#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209442.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209442_Fobs loop_ _publ_author_name 'Petrov, Ravil R.' 'Vardanyan, Ruben S.' 'Nichol, Gary S.' 'Carducci, Michael D.' 'Ma, Shou-wu' 'Lai, Josephine Y.' 'Hruby, Victor J.' _publ_section_title ; 4-{N-[2-(1,3-Dioxo-1,3-dihydroisoindol-2-yl)-3-phenylpropionyl]anilino}-1-phenethylpiperidinium chloride methanol disolvate ; _journal_coeditor_code CF2036 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2815 _journal_page_last o2816 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.498 _cell_angle_gamma 90.000 _cell_length_a 11.0144 _cell_length_b 17.1311 _cell_length_c 19.0552 _exptl_crystal_F_000 1400.00 _reflns_d_resolution_high 0.9000 _[local]_cod_data_source_file cf2036Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rp01 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6020.79 2087.60 97.16 o 2 0 0 8313.64 2825.58 137.41 o 3 0 0 668.07 409.73 42.19 o 8 0 0 343.45 -71.50 116.00 o 9 0 0 864.56 58.79 129.08 o 10 0 0 77.41 -20.73 46.66 o 11 0 0 920.17 1496.54 117.19 o 12 0 0 62.58 151.90 69.11 o 2 1 0 307.47 343.08 13.72 o 3 1 0 23.51 -0.35 8.71 o 4 1 0 1086.95 404.25 50.04 o 5 1 0 168.23 224.66 28.74 o 9 1 0 73.23 67.67 32.16 o 10 1 0 21.49 20.21 20.66 o 11 1 0 45.98 16.54 23.40 o 12 1 0 6.19 -19.66 19.66 o 0 2 0 967.82 1070.06 26.70 o 1 2 0 4847.10 5008.13 77.82 o 2 2 0 1.85 -1.05 4.87 o 4 2 0 1.14 10.08 4.78 o 5 2 0 2725.74 1822.03 60.86 o 6 2 0 2.51 8.78 5.83 o 7 2 0 224.31 294.09 30.91 o 8 2 0 248.85 323.09 29.86 o 9 2 0 0.53 -13.86 16.26 o 10 2 0 254.91 274.06 87.50 o 11 2 0 15.39 27.18 23.99 o 1 3 0 17834.88 19270.44 329.96 o 7 3 0 5.06 22.37 9.49 o 8 3 0 502.57 18.73 125.92 o 9 3 0 56.24 32.67 33.79 o 10 3 0 0.32 7.08 25.31 o 11 3 0 143.91 46.93 56.21 o 0 4 0 243.42 262.16 11.04 o 1 4 0 20224.88 22072.21 453.66 o 3 4 0 467.07 531.76 24.87 o 4 4 0 1605.40 1836.00 79.82 o 5 4 0 188.53 25.75 25.69 o 6 4 0 21.31 11.70 7.51 o 7 4 0 502.09 477.64 105.43 o 8 4 0 77.51 54.52 19.46 o 9 4 0 169.04 62.47 49.94 o 10 4 0 1.71 -3.20 25.50 o 11 4 0 43.61 108.61 39.23 o 1 5 0 1555.84 1676.70 27.04 o 2 5 0 108.63 71.92 9.08 o 3 5 0 239.33 178.81 10.88 o 4 5 0 23.11 21.21 7.59 o 5 5 0 304.39 140.23 60.16 o 6 5 0 91.48 66.43 25.39 o 