#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209430.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209430_Fobs loop_ _publ_author_name 'Boyd, Peter D. W.' 'Hosseini, Ali' _publ_section_title ; [4-(Ferrocene-1-carboxamido)pyridine](tetraphenylporphyrinato)zinc(II) toluene sesquisolvate ; _journal_coeditor_code BV2018 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1542 _journal_page_last m1544 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.020 _cell_angle_beta 89.865 _cell_angle_gamma 73.035 _cell_length_a 11.0337 _cell_length_b 11.2671 _cell_length_c 22.8406 _exptl_crystal_F_000 1164.77 _reflns_d_resolution_high 0.7936 _[local]_cod_data_source_file bv2018Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' amh998 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 376.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3297.92 3217.78 230.06 o 2 0 0 13292.75 15890.80 673.57 o 3 0 0 259.65 283.35 43.51 o 4 0 0 4706.28 5769.28 203.63 o 5 0 0 2633.77 3639.66 133.94 o 6 0 0 362.57 388.77 32.39 o 7 0 0 3206.06 3788.66 145.04 o 8 0 0 155.58 179.24 61.39 o 9 0 0 3627.10 4334.32 304.16 o 10 0 0 137.09 206.47 68.65 o 11 0 0 104.57 144.16 57.29 o 12 0 0 338.00 443.04 108.25 o 13 0 0 240.68 257.69 73.40 o -12 1 0 542.61 496.64 87.39 o -11 1 0 23.62 62.31 50.69 o -10 1 0 63.22 94.79 43.83 o -9 1 0 54.36 137.35 37.17 o -8 1 0 2129.69 2092.92 114.52 o -7 1 0 3.51 39.42 25.56 o -6 1 0 8274.08 8873.59 310.70 o -5 1 0 161.44 231.96 20.94 o -4 1 0 2630.83 2601.31 96.89 o -3 1 0 541.92 542.70 27.75 o -2 1 0 2518.14 2652.34 137.51 o -1 1 0 802.82 856.59 44.31 o 0 1 0 3711.56 3687.74 133.12 o 1 1 0 362.50 488.74 17.27 o 2 1 0 8046.43 10033.93 304.42 o 3 1 0 15.79 165.97 139.06 o 4 1 0 13.73 5.98 12.22 o 5 1 0 6909.17 7226.49 365.74 o 6 1 0 1517.39 1836.82 74.95 o 7 1 0 4375.87 4538.56 379.40 o 8 1 0 1215.20 1227.04 58.66 o 9 1 0 370.77 441.99 82.11 o 10 1 0 1739.74 1690.59 147.86 o 11 1 0 15.52 6.34 47.00 o 12 1 0 900.12 859.15 133.07 o 13 1 0 293.30 284.62 74.46 o -12 2 0 241.74 113.53 74.46 o -11 2 0 51.13 20.59 48.85 o -10 2 0 238.95 240.53 69.97 o -9 2 0 75.66 64.32 32.36 o -8 2 0 36.87 92.72 29.81 o -7 2 0 500.16 642.13 66.67 o -6 2 0 0.95 95.35 93.07 o -5 2 0 3579.66 3873.64 141.66 o -4 2 0 2394.51 2582.33 161.19 o -3 2 0 5936.63 6620.22 