#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:23:16 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181014 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209420.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209420_Fobs loop_ _publ_author_name 'Behrman, David M.' 'Behrman, E. J.' 'Parkin, Sean' _publ_section_title ; 2-Methoxy-3-nitrophenol ; _journal_coeditor_code BT2114 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3119 _journal_page_last o3121 _journal_volume 62 _journal_year 2006 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.9581 _cell_length_b 13.1337 _cell_length_c 4.0110 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high .7697 _cod_data_source_file bt2114Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3-nitroguaiacol - P na2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3056.13 2908.18 71.82 o 4 0 0 6.40 4.41 .88 o 6 0 0 1.36 .88 1.32 o 8 0 0 .35 -1.32 1.32 o 10 0 0 312.11 291.70 11.02 o 12 0 0 127.16 144.09 7.93 o 14 0 0 105.08 105.75 9.25 o 16 0 0 7.72 10.58 6.17 o 18 0 0 24.02 41.42 17.18 o 1 1 0 187.69 175.37 2.64 o 2 1 0 2676.38 2470.19 31.73 o 3 1 0 892.68 835.88 12.78 o 4 1 0 1803.54 1768.26 30.40 o 5 1 0 30.02 29.08 1.32 o 6 1 0 77.02 70.06 1.76 o 7 1 0 187.73 192.12 3.53 o 8 1 0 43.18 41.86 2.20 o 9 1 0 127.15 132.19 3.97 o 10 1 0 39.56 37.45 2.64 o 11 1 0 2.17 2.64 2.20 o 12 1 0 108.10 109.28 4.85 o 13 1 0 620.92 714.71 17.63 o 14 1 0 5.69 9.25 3.53 o 15 1 0 18.00 15.42 4.41 o 16 1 0 18.73 18.95 5.29 o 17 1 0 .85 -3.97 7.05 o 18 1 0 34.93 25.56 9.25 o 0 2 0 2303.07 2111.08 38.78 o 1 2 0 416.88 378.95 6.61 o 2 2 0 496.64 454.73 7.49 o 3 2 0 .31 .88 .44 o 4 2 0 .66 .00 .44 o 5 2 0 361.03 375.86 5.73 o 6 2 0 3312.30 3571.34 54.64 o 7 2 0 756.71 814.29 12.34 o 8 2 0 29.27 31.73 1.76 o 9 2 0 784.18 841.17 16.30 o 10 2 0 18.14 14.10 1.76 o 11 2 0 79.47 72.70 3.53 o 12 2 0 238.93 259.97 7.49 o 13 2 0 566.63 620.85 17.18 o 14 2 0 149.25 155.54 6.61 o 15 2 0 475.85 529.20 17.18 o 16 2 0 79.61 70.06 7.93 o 17 2 0 14.50 14.54 7.05 o 18 2 0 .33 14.98 14.54 o 1 3 0 6.06 4.41 .44 o 2 3 0 1776.95 1658.99 30.40 o 3 3 0 256.47 259.09 4.41 o 4 3 0 2078.81 1972.72 30.40 o 5 3 0 672.06 641.12 8.37 o 6 3 0 481.08 467.51 7.05 o 7 3 0 609.44 668.44 10.58 o 8 3 0 16.63 14.54 1.32 o 9 3 0 50.35 50.67 2.64 o 10 3 0 72.48 80.20 3.08 o 11 3 0 .68 2.20 2.20 o 12 3 0 8.33 2.20 2.64 o 13 3 0 133.80 134.83 6.17 o 14 3 0 2.34 2.20 3.53 o 15 3 0 119.77 137.48 7.93 o 16 3 0 53.52 48.03 7.93 o 17 3 0 4.42 -4.41 6.61 o 0 4 0 2731.59 2438.47 45.83 o 1 4 0 252.08 224.72 3.53 o 2 4 0 .15 .44 .44 o 3 4 0 2675.74 2657.02 41.86 o 4 4 0 17.74 21.15 .88 o 5 4 0 136.59 138.36 3.08 o 6 4 0 758.47 815.17 11.90 o 7 4 0 465.35 471.04 8.37 o 8 4 0 349.33 428.74 9.25 o 9 4 0 322.85 341.05 8.37 o 10 4 0 49.97 49.79 3.08 o 11 4 0 4.11 2.64 2.20 o 12 4 0 25.58 29.08 3.08 o 13 4 0 283.96 285.97 10.13 o 14 4 0 26.74 30.84 3.97 o 15 4 0 111.58 94.30 8.37 o 16 4 0 9.04 13.66 7.93 o 17 4 0 56.13 59.93 10.58 o 1 5 0 8.43 8.37 .88 o 2 5 0 320.11 303.60 5.29 o 3 5 0 281.91 285.53 4.85 o 4 5 0 242.39 267.91 4.85 o 5 5 0 69.18 62.13 2.20 o 6 5 0 2.21 .88 1.32 o 7 5 0 367.39 408.03 8.37 o 8 5 0 2.19 2.20 1.32 o 9 5 0 30.61 32.17 2.64 o 10 5 0 187.40 