7 5 0 442.91 419.01 229.55 o 8 5 0 0.03 -0.72 9.56 o 9 5 0 38.27 44.99 17.31 o 10 5 0 74.00 89.89 39.08 o 11 5 0 1.15 -32.66 34.80 o 0 6 0 20707.70 22765.69 391.18 o 1 6 0 3386.62 3629.01 53.60 o 2 6 0 5117.44 5406.18 77.88 o 3 6 0 266.96 322.08 16.02 o 4 6 0 2097.68 2567.98 146.11 o 5 6 0 1323.23 1384.30 87.80 o 7 6 0 1397.12 1652.09 41.89 o 8 6 0 246.25 343.15 60.23 o 9 6 0 7.20 -11.23 15.62 o 10 6 0 708.07 -28.09 164.70 o 11 6 0 354.25 508.24 70.00 o 1 7 0 9.51 15.80 6.14 o 2 7 0 53.24 50.79 8.98 o 3 7 0 1412.48 1476.78 33.68 o 4 7 0 0.33 8.42 6.98 o 5 7 0 319.31 402.92 19.15 o 6 7 0 10.63 0.29 8.51 o 7 7 0 216.94 256.68 40.46 o 8 7 0 98.25 115.79 18.37 o 9 7 0 141.06 162.55 45.92 o 10 7 0 290.61 -6.51 62.02 o 11 7 0 30.32 20.83 42.58 o 0 8 0 146.74 89.08 15.78 o 1 8 0 1609.10 1676.85 39.82 o 2 8 0 1603.51 1657.89 36.54 o 3 8 0 505.06 299.17 103.00 o 4 8 0 410.68 435.65 20.08 o 5 8 0 165.94 168.75 31.53 o 6 8 0 34.28 39.35 18.67 o 7 8 0 384.36 460.16 33.12 o 8 8 0 323.47 335.50 47.34 o 9 8 0 18.52 16.15 23.19 o 10 8 0 44.02 65.33 73.55 o 1 9 0 25.63 16.73 7.40 o 2 9 0 75.61 79.99 15.88 o 3 9 0 150.80 135.12 12.02 o 4 9 0 157.18 186.83 25.15 o 5 9 0 39.01 27.13 12.77 o 6 9 0 62.58 62.09 15.64 o 7 9 0 51.38 23.77 13.99 o 8 9 0 48.17 23.48 27.16 o 9 9 0 18.73 28.90 21.12 o 10 9 0 11.44 -5.93 38.15 o 0 10 0 1680.87 2024.36 54.67 o 1 10 0 2.27 8.72 7.50 o 2 10 0 1.97 3.23 8.28 o 3 10 0 123.20 102.83 22.22 o 4 10 0 1629.14 1782.86 47.29 o 5 10 0 54.00 60.87 16.36 o 6 10 0 70.74 79.38 17.30 o 7 10 0 123.80 182.37 23.24 o 8 10 0 50.58 44.51 20.66 o 9 10 0 155.50 153.25 55.45 o 10 10 0 27.88 93.16 45.71 o 1 11 0 122.14 94.64 20.86 o 2 11 0 82.60 67.43 11.66 o 3 11 0 50.19 45.48 13.02 o 4 11 0 740.54 683.14 28.82 o 5 11 0 1075.02 1072.07 41.34 o 6 11 0 7.45 -17.11 19.55 o 7 11 0 229.59 189.03 31.86 o 8 11 0 110.91 98.68 39.79 o 9 11 0 20.54 17.20 22.76 o 0 12 0 1054.96 1054.59 50.96 o 1 12 0 476.99 418.98 19.39 o 2 12 0 5.54 9.78 11.21 o 3 12 0 577.35 601.93 24.80 o 4 12 0 737.03 823.22 30.27 o 5 12 0 183.32 164.67 44.34 o 6 12 0 0.09 1.07 14.38 o 7 12 0 503.51 703.53 71.43 o 8 12 0 23.58 -24.94 28.89 o 9 12 0 240.76 345.09 34.42 o 1 13 0 0.92 -12.30 12.30 o 2 13 0 17.37 5.39 11.92 o 3 13 0 35.38 39.23 14.79 o 4 13 0 211.48 235.48 39.23 o 5 13 0 