384.16 o -2 2 0 5009.26 5382.83 415.45 o -1 2 0 26290.35 31350.61 3652.73 o 0 2 0 414.98 358.60 20.78 o 1 2 0 37998.73 37854.30 1132.47 o 2 2 0 4729.85 5613.37 174.06 o 3 2 0 1644.81 2070.33 105.62 o 4 2 0 242.66 217.04 18.75 o 5 2 0 2047.09 2409.23 123.42 o 6 2 0 12.91 160.93 51.50 o 7 2 0 28.40 28.46 17.02 o 8 2 0 2739.58 2967.16 145.05 o 9 2 0 513.49 571.89 86.34 o 10 2 0 46.53 69.70 49.37 o 11 2 0 66.35 54.65 58.88 o 12 2 0 1123.72 1257.05 128.85 o 13 2 0 227.61 176.64 71.82 o -12 3 0 2.21 110.36 87.13 o -11 3 0 1.99 -32.21 54.92 o -10 3 0 1.22 29.39 35.19 o -9 3 0 12.54 52.14 32.68 o -8 3 0 148.95 180.58 42.38 o -7 3 0 24.92 5.28 28.26 o -6 3 0 1.41 19.92 22.50 o -5 3 0 4555.71 5149.36 235.76 o -4 3 0 13.67 33.00 30.10 o -3 3 0 15803.32 16794.56 711.67 o -2 3 0 171.18 146.95 26.67 o -1 3 0 2507.54 2649.46 124.05 o 0 3 0 3255.95 3275.62 123.36 o 1 3 0 67.99 330.35 134.69 o 2 3 0 423.65 751.17 163.68 o 3 3 0 7.44 5.75 15.47 o 4 3 0 17386.16 21695.27 585.46 o 5 3 0 325.71 794.99 352.70 o 6 3 0 6273.16 7609.55 391.58 o 7 3 0 240.43 187.01 22.33 o 8 3 0 350.59 378.20 41.58 o 9 3 0 1013.20 1067.02 70.19 o 10 3 0 747.19 845.43 96.11 o 11 3 0 106.63 161.59 61.26 o 12 3 0 332.73 326.08 76.83 o 13 3 0 538.88 547.07 125.94 o -11 4 0 462.28 387.33 94.79 o -10 4 0 131.91 93.11 36.96 o -9 4 0 567.85 577.85 71.68 o -8 4 0 818.38 739.17 77.62 o -7 4 0 177.20 267.50 43.95 o -6 4 0 358.71 308.71 49.77 o -5 4 0 304.60 221.19 36.05 o -4 4 0 3605.18 4178.15 453.74 o -3 4 0 7.34 6.65 14.55 o -2 4 0 10362.82 11171.32 467.63 o -1 4 0 123.83 70.71 31.99 o 0 4 0 1374.92 1213.71 47.24 o 1 4 0 96.86 55.43 15.12 o 2 4 0 687.15 592.21 33.69 o 3 4 0 915.95 962.15 39.77 o 4 4 0 1220.02 1351.12 52.12 o 5 4 0 122.88 218.49 24.77 o 6 4 0 22.92 32.80 11.56 o 7 4 0 343.87 291.25 95.71 o 8 4 0 385.21 432.92 48.95 o 9 4 0 4630.73 5035.60 303.77 o 10 4 0 2729.51 2918.49 153.36 o 11 4 0 1363.27 1567.02 155.51 o 12 4 0 119.41 201.46 100.33 o 13 4 0 488.68 478.42 96.11 o -10 5 0 167.74 238.89 58.82 o -9 5 0 577.95 589.58 71.96 o -8 5 0 789.30 786.78 71.07 o -7 5 0 550.85 489.40 61.39 o -6 5 0 540.38 569.44 59.01 o -5 5 0 5.33 16.78 39.87 o -4 5 0 1691.58 2052.65 162.77 o -3 5 0 24.51 23.06 23.05 o -2 5 0 442.39 456.66 33.68 o -1 5 0 3.98 -6.97 21.09 o 0 5 0 76.44 338.12 150.53 o 1 5 0 1302.09 