195.20 6.17 o 11 5 0 61.54 55.08 3.97 o 12 5 0 12.16 11.46 2.64 o 13 5 0 13.28 18.07 3.08 o 14 5 0 4.42 .44 4.85 o 15 5 0 3.61 3.97 5.73 o 16 5 0 37.75 33.49 7.49 o 17 5 0 2.67 6.61 10.13 o 0 6 0 1733.15 1866.53 41.42 o 1 6 0 986.89 1047.39 15.42 o 2 6 0 42.87 54.20 1.76 o 3 6 0 112.51 119.41 2.64 o 4 6 0 3.18 2.64 .88 o 5 6 0 .46 .44 1.32 o 6 6 0 147.60 122.50 3.53 o 7 6 0 320.28 339.29 7.49 o 8 6 0 379.62 404.50 9.25 o 9 6 0 39.99 36.57 3.08 o 10 6 0 23.31 18.95 3.08 o 11 6 0 9.99 6.17 2.64 o 12 6 0 69.27 66.98 4.85 o 13 6 0 .19 -.44 3.97 o 14 6 0 50.22 53.76 7.05 o 15 6 0 .19 1.76 5.73 o 16 6 0 26.44 42.30 11.90 o 1 7 0 434.04 428.74 7.93 o 2 7 0 112.64 119.85 2.64 o 3 7 0 171.38 176.25 3.97 o 4 7 0 165.49 172.29 3.97 o 5 7 0 248.47 251.16 5.29 o 6 7 0 263.16 263.50 5.73 o 7 7 0 160.94 157.75 4.85 o 8 7 0 134.61 134.83 5.29 o 9 7 0 356.03 367.93 12.34 o 10 7 0 4.08 4.85 2.20 o 11 7 0 41.79 39.22 3.53 o 12 7 0 269.85 293.02 12.78 o 13 7 0 4.00 18.07 6.61 o 14 7 0 42.75 38.78 9.25 o 15 7 0 .69 .44 7.49 o 16 7 0 14.49 4.41 9.25 o 0 8 0 1969.80 2057.32 56.40 o 1 8 0 126.39 136.60 3.97 o 2 8 0 70.99 77.11 2.64 o 3 8 0 113.92 118.53 3.53 o 4 8 0 163.63 162.15 4.41 o 5 8 0 3.40 .00 1.32 o 6 8 0 513.27 525.24 11.46 o 7 8 0 715.54 744.23 15.42 o 8 8 0 260.14 260.86 7.93 o 9 8 0 55.52 50.67 3.97 o 10 8 0 195.47 196.96 7.93 o 11 8 0 .08 .44 2.64 o 12 8 0 5.43 7.49 5.29 o 13 8 0 28.90 22.47 5.73 o 14 8 0 20.76 28.20 9.25 o 15 8 0 41.38 32.61 11.46 o 16 8 0 1.51 -13.22 16.74 o 1 9 0 9.55 7.05 1.76 o 2 9 0 260.96 259.53 7.05 o 3 9 0 422.85 445.92 10.58 o 4 9 0 3.53 3.53 1.32 o 5 9 0 143.50 148.93 5.29 o 6 9 0 345.86 360.44 9.25 o 7 9 0 343.98 356.47 8.81 o 8 9 0 416.78 411.11 11.90 o 9 9 0 95.10 96.06 4.85 o 10 9 0 34.88 33.05 3.97 o 11 9 0 6.44 3.97 5.29 o 12 9 0 .73 -2.64 4.41 o 13 9 0 226.05 249.40 14.54 o 14 9 0 1.69 5.73 7.93 o 15 9 0 31.27 32.17 13.66 o 0 10 0 304.72 353.39 13.22 o 1 10 0 2.96 -1.76 2.20 o 2 10 0 76.53 72.26 3.53 o 3 10 0 37.36 32.17 2.64 o 4 10 0 40.20 37.01 3.08 o 5 10 0 193.44 196.96 6.61 o 6 10 0 1195.07 1255.81 31.29 o 7 10 0 64.41 63.45 4.41 o 8 10 0 541.53 554.76 14.10 o 9 10 0 65.19 69.18 5.29 o 10 10 0 36.68 40.98 4.85 o 11 10 0 19.12 27.76 5.73 o 12 10 0 60.95 66.10 7.49 o 13 10 0 .74 3.08 6.61 o 14 10 0 76.92 66.10 11.02 o 1 11 0 25.09 22.91 3.08 o 2 11 0 3.74 1.76 2.20 o 3 11 0 185.82 189.03 7.93 o 4 11 0 204.91 202.25 7.93 o 5 11 0 363.78 369.69 9.69 o 6 11 0 307.75 334.44 9.69 o 7 11 0 521.05 556.52 14.98 o 8 11 0 60.82 68.74 4.41 o 9 11 0 34.75 37.01 4.85 o 10 11 0 11.67 7.93 4.85 o 11 11 0 48.03 55.08 7.49 o 12 11 0 .02 -5.29 5.29 o 13 11 0 .99 9.69 7.93 o 0 12 0 240.20 225.16 12.34 o 1 12 0 .94 -1.32 2.64 o 2 12 0 42.06 40.10 3.97 o 3 12 0 79.45 76.23 6.17 o 4 12 0 115.91 108.40 5.29 o 5 12 0 27.69 25.12 3.53 o 6 12 0 2.56 -3.08 3.53 o 7 12 0 632.07 677.70 21.15 o 8 12 0 7.25 3.08 3.53 o 9 12 0 6.48 8.81 4.41 o 10 12 0 64.46 63.01 7.05 o 11 12 0 .15 -1.32 5.73 o 12 12 0 92.53 101.79 14.54 o 1 13 0 351.15 334.44 12.78 o 2 13 0 72.26 61.69 4.85 o 3 13 0 33.44 29.96 4.85 o 4 13 0 .38 1.32 3.53 o 5 13 0 1.36 1.32 3.97 o 6 13 0 58.64 56.40 6.17 o 7 13 0 .02 3.08 3.97 o 8 13 0 116.25 122.50 8.37 o 9 13 0 14.27 14.10 5.29 o 10 13 0 2.34 