#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209413.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209413_Fobs loop_ _publ_author_name 'Srinivasan, Bikshandarkoil R.' 'N\"ather, Christian' 'Naik, Ashish R.' 'Bensch, Wolfgang' _publ_section_title ; Bis(methylammonium) tetrathiomolybdate(VI) ; _journal_coeditor_code BT2106 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1635 _journal_page_last m1637 _journal_volume 62 _journal_year 2006 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.5190 _cell_length_b 6.9424 _cell_length_c 15.7041 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7560 _[local]_cod_data_source_file bt2106Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ash1 Pnma R = 0.03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 12220.53 11886.86 80.36 o 6 0 0 1755.04 1524.20 27.01 o 8 0 0 10844.76 11015.85 59.64 o 10 0 0 12420.48 12578.88 62.72 o 12 0 0 1672.26 1657.71 45.61 o 2 1 0 313.78 308.19 19.77 o 4 1 0 20.68 11.49 20.23 o 6 1 0 175.04 206.82 14.85 o 8 1 0 3399.10 3404.00 26.65 o 10 1 0 49.25 39.13 16.95 o 12 1 0 1195.50 1074.95 26.87 o 2 2 0 8487.38 7443.98 92.08 o 4 2 0 52205.28 48055.90 155.81 o 6 2 0 14633.62 14514.33 74.35 o 8 2 0 2566.48 2784.67 46.31 o 10 2 0 1386.29 1463.67 25.32 o 12 2 0 1680.33 1610.02 128.42 o 2 3 0 1.11 11.55 10.49 o 4 3 0 180.40 149.64 14.60 o 6 3 0 81.27 64.98 17.49 o 8 3 0 2175.96 2240.49 67.28 o 10 3 0 40.40 37.83 17.41 o 2 4 0 12126.26 11651.05 202.28 o 4 4 0 6588.65 6821.42 115.41 o 6 4 0 1112.70 1119.48 26.39 o 8 4 0 7440.74 7512.27 58.30 o 10 4 0 9338.44 8888.51 254.60 o 2 5 0 127.05 132.82 13.21 o 4 5 0 48.23 52.89 13.18 o 6 5 0 121.65 129.53 13.70 o 8 5 0 1989.50 1972.88 25.23 o 10 5 0 23.25 29.49 15.59 o 0 6 0 8468.25 8749.70 86.24 o 2 6 0 3465.37 3562.79 29.27 o 4 6 0 20168.97 20240.89 128.18 o 6 6 0 7314.49 7499.63 254.15 o 8 6 0 1448.97 1374.43 23.05 o 2 7 0 22.18 27.75 15.19 o 4 7 0 172.26 182.63 16.54 o 6 7 0 0.29 7.50 24.59 o 8 7 0 533.87 527.72 24.80 o 0 8 0 20196.08 19948.32 135.68 o 2 8 0 4215.06 4453.35 89.42 o 4 8 0 2035.24 2040.76 34.62 o 6 8 0 648.08 615.71 50.73 o 2 9 0 85.30 88.91 53.59 o 1 0 1 62.71 42.49 21.09 o 2 0 1 109.98 63.19 16.51 o 3 0 1 27199.45 23998.25 125.53 o 4 0 1 743.12 804.39 24.70 o 5 0 1 12.91 25.86 20.33 o 6 0 1 4167.84 4048.74 219.64 o 7 0 1 352.85 375.98 17.97 o 8 0 1 189.71 172.79 32.32 o 9 0 1 39.93 32.60 13.81 o 10 0 1 103.70 101.60 24.80 o 11 0 1 827.41 801.63 21.11 o 12 0 1 321.32 345.20 28.44 o 0 1 1 1579.47 1307.86 33.97 o 2 1 1 2092.88 1698.71 33.20 o 3 1 1 23365.85 20764.26 195.62 o 4 1 1 502.10 446.34 11.60 o 5 1 1 21624.87 20414.19 54.44 o 6 1 1 6.70 -2.74 11.76 o 7 1 1 6083.38 6873.69 88.35 o 8 1 1 607.19 666.51 23.43 o 9 1 1 7625.00 7984.69 125.72 o 10 1 1 396.09 387.60 12.18 o 11 1 1 768.62 768.37 16.70 o 12 1 1 473.21 450.25 18.56 o 1 2 1 7665.83 6975.58 44.63 o 2 2 1 11292.47 10153.80 111.73 o 3 2 1 275.86 225.26 12.11 o 4 2 1 342.68 328.14 13.06 o 5 2 1 297.07 263.59 11.65 o 6 2 1 113.46 146.39 21.08 o 7 2 1 4176.03 4328.09 110.96 o 8 2 1 1375.87 1393.89 17.00 o 9 2 1 866.58 870.45 12.77 o 10 2 1 409.94 408.89 12.30 o 11 2 1 186.83 220.58 17.12 o 12 2 1 251.10 262.30 21.28 o 0 3 1 1550.73 1370.63 20.16 o 1 3 1 17963.12 16354.01 155.88 o 2 3 1 605.29 615.43 11.18 o 3 3 1 13967.10 14006.43 116.67 o 4 3 1 352.04 364.27 9.99 o 5 3 1 14490.18 