2 411.63 422.13 8.88 o -6 9 2 12.63 17.93 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