4.85 5.29 o 11 13 0 2.38 11.02 7.49 o 0 14 0 97.39 79.31 12.78 o 1 14 0 203.82 211.50 14.54 o 2 14 0 106.84 95.62 7.49 o 3 14 0 .91 .00 5.29 o 4 14 0 17.37 14.54 4.85 o 5 14 0 18.57 22.91 6.61 o 6 14 0 19.20 26.44 5.73 o 7 14 0 14.52 9.25 5.29 o 8 14 0 .29 8.81 5.73 o 9 14 0 10.55 9.69 6.61 o 10 14 0 16.01 2.64 5.73 o 1 15 0 5.84 9.25 6.61 o 2 15 0 2.56 -.44 7.05 o 3 15 0 .05 7.49 8.37 o 4 15 0 .80 -7.49 7.49 o 5 15 0 82.94 72.26 10.13 o 6 15 0 1.95 -1.76 6.17 o 7 15 0 37.14 34.81 9.69 o 8 15 0 8.01 8.81 7.05 o 0 16 0 14.96 24.68 14.10 o 1 16 0 30.08 23.35 10.13 o 2 16 0 8.74 11.90 8.37 o 3 16 0 3.31 3.08 7.93 o 4 16 0 34.25 33.05 8.37 o 5 16 0 5.30 -1.32 7.05 o 6 16 0 22.73 14.54 11.46 o 1 17 0 34.64 22.03 15.42 o 2 0 1 13697.09 11803.70 268.35 o 4 0 1 303.25 259.53 4.85 o 6 0 1 61.44 54.20 1.76 o 8 0 1 366.00 371.45 7.49 o 10 0 1 784.51 831.04 18.07 o 12 0 1 637.48 670.20 17.63 o 14 0 1 7.61 4.41 3.08 o 16 0 1 30.41 8.81 7.05 o 0 1 1 6498.76 5715.46 129.11 o 1 1 1 383.12 344.46 5.13 o 2 1 1 4512.26 4176.42 87.03 o 3 1 1 1065.19 1019.71 17.41 o 4 1 1 585.40 573.42 6.77 o 5 1 1 454.50 449.48 5.45 o 6 1 1 20.11 16.09 .62 o 7 1 1 254.36 228.91 3.12 o 8 1 1 358.62 375.56 5.45 o 9 1 1 447.03 465.77 6.77 o 10 1 1 131.00 127.05 2.63 o 11 1 1 495.95 520.51 9.09 o 12 1 1 115.50 123.66 3.57 o 13 1 1 46.74 46.07 4.63 o 14 1 1 50.72 49.06 3.53 o 15 1 1 43.14 42.76 4.20 o 16 1 1 1.00 7.15 4.82 o 17 1 1 76.24 72.18 7.27 o 1 2 1 861.40 789.36 10.58 o 2 2 1 779.87 736.54 17.63 o 3 2 1 1312.42 1207.58 17.18 o 4 2 1 2549.19 2561.11 27.51 o 5 2 1 422.15 448.82 5.30 o 6 2 1 444.42 452.70 5.45 o 7 2 1 90.66 84.11 2.86 o 8 2 1 320.74 325.18 4.82 o 9 2 1 137.00 138.62 2.63 o 10 2 1 27.46 25.78 1.56 o 11 2 1 11.15 8.29 1.54 o 12 2 1 96.14 92.77 3.97 o 13 2 1 407.16 418.41 8.40 o 14 2 1 6.11 5.45 2.95 o 15 2 1 221.92 238.23 10.80 o 16 2 1 .19 -1.32 4.36 o 17 2 1 29.31 30.36 6.00 o 0 3 1 2796.91 2634.99 49.79 o 1 3 1 187.73 176.96 2.86 o 2 3 1 146.84 140.13 2.18 o 3 3 1 1722.07 1647.80 17.69 o 4 3 1 1478.02 1541.86 31.06 o 5 3 1 583.89 600.29 9.25 o 6 3 1 707.68 768.77 9.41 o 7 3 1 7.43 6.17 .73 o 8 3 1 63.31 63.46 1.56 o 9 3 1 37.54 38.50 2.20 o 10 3 1 12.72 12.78 1.38 o 11 3 1 261.53 256.21 5.90 o 12 3 1 56.98 60.76 2.95 o 13 3 1 81.13 71.19 4.63 o 14 3 1 66.70 67.74 4.33 o 15 3 1 79.32 83.14 11.68 o 16 3 1 24.13 27.32 6.61 o 17 3 1 93.99 84.89 8.39 o 1 4 1 352.84 357.00 17.18 o 2 4 1 281.90 249.00 3.43 o 3 4 1 72.15 72.27 1.25 o 4 4 1 488.09 507.98 6.14 o 5 4 1 442.95 440.22 5.61 o 6 4 1 147.17 179.78 2.95 o 7 4 1 358.53 374.12 6.21 o 8 4 1 8.83 7.72 1.13 o 9 4 1 195.49 209.53 5.73 o 10 4 1 30.32 27.31 1.47 o 11 4 1 23.67 19.54 1.79 o 12 4 1 5.89 7.87 2.12 o 13 4 1 56.76 58.55 4.20 o 14 4 1 54.54 55.76 5.29 o 15 4 1 117.16 124.25 9.47 o 16 4 1 49.94 45.49 6.19 o 17 4 1 40.81 31.18 7.65 o 0 5 1 55.13 59.93 1.76 o 1 5 1 364.67 366.43 4.67 o 2 5 1 356.70 353.01 4.85 o 3 5 1 453.80 455.97 7.71 o 4 5 1 344.47 373.17 8.15 o 5 5 1 133.35 138.81 2.49 o 6 5 1 288.76 313.08 8.15 o 7 5 1 36.64 40.49 3.97 o 8 5 1 119.86 126.81 3.17 o 9 5 1 144.76 149.34 3.81 o 10 5 1 40.48 36.48 3.53 o 11 5 1 19.74 16.77 2.12 o 12 5 1 154.37 157.63 5.73 o 13 5 1 8.14 1.62 2.75 o 14 5 1 50.16 50.36 4.51 o 15 