395.40 374.57 31.27 o 6 13 0 168.41 136.92 18.35 o 7 13 0 3.90 -8.40 17.22 o 8 13 0 56.05 72.85 24.49 o 0 14 0 158.31 143.69 36.36 o 1 14 0 457.83 478.42 26.70 o 2 14 0 758.19 714.60 32.73 o 3 14 0 69.30 57.97 18.60 o 4 14 0 1216.90 1196.48 39.06 o 5 14 0 2.86 -1.89 15.16 o 6 14 0 254.84 259.63 22.40 o 7 14 0 545.72 596.40 29.56 o 8 14 0 115.29 157.04 28.81 o 1 15 0 302.52 271.41 22.63 o 2 15 0 612.98 530.05 29.82 o 3 15 0 919.95 824.98 46.45 o 4 15 0 11.95 -14.79 15.75 o 5 15 0 834.47 847.91 33.35 o 6 15 0 110.60 103.41 20.05 o 7 15 0 535.70 552.92 31.38 o 0 16 0 122.04 116.19 36.63 o 1 16 0 51.03 47.59 18.88 o 2 16 0 139.65 175.93 20.89 o 3 16 0 117.32 141.80 22.01 o 4 16 0 78.05 73.31 22.54 o 5 16 0 102.02 88.73 22.65 o 6 16 0 1.35 -12.98 19.14 o 1 17 0 134.57 161.46 31.52 o 2 17 0 44.07 28.74 19.26 o 3 17 0 266.71 293.94 29.32 o 4 17 0 42.76 46.77 23.08 o 5 17 0 28.13 26.72 21.69 o 0 18 0 3.03 11.16 28.63 o 1 18 0 459.02 426.06 30.12 o 2 18 0 4.53 -19.92 20.28 o 3 18 0 3.56 -8.18 21.83 o -12 1 1 5.84 -2.08 28.17 o -11 1 1 90.05 84.45 67.56 o -10 1 1 198.55 -9.49 40.44 o -9 1 1 86.67 82.75 20.67 o -8 1 1 4.23 19.60 9.74 o -7 1 1 5.68 -1.23 8.59 o -6 1 1 55.97 -16.49 16.49 o -3 1 1 84.99 21.07 17.87 o -1 1 1 1413.13 1378.47 24.72 o 0 1 1 3950.08 4233.13 133.70 o 1 1 1 197.79 131.92 9.92 o 2 1 1 18836.65 8439.47 365.16 o 3 1 1 1886.58 892.23 61.47 o 4 1 1 2154.32 836.72 66.33 o 5 1 1 1738.79 817.81 79.89 o 6 1 1 2003.02 833.37 88.22 o 7 1 1 620.47 150.29 126.88 o 8 1 1 2.68 7.60 8.30 o 9 1 1 654.20 313.76 235.60 o 10 1 1 4.19 -2.09 21.11 o 11 1 1 25.62 19.19 26.33 o -12 2 1 9.70 -10.67 38.52 o -11 2 1 72.71 65.42 47.71 o -10 2 1 168.35 -36.74 37.11 o -9 2 1 47.49 60.51 33.30 o -8 2 1 514.78 536.58 103.94 o -7 2 1 0.37 -4.81 5.81 o -6 2 1 28.85 27.07 6.36 o -5 2 1 1689.04 834.29 33.87 o -4 2 1 747.37 374.77 19.27 o -3 2 1 0.48 -4.59 4.59 o -2 2 1 1824.89 1859.86 29.20 o -1 2 1 1225.49 1317.17 19.96 o 0 2 1 8978.71 9068.82 139.44 o 1 2 1 29132.55 30918.63 391.23 o 2 2 1 743.02 226.75 62.30 o 3 2 1 10760.66 3608.67 168.72 o 5 2 1 444.44 179.99 111.11 o 6 2 1 527.63 206.00 57.08 o 8 2 1 0.71 -3.69 7.89 o 9 2 1 296.22 422.42 53.44 o 10 2 1 14.02 4.77 20.38 o 11 2 1 16.40 -25.00 32.61 o -11 3 1 166.60 189.75 44.71 o -10 3 1 151.23 39.43 41.25 o -9 3 