14833.83 243.89 o 6 3 1 0.41 17.50 13.45 o 7 3 1 5000.41 5044.09 124.15 o 8 3 1 551.84 623.37 23.58 o 9 3 1 6912.05 7366.10 130.76 o 10 3 1 421.27 405.29 16.03 o 11 3 1 843.97 836.22 18.24 o 1 4 1 49.75 47.92 6.66 o 2 4 1 105.29 100.43 7.35 o 3 4 1 9423.20 9495.93 67.49 o 4 4 1 448.16 437.70 11.10 o 5 4 1 0.18 15.24 9.37 o 6 4 1 2497.01 2511.27 61.32 o 7 4 1 262.47 265.96 9.62 o 8 4 1 106.07 118.37 12.08 o 9 4 1 18.11 41.18 13.43 o 10 4 1 48.58 59.90 15.75 o 11 4 1 561.37 556.71 18.44 o 0 5 1 591.58 609.81 17.17 o 1 5 1 9009.48 9569.90 64.17 o 2 5 1 198.09 231.38 9.36 o 3 5 1 8523.55 9053.70 104.01 o 4 5 1 493.98 537.91 10.44 o 5 5 1 10922.88 10990.62 41.87 o 6 5 1 41.05 47.88 8.55 o 7 5 1 3879.48 3918.77 99.06 o 8 5 1 379.02 392.63 12.96 o 9 5 1 4420.02 4359.61 45.32 o 10 5 1 203.95 175.14 15.32 o 1 6 1 1842.76 1885.29 17.62 o 2 6 1 2219.34 2288.87 19.34 o 3 6 1 0.28 11.60 8.90 o 4 6 1 149.50 148.68 10.96 o 5 6 1 90.55 107.72 11.82 o 6 6 1 9.89 17.36 12.69 o 7 6 1 1937.13 1947.47 59.30 o 8 6 1 671.66 641.41 15.74 o 9 6 1 385.09 355.11 14.71 o 0 7 1 756.11 833.79 25.98 o 1 7 1 6462.15 6833.42 55.93 o 2 7 1 211.01 216.28 12.24 o 3 7 1 4572.85 4725.29 56.85 o 4 7 1 182.27 212.92 12.81 o 5 7 1 4997.34 4827.75 50.97 o 6 7 1 3.70 -3.91 15.27 o 7 7 1 2266.13 2101.07 46.47 o 8 7 1 314.18 296.03 23.73 o 1 8 1 41.56 49.80 17.46 o 2 8 1 112.08 116.23 21.47 o 3 8 1 2481.22 2593.29 30.96 o 4 8 1 142.64 145.83 16.29 o 5 8 1 1.30 6.73 15.91 o 6 8 1 703.46 631.06 20.00 o 0 9 1 183.14 196.33 46.04 o 1 9 1 2543.15 2574.18 72.43 o 2 9 1 94.89 85.04 31.95 o 1 0 2 11777.33 9538.45 180.38 o 2 0 2 17851.12 15061.18 81.22 o 3 0 2 1297.92 1206.98 25.20 o 4 0 2 8621.43 8301.33 67.48 o 5 0 2 907.36 990.10 28.12 o 6 0 2 4581.83 4703.37 43.88 o 7 0 2 235.07 257.51 14.83 o 8 0 2 5885.78 6120.01 74.49 o 9 0 2 10234.76 11014.62 89.10 o 10 0 2 3550.56 3617.98 27.03 o 11 0 2 1487.21 1409.29 23.78 o 12 0 2 1203.08 1113.89 50.80 o 1 1 2 16.40 11.52 8.15 o 2 1 2 26.88 25.82 9.10 o 3 1 2 893.15 870.22 29.28 o 4 1 2 1015.35 979.27 40.85 o 5 1 2 1236.16 1043.58 12.75 o 6 1 2 0.70 5.01 10.46 o 7 1 2 69.69 75.52 11.94 o 8 1 2 913.57 926.49 18.71 o 9 1 2 968.90 1035.75 13.62 o 10 1 2 2.23 9.78 11.99 o 11 1 2 292.95 295.27 17.36 o 12 1 2 250.66 173.63 26.58 o 0 2 2 11406.51 9799.22 304.90 o 1 2 2 2127.42 1976.24 19.21 o 2 2 2 10854.07 9729.36 114.20 o 3 2 2 1309.72 1153.58 13.94 o 4 2 2 15718.38 14830.31 89.47 o 5 2 2 22541.29 21705.01 126.06 o 6 2 2 6856.26 7348.06 131.00 o 7 2 2 753.51 840.84 26.21 o 8 2 2 3430.84 3540.75 58.37 o 9 2 2 578.06 652.02 15.20 o 10 2 2 1580.01 1608.83 46.19 o 11 2 2 1.14 7.36 15.25 o 12 2 2 1308.95 1267.78 29.89 o 1 3 2 31.28 31.35 6.81 o 2 3 2 0.58 4.92 7.21 o 3 3 2 646.93 610.13 12.07 o 4 3 2 670.75 631.93 10.46 o 5 3 2 756.26 820.41 16.69 o 6 3 2 9.83 16.68 9.40 o 7 3 2 134.79 141.47 10.08 o 8 3 2 611.89 564.70 14.10 o 9 3 2 958.88 940.73 24.37 o 10 3 2 1.71 1.11 11.32 o 11 3 2 178.90 183.70 17.51 o 0 4 2 15043.79 14686.86 113.57 o 1 4 2 6670.04 6503.68 54.53 o 2 4 2 7540.70 7276.99 41.90 o 3 4 2 87.75 87.33 9.31 o 4 4 2 6006.70 5991.54 40.81 o 5 4 2 418.79 452.13 11.39 o 6 4 2 2842.37 2949.99 35.96 o 7 4 2 193.52 206.28 10.23 o 8 4 2 4140.83 4333.77 65.48 o 9 4 2 7448.71 7729.72 113.21 o 10 4 2 2725.29 2666.04 67.10 o 11 4 2 1207.45 1143.52 19.34 o 1 5 2 249.32 247.01 8.64 o 2 5 2 