5 1 25.52 20.83 4.20 o 16 5 1 1.05 1.96 6.61 o 1 6 1 757.62 806.21 9.16 o 2 6 1 423.72 435.16 5.45 o 3 6 1 330.19 339.99 5.29 o 4 6 1 330.99 326.71 7.05 o 5 6 1 58.66 60.57 3.53 o 6 6 1 18.92 15.88 1.25 o 7 6 1 76.88 75.79 2.32 o 8 6 1 3.41 2.20 1.32 o 9 6 1 307.15 330.22 7.32 o 10 6 1 102.48 104.10 10.13 o 11 6 1 44.60 42.00 3.07 o 12 6 1 160.64 148.77 9.69 o 13 6 1 25.53 23.61 3.89 o 14 6 1 3.79 .22 3.43 o 15 6 1 1.39 .87 4.45 o 16 6 1 45.55 38.33 6.52 o 0 7 1 690.43 678.14 14.10 o 1 7 1 84.02 82.18 1.87 o 2 7 1 506.81 571.55 7.91 o 3 7 1 2.87 1.70 1.10 o 4 7 1 35.76 33.69 1.38 o 5 7 1 119.17 133.22 4.41 o 6 7 1 12.50 12.18 1.06 o 7 7 1 74.72 73.02 2.53 o 8 7 1 244.19 249.09 5.39 o 9 7 1 348.98 366.44 8.80 o 10 7 1 62.36 54.28 3.07 o 11 7 1 172.15 168.41 5.45 o 12 7 1 30.37 22.14 3.81 o 13 7 1 .66 1.28 3.57 o 14 7 1 1.30 .31 5.95 o 15 7 1 10.79 11.93 7.27 o 16 7 1 17.85 22.07 7.94 o 1 8 1 32.08 33.05 1.25 o 2 8 1 104.03 97.34 2.43 o 3 8 1 368.28 390.27 6.93 o 4 8 1 34.45 28.64 1.69 o 5 8 1 270.53 281.35 7.05 o 6 8 1 243.51 248.31 4.82 o 7 8 1 48.20 45.99 2.64 o 8 8 1 283.94 302.32 7.72 o 9 8 1 152.73 157.45 5.08 o 10 8 1 187.32 198.29 6.45 o 11 8 1 2.33 -2.85 2.85 o 12 8 1 140.72 135.08 7.15 o 13 8 1 7.59 8.81 4.05 o 14 8 1 41.29 36.42 6.65 o 15 8 1 28.70 23.01 6.67 o 0 9 1 150.48 147.61 4.41 o 1 9 1 295.27 312.25 5.45 o 2 9 1 6.86 5.63 1.38 o 3 9 1 174.62 177.47 3.91 o 4 9 1 903.34 964.45 14.98 o 5 9 1 272.85 263.02 5.87 o 6 9 1 259.31 271.14 16.96 o 7 9 1 134.30 122.64 4.63 o 8 9 1 124.09 135.11 4.55 o 9 9 1 64.01 60.43 3.49 o 10 9 1 59.43 66.91 4.13 o 11 9 1 147.90 143.64 11.46 o 12 9 1 5.15 9.24 5.95 o 13 9 1 1.75 -3.23 4.64 o 14 9 1 7.59 7.05 5.30 o 15 9 1 23.27 -9.13 9.70 o 1 10 1 151.02 143.70 3.74 o 2 10 1 254.54 244.82 5.39 o 3 10 1 90.67 84.38 2.95 o 4 10 1 447.80 467.97 9.52 o 5 10 1 191.54 197.78 5.29 o 6 10 1 577.08 603.76 22.47 o 7 10 1 72.18 75.00 3.74 o 8 10 1 178.18 190.23 14.32 o 9 10 1 196.32 214.26 6.76 o 10 10 1 39.56 35.38 3.75 o 11 10 1 8.17 7.41 5.29 o 12 10 1 2.90 3.82 5.07 o 13 10 1 23.27 19.53 6.07 o 14 10 1 5.74 .51 5.71 o 0 11 1 31.84 28.20 2.20 o 1 11 1 34.60 32.88 2.20 o 2 11 1 29.97 29.01 2.53 o 3 11 1 33.52 30.12 2.63 o 4 11 1 214.78 214.64 9.69 o 5 11 1 521.84 541.22 11.21 o 6 11 1 142.92 138.85 10.80 o 7 11 1 278.23 311.50 10.35 o 8 11 1 32.69 31.59 3.81 o 9 11 1 43.35 41.28 7.71 o 10 11 1 6.47 6.61 3.74 o 11 11 1 70.31 64.83 5.76 o 12 11 1 18.20 22.72 5.82 o 13 11 1 4.25 -.64 6.85 o 1 12 1 50.97 41.74 3.26 o 2 12 1 119.57 102.33 6.83 o 3 12 1 89.36 89.87 4.23 o 4 12 1 55.02 46.20 3.97 o 5 12 1 .49 -2.43 2.43 o 6 12 1 56.46 60.93 3.70 o 7 12 1 27.83 25.31 3.43 o 8 12 1 22.81 18.97 4.85 o 9 12 1 220.55 253.52 9.50 o 10 12 1 80.04 86.44 7.77 o 11 12 1 30.92 33.63 6.65 o 12 12 1 72.67 80.73 11.68 o 0 13 1 110.45 109.72 7.49 o 1 13 1 197.44 191.36 9.69 o 2 13 1 97.77 92.25 5.29 o 3 13 1 15.50 12.30 3.26 o 4 13 1 137.26 138.60 5.92 o 5 13 1 3.92 -1.99 3.26 o 6 13 1 20.59 24.93 4.20 o 7 13 1 26.60 21.88 3.89 o 8 13 1 19.34 18.06 4.33 o 9 13 1 79.20 73.84 7.40 o 10 13 1 151.00 164.58 10.27 o 11 13 1 22.22 8.04 6.45 o 1 14 1 9.58 4.97 3.53 o 2 14 1 27.80 29.98 3.70 o 3 14 1 225.98 239.78 11.24 o 4 14 1 11.33 8.79 3.70 o 5 14 1 