1 9.60 -15.19 15.19 o -7 3 1 134.11 166.21 19.53 o -5 3 1 174.17 186.26 16.13 o -4 3 1 8256.27 8673.89 124.08 o -3 3 1 22099.42 25069.36 421.57 o -1 3 1 20019.76 21660.99 290.11 o 0 3 1 668.29 706.85 13.25 o 1 3 1 20008.26 22069.63 545.87 o 2 3 1 9393.73 9021.83 399.59 o 3 3 1 31270.86 11024.33 1039.67 o 4 3 1 20.19 22.24 5.66 o 5 3 1 47.84 32.28 11.58 o 6 3 1 340.60 90.39 92.93 o 7 3 1 890.91 196.49 155.55 o 8 3 1 630.28 30.89 131.81 o 9 3 1 38.07 38.67 15.73 o 10 3 1 104.92 54.25 41.82 o 11 3 1 473.39 260.53 103.90 o -11 4 1 15.70 1.01 34.41 o -10 4 1 62.26 22.33 27.08 o -9 4 1 7.13 0.29 22.50 o -8 4 1 257.99 250.06 107.18 o -7 4 1 238.53 306.06 44.24 o -5 4 1 46.79 58.98 10.98 o -4 4 1 124.11 75.21 11.61 o -3 4 1 2090.53 2234.52 63.79 o -2 4 1 1554.41 1594.28 31.92 o -1 4 1 273.35 193.77 7.12 o 0 4 1 0.81 1.35 3.23 o 1 4 1 1442.82 1561.34 26.25 o 2 4 1 1.02 -2.75 3.83 o 3 4 1 2251.35 2531.59 51.39 o 4 4 1 608.92 96.37 97.28 o 5 4 1 1302.47 636.99 45.72 o 6 4 1 349.10 422.44 56.32 o 7 4 1 2.91 5.88 8.96 o 8 4 1 299.10 293.60 61.29 o 9 4 1 6.06 -9.44 12.16 o 10 4 1 142.00 114.87 47.43 o 11 4 1 4.16 19.39 39.64 o -11 5 1 103.61 95.60 65.49 o -10 5 1 200.45 260.96 120.36 o -9 5 1 117.83 62.55 43.59 o -8 5 1 2.13 -10.39 11.09 o -7 5 1 355.21 332.52 101.76 o -6 5 1 2.91 2.30 7.08 o -5 5 1 257.36 260.03 17.70 o -4 5 1 2084.75 2342.16 43.10 o -3 5 1 275.75 337.26 77.70 o -2 5 1 387.00 299.98 11.19 o -1 5 1 7687.17 8768.11 108.89 o 0 5 1 4029.60 4647.00 59.56 o 1 5 1 461.80 488.51 13.00 o 2 5 1 163.81 145.34 12.11 o 3 5 1 3.01 -0.01 4.84 o 4 5 1 7315.96 8842.14 191.30 o 5 5 1 1554.34 1587.19 71.97 o 6 5 1 70.64 57.27 11.30 o 7 5 1 372.13 262.32 57.61 o 8 5 1 493.83 291.40 114.91 o 9 5 1 10.81 -3.50 18.75 o 10 5 1 799.15 49.55 166.22 o 11 5 1 12.21 2.07 37.38 o -11 6 1 47.64 49.36 38.63 o -10 6 1 206.74 174.25 97.15 o -7 6 1 57.03 63.31 16.76 o -6 6 1 13.32 0.28 7.99 o -5 6 1 0.27 8.41 7.14 o -4 6 1 612.65 425.82 110.87 o -3 6 1 138.73 118.45 20.05 o -2 6 1 3097.31 3403.17 57.40 o -1 6 1 283.01 252.31 9.54 o 0 6 1 34.96 19.90 5.17 o 1 6 1 5590.99 6179.75 145.47 o 2 6 1 2279.54 2296.92 43.64 o 3 6 1 1307.61 1395.44 40.87 o 4 6 1 3036.91 3527.91 79.69 o 5 6 1 2164.44 2871.14 110.37 o 6 6 1 249.95 162.59 43.02 o 8 6 1 65.24 64.26 15.35 o 9 6 1 198.67 