13.60 16.71 7.69 o 3 5 2 60.44 68.56 10.27 o 4 5 2 269.95 297.88 10.25 o 5 5 2 455.68 477.08 10.47 o 6 5 2 0.01 6.70 7.73 o 7 5 2 0.69 -0.85 11.52 o 8 5 2 480.30 481.46 13.64 o 9 5 2 405.12 364.93 17.51 o 10 5 2 1.25 -3.01 15.57 o 0 6 2 4164.75 4322.55 56.14 o 1 6 2 146.21 135.86 9.87 o 2 6 2 3435.53 3562.14 23.04 o 3 6 2 1032.88 1089.72 14.12 o 4 6 2 6469.89 6405.84 37.25 o 5 6 2 9418.96 9749.98 48.94 o 6 6 2 3289.77 3320.13 45.09 o 7 6 2 507.66 503.63 14.22 o 8 6 2 1850.67 1773.84 40.43 o 9 6 2 313.59 276.95 15.22 o 1 7 2 16.62 21.89 12.43 o 2 7 2 6.25 4.88 13.52 o 3 7 2 320.93 324.61 14.14 o 4 7 2 187.66 212.39 12.27 o 5 7 2 230.36 209.03 11.63 o 6 7 2 3.87 5.28 14.75 o 7 7 2 72.69 76.90 15.06 o 8 7 2 155.33 156.80 20.64 o 0 8 2 4736.24 4688.08 63.25 o 1 8 2 2804.08 2916.65 36.20 o 2 8 2 2383.87 2424.68 38.99 o 3 8 2 1.89 10.41 16.69 o 4 8 2 1984.23 1976.84 21.48 o 5 8 2 145.99 134.15 14.12 o 6 8 2 1238.36 949.54 40.37 o 1 9 2 90.86 83.61 34.64 o 2 9 2 8.51 22.73 43.78 o 1 0 3 2.61 8.57 9.51 o 2 0 3 1102.90 1130.90 19.77 o 3 0 3 3918.44 3596.88 87.18 o 4 0 3 1270.29 1198.05 21.78 o 5 0 3 14.36 17.54 18.94 o 6 0 3 7769.22 8000.71 55.03 o 7 0 3 626.46 709.09 22.40 o 8 0 3 871.59 868.21 70.19 o 9 0 3 56.75 64.55 14.03 o 10 0 3 510.33 514.46 22.17 o 11 0 3 3.10 10.23 21.36 o 12 0 3 719.37 577.88 36.43 o 0 1 3 17827.20 14517.58 75.81 o 1 1 3 10708.04 9033.83 85.65 o 2 1 3 689.72 508.69 11.98 o 3 1 3 2787.38 2613.42 50.04 o 4 1 3 8542.58 8015.72 35.97 o 5 1 3 3442.85 3391.11 78.51 o 6 1 3 1035.65 1096.12 29.34 o 7 1 3 1241.42 1269.36 25.10 o 8 1 3 4471.73 4592.47 25.44 o 9 1 3 1340.87 1419.63 23.67 o 10 1 3 3094.37 3208.07 63.92 o 11 1 3 1275.69 1322.83 19.22 o 12 1 3 1924.75 1814.52 25.88 o 1 2 3 1235.55 1110.97 13.59 o 2 2 3 13673.01 13042.49 67.31 o 3 2 3 9.56 7.00 7.53 o 4 2 3 1124.66 1075.68 11.94 o 5 2 3 24.90 33.43 9.73 o 6 2 3 72.82 88.14 9.27 o 7 2 3 159.01 149.50 18.71 o 8 2 3 1916.22 1966.01 49.21 o 9 2 3 50.78 69.32 13.07 o 10 2 3 1604.39 1666.40 23.76 o 11 2 3 225.08 192.26 17.48 o 12 2 3 572.42 555.73 20.35 o 0 3 3 12171.77 10959.19 132.62 o 1 3 3 5332.72 5316.89 55.45 o 2 3 3 1353.86 1137.91 12.88 o 3 3 3 2094.93 2093.67 16.55 o 4 3 3 5626.74 5528.02 96.91 o 5 3 3 2664.87 2817.53 28.30 o 6 3 3 817.00 904.18 11.74 o 7 3 3 1077.91 1127.92 24.64 o 8 3 3 3874.59 3868.31 50.53 o 9 3 3 1132.79 1241.61 39.12 o 10 3 3 3049.55 2945.11 44.21 o 11 3 3 1065.69 1035.77 23.91 o 1 4 3 56.59 45.32 6.72 o 2 4 3 1086.45 933.98 16.63 o 3 4 3 1255.08 1310.83 13.78 o 4 4 3 577.96 645.77 11.76 o 5 4 3 0.11 13.21 8.90 o 6 4 3 5200.92 5109.32 85.32 o 7 4 3 471.30 459.86 9.71 o 8 4 3 582.39 605.69 16.50 o 9 4 3 40.85 41.28 13.65 o 10 4 3 273.83 250.56 14.90 o 11 4 3 2.21 11.44 15.39 o 0 5 3 5000.73 5421.14 102.80 o 1 5 3 3083.03 3275.67 31.26 o 2 5 3 757.01 779.45 12.32 o 3 5 3 1466.98 1557.16 14.21 o 4 5 3 4908.72 5056.10 54.32 o 5 5 3 1578.88 1614.19 22.72 o 6 5 3 1197.93 1257.84 26.15 o 7 5 3 781.00 805.84 18.95 o 8 5 3 2645.12 2601.99 40.42 o 9 5 3 928.42 916.26 17.65 o 10 5 3 1744.19 1679.97 69.97 o 1 6 3 255.83 262.67 10.23 o 2 6 3 3804.56 3909.60 53.63 o 3 6 3 58.33 53.94 7.41 o 4 6 3 364.67 383.10 11.53 o 5 6 3 5.72 0.78 11.61 o 6 6 3 6.73 11.91 10.59 o 7 6 3 86.97 73.98 10.51 o 8 6 3 1070.34 1041.81 43.14 o 9 6 3 27.40 -1.35 20.50 o 0 7 3 4609.60 4838.76 37.89 o 1 7 3 1580.73 