22.29 15.07 4.51 o 6 14 1 49.63 44.97 5.45 o 7 14 1 11.90 4.31 5.20 o 8 14 1 6.69 3.80 4.55 o 9 14 1 23.64 21.59 7.01 o 0 15 1 2.98 -2.20 5.29 o 1 15 1 11.56 9.56 4.51 o 2 15 1 8.18 7.77 4.55 o 3 15 1 28.24 20.52 4.76 o 4 15 1 22.69 21.04 4.76 o 5 15 1 8.03 5.99 4.20 o 6 15 1 11.87 6.45 5.54 o 7 15 1 5.46 -.44 5.08 o 1 16 1 43.32 36.68 6.83 o 2 16 1 18.83 23.98 6.69 o 3 16 1 11.08 9.62 5.45 o 4 16 1 16.70 3.35 5.61 o 5 16 1 8.06 8.89 20.49 o 0 0 2 2089.49 2007.97 51.55 o 2 0 2 1419.06 1511.82 30.84 o 4 0 2 812.56 804.60 21.59 o 6 0 2 51.83 53.76 2.20 o 8 0 2 891.44 955.29 37.89 o 10 0 2 213.13 244.55 12.78 o 12 0 2 65.75 69.62 7.49 o 14 0 2 49.99 55.08 8.81 o 16 0 2 14.66 12.34 8.37 o 1 1 2 719.68 727.31 12.28 o 2 1 2 89.93 81.65 3.53 o 3 1 2 268.21 261.47 4.51 o 4 1 2 781.73 819.27 16.52 o 5 1 2 700.26 751.26 12.39 o 6 1 2 104.43 106.31 3.53 o 7 1 2 136.01 138.16 3.43 o 8 1 2 268.64 287.44 7.40 o 9 1 2 140.89 154.81 4.64 o 10 1 2 1047.39 1142.75 29.74 o 11 1 2 62.74 59.51 4.45 o 12 1 2 69.03 71.93 12.78 o 13 1 2 56.50 62.18 5.90 o 14 1 2 33.15 34.38 9.03 o 15 1 2 52.79 57.65 10.13 o 16 1 2 79.44 77.44 7.15 o 0 2 2 188.78 186.39 6.17 o 1 2 2 161.76 142.02 4.41 o 2 2 2 14.18 12.34 1.53 o 3 2 2 831.63 829.66 12.39 o 4 2 2 134.48 128.58 2.75 o 5 2 2 569.70 588.40 9.33 o 6 2 2 380.44 390.84 6.54 o 7 2 2 111.89 113.52 2.95 o 8 2 2 41.46 37.71 2.01 o 9 2 2 67.23 69.09 3.07 o 10 2 2 30.96 25.64 3.70 o 11 2 2 264.13 304.63 10.27 o 12 2 2 40.39 40.62 4.96 o 13 2 2 14.85 14.87 5.73 o 14 2 2 44.15 50.41 6.65 o 15 2 2 26.82 32.57 5.82 o 16 2 2 9.05 9.95 6.76 o 1 3 2 162.81 150.54 3.57 o 2 3 2 1258.17 1318.22 18.62 o 3 3 2 335.34 370.38 6.38 o 4 3 2 903.47 987.10 13.24 o 5 3 2 750.33 785.57 13.44 o 6 3 2 19.39 18.18 1.18 o 7 3 2 39.29 38.40 2.32 o 8 3 2 137.10 139.12 4.45 o 9 3 2 3.03 1.51 2.12 o 10 3 2 28.24 28.15 6.61 o 11 3 2 3.81 -.25 2.49 o 12 3 2 6.69 4.87 3.53 o 13 3 2 54.44 40.77 5.51 o 14 3 2 17.56 10.76 4.23 o 15 3 2 17.36 17.60 5.73 o 16 3 2 22.86 15.82 6.52 o 0 4 2 93.72 94.30 3.53 o 1 4 2 25.99 23.87 1.32 o 2 4 2 431.43 468.86 7.15 o 3 4 2 532.57 569.47 9.02 o 4 4 2 111.84 130.15 3.26 o 5 4 2 774.14 830.59 20.49 o 6 4 2 9.72 7.21 1.69 o 7 4 2 54.68 57.96 2.80 o 8 4 2 140.88 142.67 4.82 o 9 4 2 25.14 23.67 2.63 o 10 4 2 11.44 10.08 2.18 o 11 4 2 29.61 27.15 3.99 o 12 4 2 24.25 13.87 8.15 o 13 4 2 17.68 22.07 4.55 o 14 4 2 7.79 3.85 4.64 o 15 4 2 23.52 16.58 6.77 o 16 4 2 20.32 20.40 5.93 o 1 5 2 93.89 88.12 2.64 o 2 5 2 36.66 38.62 1.56 o 3 5 2 4.64 3.02 1.10 o 4 5 2 42.75 42.53 3.08 o 5 5 2 127.97 125.64 3.57 o 6 5 2 140.72 148.93 3.81 o 7 5 2 10.44 9.20 1.87 o 8 5 2 130.23 130.41 4.87 o 9 5 2 34.73 31.66 2.95 o 10 5 2 50.37 36.24 8.81 o 11 5 2 129.04 121.67 5.94 o 12 5 2 40.29 43.53 5.29 o 13 5 2 5.98 9.38 4.23 o 14 5 2 44.08 42.54 6.02 o 15 5 2 1.86 6.17 5.73 o 0 6 2 340.79 351.63 7.93 o 1 6 2 190.15 194.98 3.74 o 2 6 2 53.12 54.50 1.79 o 3 6 2 69.67 74.76 3.97 o 4 6 2 22.79 20.71 1.38 o 5 6 2 127.11 133.71 4.33 o 6 6 2 99.72 97.77 3.26 o 7 6 2 182.23 166.49 4.96 o 8 6 2 21.02 13.70 3.53 o 9 6 2 41.07 36.26 3.17 o 10 6 2 152.40 136.88 6.02 o 11 6 2 111.80 115.35 5.45 o 12 6 2 117.96 125.28 7.94 o 13 6 2 52.05 60.04 6.76 o 14 6 2 24.70 20.64 6.07 o 15 6 2 