#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/94/2209456.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209456_Fobs loop_ _publ_author_name 'Boyd, Peter D. W.' 'Chaker, Leila' 'Rickard, Clifton E.F.' _publ_section_title ; 5,15-Bis(3,5-di-tert-butylphenyl)-3,7,13,17-tetramethyl-2,8,12,18-tetrapropylporphyrin ; _journal_coeditor_code CV2058 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2627 _journal_page_last o2629 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.486 _cell_angle_gamma 90.000 _cell_length_a 20.9467 _cell_length_b 16.3352 _cell_length_c 8.0916 _exptl_crystal_F_000 996.00 _reflns_d_resolution_high 0.8380 _[local]_cod_data_source_file cv2058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lc2a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 238.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 809.77 908.98 53.13 o 4 0 0 56725.20 65603.97 1919.82 o 5 0 0 942.46 890.00 38.35 o 6 0 0 2540.36 2456.98 79.07 o 7 0 0 72.27 67.85 12.25 o 8 0 0 2081.41 2309.47 76.84 o 9 0 0 2238.10 2452.01 81.09 o 10 0 0 7021.04 8077.86 270.17 o 11 0 0 2258.24 2565.31 87.15 o 12 0 0 2056.44 2114.40 115.94 o 13 0 0 2344.44 2433.99 131.12 o 14 0 0 358.55 420.47 56.09 o 15 0 0 37.51 73.96 30.15 o 16 0 0 232.67 269.07 46.18 o 17 0 0 515.18 503.97 66.94 o 18 0 0 125.38 168.67 41.46 o 19 0 0 512.82 398.81 54.21 o 20 0 0 26.56 111.64 47.11 o 21 0 0 558.56 512.88 64.11 o 22 0 0 11.36 132.37 57.94 o 23 0 0 1.27 -29.68 29.68 o 24 0 0 13.87 88.56 48.05 o 3 1 0 231.11 209.54 11.33 o 4 1 0 475.85 448.37 15.59 o 5 1 0 44.91 29.68 14.13 o 6 1 0 140.84 136.69 11.78 o 7 1 0 154.64 153.65 11.78 o 8 1 0 1025.95 1099.84 32.61 o 9 1 0 107.85 109.32 11.78 o 10 1 0 0.98 0.47 8.95 o 11 1 0 152.79 166.81 11.78 o 12 1 0 0.00 11.31 11.78 o 13 1 0 11.48 13.66 20.73 o 14 1 0 28.70 30.62 24.02 o 15 1 0 37.10 54.17 28.74 o 16 1 0 246.46 227.61 38.17 o 17 1 0 327.24 342.16 41.95 o 18 1 0 118.86 86.22 24.97 o 19 1 0 4.95 -1.88 24.02 o 20 1 0 10.01 9.42 24.49 o 21 1 0 1.07 12.72 27.79 o 22 1 0 12.80 -8.95 41.45 o 23 1 0 1.72 -9.42 23.55 o 24 1 0 0.08 -9.42 41.92 o 1 2 0 3040.93 3012.98 93.08 o 2 2 0 2228.30 2201.86 70.50 o 3 2 0 167.39 120.25 8.96 o 4 2 0 1356.28 1287.18 32.75 o 5 2 0 574.27 518.15 19.37 o 6 2 0 2520.78 2408.49 57.11 o 7 2 0 38.00 28.27 