1042.53 43.25 o 2 5 0 43.74 25.81 13.80 o 3 5 0 2759.08 2687.57 118.03 o 4 5 0 593.68 694.85 34.65 o 5 5 0 7098.54 8539.81 268.31 o 6 5 0 10.65 20.01 22.56 o 7 5 0 172.06 210.59 30.76 o 8 5 0 84.60 49.62 30.82 o 9 5 0 289.56 395.78 87.92 o 10 5 0 591.23 538.49 54.28 o 11 5 0 173.77 254.79 39.02 o 12 5 0 1640.58 1855.34 175.05 o 13 5 0 268.90 327.13 90.83 o -10 6 0 921.78 826.05 76.56 o -9 6 0 37.25 13.00 40.78 o -8 6 0 130.96 167.65 113.80 o -7 6 0 1078.49 1014.43 81.87 o -6 6 0 223.63 329.48 52.08 o -5 6 0 254.15 262.15 63.76 o -4 6 0 819.83 792.32 63.69 o -3 6 0 7805.71 8103.13 361.23 o -2 6 0 58.06 60.85 18.07 o -1 6 0 1396.43 1192.91 49.61 o 0 6 0 2131.03 2347.08 83.52 o 1 6 0 2877.42 2542.85 88.65 o 2 6 0 3811.92 4151.98 136.43 o 3 6 0 1027.67 1091.51 46.84 o 4 6 0 157.67 299.25 44.70 o 5 6 0 1.54 10.64 14.49 o 6 6 0 1960.49 2157.37 80.24 o 7 6 0 324.61 363.08 37.34 o 8 6 0 1011.81 1107.97 82.88 o 9 6 0 81.82 196.17 71.55 o 10 6 0 2964.81 2911.35 256.64 o 11 6 0 3656.90 3677.65 191.02 o 12 6 0 348.37 256.64 77.10 o 13 6 0 133.49 150.50 75.25 o -9 7 0 78.11 122.60 47.14 o -8 7 0 111.23 135.91 47.63 o -7 7 0 632.52 655.42 66.61 o -6 7 0 114.48 56.09 42.68 o -5 7 0 888.80 908.53 70.06 o -4 7 0 83.77 73.10 35.20 o -3 7 0 581.30 563.30 42.91 o -2 7 0 1.11 0.26 54.92 o -1 7 0 25.99 13.65 18.18 o 0 7 0 1226.90 1013.92 59.83 o 1 7 0 3.70 27.86 15.75 o 2 7 0 2634.16 2109.24 77.05 o 3 7 0 1.60 5.63 16.96 o 4 7 0 3975.36 4082.91 136.98 o 5 7 0 1916.47 1828.36 72.06 o 6 7 0 2043.09 2181.31 97.53 o 7 7 0 444.99 442.31 39.55 o 8 7 0 882.57 938.87 77.78 o 9 7 0 495.01 500.91 54.02 o 10 7 0 621.28 749.51 119.21 o 11 7 0 120.91 166.81 47.74 o 12 7 0 24.23 40.93 38.88 o 13 7 0 770.43 784.61 81.65 o -8 8 0 64.59 66.35 53.20 o -7 8 0 193.40 137.74 44.79 o -6 8 0 268.16 352.71 68.25 o -5 8 0 398.25 388.00 97.43 o -4 8 0 510.46 545.79 109.18 o -3 8 0 656.91 753.02 160.40 o -2 8 0 1210.25 1156.08 84.37 o -1 8 0 668.16 641.74 44.43 o 0 8 0 643.80 622.82 44.52 o 1 8 0 116.68 87.91 26.67 o 2 8 0 352.89 326.68 34.82 o 3 8 0 614.12 564.43 50.49 o 4 8 0 67.52 71.55 60.24 o 5 8 0 3019.35 3155.08 128.89 o 6 8 0 16.76 72.13 40.00 o 7 8 0 621.48 608.59 58.76 o 8 8 0 80.65 77.83 40.29 o 9 8 0 1690.72 1853.31 117.65 o 10 8 0 722.65 691.05 72.54 o 11 8 0 109.54 133.04 46.46 o 12 8 0 112.09 