10.90 8.10 7.32 o 1 7 2 138.22 139.90 4.05 o 2 7 2 14.94 12.31 1.56 o 3 7 2 182.98 185.00 5.29 o 4 7 2 214.02 221.20 5.45 o 5 7 2 6.15 3.41 1.79 o 6 7 2 1.59 1.76 1.25 o 7 7 2 12.36 9.25 2.20 o 8 7 2 63.97 50.80 3.17 o 9 7 2 38.96 31.54 4.01 o 10 7 2 266.42 262.98 11.24 o 11 7 2 240.58 274.57 9.72 o 12 7 2 3.42 2.75 3.89 o 13 7 2 150.97 158.68 9.66 o 14 7 2 72.43 61.98 8.08 o 0 8 2 309.55 326.51 16.74 o 1 8 2 241.69 258.31 6.14 o 2 8 2 512.81 550.64 9.96 o 3 8 2 183.41 199.00 4.82 o 4 8 2 29.80 26.83 1.97 o 5 8 2 163.83 176.55 11.68 o 6 8 2 69.72 77.35 3.70 o 7 8 2 11.02 14.48 2.32 o 8 8 2 12.05 12.34 3.43 o 9 8 2 35.14 34.92 4.76 o 10 8 2 20.59 17.50 4.01 o 11 8 2 65.63 58.25 7.49 o 12 8 2 8.45 9.86 9.69 o 13 8 2 30.91 18.86 5.79 o 14 8 2 12.49 24.76 7.27 o 1 9 2 406.51 444.29 9.78 o 2 9 2 555.09 593.11 29.08 o 3 9 2 43.96 38.47 3.08 o 4 9 2 113.71 112.88 10.35 o 5 9 2 47.14 42.81 3.12 o 6 9 2 64.60 65.00 3.39 o 7 9 2 1.43 -.22 2.43 o 8 9 2 57.90 66.11 4.64 o 9 9 2 20.42 25.63 7.27 o 10 9 2 64.30 61.90 6.61 o 11 9 2 4.38 2.45 4.33 o 12 9 2 27.41 22.56 5.58 o 13 9 2 22.46 21.62 7.26 o 0 10 2 190.13 192.56 8.37 o 1 10 2 40.28 35.67 3.17 o 2 10 2 87.52 89.68 7.05 o 3 10 2 345.41 368.84 35.91 o 4 10 2 418.71 450.26 35.03 o 5 10 2 99.06 97.91 4.45 o 6 10 2 37.35 38.80 3.75 o 7 10 2 104.89 103.91 5.82 o 8 10 2 2.62 6.95 4.19 o 9 10 2 8.14 6.75 3.89 o 10 10 2 31.65 29.92 5.58 o 11 10 2 17.47 4.97 5.13 o 12 10 2 5.93 3.48 6.17 o 1 11 2 19.07 19.97 4.41 o 2 11 2 255.04 267.62 20.27 o 3 11 2 311.16 341.24 24.90 o 4 11 2 216.88 238.37 8.46 o 5 11 2 31.99 30.33 3.91 o 6 11 2 22.40 19.43 3.91 o 7 11 2 121.28 120.95 6.85 o 8 11 2 13.15 9.55 3.70 o 9 11 2 70.65 64.19 6.02 o 10 11 2 12.86 5.22 5.60 o 11 11 2 6.40 6.82 6.21 o 0 12 2 82.39 69.18 5.73 o 1 12 2 36.53 43.83 3.89 o 2 12 2 13.37 10.91 4.63 o 3 12 2 37.09 37.95 4.23 o 4 12 2 25.04 19.42 4.20 o 5 12 2 26.31 25.69 4.41 o 6 12 2 77.16 70.63 6.21 o 7 12 2 6.35 6.30 5.27 o 8 12 2 16.73 18.73 5.92 o 9 12 2 172.95 217.03 11.42 o 10 12 2 45.38 38.64 8.22 o 1 13 2 2.63 2.64 3.12 o 2 13 2 48.34 46.88 5.13 o 3 13 2 99.64 94.01 9.69 o 4 13 2 5.40 6.83 4.67 o 5 13 2 15.65 10.44 4.45 o 6 13 2 12.31 14.87 5.45 o 7 13 2 16.16 15.59 5.45 o 8 13 2 115.76 127.73 9.29 o 9 13 2 4.90 18.09 8.81 o 0 14 2 13.27 11.90 4.85 o 1 14 2 34.28 26.84 4.64 o 2 14 2 8.54 9.49 5.13 o 3 14 2 22.49 22.20 6.83 o 4 14 2 52.55 55.30 11.02 o 5 14 2 46.30 41.98 6.88 o 6 14 2 .49 -4.41 5.61 o 7 14 2 12.92 10.27 6.21 o 1 15 2 33.84 38.10 6.07 o 2 15 2 5.77 1.54 6.61 o 3 15 2 93.09 105.33 8.66 o 4 15 2 12.75 4.96 11.02 o 5 15 2 19.45 19.39 8.72 o 2 0 3 315.17 307.56 10.13 o 4 0 3 7.72 8.37 2.64 o 6 0 3 455.12 510.69 14.54 o 8 0 3 486.39 516.86 19.39 o 10 0 3 61.84 56.84 7.93 o 12 0 3 76.66 67.86 9.69 o 14 0 3 68.37 61.25 11.90 o 0 1 3 44.02 40.98 3.53 o 1 1 3 122.33 109.51 3.70 o 2 1 3 329.41 361.65 7.59 o 3 1 3 35.49 28.74 2.32 o 4 1 3 41.71 37.97 4.41 o 5 1 3 163.34 172.57 5.13 o 6 1 3 305.05 327.39 8.97 o 7 1 3 76.75 87.39 5.45 o 8 1 3 560.16 645.94 15.23 o 9 1 3 13.47 12.74 9.69 o 10 1 3 .37 -3.31 3.57 o 11 1 3 48.84 51.49 5.82 o 12 1 3 64.96 62.30 6.61 o 13 1 3 .14 -3.08 5.38 o 14 1 3 71.14 61.05 8.03 o 1 2 3 331.52 359.69 6.96 o 2 2 3 72.37 66.62 3.89 o 