1646.65 21.88 o 2 7 3 790.78 831.55 17.08 o 3 7 3 1025.09 1041.02 16.46 o 4 7 3 2135.67 2141.03 26.45 o 5 7 3 1207.71 1196.78 15.39 o 6 7 3 473.74 506.60 20.74 o 7 7 3 662.75 614.57 20.60 o 1 8 3 27.45 28.45 19.77 o 2 8 3 408.56 428.02 21.75 o 3 8 3 331.14 316.79 17.16 o 4 8 3 308.58 312.12 18.17 o 5 8 3 0.01 2.02 15.45 o 0 9 3 1477.57 1505.36 53.78 o 0 0 4 18898.51 15372.88 79.76 o 1 0 4 19141.41 16408.56 238.69 o 2 0 4 106.76 97.54 12.82 o 3 0 4 3604.31 3135.69 102.95 o 4 0 4 3685.85 3226.57 28.40 o 5 0 4 4516.10 4260.66 206.47 o 6 0 4 3371.15 3756.18 42.29 o 7 0 4 2691.06 2872.49 33.69 o 8 0 4 3.95 -2.88 16.15 o 9 0 4 10154.32 11149.31 74.73 o 10 0 4 469.49 478.88 18.95 o 11 0 4 2555.65 2560.93 53.90 o 12 0 4 336.78 333.70 31.36 o 1 1 4 3137.86 2919.27 22.58 o 2 1 4 16.57 17.61 6.41 o 3 1 4 503.81 483.13 12.36 o 4 1 4 26.35 24.15 6.96 o 5 1 4 1854.94 1664.67 16.83 o 6 1 4 14.56 16.78 10.44 o 7 1 4 100.03 104.22 12.35 o 8 1 4 1005.16 1004.44 29.36 o 9 1 4 234.76 261.84 15.10 o 10 1 4 8.06 14.22 13.08 o 11 1 4 213.64 242.83 19.23 o 12 1 4 322.04 314.73 18.51 o 0 2 4 1326.55 1290.50 30.79 o 1 2 4 2767.50 2528.90 34.96 o 2 2 4 2373.02 2268.34 16.50 o 3 2 4 7344.46 7117.44 84.33 o 4 2 4 2308.69 2109.00 16.27 o 5 2 4 15047.66 15692.79 342.95 o 6 2 4 137.40 119.92 8.59 o 7 2 4 2702.67 2963.22 18.18 o 8 2 4 1493.87 1526.58 28.67 o 9 2 4 3334.64 3540.65 48.62 o 10 2 4 1397.16 1419.47 47.66 o 11 2 4 1127.94 1067.98 18.05 o 12 2 4 366.98 248.57 34.84 o 1 3 4 1431.98 1351.90 17.36 o 2 3 4 0.47 6.96 7.34 o 3 3 4 394.37 354.48 9.45 o 4 3 4 99.14 72.47 8.92 o 5 3 4 1029.37 1121.08 12.99 o 6 3 4 0.15 -6.90 9.39 o 7 3 4 112.31 130.99 9.01 o 8 3 4 571.30 585.50 25.13 o 9 3 4 224.63 226.91 12.62 o 10 3 4 11.51 -3.39 13.62 o 11 3 4 123.36 110.29 13.86 o 0 4 4 5972.57 5743.93 130.10 o 1 4 4 9396.35 9697.64 274.95 o 2 4 4 140.11 161.69 8.24 o 3 4 4 2016.48 2371.15 17.99 o 4 4 4 1640.65 1819.91 21.03 o 5 4 4 2682.08 2792.57 52.65 o 6 4 4 2442.24 2504.99 51.32 o 7 4 4 2017.22 2109.41 19.05 o 8 4 4 3.43 -1.36 11.60 o 9 4 4 7533.82 7680.09 164.36 o 10 4 4 338.24 333.92 18.01 o 11 4 4 2023.48 1911.98 33.40 o 1 5 4 954.82 988.33 13.45 o 2 5 4 61.67 76.35 9.41 o 3 5 4 50.56 52.56 9.27 o 4 5 4 12.42 12.55 9.01 o 5 5 4 562.87 592.12 9.66 o 6 5 4 12.38 0.63 11.49 o 7 5 4 3.69 -2.20 10.67 o 8 5 4 573.56 568.86 14.73 o 9 5 4 86.03 83.06 14.21 o 10 5 4 5.32 14.58 22.92 o 0 6 4 892.69 866.03 30.71 o 1 6 4 1517.26 1635.14 20.88 o 2 6 4 986.46 979.40 14.43 o 3 6 4 3380.96 3589.98 28.47 o 4 6 4 935.66 950.82 13.62 o 5 6 4 7306.80 7463.90 38.96 o 6 6 4 54.94 50.05 10.12 o 7 6 4 1651.63 1675.94 42.47 o 8 6 4 835.74 779.02 22.89 o 9 6 4 1982.78 1867.74 63.22 o 1 7 4 230.22 252.26 12.92 o 2 7 4 20.06 31.76 15.47 o 3 7 4 186.03 181.33 14.24 o 4 7 4 59.68 58.55 10.74 o 5 7 4 309.27 282.92 13.17 o 6 7 4 2.43 3.50 12.84 o 7 7 4 55.75 46.14 11.99 o 0 8 4 1480.80 1550.65 30.91 o 1 8 4 3890.30 4089.70 67.89 o 2 8 4 75.18 72.69 20.01 o 3 8 4 1114.37 1080.99 24.08 o 4 8 4 837.31 800.32 20.79 o 5 8 4 1373.70 1322.73 24.21 o 1 0 5 383.52 333.60 11.05 o 2 0 5 309.94 278.74 10.64 o 3 0 5 14738.33 13919.73 384.12 o 4 0 5 90.71 88.66 11.31 o 5 0 5 4.32 -2.45 10.49 o 6 0 5 106.69 133.72 14.10 o 7 0 5 820.49 835.20 27.92 o 8 0 5 94.65 73.97 17.16 o 9 0 5 20.00 77.09 29.08 o 10 0 5 217.62 246.59 26.55 o 11 0 5 1069.54 1118.06 25.46 o 12 