8.95 o 8 2 0 778.20 806.54 26.44 o 9 2 0 2993.54 3281.42 77.44 o 10 2 0 457.90 559.33 23.58 o 11 2 0 3.35 -3.30 22.14 o 12 2 0 22.91 20.73 11.31 o 13 2 0 79.82 54.65 22.14 o 14 2 0 95.84 114.48 19.79 o 15 2 0 265.20 208.30 74.93 o 16 2 0 237.02 211.11 33.46 o 17 2 0 311.45 336.02 39.59 o 18 2 0 8.60 38.63 22.61 o 19 2 0 268.59 222.42 53.25 o 20 2 0 272.62 403.84 87.65 o 21 2 0 0.44 14.60 31.09 o 22 2 0 1.40 50.40 31.09 o 23 2 0 0.05 -13.66 39.10 o 24 2 0 5.34 45.69 75.84 o 1 3 0 268.22 277.95 16.99 o 2 3 0 10.62 10.36 7.07 o 3 3 0 86.35 85.77 9.43 o 4 3 0 281.43 258.01 11.79 o 5 3 0 26.43 22.14 7.54 o 6 3 0 204.71 203.65 10.84 o 7 3 0 130.43 147.97 9.90 o 8 3 0 1009.80 1017.73 30.71 o 9 3 0 11.03 7.07 12.25 o 10 3 0 102.60 111.67 12.25 o 11 3 0 150.70 192.72 16.49 o 12 3 0 114.83 111.67 16.02 o 13 3 0 218.68 206.41 16.97 o 14 3 0 3.53 -2.36 19.31 o 15 3 0 86.37 73.49 26.38 o 16 3 0 839.02 859.45 41.04 o 17 3 0 1249.75 1242.73 67.02 o 18 3 0 448.98 412.44 41.01 o 19 3 0 21.53 103.63 30.62 o 20 3 0 94.11 100.82 32.04 o 21 3 0 51.93 21.20 28.74 o 22 3 0 73.80 108.82 30.15 o 23 3 0 2.18 -10.83 26.85 o 24 3 0 6.62 8.95 34.39 o 0 4 0 2.86 31.09 21.67 o 1 4 0 7914.95 7891.19 233.66 o 2 4 0 1623.87 1780.37 50.80 o 3 4 0 343.38 314.67 12.74 o 4 4 0 763.63 800.94 21.74 o 5 4 0 1864.08 1804.35 39.37 o 6 4 0 1838.85 1764.66 39.34 o 7 4 0 1161.93 1110.94 28.36 o 8 4 0 2328.88 2352.73 51.21 o 9 4 0 809.19 838.81 24.07 o 10 4 0 835.76 869.88 30.21 o 11 4 0 1.22 -1.88 10.36 o 12 4 0 1821.47 1845.95 51.54 o 13 4 0 91.23 63.13 14.60 o 14 4 0 661.50 659.79 37.73 o 15 4 0 16.01 38.63 19.78 o 16 4 0 118.30 176.68 32.04 o 17 4 0 21.47 37.68 24.02 o 18 4 0 321.10 265.80 27.80 o 19 4 0 2.11 66.89 37.21 o 20 4 0 47.42 65.48 31.56 o 21 4 0 0.48 73.48 29.68 o 22 4 0 1.76 51.81 30.62 o 23 4 0 0.37 40.04 47.10 o 24 4 0 67.14 135.20 38.16 o 1 5 0 95.04 128.65 21.21 o 2 5 0 89.87 77.28 11.78 o 3 5 0 93.19 78.69 8.48 o 4 5 0 2.35 10.36 7.07 o 5 5 0 13.01 19.31 10.36 o 6 5 0 3.00 5.18 8.01 o 7 5 0 72.27 85.28 8.95 o 8 5 0 179.45 184.74 11.78 o 9 5 0 616.56 676.97 21.70 o 10 5 0 540.48 606.98 25.47 o 11 5 0 62.25 81.50 31.09 o 12 5 0 455.79 494.11 25.93 o 13 5 0 525.46 578.55 28.29 o 14 5 0 151.77 182.34 17.90 o 15 5 0 23.72 23.08 17.90 o 16 5 0 47.41 6.12 20.73 o 17 5 0 75.03 