#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209414.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209414_Fobs loop_ _publ_author_name 'Zhang, Wen-Zhi' _publ_section_title ; Poly[diaqua-\m~4~-benzene-1,4-dicarboxylato-di-\m~2~-benzene-1,4-dicarboxylato-bis(N,N'-dimethylformamide)digadolinium(III)] ; _journal_coeditor_code BT2107 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1600 _journal_page_last m1602 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 65.258 _cell_angle_beta 71.756 _cell_angle_gamma 78.677 _cell_length_a 8.6066 _cell_length_b 10.1562 _cell_length_c 11.1612 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file bt2107Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4.75 16.85 5.07 o 3 0 0 1879.73 1739.16 22.96 o 4 0 0 10188.84 10133.86 138.12 o 5 0 0 1323.77 1235.19 19.27 o 6 0 0 998.67 986.39 23.29 o 7 0 0 2864.61 2722.79 41.75 o 8 0 0 1567.18 1666.04 36.15 o 9 0 0 99.40 100.18 13.04 o 10 0 0 452.43 466.47 25.65 o -10 1 0 1028.44 1130.56 36.83 o -9 1 0 21.16 19.98 12.12 o -8 1 0 958.67 956.40 42.05 o -7 1 0 2261.51 2265.25 35.02 o -6 1 0 892.90 885.21 22.88 o -5 1 0 745.75 748.46 14.19 o -4 1 0 7904.19 7666.76 90.09 o -3 1 0 21698.65 22482.44 325.98 o -2 1 0 11359.44 11647.46 144.49 o -1 1 0 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