0 5 13.30 4.99 23.40 o 0 1 5 17824.63 15229.59 99.58 o 1 1 5 2276.91 2173.65 25.64 o 2 1 5 7492.58 6706.28 44.20 o 3 1 5 964.84 812.27 11.16 o 4 1 5 10719.13 10120.60 127.59 o 5 1 5 2876.48 2684.70 78.43 o 6 1 5 6624.34 6927.99 71.32 o 7 1 5 57.57 61.40 12.44 o 8 1 5 5079.58 5294.21 84.56 o 9 1 5 746.23 829.22 16.88 o 10 1 5 4266.75 4360.22 125.97 o 11 1 5 472.35 516.97 17.83 o 12 1 5 2453.92 2347.41 54.48 o 1 2 5 6351.92 5818.85 50.11 o 2 2 5 1.63 8.32 5.89 o 3 2 5 303.71 317.89 18.46 o 4 2 5 10.16 2.28 7.80 o 5 2 5 190.96 183.96 10.06 o 6 2 5 237.45 231.22 9.42 o 7 2 5 4696.49 4982.56 72.51 o 8 2 5 2.72 9.17 7.21 o 9 2 5 1033.00 1120.62 16.97 o 10 2 5 295.68 315.20 15.57 o 11 2 5 269.60 267.65 15.21 o 0 3 5 12641.21 12068.29 305.14 o 1 3 5 1836.79 1639.43 28.01 o 2 3 5 5390.99 4979.27 23.98 o 3 3 5 271.38 294.57 9.46 o 4 3 5 8753.70 9104.77 103.73 o 5 3 5 1432.74 1490.63 13.21 o 6 3 5 5141.22 5492.64 107.17 o 7 3 5 55.08 57.39 8.78 o 8 3 5 4398.73 4707.28 30.52 o 9 3 5 767.33 819.29 14.37 o 10 3 5 3800.98 3823.70 37.38 o 11 3 5 287.94 219.62 16.39 o 1 4 5 186.34 219.53 10.47 o 2 4 5 105.35 108.12 9.86 o 3 4 5 7906.49 7968.95 131.29 o 4 4 5 31.29 37.08 9.38 o 5 4 5 14.67 21.60 9.32 o 6 4 5 87.20 82.74 9.46 o 7 4 5 537.54 537.93 12.54 o 8 4 5 78.51 64.92 11.12 o 9 4 5 10.74 16.57 15.06 o 10 4 5 125.01 134.54 15.66 o 0 5 5 7343.27 7407.81 38.33 o 1 5 5 511.38 515.85 16.50 o 2 5 5 3566.13 3688.30 41.73 o 3 5 5 236.66 288.44 10.14 o 4 5 5 6137.34 6249.19 55.87 o 5 5 5 1469.76 1476.82 15.39 o 6 5 5 3763.52 3923.29 48.89 o 7 5 5 5.48 6.30 11.68 o 8 5 5 3181.48 3195.53 133.40 o 9 5 5 289.46 302.72 17.56 o 10 5 5 2861.89 2681.19 64.13 o 1 6 5 2115.67 2114.62 17.35 o 2 6 5 6.08 10.88 8.52 o 3 6 5 222.70 232.19 9.78 o 4 6 5 9.97 16.49 10.89 o 5 6 5 54.38 54.25 11.25 o 6 6 5 94.99 66.09 10.91 o 7 6 5 2233.85 2285.91 46.16 o 8 6 5 1.32 9.67 13.99 o 9 6 5 453.27 365.65 34.80 o 0 7 5 4807.59 5137.29 36.24 o 1 7 5 686.05 717.33 13.86 o 2 7 5 2409.93 2465.13 49.14 o 3 7 5 79.36 78.21 14.07 o 4 7 5 3614.39 3503.07 41.64 o 5 7 5 259.05 269.90 15.09 o 6 7 5 2539.40 2359.64 19.49 o 7 7 5 20.95 17.76 15.28 o 1 8 5 88.00 81.62 18.08 o 2 8 5 31.15 37.45 20.34 o 3 8 5 2357.61 2343.41 79.11 o 4 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11 0.80 -2.52 16.20 o 10 0 11 167.93 141.96 22.57 o 0 1 11 2929.54 3040.12 46.32 o 1 1 11 3474.82 3694.08 41.07 o 2 1 11 132.22 142.46 6.75 o 3 1 11 4935.22 5245.32 53.35 o 4 1 11 1539.52 1598.21 11.78 o 5 1 11 218.62 261.65 8.57 o 6 1 11 638.95 663.92 9.82 o 7 1 11 4286.13 4433.80 28.56 o 8 1 11 678.37 688.29 18.92 o 9 1 11 889.94 924.16 13.56 o 10 1 11 802.58 753.67 27.70 o 1 2 11 617.86 607.12 9.25 o 2 2 11 1310.61 1334.39 14.78 o 3 2 11 160.31 167.96 7.30 o 4 2 11 92.57 106.79 7.12 o 5 2 11 164.00 159.77 8.09 o 6 2 11 569.87 594.36 10.23 o 7 2 11 1869.57 1944.29 15.21 o 8 2 11 630.49 608.25 14.74 o 9 2 11 33.26 41.05 13.16 o 10 2 11 56.92 22.74 15.59 o 0 3 11 2007.59 2079.78 23.46 o 1 3 11 2323.53 2431.35 13.20 o 2 3 11 145.30 146.44 7.19 o 3 3 11 4389.78 4472.19 34.61 o 4 3 11 1515.43 1448.72 14.80 o 5 3 11 417.67 464.03 17.17 o 6 3 11 631.23 677.36 13.30 o 7 3 11 3792.18 3889.59 20.20 o 8 3 11 598.83 633.71 15.05 o 9 3 11 677.79 624.90 18.51 o 1 4 11 126.10 117.80 8.40 o 2 4 11 979.92 990.89 12.27 o 3 4 11 3112.90 3165.20 30.86 o 4 4 11 545.96 567.09 