26.38 22.14 o 18 5 0 34.63 56.53 20.26 o 19 5 0 7.11 18.37 26.38 o 20 5 0 6.42 53.70 27.32 o 21 5 0 7.84 7.07 26.85 o 22 5 0 0.81 52.29 29.68 o 23 5 0 3.77 16.02 30.62 o 0 6 0 17587.08 18258.22 749.96 o 1 6 0 5023.91 5164.55 160.54 o 2 6 0 890.42 879.26 53.39 o 3 6 0 449.03 467.96 16.04 o 4 6 0 68.59 70.20 8.48 o 5 6 0 261.98 265.40 12.73 o 6 6 0 182.00 163.06 11.31 o 7 6 0 85.17 41.93 9.42 o 8 6 0 140.84 124.40 11.31 o 9 6 0 178.63 162.58 11.78 o 10 6 0 37.78 45.22 13.66 o 11 6 0 0.02 -8.01 12.72 o 12 6 0 398.22 347.90 23.57 o 13 6 0 93.25 66.90 16.49 o 14 6 0 12.15 23.55 20.26 o 15 6 0 223.17 296.87 39.11 o 16 6 0 988.44 1141.70 50.01 o 17 6 0 85.78 107.41 41.46 o 18 6 0 135.08 183.74 25.91 o 19 6 0 0.00 -18.84 18.84 o 20 6 0 46.75 34.86 27.32 o 21 6 0 0.06 -21.20 22.61 o 22 6 0 1.03 -21.67 40.04 o 23 6 0 0.21 61.24 33.92 o 1 7 0 1.95 3.77 21.67 o 2 7 0 50.56 61.72 16.02 o 3 7 0 59.12 59.83 7.54 o 4 7 0 248.46 297.90 13.20 o 5 7 0 144.11 119.69 10.37 o 6 7 0 11.82 23.55 9.42 o 7 7 0 11.34 28.73 8.95 o 8 7 0 1000.17 1084.44 30.22 o 9 7 0 515.16 541.83 20.28 o 10 7 0 66.32 60.30 17.43 o 11 7 0 0.10 -9.89 11.31 o 12 7 0 185.07 164.92 17.43 o 13 7 0 150.70 174.80 24.97 o 14 7 0 150.19 184.70 21.67 o 15 7 0 145.72 137.11 19.79 o 16 7 0 79.39 97.05 21.67 o 17 7 0 351.25 391.64 31.10 o 18 7 0 120.39 154.53 25.91 o 19 7 0 33.04 10.36 22.14 o 20 7 0 18.55 76.78 31.56 o 21 7 0 0.03 24.02 31.09 o 22 7 0 3.76 21.67 76.31 o 23 7 0 0.52 80.55 37.21 o 0 8 0 25.63 51.35 21.20 o 1 8 0 35.01 48.52 27.79 o 2 8 0 77.35 109.30 19.79 o 3 8 0 2059.96 2181.94 54.45 o 4 8 0 1557.99 1644.12 51.07 o 5 8 0 795.12 863.18 24.54 o 6 8 0 296.99 314.87 15.08 o 7 8 0 57.56 68.31 10.84 o 8 8 0 1490.02 1583.41 39.69 o 9 8 0 106.89 124.38 21.67 o 10 8 0 124.62 147.47 16.49 o 11 8 0 0.00 -8.01 11.78 o 12 8 0 151.10 155.01 17.43 o 13 8 0 1353.46 1363.46 44.85 o 14 8 0 1051.84 1040.88 40.11 o 15 8 0 257.94 285.09 30.16 o 16 8 0 671.61 786.48 42.91 o 17 8 0 480.54 484.56 34.88 o 18 8 0 102.89 122.49 26.38 o 19 8 0 44.04 29.21 35.80 o 20 8 0 7.65 32.50 26.85 o 21 8 0 59.53 68.78 37.22 o 22 8 0 6.12 47.58 41.45 o 1 9 0 0.34 23.08 26.38 o 2 9 0 76.30 100.82 34.39 o 3 9 0 112.06 144.18 21.20 o 4 9 0 121.87 127.22 18.38 o 5 9 0 63.21 65.48 14.60 o 6 9 0 161.20 175.29 22.62 o 7 9 0 14.76 