96.94 144.69 o 13 8 0 253.77 335.42 67.21 o -7 9 0 56.06 86.34 55.34 o -6 9 0 918.34 919.75 80.19 o -5 9 0 49.58 77.00 104.03 o -4 9 0 332.00 491.32 165.15 o -3 9 0 712.43 654.59 67.25 o -2 9 0 10.70 22.29 32.88 o -1 9 0 122.52 176.83 44.41 o 0 9 0 461.18 560.02 61.55 o 1 9 0 1914.88 1916.32 137.35 o 2 9 0 83.32 57.60 24.82 o 3 9 0 3970.20 4053.03 168.81 o 4 9 0 985.12 1002.78 71.69 o 5 9 0 3141.42 2942.70 125.48 o 6 9 0 639.37 617.58 88.32 o 7 9 0 712.49 692.61 130.83 o 8 9 0 548.81 509.82 60.01 o 9 9 0 2712.36 2383.42 137.83 o 10 9 0 62.11 102.99 52.82 o 11 9 0 12.67 80.76 40.87 o 12 9 0 339.72 296.45 56.34 o -6 10 0 11.82 -20.33 64.95 o -5 10 0 140.32 203.46 53.14 o -4 10 0 263.91 280.30 128.45 o -3 10 0 1374.79 1220.75 203.17 o -2 10 0 216.14 219.99 55.24 o -1 10 0 907.54 949.42 198.55 o 0 10 0 2946.09 2964.65 370.83 o 1 10 0 342.91 361.62 42.06 o 2 10 0 289.23 279.28 58.55 o 3 10 0 106.16 81.36 31.12 o 4 10 0 578.80 588.50 72.37 o 5 10 0 151.05 319.72 187.86 o 6 10 0 1716.26 1608.52 120.93 o 7 10 0 543.42 523.97 68.72 o 8 10 0 849.89 1021.73 88.06 o 9 10 0 730.79 762.16 99.94 o 10 10 0 617.63 770.95 80.11 o 11 10 0 215.60 278.80 57.03 o 12 10 0 48.72 61.77 51.58 o -5 11 0 33.09 111.00 54.34 o -4 11 0 16.56 36.26 132.81 o -3 11 0 189.29 344.09 122.64 o -2 11 0 784.19 746.62 231.16 o -1 11 0 892.45 957.33 142.05 o 0 11 0 757.14 779.47 69.68 o 1 11 0 600.34 607.67 50.60 o 2 11 0 3003.39 3256.83 337.05 o 3 11 0 124.99 79.02 29.77 o 4 11 0 1953.94 1980.39 134.63 o 5 11 0 813.29 804.28 190.10 o 6 11 0 229.72 295.83 90.96 o 7 11 0 1047.53 949.34 88.94 o 8 11 0 79.69 118.24 53.58 o 9 11 0 1108.11 987.05 114.06 o 10 11 0 13.20 54.75 122.77 o 11 11 0 317.31 340.84 70.24 o -3 12 0 241.25 356.20 57.45 o -2 12 0 1171.35 1352.02 137.56 o -1 12 0 4.92 -30.18 37.45 o 0 12 0 808.22 1012.53 262.31 o 1 12 0 15.26 19.59 53.60 o 2 12 0 57.83 101.14 43.56 o 3 12 0 375.67 322.69 102.76 o 4 12 0 195.50 236.47 104.82 o 5 12 0 410.27 390.66 85.68 o 6 12 0 222.69 285.39 155.12 o 7 12 0 818.72 799.98 87.85 o 8 12 0 297.52 322.04 58.53 o 9 12 0 508.34 524.92 78.95 o 10 12 0 343.66 380.67 73.70 o -1 13 0 439.95 484.53 76.83 o 0 13 0 7.94 7.05 41.94 o 1 13 0 795.45 794.97 74.86 o 2 13 0 414.12 403.48 116.57 o 3 13 0 928.05 950.78 70.36 o 4 13 0 39.98 93.68 58.29 o 5 13 0 449.81 455.86 