12.65 o 5 4 11 3.15 0.52 9.22 o 6 4 11 159.57 169.06 9.67 o 7 4 11 10.96 8.25 11.77 o 8 4 11 338.26 308.99 13.29 o 9 4 11 2.33 13.54 15.15 o 0 5 11 1562.55 1674.21 28.02 o 1 5 11 2417.96 2630.80 81.09 o 2 5 11 189.02 203.89 10.61 o 3 5 11 2910.46 2953.98 20.17 o 4 5 11 981.42 888.57 21.78 o 5 5 11 191.58 176.32 11.43 o 6 5 11 375.69 395.46 14.59 o 7 5 11 2739.51 2563.28 71.82 o 8 5 11 431.85 427.69 19.41 o 1 6 11 364.38 361.57 20.41 o 2 6 11 652.28 658.73 13.30 o 3 6 11 27.37 30.07 10.00 o 4 6 11 77.08 60.32 16.24 o 5 6 11 53.07 44.95 16.53 o 6 6 11 303.79 263.54 15.88 o 0 7 11 781.78 728.44 27.73 o 1 7 11 1140.58 1021.64 39.81 o 2 7 11 126.19 124.64 12.98 o 3 7 11 2358.43 2050.05 33.48 o 4 7 11 724.08 707.31 26.81 o 0 0 12 58.43 88.51 10.93 o 1 0 12 1216.36 1313.24 27.54 o 2 0 12 1837.59 1924.57 36.06 o 3 0 12 6887.21 7102.60 154.33 o 4 0 12 704.50 729.58 26.16 o 5 0 12 7476.20 7666.62 221.19 o 6 0 12 2926.47 3042.58 38.02 o 7 0 12 2391.13 2645.22 22.84 o 8 0 12 598.44 587.96 40.23 o 9 0 12 134.97 115.48 17.01 o 10 0 12 1409.09 1340.94 30.70 o 1 1 12 18.13 24.19 6.38 o 2 1 12 262.48 252.52 7.28 o 3 1 12 128.66 124.81 7.60 o 4 1 12 1045.29 1072.88 12.27 o 5 1 12 12.44 15.02 6.83 o 6 1 12 86.69 100.07 9.95 o 7 1 12 21.52 28.95 10.03 o 8 1 12 1760.04 1767.50 38.57 o 9 1 12 57.47 57.77 14.15 o 10 1 12 0.48 1.46 16.13 o 0 2 12 138.85 163.26 9.39 o 1 2 12 11105.72 11693.88 81.23 o 2 2 12 1494.20 1645.17 12.87 o 3 2 12 1998.99 2153.66 17.79 o 4 2 12 352.46 380.96 8.76 o 5 2 12 42.61 44.41 7.81 o 6 2 12 3102.90 3326.44 36.49 o 7 2 12 1535.62 1599.17 18.89 o 8 2 12 1137.78 1145.49 24.89 o 9 2 12 3747.40 3600.26 63.20 o 1 3 12 0.80 6.92 6.99 o 2 3 12 101.54 116.67 7.42 o 3 3 12 165.31 173.14 7.11 o 4 3 12 837.75 844.28 16.41 o 5 3 12 5.91 19.54 10.12 o 6 3 12 125.14 126.33 10.16 o 7 3 12 57.16 47.79 11.23 o 8 3 12 1253.02 1232.96 36.38 o 9 3 12 80.13 82.60 14.89 o 0 4 12 79.36 82.39 11.36 o 1 4 12 818.73 882.67 10.20 o 2 4 12 1448.02 1511.41 22.74 o 3 4 12 4546.59 4981.18 21.97 o 4 4 12 539.30 556.18 12.74 o 5 4 12 5444.52 5484.44 44.25 o 6 4 12 2127.73 2121.43 37.64 o 7 4 12 1896.83 1897.66 35.71 o 8 4 12 518.87 461.32 21.21 o 1 5 12 23.84 7.52 9.61 o 2 5 12 160.29 180.23 11.58 o 3 5 12 9.49 5.74 10.41 o 4 5 12 426.90 406.66 12.76 o 5 5 12 6.49 3.49 13.85 o 6 5 12 35.26 39.91 14.43 o 7 5 12 1.01 -0.65 14.75 o 0 6 12 178.78 129.66 16.92 o 1 6 12 5634.90 5553.25 51.45 o 2 6 12 1045.60 1025.73 17.09 o 3 6 12 1066.23 1166.59 28.21 o 4 6 12 319.50 304.47 18.73 o 5 6 12 41.98 37.07 15.32 o 6 6 12 1837.53 1655.96 29.56 o 1 7 12 2.12 25.29 15.79 o 2 7 12 14.02 7.43 14.61 o 3 7 12 101.46 86.36 19.65 o 1 0 13 683.58 759.37 21.30 o 2 0 13 376.39 370.83 10.76 o 3 0 13 0.11 3.17 9.44 o 4 0 13 1.78 0.11 10.81 o 5 0 13 21.66 23.88 12.13 o 6 0 13 1652.84 1758.11 28.70 o 7 0 13 1443.48 1578.25 29.59 o 8 0 13 346.49 384.54 19.27 o 9 0 13 213.88 189.35 21.99 o 0 1 13 3022.77 3153.26 21.76 o 1 1 13 86.95 115.53 6.68 o 2 1 13 10894.04 11281.44 65.21 o 3 1 13 776.98 819.44 9.32 o 4 1 13 4202.74 4268.62 37.85 o 5 1 13 12.91 8.46 8.59 o 6 1 13 6136.55 6266.85 31.06 o 7 1 13 1337.87 1328.58 24.47 o 8 1 13 3491.34 3543.79 26.39 o 9 1 13 147.94 114.65 13.74 o 1 2 13 7.24 14.75 6.74 o 2 2 13 2193.21 2178.35 18.31 o 3 2 13 1801.29 1827.70 19.93 o 4 2 13 802.74 842.09 10.90 o 5 2 13 6.99 11.74 8.45 o 6 2 13 10.95 