8.01 16.02 o 8 9 0 5.90 3.30 14.13 o 9 9 0 0.55 -5.65 18.84 o 10 9 0 52.88 16.49 21.20 o 11 9 0 30.08 24.50 16.49 o 12 9 0 26.28 32.50 33.45 o 13 9 0 21.32 74.90 26.38 o 14 9 0 79.64 110.71 21.20 o 15 9 0 126.00 118.25 22.14 o 16 9 0 98.55 135.68 39.10 o 17 9 0 663.15 645.45 48.09 o 18 9 0 419.98 486.86 90.96 o 19 9 0 87.86 96.10 35.33 o 20 9 0 9.46 -12.72 41.45 o 21 9 0 19.44 -3.77 40.04 o 0 10 0 74.06 100.35 28.74 o 1 10 0 130.36 121.56 23.56 o 2 10 0 128.58 82.93 50.42 o 3 10 0 176.22 163.04 19.79 o 4 10 0 150.61 143.71 21.67 o 5 10 0 477.23 612.94 38.66 o 6 10 0 42.67 63.13 16.49 o 7 10 0 200.23 213.93 28.27 o 8 10 0 1071.44 1167.65 46.25 o 9 10 0 206.23 221.94 30.63 o 10 10 0 317.35 350.65 54.20 o 11 10 0 50.00 29.21 22.61 o 12 10 0 59.64 54.18 24.03 o 13 10 0 17.01 57.94 27.79 o 14 10 0 1195.13 1258.03 69.37 o 15 10 0 29.50 37.21 25.91 o 16 10 0 292.55 300.18 36.76 o 17 10 0 198.78 234.64 56.54 o 18 10 0 17.43 46.63 47.58 o 19 10 0 0.45 -34.86 34.86 o 20 10 0 15.43 -32.97 32.97 o 21 10 0 1.22 34.39 51.81 o 1 11 0 5.32 16.96 17.90 o 2 11 0 0.11 16.96 16.96 o 3 11 0 120.90 95.17 18.37 o 4 11 0 17.98 18.37 14.60 o 5 11 0 0.69 46.16 24.97 o 6 11 0 0.18 7.07 15.54 o 7 11 0 20.94 49.46 18.37 o 8 11 0 5.71 -32.97 32.97 o 9 11 0 69.80 59.36 25.44 o 10 11 0 46.13 26.38 23.08 o 11 11 0 21.18 28.26 21.20 o 12 11 0 9.77 16.02 37.21 o 13 11 0 4.92 -2.83 24.49 o 14 11 0 30.10 40.98 25.44 o 15 11 0 8.47 25.44 41.45 o 16 11 0 78.22 129.55 32.03 o 17 11 0 356.73 436.86 61.74 o 18 11 0 150.70 50.41 49.00 o 19 11 0 37.82 44.28 44.75 o 20 11 0 0.02 -33.44 40.51 o 0 12 0 126.88 123.91 38.63 o 1 12 0 40.75 25.44 24.02 o 2 12 0 163.77 142.30 32.51 o 3 12 0 163.58 217.69 23.56 o 4 12 0 719.92 809.33 39.15 o 5 12 0 820.78 932.57 43.87 o 6 12 0 19.57 27.79 16.02 o 7 12 0 176.83 182.35 21.67 o 8 12 0 1.75 3.77 18.84 o 9 12 0 0.38 -16.49 28.26 o 10 12 0 13.89 86.67 43.34 o 11 12 0 10.65 -22.61 22.61 o 12 12 0 61.89 89.98 31.09 o 13 12 0 47.75 61.24 28.74 o 14 12 0 167.25 131.45 32.04 o 15 12 0 158.57 178.56 33.45 o 16 12 0 152.30 108.83 50.88 o 17 12 0 245.68 142.77 47.59 o 18 12 0 46.50 69.25 52.29 o 19 12 0 4.72 20.25 48.05 o 1 13 0 23.51 44.75 21.20 o 2 13 0 11.53 17.43 18.37 o 3 13 0 16.22 27.79 21.67 o 4 13 0 9.07 32.97 20.73 o 5 13 0 0.85 33.92 19.31 o 6 13 0 