0.94 57.00 o 10 6 1 437.56 -66.80 108.37 o 11 6 1 48.03 37.72 40.09 o -11 7 1 523.97 290.01 204.47 o -10 7 1 26.35 0.86 33.50 o -9 7 1 422.25 502.90 138.28 o -8 7 1 0.45 8.22 15.60 o -7 7 1 79.99 69.20 14.09 o -6 7 1 428.93 420.35 18.83 o -5 7 1 1392.73 1557.88 37.43 o -4 7 1 524.91 669.28 107.19 o -3 7 1 444.07 412.59 26.45 o -2 7 1 1251.53 1420.89 27.12 o -1 7 1 2172.80 2258.09 38.95 o 0 7 1 425.55 488.18 13.00 o 1 7 1 8489.42 9132.38 129.01 o 2 7 1 38.71 53.54 9.79 o 3 7 1 69.46 54.64 18.13 o 4 7 1 480.65 496.42 27.78 o 5 7 1 336.76 355.51 14.94 o 6 7 1 93.57 90.48 21.73 o 7 7 1 614.90 65.18 138.14 o 8 7 1 60.51 56.99 16.27 o 9 7 1 66.92 28.13 41.39 o 10 7 1 61.23 99.65 44.39 o 11 7 1 58.55 46.45 43.71 o -11 8 1 10.50 -5.60 40.24 o -10 8 1 92.84 77.21 40.45 o -9 8 1 5.12 -17.03 28.63 o -8 8 1 580.31 616.19 75.81 o -7 8 1 246.80 260.49 25.35 o -6 8 1 523.63 613.45 23.50 o -5 8 1 2.51 -8.98 8.98 o -4 8 1 1141.42 1058.33 131.63 o -3 8 1 108.34 52.18 11.37 o -2 8 1 4.58 1.08 6.07 o -1 8 1 57.10 40.38 7.18 o 0 8 1 904.11 1056.06 23.87 o 1 8 1 927.17 855.98 20.21 o 2 8 1 1157.60 1226.67 27.35 o 3 8 1 2695.37 2640.58 55.84 o 4 8 1 4588.75 5049.73 92.17 o 5 8 1 1216.69 1436.01 40.06 o 6 8 1 1.20 12.08 11.06 o 7 8 1 119.97 127.53 26.45 o 8 8 1 470.73 525.20 83.62 o 9 8 1 6.11 15.54 18.78 o 10 8 1 20.38 38.07 40.55 o -10 9 1 169.52 157.40 139.79 o -9 9 1 316.70 224.94 89.52 o -8 9 1 223.70 320.50 25.70 o -7 9 1 182.33 169.60 26.59 o -6 9 1 855.52 985.11 31.56 o -5 9 1 77.99 82.36 18.17 o -4 9 1 2817.98 3143.40 66.70 o -3 9 1 667.03 532.53 22.98 o -2 9 1 968.23 993.42 23.41 o -1 9 1 76.16 45.24 7.80 o 0 9 1 45.34 47.08 9.95 o 1 9 1 8640.25 8717.16 129.17 o 2 9 1 108.67 138.85 15.35 o 3 9 1 747.63 628.11 25.34 o 4 9 1 3109.69 3353.52 106.86 o 5 9 1 604.56 620.06 25.85 o 6 9 1 13.49 8.68 12.33 o 7 9 1 3.79 0.49 12.94 o 8 9 1 454.32 553.77 106.32 o 9 9 1 14.68 3.31 29.39 o 10 9 1 106.48 -50.85 59.01 o -10 10 1 0.09 -14.18 37.93 o -9 10 1 86.61 44.09 50.05 o -8 10 1 4.59 7.17 20.26 o -7 10 1 0.12 -12.53 12.53 o -6 10 1 551.25 609.67 25.62 o -5 10 1 79.17 79.29 14.42 o -4 10 1 0.22 -8.83 10.57 o -3 10 1 197.70 159.07 13.26 o -2 10 1 1.04 3.49 8.09 o -1 10 1 988.48 929.49 24.31 o 0 10 1 181.06 247.19 12.15 o 1 10 1 139.67 162.52 9.30 o 2 10 1 9.89 8.23 8.70 