7.74 9.31 o 7 2 13 7.00 -3.83 10.90 o 8 2 13 351.09 335.67 13.79 o 9 2 13 19.13 12.77 15.08 o 0 3 13 2013.21 2110.94 58.08 o 1 3 13 104.16 107.39 6.97 o 2 3 13 8583.38 8771.71 124.74 o 3 3 13 714.35 735.65 9.97 o 4 3 13 4075.47 4311.82 33.23 o 5 3 13 23.66 20.41 9.70 o 6 3 13 5617.35 5594.92 61.64 o 7 3 13 1092.46 1105.55 18.12 o 8 3 13 2881.44 2798.92 65.07 o 1 4 13 497.76 512.22 11.50 o 2 4 13 295.33 282.11 9.85 o 3 4 13 6.72 16.29 9.60 o 4 4 13 0.14 1.49 11.48 o 5 4 13 5.39 7.02 12.51 o 6 4 13 1175.73 1236.09 31.17 o 7 4 13 989.77 893.37 23.11 o 8 4 13 235.48 231.35 31.06 o 0 5 13 2354.77 2599.28 81.37 o 1 5 13 107.24 109.02 14.02 o 2 5 13 6409.70 6526.53 93.03 o 3 5 13 527.90 496.67 11.83 o 4 5 13 2393.75 2400.52 50.94 o 5 5 13 35.35 40.76 12.35 o 6 5 13 3418.27 3141.20 110.78 o 7 5 13 927.18 821.21 35.61 o 1 6 13 8.75 16.10 15.94 o 2 6 13 1045.71 1119.39 25.20 o 3 6 13 815.82 784.00 18.18 o 4 6 13 327.76 271.38 21.76 o 5 6 13 3.78 4.10 20.26 o 0 7 13 960.67 907.85 68.27 o 1 7 13 115.06 101.17 20.78 o 0 0 14 1139.82 1170.48 72.43 o 1 0 14 7903.59 8276.27 97.45 o 2 0 14 658.68 691.87 12.06 o 3 0 14 10198.23 10559.31 144.83 o 4 0 14 1289.23 1338.58 16.79 o 5 0 14 5597.58 5995.80 85.04 o 6 0 14 233.86 213.33 21.38 o 7 0 14 5223.96 5143.00 161.58 o 8 0 14 173.93 138.34 22.05 o 9 0 14 766.69 701.18 23.79 o 1 1 14 878.28 888.00 11.42 o 2 1 14 29.61 28.50 5.53 o 3 1 14 141.12 140.61 7.13 o 4 1 14 84.98 103.29 8.74 o 5 1 14 673.25 714.83 12.47 o 6 1 14 14.11 2.58 9.48 o 7 1 14 280.07 275.99 11.55 o 8 1 14 6.63 6.60 11.85 o 9 1 14 218.69 216.70 17.65 o 0 2 14 1630.93 1697.09 25.47 o 1 2 14 10536.17 10579.86 54.01 o 2 2 14 27.42 34.84 6.21 o 3 2 14 7037.22 7592.79 62.40 o 4 2 14 500.51 548.44 11.47 o 5 2 14 2819.00 2883.24 32.00 o 6 2 14 781.04 771.95 13.32 o 7 2 14 5820.83 5830.25 55.56 o 8 2 14 88.40 110.92 14.26 o 1 3 14 596.29 631.14 9.82 o 2 3 14 11.98 12.68 9.00 o 3 3 14 215.36 220.58 9.17 o 4 3 14 38.19 36.03 10.48 o 5 3 14 561.53 603.53 19.10 o 6 3 14 10.90 11.71 12.05 o 7 3 14 309.00 300.13 14.75 o 8 3 14 23.19 12.23 16.04 o 0 4 14 919.97 943.15 16.17 o 1 4 14 5571.47 5880.45 84.68 o 2 4 14 459.34 442.41 10.04 o 3 4 14 7367.22 7423.07 70.00 o 4 4 14 844.33 882.59 23.17 o 5 4 14 4192.72 4245.44 26.30 o 6 4 14 167.86 164.05 15.27 o 7 4 14 3869.92 3575.60 102.83 o 1 5 14 564.12 578.92 16.39 o 2 5 14 46.53 43.94 11.47 o 3 5 14 40.56 30.45 13.57 o 4 5 14 66.69 46.24 13.59 o 5 5 14 319.46 332.00 15.12 o 6 5 14 0.33 4.40 16.67 o 0 6 14 742.43 738.45 27.49 o 1 6 14 5418.83 5427.53 194.36 o 2 6 14 9.27 22.17 16.14 o 3 6 14 3712.82 3391.14 158.14 o 4 6 14 353.54 277.88 20.99 o 1 0 15 434.53 422.19 10.38 o 2 0 15 595.66 640.54 12.61 o 3 0 15 1388.66 1454.48 26.33 o 4 0 15 117.66 112.58 12.51 o 5 0 15 10.21 5.74 12.43 o 6 0 15 728.50 746.67 26.20 o 7 0 15 391.59 415.57 19.56 o 8 0 15 95.12 68.80 17.15 o 0 1 15 4722.59 5013.02 80.72 o 1 1 15 72.87 79.39 6.08 o 2 1 15 11127.59 11967.70 144.18 o 3 1 15 191.57 190.19 8.92 o 4 1 15 4274.20 4475.07 38.18 o 5 1 15 10.27 14.61 9.30 o 6 1 15 5140.60 4972.78 81.53 o 7 1 15 150.67 148.68 11.95 o 8 1 15 2663.53 2379.46 56.09 o 1 2 15 391.17 415.08 8.89 o 2 2 15 5.08 -2.75 8.44 o 3 2 15 448.90 487.57 13.54 o 4 2 15 28.06 28.07 9.19 o 5 2 15 49.11 56.35 10.86 o 6 2 15 1074.64 1129.03 14.97 o 7 2 15 873.40 821.44 13.96 o 8 2 15 73.05 83.41 18.76 o 0 