3.40 -8.01 22.61 o 7 13 0 4.28 -5.65 22.14 o 8 13 0 61.71 59.36 26.38 o 9 13 0 77.21 71.14 25.91 o 10 13 0 15.84 33.92 26.85 o 11 13 0 0.90 -18.84 18.84 o 12 13 0 0.08 18.84 22.61 o 13 13 0 44.65 29.68 32.98 o 14 13 0 10.07 4.24 35.33 o 15 13 0 0.06 -30.62 34.86 o 16 13 0 9.14 51.34 32.03 o 17 13 0 6.47 98.92 70.66 o 18 13 0 17.79 -39.10 46.16 o 0 14 0 1597.02 1541.33 99.64 o 1 14 0 7.02 -2.36 23.08 o 2 14 0 171.86 203.55 31.10 o 3 14 0 99.23 60.77 20.73 o 4 14 0 20.91 -6.59 21.67 o 5 14 0 42.94 33.92 20.73 o 6 14 0 64.19 75.85 22.61 o 7 14 0 90.48 45.23 24.97 o 8 14 0 50.92 55.59 46.17 o 9 14 0 0.74 24.49 34.39 o 10 14 0 62.67 -0.47 38.63 o 11 14 0 334.85 352.50 41.00 o 12 14 0 46.22 38.16 30.15 o 13 14 0 59.16 73.49 32.03 o 14 14 0 115.80 143.69 73.02 o 15 14 0 194.49 238.88 41.93 o 16 14 0 55.26 -2.83 28.26 o 17 14 0 62.65 12.72 47.11 o 1 15 0 10.69 65.48 32.97 o 2 15 0 64.35 62.65 28.27 o 3 15 0 7.81 4.71 19.78 o 4 15 0 68.78 86.21 24.03 o 5 15 0 17.55 -18.84 18.84 o 6 15 0 0.39 30.15 26.38 o 7 15 0 55.33 41.46 24.97 o 8 15 0 163.91 126.27 31.10 o 9 15 0 1.62 -32.03 32.03 o 10 15 0 9.17 -1.88 55.11 o 11 15 0 8.19 32.50 30.62 o 12 15 0 0.64 -7.07 27.79 o 13 15 0 60.03 97.51 33.92 o 14 15 0 11.90 47.58 94.68 o 15 15 0 1.22 80.55 48.52 o 0 16 0 3.05 42.39 38.15 o 1 16 0 280.13 297.82 37.70 o 2 16 0 294.07 277.09 27.80 o 3 16 0 125.77 63.13 35.33 o 4 16 0 168.34 185.16 41.46 o 5 16 0 240.19 244.08 36.75 o 6 16 0 83.43 72.55 30.15 o 7 16 0 32.04 59.35 46.16 o 8 16 0 20.87 2.36 23.55 o 9 16 0 428.88 419.46 91.43 o 10 16 0 25.63 -26.85 26.85 o 11 16 0 87.94 89.98 62.66 o 12 16 0 27.55 66.42 33.45 o 13 16 0 78.25 142.27 72.55 o 14 16 0 92.27 -21.20 41.93 o 1 17 0 26.22 70.66 23.08 o 2 17 0 18.12 32.97 38.63 o 3 17 0 10.39 -18.84 19.31 o 4 17 0 10.41 59.35 23.55 o 5 17 0 0.82 28.26 28.73 o 6 17 0 14.49 6.59 31.09 o 7 17 0 68.47 16.49 37.69 o 8 17 0 0.46 -36.74 36.74 o 9 17 0 49.76 203.50 63.59 o 10 17 0 28.05 -19.31 32.50 o 11 17 0 3.23 106.93 40.04 o 12 17 0 19.12 170.99 43.81 o 0 18 0 20.98 14.13 27.79 o 1 18 0 161.14 144.64 29.68 o 2 18 0 141.96 133.33 28.27 o 3 18 0 45.43 53.70 27.79 o 4 18 0 36.78 100.81 29.21 o 5 18 0 3.11 10.83 28.26 o 6 18 0 0.02 -20.25 39.10 o 7 18 0 4.54 -19.31 50.40 o 8 18 0 15.94 -20.26 29.21 o 9 18 0 49.30 -18.84 46.17 o 