o 3 10 1 9.31 15.84 10.19 o 4 10 1 183.59 175.70 15.08 o 5 10 1 434.42 456.29 21.68 o 6 10 1 55.17 83.95 16.27 o 7 10 1 11.45 6.57 14.32 o 8 10 1 140.21 188.66 27.47 o 9 10 1 80.54 72.94 26.43 o 10 10 1 263.53 266.03 52.29 o -9 11 1 17.43 -1.71 36.47 o -8 11 1 1.77 7.35 18.72 o -7 11 1 737.78 769.98 40.26 o -6 11 1 418.61 420.56 35.73 o -5 11 1 851.70 832.82 30.70 o -4 11 1 24.15 4.44 12.31 o -3 11 1 0.22 -0.64 10.49 o -2 11 1 465.34 462.56 20.49 o -1 11 1 176.66 136.12 10.76 o 0 11 1 3.94 1.28 8.38 o 1 11 1 2455.85 2328.36 51.99 o 2 11 1 286.53 274.42 15.91 o 3 11 1 2120.26 2066.80 47.85 o 4 11 1 990.27 1031.29 32.74 o 5 11 1 190.93 189.08 16.30 o 6 11 1 54.48 26.16 14.30 o 7 11 1 353.66 356.95 28.85 o 8 11 1 8.60 8.82 16.06 o 9 11 1 122.56 153.92 43.92 o -9 12 1 4.42 -7.60 24.02 o -8 12 1 70.27 62.15 24.29 o -7 12 1 305.08 299.59 41.35 o -6 12 1 85.96 99.14 18.61 o -5 12 1 36.92 44.58 14.68 o -4 12 1 275.68 263.42 19.01 o -3 12 1 4.75 2.60 11.34 o -2 12 1 55.58 53.66 13.35 o -1 12 1 369.61 336.05 17.75 o 0 12 1 465.99 516.89 20.51 o 1 12 1 8.94 1.85 9.40 o 2 12 1 292.58 231.54 15.30 o 3 12 1 394.62 448.90 21.54 o 4 12 1 45.70 52.15 28.78 o 5 12 1 131.00 106.55 21.52 o 6 12 1 17.85 28.64 17.67 o 7 12 1 396.94 419.81 34.36 o 8 12 1 176.47 148.14 37.64 o 9 12 1 29.82 75.18 32.52 o -8 13 1 46.33 44.65 28.04 o -7 13 1 23.76 16.66 17.90 o -6 13 1 1378.97 1494.76 46.39 o -5 13 1 75.60 108.84 18.50 o -4 13 1 547.12 581.56 25.42 o -3 13 1 320.17 329.01 18.90 o -2 13 1 0.18 -5.79 13.22 o -1 13 1 202.20 210.56 17.05 o 0 13 1 39.59 27.16 13.24 o 1 13 1 563.15 680.22 27.21 o 2 13 1 200.64 156.34 18.72 o 3 13 1 253.03 225.86 35.83 o 4 13 1 531.26 505.32 24.72 o 5 13 1 227.70 251.69 27.45 o 6 13 1 140.54 164.96 29.49 o 7 13 1 203.04 202.98 45.77 o 8 13 1 9.25 -14.33 22.73 o -8 14 1 22.64 2.32 34.65 o -7 14 1 266.25 201.30 20.52 o -6 14 1 386.46 395.58 28.45 o -5 14 1 0.01 -9.96 15.60 o -4 14 1 240.72 238.13 18.66 o -3 14 1 7.59 -12.36 15.07 o -2 14 1 217.33 204.20 18.07 o -1 14 1 696.49 622.98 31.90 o 0 14 1 190.13 172.68 18.77 o 1 14 1 56.44 77.75 18.70 o 2 14 1 0.73 -10.40 14.43 o 3 14 1 879.72 892.53 32.60 o 4 14 1 22.32 32.42 15.52 o 5 14 1 415.67 355.70 31.05 o 6 14 1 102.93 114.21 23.37 o 7 14 1 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