3 2 3 41.70 32.90 3.26 o 4 2 3 19.59 18.01 1.87 o 5 2 3 176.51 181.13 5.45 o 6 2 3 1.77 2.64 2.12 o 7 2 3 578.00 651.96 17.13 o 8 2 3 113.73 122.28 6.83 o 9 2 3 55.38 53.38 7.05 o 10 2 3 .74 -1.11 4.82 o 11 2 3 19.81 22.39 5.71 o 12 2 3 3.95 -.66 5.38 o 13 2 3 10.21 8.18 8.59 o 14 2 3 .09 2.50 5.82 o 0 3 3 155.02 175.37 7.05 o 1 3 3 99.80 91.89 3.70 o 2 3 3 106.41 105.15 3.49 o 3 3 3 74.59 69.93 6.17 o 4 3 3 174.49 178.87 5.76 o 5 3 3 377.55 401.22 9.78 o 6 3 3 70.04 68.93 4.14 o 7 3 3 90.88 85.89 10.80 o 8 3 3 11.50 7.38 4.55 o 9 3 3 74.21 73.34 8.81 o 10 3 3 21.14 24.07 5.08 o 11 3 3 2.75 3.04 4.96 o 12 3 3 97.47 99.91 10.58 o 13 3 3 .62 1.54 6.54 o 14 3 3 70.18 90.93 11.03 o 1 4 3 204.50 204.46 5.92 o 2 4 3 8.64 9.09 2.20 o 3 4 3 79.31 84.67 4.41 o 4 4 3 14.54 12.75 2.18 o 5 4 3 75.96 82.51 3.91 o 6 4 3 106.23 104.03 10.80 o 7 4 3 257.26 274.88 9.19 o 8 4 3 48.43 51.56 4.20 o 9 4 3 130.11 128.49 9.69 o 10 4 3 13.04 11.28 5.27 o 11 4 3 5.26 .97 4.47 o 12 4 3 16.27 16.58 6.83 o 13 4 3 56.74 45.00 9.02 o 14 4 3 86.37 96.69 18.95 o 0 5 3 171.44 174.93 7.05 o 1 5 3 6.31 6.03 2.01 o 2 5 3 47.44 43.70 6.39 o 3 5 3 11.44 6.17 2.49 o 4 5 3 123.55 128.51 4.99 o 5 5 3 85.48 84.78 7.05 o 6 5 3 54.93 52.55 11.02 o 7 5 3 1.78 -.44 2.80 o 8 5 3 28.75 22.71 3.74 o 9 5 3 74.51 75.13 7.79 o 10 5 3 43.93 51.34 16.74 o 11 5 3 20.98 34.43 8.03 o 12 5 3 18.81 22.94 7.32 o 13 5 3 34.66 26.55 8.72 o 1 6 3 324.54 349.28 8.68 o 2 6 3 33.65 31.07 3.17 o 3 6 3 15.82 17.79 2.32 o 4 6 3 58.00 52.23 3.97 o 5 6 3 43.58 36.78 4.53 o 6 6 3 2.03 -.66 4.41 o 7 6 3 2.35 1.52 3.70 o 8 6 3 45.62 34.46 4.53 o 9 6 3 4.21 6.42 5.76 o 10 6 3 4.62 .66 5.30 o 11 6 3 63.71 63.77 8.56 o 12 6 3 10.72 9.02 8.53 o 13 6 3 81.33 82.74 22.25 o 0 7 3 266.14 305.36 10.58 o 1 7 3 181.32 203.35 6.54 o 2 7 3 267.87 306.14 8.89 o 3 7 3 62.02 63.08 4.55 o 4 7 3 13.92 12.38 3.57 o 5 7 3 54.73 57.23 4.76 o 6 7 3 65.44 50.36 5.51 o 7 7 3 45.68 48.83 6.02 o 8 7 3 114.67 105.98 7.09 o 9 7 3 28.96 22.12 6.25 o 10 7 3 6.71 7.82 6.39 o 11 7 3 9.84 -7.71 7.71 o 12 7 3 .18 -8.72 8.72 o 1 8 3 382.62 434.50 18.95 o 2 8 3 .84 2.55 3.49 o 3 8 3 27.16 19.22 3.81 o 4 8 3 27.09 23.35 4.64 o 5 8 3 23.80 26.57 5.27 o 6 8 3 21.10 11.72 5.39 o 7 8 3 92.98 109.20 20.71 o 8 8 3 5.47 3.54 4.55 o 9 8 3 8.69 6.48 4.64 o 10 8 3 38.60 27.77 6.85 o 11 8 3 14.27 8.09 8.40 o 12 8 3 24.61 8.81 8.61 o 0 9 3 471.83 569.30 18.95 o 1 9 3 18.47 11.37 7.93 o 2 9 3 135.81 143.44 11.90 o 3 9 3 15.13 8.92 3.81 o 4 9 3 68.44 68.49 8.37 o 5 9 3 41.99 39.58 9.03 o 6 9 3 16.74 11.84 4.96 o 7 9 3 41.82 42.75 6.54 o 8 9 3 76.25 71.16 9.03 o 9 9 3 16.69 .77 4.93 o 10 9 3 19.79 19.68 7.52 o 11 9 3 33.40 36.21 13.88 o 1 10 3 96.24 101.99 6.02 o 2 10 3 148.03 153.78 8.57 o 3 10 3 48.23 45.88 5.61 o 4 10 3 21.14 29.78 7.93 o 5 10 3 33.78 33.52 5.76 o 6 10 3 46.32 40.29 5.58 o 7 10 3 3.81 5.83 5.05 o 8 10 3 75.66 78.23 12.34 o 9 10 3 26.24 26.41 7.30 o 10 10 3 4.46 4.38 9.00 o 0 11 3 208.38 239.70 14.10 o 1 11 3 96.91 116.98 14.76 o 2 11 3 102.87 119.85 7.62 o 3 11 3 7.94 .64 5.73 o 4 11 3 22.42 20.44 6.02 o 5 11 3 129.68 164.94 9.96 o 6 11 3 33.17 32.13 6.45 o 7 11 3 9.87 -1.55 5.58 o 8 11 3 20.09 22.15 7.01 o 9 11 3 9.14 9.57 7.66 o 1 12 3 300.78 368.28 16.61 o 2 