1 19 0 68.74 45.22 56.06 o 2 19 0 17.74 20.73 27.32 o 3 19 0 4.20 24.49 43.34 o 4 19 0 0.06 41.92 36.27 o 5 19 0 16.70 -30.15 42.87 o -24 1 1 64.76 83.85 34.39 o -23 1 1 1.33 -6.59 63.59 o -22 1 1 16.73 9.89 32.50 o -21 1 1 33.20 91.39 34.39 o -20 1 1 224.87 236.07 34.40 o -19 1 1 37.80 61.24 62.65 o -18 1 1 157.97 190.35 49.94 o -17 1 1 647.53 628.10 51.40 o -16 1 1 2.51 21.67 28.73 o -15 1 1 21.39 0.94 34.86 o -14 1 1 18.79 36.74 17.90 o -13 1 1 779.84 794.54 36.80 o -12 1 1 403.48 455.44 25.93 o -11 1 1 214.76 190.87 16.97 o -10 1 1 1555.58 1768.55 47.30 o -9 1 1 52.85 40.04 9.42 o -8 1 1 353.52 398.49 16.98 o -7 1 1 159.15 153.65 15.08 o -6 1 1 0.49 -0.94 7.54 o -5 1 1 414.74 440.37 16.99 o -4 1 1 248.20 212.74 11.32 o -3 1 1 270.07 263.33 10.85 o -2 1 1 13022.21 13197.28 272.99 o -1 1 1 1453.98 1404.41 37.22 o 0 1 1 610.30 606.32 18.95 o 1 1 1 10802.29 10380.78 194.60 o 2 1 1 431.29 475.34 15.12 o 3 1 1 94.51 106.99 11.31 o 4 1 1 58.60 64.55 12.25 o 5 1 1 251.99 277.75 19.33 o 6 1 1 0.19 9.42 25.44 o 7 1 1 869.38 1000.15 44.88 o 8 1 1 191.62 213.98 23.57 o 9 1 1 5250.65 5244.09 203.55 o 10 1 1 110.03 70.68 22.15 o 11 1 1 2124.05 2201.12 66.27 o 12 1 1 73.44 93.28 24.97 o 13 1 1 882.81 830.97 36.81 o 14 1 1 181.88 196.96 35.81 o 15 1 1 242.52 237.98 40.06 o 16 1 1 455.07 484.13 62.23 o 17 1 1 285.56 155.99 28.75 o 18 1 1 62.46 43.81 51.35 o 19 1 1 621.95 543.60 55.16 o 20 1 1 27.31 47.58 31.56 o 21 1 1 6.45 33.92 41.92 o 22 1 1 36.70 28.26 30.15 o 23 1 1 47.41 38.63 44.28 o 24 1 1 77.88 237.90 53.70 o -24 2 1 0.22 10.83 32.03 o -23 2 1 23.38 5.65 32.50 o -22 2 1 4.61 29.68 49.93 o -21 2 1 95.00 148.40 35.33 o -20 2 1 27.25 43.81 27.32 o -19 2 1 199.25 202.61 32.98 o -18 2 1 587.98 499.76 42.90 o -17 2 1 1.49 41.92 82.43 o -16 2 1 226.92 162.10 38.64 o -15 2 1 187.79 192.25 28.74 o -14 2 1 412.45 425.69 30.64 o -13 2 1 1010.10 941.22 40.59 o -12 2 1 436.99 470.56 22.16 o -11 2 1 875.19 872.79 30.21 o -10 2 1 766.57 769.81 27.85 o -9 2 1 3330.06 3564.99 83.22 o -8 2 1 2276.56 2158.19 53.61 o -7 2 1 0.39 8.95 8.95 o -6 2 1 1.39 -5.65 10.36 o -5 2 1 2951.66 2744.95 63.48 o -4 2 1 3318.70 3304.71 73.78 o -3 2 1 10545.85 10335.84 215.86 o -2 2 1 24645.54 24755.06 580.21 o -1 2 1 3512.48 3329.05 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