69.41 o 6 13 0 111.33 93.53 53.20 o 7 13 0 329.21 251.95 55.58 o 8 13 0 3.22 87.92 79.47 o 4 14 0 489.05 447.01 68.77 o 5 14 0 90.63 22.79 49.97 o -8 -13 1 915.58 893.62 84.76 o -7 -13 1 238.29 317.71 62.17 o -6 -13 1 424.63 351.92 61.92 o -5 -13 1 41.74 274.35 96.90 o -4 -13 1 43.73 127.41 53.94 o -3 -13 1 406.06 384.35 116.54 o -2 -13 1 1.59 136.93 101.92 o -1 -13 1 77.00 41.45 63.37 o 0 -13 1 186.68 248.17 55.47 o 1 -13 1 53.65 129.11 58.09 o -10 -12 1 266.37 241.31 78.95 o -9 -12 1 347.48 351.28 64.99 o -8 -12 1 11.91 -20.27 37.69 o -7 -12 1 314.58 271.15 55.07 o -6 -12 1 472.49 455.90 91.49 o -5 -12 1 1492.74 1593.19 273.54 o -4 -12 1 568.64 717.36 153.67 o -3 -12 1 43.87 35.67 43.25 o -2 -12 1 1576.12 1583.36 83.93 o -1 -12 1 94.39 89.51 85.55 o 0 -12 1 899.39 779.18 138.09 o 1 -12 1 0.32 85.78 43.76 o 2 -12 1 3.52 40.22 100.33 o 3 -12 1 612.68 728.86 74.98 o -11 -11 1 661.78 643.30 82.35 o -10 -11 1 553.26 549.34 68.07 o -9 -11 1 32.12 118.13 47.08 o -8 -11 1 1122.85 1064.75 88.60 o -7 -11 1 209.69 91.53 70.63 o -6 -11 1 1893.47 1979.76 127.84 o -5 -11 1 981.04 1055.88 153.01 o -4 -11 1 28.18 70.47 46.32 o -3 -11 1 506.10 504.15 65.56 o -2 -11 1 1.59 230.50 92.15 o -1 -11 1 623.72 711.56 128.85 o 0 -11 1 473.35 462.17 60.11 o 1 -11 1 816.46 949.46 144.16 o 2 -11 1 16.57 -59.14 59.14 o 3 -11 1 454.70 543.62 70.66 o 4 -11 1 64.78 302.78 64.57 o -12 -10 1 864.66 867.23 94.28 o -11 -10 1 301.74 269.39 90.30 o -10 -10 1 923.62 767.18 72.51 o -9 -10 1 69.83 47.88 56.64 o -8 -10 1 66.65 92.78 48.71 o -7 -10 1 612.14 637.07 79.79 o -6 -10 1 1184.79 1131.49 90.31 o -5 -10 1 4970.21 5700.96 498.62 o -4 -10 1 1617.12 1495.22 76.86 o -3 -10 1 216.34 235.18 35.00 o -2 -10 1 873.75 901.40 61.24 o -1 -10 1 182.37 300.84 54.79 o 0 -10 1 99.04 79.38 145.61 o 1 -10 1 82.05 115.79 67.46 o 2 -10 1 125.53 264.64 114.59 o 3 -10 1 214.65 237.09 50.10 o 4 -10 1 1321.87 1559.23 110.87 o 5 -10 1 214.79 237.96 59.27 o 6 -10 1 225.69 202.94 76.96 o -12 -9 1 21.23 75.48 46.34 o -11 -9 1 946.75 822.84 72.78 o -10 -9 1 584.44 576.04 73.93 o -9 -9 1 36.81 109.31 71.29 o -8 -9 1 1406.11 1287.57 90.53 o -7 -9 1 795.92 761.42 69.24 o -6 -9 1 49.21 56.81 32.90 o -5 -9 1 1686.35 1691.10 110.57 o -4 -9 1 115.93 124.73 64.19 o -3 -9 1 1171.27 1032.34 139.15 o -2 -9 1 188.84 151.91 29.08 