3 15 3869.00 4221.03 61.87 o 1 3 15 28.89 36.56 8.53 o 2 3 15 9314.13 9759.57 64.17 o 3 3 15 206.74 216.30 8.81 o 4 3 15 3771.51 3755.56 68.35 o 5 3 15 2.76 -0.43 12.42 o 6 3 15 4518.22 4429.17 82.47 o 7 3 15 160.86 107.77 17.23 o 1 4 15 364.45 381.44 11.95 o 2 4 15 406.91 439.82 11.10 o 3 4 15 996.35 1007.26 12.87 o 4 4 15 86.51 91.14 13.39 o 5 4 15 10.53 12.42 12.72 o 6 4 15 423.89 404.47 17.76 o 0 5 15 3129.72 3331.48 53.23 o 1 5 15 125.12 127.92 13.67 o 2 5 15 6757.45 6942.77 169.26 o 3 5 15 116.16 99.75 13.55 o 4 5 15 2552.30 2427.94 78.28 o 5 5 15 15.39 8.46 17.75 o 1 6 15 196.75 190.00 25.24 o 2 6 15 0.11 -15.11 17.91 o 0 0 16 225.52 220.38 19.47 o 1 0 16 8372.94 8927.35 63.72 o 2 0 16 807.50 872.27 15.30 o 3 0 16 3931.81 4088.17 34.52 o 4 0 16 551.88 562.97 14.33 o 5 0 16 594.86 579.09 13.94 o 6 0 16 1454.91 1479.27 45.53 o 7 0 16 2943.08 2760.25 52.89 o 1 1 16 264.08 283.64 8.29 o 2 1 16 15.01 18.55 7.42 o 3 1 16 17.23 22.47 9.08 o 4 1 16 336.10 342.81 12.99 o 5 1 16 387.72 380.44 10.62 o 6 1 16 0.06 10.19 11.29 o 7 1 16 71.73 62.59 12.69 o 0 2 16 456.36 457.89 20.28 o 1 2 16 2007.32 2155.10 13.62 o 2 2 16 1111.62 1133.34 17.04 o 3 2 16 5959.71 6158.41 43.06 o 4 2 16 45.55 53.52 9.54 o 5 2 16 4806.14 4939.86 93.52 o 6 2 16 489.48 490.82 12.78 o 7 2 16 3784.51 3615.58 115.90 o 1 3 16 220.93 218.40 8.82 o 2 3 16 0.02 -7.31 9.22 o 3 3 16 5.66 -1.90 8.99 o 4 3 16 338.84 365.54 12.08 o 5 3 16 340.34 321.15 14.42 o 6 3 16 7.98 7.84 13.19 o 0 4 16 94.08 99.59 17.99 o 1 4 16 5941.20 6233.06 74.13 o 2 4 16 609.38 597.43 12.64 o 3 4 16 2886.62 2855.08 31.29 o 4 4 16 516.53 491.98 13.40 o 5 4 16 488.13 411.89 15.54 o 1 5 16 124.99 107.02 17.78 o 2 5 16 48.59 25.17 13.71 o 3 5 16 17.66 3.51 15.34 o 4 5 16 138.88 124.61 22.68 o 1 0 17 147.56 183.65 12.61 o 2 0 17 1138.66 1164.49 14.75 o 3 0 17 507.91 491.68 12.91 o 4 0 17 288.97 278.23 19.34 o 5 0 17 12.80 0.18 17.83 o 6 0 17 89.57 37.37 21.51 o 7 0 17 406.37 336.46 21.70 o 0 1 17 1181.38 1198.82 26.91 o 1 1 17 588.83 570.67 12.47 o 2 1 17 2180.03 2289.41 36.23 o 3 1 17 1438.33 1444.84 24.59 o 4 1 17 1200.26 1224.66 14.07 o 5 1 17 171.85 178.93 13.84 o 6 1 17 1703.64 1583.22 26.02 o 7 1 17 1956.90 1815.32 61.92 o 1 2 17 114.84 91.35 8.51 o 2 2 17 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1671.04 1572.90 23.77 o 5 2 18 1020.06 995.48 30.11 o 1 3 18 24.78 32.36 11.15 o 2 3 18 21.56 10.27 10.89 o 3 3 18 18.33 23.39 12.01 o 4 3 18 246.84 221.08 18.47 o 0 4 18 1172.42 984.04 48.90 o 1 4 18 751.88 722.33 24.68 o 2 4 18 2157.53 2023.47 32.93 o 3 4 18 47.16 45.12 37.85 o 1 0 19 373.24 368.88 14.34 o 2 0 19 6.52 32.27 15.85 o 3 0 19 9.78 8.02 20.67 o 4 0 19 54.86 49.58 18.35 o 5 0 19 31.60 37.58 31.24 o 0 1 19 98.36 92.34 15.80 o 1 1 19 1967.74 1936.53 30.73 o 2 1 19 586.05 579.52 11.51 o 3 1 19 2199.91 2112.47 45.11 o 4 1 19 1.54 6.65 13.11 o 1 2 19 66.56 77.68 10.90 o 2 2 19 140.28 116.94 11.24 o 3 2 19 1308.98 1161.20 27.60 o 4 2 19 41.95 12.98 16.00 o 0 3 19 139.56 120.49 15.45 o 1 3 19 1928.80 1742.16 38.35 o 2 3 19 433.51 425.07 14.78 o 3 3 19 1942.66 1495.26 41.91 o 0 0 20 3135.63 2829.68 29.60 o 1 0 20 1751.01 1800.07 54.29 o 2 0 20 3218.99 3242.22 130.77 o 3 0 20 865.30 859.48 37.57 o 1 1 20 318.35 303.57 16.98 o 2 1 20 13.40 23.86 12.11 o 3 1 20 186.54 111.02 32.97 o 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