12 3 13.69 17.88 6.21 o 3 12 3 15.60 24.26 6.96 o 4 12 3 31.15 29.34 11.24 o 5 12 3 9.81 14.45 7.40 o 6 12 3 7.86 7.59 6.34 o 7 12 3 9.79 7.44 6.34 o 0 13 3 24.88 27.76 12.78 o 1 13 3 27.35 14.75 9.25 o 2 13 3 47.96 39.50 9.04 o 3 13 3 13.14 26.30 13.00 o 4 13 3 14.38 13.94 8.15 o 5 13 3 6.51 12.94 6.45 o 0 0 4 275.78 298.31 16.30 o 2 0 4 104.95 115.89 6.61 o 4 0 4 13.90 11.90 5.73 o 6 0 4 167.29 187.27 10.13 o 8 0 4 10.63 13.66 10.13 o 10 0 4 49.28 48.91 9.25 o 1 1 4 49.50 44.64 4.41 o 2 1 4 81.30 84.28 4.51 o 3 1 4 170.04 181.53 6.52 o 4 1 4 207.10 232.61 8.89 o 5 1 4 17.13 7.78 4.82 o 6 1 4 85.04 73.91 6.34 o 7 1 4 33.00 32.26 6.52 o 8 1 4 21.87 5.73 5.61 o 9 1 4 47.03 38.28 6.65 o 10 1 4 23.28 13.32 6.52 o 11 1 4 29.86 22.62 7.32 o 0 2 4 18.19 14.54 4.41 o 1 2 4 100.92 106.58 4.82 o 2 2 4 4.50 3.08 2.63 o 3 2 4 1.56 -.17 5.73 o 4 2 4 50.12 48.66 4.82 o 5 2 4 160.43 158.47 8.40 o 6 2 4 75.75 64.31 5.93 o 7 2 4 8.60 15.25 4.64 o 8 2 4 4.29 -.56 5.19 o 9 2 4 63.99 58.12 6.65 o 10 2 4 33.15 35.45 7.28 o 11 2 4 5.69 5.88 6.88 o 1 3 4 6.63 .19 3.26 o 2 3 4 26.72 26.06 3.12 o 3 3 4 118.90 120.01 6.23 o 4 3 4 15.28 13.27 3.89 o 5 3 4 85.24 74.87 6.35 o 6 3 4 75.82 78.45 6.11 o 7 3 4 189.07 209.92 11.24 o 8 3 4 25.57 23.08 6.38 o 9 3 4 56.43 48.51 8.71 o 10 3 4 55.46 30.60 9.60 o 11 3 4 35.87 17.52 8.96 o 0 4 4 27.41 31.29 4.85 o 1 4 4 2.90 4.19 3.12 o 2 4 4 .30 2.34 3.08 o 3 4 4 1.66 3.49 3.39 o 4 4 4 3.49 .67 4.51 o 5 4 4 53.50 56.05 8.22 o 6 4 4 8.11 3.53 4.99 o 7 4 4 88.11 88.53 10.58 o 8 4 4 57.11 43.10 9.41 o 9 4 4 137.56 125.98 11.85 o 10 4 4 20.05 5.97 9.91 o 1 5 4 44.02 33.58 6.17 o 2 5 4 60.13 52.78 7.71 o 3 5 4 31.57 26.19 4.96 o 4 5 4 98.13 105.98 7.01 o 5 5 4 11.54 2.10 12.56 o 6 5 4 5.45 10.57 7.46 o 7 5 4 30.50 15.73 7.59 o 8 5 4 47.00 33.02 8.84 o 9 5 4 14.96 3.70 8.31 o 10 5 4 63.21 53.05 10.58 o 0 6 4 70.07 69.18 8.37 o 1 6 4 133.86 136.40 6.83 o 2 6 4 19.94 20.11 5.13 o 3 6 4 167.90 199.94 8.84 o 4 6 4 49.61 56.26 6.21 o 5 6 4 31.94 25.00 7.20 o 6 6 4 15.82 7.52 7.52 o 7 6 4 1.73 -.44 10.58 o 8 6 4 10.16 -2.31 7.71 o 9 6 4 3.92 15.51 9.95 o 1 7 4 62.53 56.30 6.40 o 2 7 4 40.78 38.40 5.93 o 3 7 4 195.45 243.81 10.72 o 4 7 4 85.78 81.02 11.46 o 5 7 4 39.40 58.19 8.59 o 6 7 4 7.46 6.23 7.60 o 7 7 4 31.32 27.71 8.84 o 8 7 4 11.89 11.59 9.47 o 0 8 4 177.11 186.83 15.42 o 1 8 4 69.87 65.79 6.77 o 2 8 4 25.17 17.76 5.90 o 3 8 4 42.18 29.48 7.32 o 4 8 4 23.86 35.71 8.37 o 5 8 4 39.06 30.46 8.81 o 6 8 4 2.46 -7.41 7.41 o 7 8 4 2.85 -7.94 7.94 o 1 9 4 1.24 -1.78 9.25 o 2 9 4 40.14 29.02 7.32 o 3 9 4 27.37 27.13 14.10 o 4 9 4 .37 -3.24 5.82 o 5 9 4 20.05 12.88 6.65 o 6 9 4 9.21 7.61 8.23 o 0 10 4 44.19 43.62 14.54 o 1 10 4 18.79 23.62 8.23 o 2 10 4 1.32 3.15 6.65 o 3 10 4 36.81 39.84 7.71 o 4 10 4 .19 2.61 7.49 o 2 0 5 46.90 35.25 10.58 o 4 0 5 96.60 107.07 11.90 o 0 1 5 5.73 .00 9.69 o 1 1 5 67.97 58.78 12.12 o 2 1 5 1.30 3.73 7.05 o 3 1 5 36.17 17.85 7.49 o 4 1 5 12.62 17.20 10.35 o 5 1 5 8.34 5.25 17.04 o 1 2 5 35.66 24.02 7.77 o 2 2 5 30.93 31.66 12.12 o 3 2 5 104.68 93.88 9.04 o 4 2 5 57.70 43.73 7.28 o 0 3 5 14.78 8.81 10.13 o 1 3 5 62.75 69.95 9.18 o 2 3 5 45.23 35.33 12.44 o 3 3 5 97.38 95.08 9.97 o 1 4 5 47.33 45.78 11.46 o 2 4 5 9.51 9.78 22.69 o