o -1 -9 1 116.50 38.20 68.91 o 0 -9 1 2477.74 2597.90 810.92 o 1 -9 1 6.05 35.97 31.72 o 2 -9 1 804.27 800.38 72.54 o 3 -9 1 106.92 148.54 86.34 o 4 -9 1 2120.36 1992.69 176.24 o 5 -9 1 107.65 78.07 43.73 o 6 -9 1 1.28 85.99 48.01 o 7 -9 1 315.42 348.33 63.72 o -13 -8 1 97.63 46.24 53.23 o -12 -8 1 403.03 335.96 55.98 o -11 -8 1 124.51 274.22 88.58 o -10 -8 1 129.28 76.12 48.32 o -9 -8 1 52.31 53.51 48.38 o -8 -8 1 1579.93 1629.38 105.75 o -7 -8 1 324.48 376.17 59.14 o -6 -8 1 2613.76 2595.62 141.38 o -5 -8 1 448.46 375.05 94.50 o -4 -8 1 4778.99 4793.36 182.85 o -3 -8 1 345.97 305.08 60.52 o -2 -8 1 198.81 135.61 36.13 o -1 -8 1 208.87 166.36 33.42 o 0 -8 1 574.54 501.19 75.10 o 1 -8 1 1.05 6.97 21.17 o 2 -8 1 5.98 21.52 44.23 o 3 -8 1 1568.22 1650.99 254.39 o 4 -8 1 1309.76 1373.60 237.36 o 5 -8 1 1695.42 1875.58 120.70 o 6 -8 1 178.54 187.29 57.89 o 7 -8 1 647.78 619.47 65.70 o 8 -8 1 26.61 23.23 49.37 o -13 -7 1 96.93 111.77 51.75 o -12 -7 1 364.27 395.15 61.79 o -11 -7 1 414.60 472.28 66.98 o -10 -7 1 2624.30 2707.82 223.77 o -9 -7 1 267.71 294.00 75.38 o -8 -7 1 1549.95 1532.48 79.73 o -7 -7 1 1133.01 1191.47 66.81 o -6 -7 1 1684.71 1769.11 84.96 o -5 -7 1 178.80 125.07 20.26 o -4 -7 1 1007.86 1049.44 49.38 o -3 -7 1 279.97 239.19 28.51 o -2 -7 1 787.25 735.75 37.60 o -1 -7 1 4210.26 4322.60 143.63 o 0 -7 1 640.17 542.46 34.73 o 1 -7 1 1211.65 1067.29 49.54 o 2 -7 1 183.57 197.58 28.68 o 3 -7 1 1038.99 1102.13 80.89 o 4 -7 1 56.29 114.05 40.57 o 5 -7 1 366.35 315.90 65.22 o 6 -7 1 1.31 -33.66 33.66 o 7 -7 1 4.85 38.41 36.66 o 8 -7 1 295.35 278.08 50.21 o 9 -7 1 35.95 49.11 95.71 o -13 -6 1 905.35 840.94 118.29 o -12 -6 1 28.03 38.96 40.42 o -11 -6 1 487.24 482.54 144.03 o -10 -6 1 134.11 146.46 42.97 o -9 -6 1 327.60 360.15 46.99 o -8 -6 1 3290.93 3576.47 204.95 o -7 -6 1 1479.37 1597.46 80.67 o -6 -6 1 64.45 61.38 36.44 o -5 -6 1 2577.41 2691.06 96.11 o -4 -6 1 665.75 635.14 35.52 o -3 -6 1 2819.62 2769.46 96.86 o -2 -6 1 147.98 157.77 46.99 o -1 -6 1 108.63 78.42 20.31 o 0 -6 1 51.40 68.44 17.37 o 1 -6 1 13.15 16.46 17.47 o 2 -6 1 6.28 -4.24 15.80 o 3 -6 1 41.98 -10.06 24.64 o 4 -6 1 5003.97 5326.21 249.05 o 5 -6 1 629.28 669.51 60.60 o 6 -6 1 4316.39 4818.18 233.48 o 7 -6 1 63.94 83.19 40.94 o 8 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