#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:23:40 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181015 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/95/2209530.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209530_Fobs loop_ _publ_author_name 'Liu, Gang' 'Xu, Chun-Yan' 'Pu, Shou-Zhi' 'Xu, Jing-Kun' _publ_section_title ; 1,2-Bis[5-(2,4-difluorophenyl)-2-methyl-3-thienyl]-3,3,4,4,5,5-hexafluorocyclopent-1-ene: a new photochromic diarylethene compound ; _journal_coeditor_code HG2043 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3028 _journal_page_last o3030 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.505 _cell_angle_beta 94.504 _cell_angle_gamma 92.914 _cell_length_a 11.8727 _cell_length_b 13.1065 _cell_length_c 16.6532 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file hg20431asup2.hkl _cod_data_source_block 1a #BEGIN Tags that were not found in dictionaries: _shelx_title ' 60509B in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 304.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.40 -4.99 3.33 o 2 0 0 7664.47 9928.06 381.02 o 3 0 0 272.81 259.30 37.20 o 4 0 0 10261.66 10813.40 137.15 o 5 0 0 446.44 464.64 25.86 o 6 0 0 227.50 213.32 17.75 o 7 0 0 497.74 433.97 21.77 o 8 0 0 19.81 -16.77 24.33 o 9 0 0 2787.36 2793.01 77.15 o 10 0 0 25.64 -10.83 32.76 o 11 0 0 108.47 66.31 74.11 o 12 0 0 237.92 207.78 86.86 o 13 0 0 62.63 168.01 90.09 o 14 0 0 0.39 -47.76 83.72 o -14 1 0 6.03 113.78 83.91 o -13 1 0 5.47 68.31 78.68 o -12 1 0 25.94 22.93 73.83 o -11 1 0 164.86 163.95 40.16 o -10 1 0 121.91 164.61 36.74 o -9 1 0 5327.16 5307.83 108.55 o -8 1 0 936.70 985.48 46.83 o -7 1 0 1178.42 1130.31 44.87 o -6 1 0 238.74 201.41 26.84 o -5 1 0 7214.94 7386.39 241.88 o -4 1 0 2239.77 2197.26 66.98 o -3 1 0 3182.21 2990.90 60.27 o -2 1 0 8972.46 9220.51 146.03 o -1 1 0 1636.20 1676.97 36.72 o 0 1 0 896.98 631.51 18.36 o 1 1 0 2470.58 1974.74 39.96 o 2 1 0 4164.25 4033.87 73.83 o 3 1 0 2941.48 3008.66 52.98 o 4 1 0 100.47 165.59 15.30 o 5 1 0 84.64 76.00 14.14 o 6 1 0 304.73 393.98 32.09 o 7 1 0 31.80 -13.12 17.23 o 8 1 0 117.11 74.30 30.02 o 9 1 0 132.78 122.33 36.74 o 10 1 0 11.67 43.19 74.11 o 11 1 0 0.09 28.83 71.54 o 12 1 0 177.61 104.46 84.39 o 13 1 0 12.59 -7.04 79.53 o -14 2 0 23.85 123.11 83.72 o -13 2 0 0.28 13.89 72.21 o -12 2 0 17.75 23.66 35.66 o -11 2 0 48.88 95.36 44.14 o -10 2 0 59.42 77.42 55.75 o -9 2 0 15.31 94.60 34.44 o -8 2 0 374.99 428.30 42.10 o -7 2 0 0.60 6.71 22.46 o -6 2 0 971.23 1076.33 42.27 o -5 2 0 1436.26 1430.38 43.59 o -4 2 0 7396.43 7429.66 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4478.78 4718.73 71.57 o 5 3 0 1502.48 1512.24 37.21 o 6 3 0 15.66 4.30 17.37 o 7 3 0 93.06 85.45 26.67 o 8 3 0 2047.26 2127.44 53.00 o 9 3 0 3.91 -70.02 69.93 o 10 3 0 96.84 50.61 79.15 o 11 3 0 163.47 107.12 80.49 o 12 3 0 15.68 5.14 74.30 o 13 3 0 0.10 49.66 80.68 o -13 4 0 73.47 109.88 44.00 o -12 4 0 5.45 -8.93 37.16 o -11 4 0 2.46 7.02 36.37 o -10 4 0 169.37 236.78 43.62 o -9 4 0 235.66 193.03 40.36 o -8 4 0 157.81 108.83 47.62 o -7 4 0 173.39 192.03 35.83 o -6 4 0 412.66 462.34 35.99 o -5 4 0 43.21 68.56 24.00 o -4 4 0 342.45 431.87 29.93 o -3 4 0 1185.11 1023.70 28.26 o -2 4 0 352.96 387.87 37.63 o -1 4 0 8905.12 8114.44 109.30 o 0 4 0 375.15 501.02 26.93 o 1 4 0 782.17 726.74 60.27 o 2 4 0 170.36 145.65 18.17 o 3 4 0 121.35 133.72 19.05 o 4 4 0 2469.58 2520.86 47.61 o 5 4 0 2448.97 2560.91 56.54 o 6 4 0 269.30 272.71 29.14 o 7 4 0 55.90 40.13 23.63 o 8 4 0 987.29 1015.11 53.35 o 9 4 0 11.78 44.24 70.21 o 10 4 0 551.84 756.52 112.45 o 11 4 0 134.57 122.44 82.96 o 12 4 0 6.60 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1000.14 41.05 o 6 7 0 314.28 374.21 47.36 o 7 7 0 236.50 212.60 47.43 o 8 7 0 13.07 66.99 40.83 o 9 7 0 334.62 169.75 50.82 o 10 7 0 41.13 2.95 70.50 o 11 7 0 0.30 23.50 74.40 o 12 7 0 30.99 60.03 76.58 o -12 8 0 25.64 -17.79 51.75 o -11 8 0 3.04 -65.64 45.76 o -10 8 0 68.62 98.85 52.99 o -9 8 0 18.37 28.16 46.43 o -8 8 0 76.91 46.81 51.37 o -7 8 0 391.92 437.82 70.97 o -6 8 0 374.14 390.34 65.74 o -5 8 0 426.31 418.93 42.53 o -4 8 0 94.33 64.69 30.75 o -3 8 0 1926.39 1754.48 61.28 o -2 8 0 59.00 66.72 48.38 o -1 8 0 1772.93 1817.21 61.97 o 0 8 0 102.66 239.59 53.89 o 1 8 0 1799.49 1779.36 59.07 o 2 8 0 87.67 82.63 33.28 o 3 8 0 77.19 46.19 24.30 o 4 8 0 1071.48 957.53 40.22 o 5 8 0 543.38 598.88 42.21 o 6 8 0 41.38 41.98 42.31 o 7 8 0 321.49 355.11 53.47 o 8 8 0 323.28 442.34 56.04 o 9 8 0 110.81 148.83 55.51 o 10 8 0 205.25 261.05 80.20 o 11 8 0 75.61 256.20 87.43 o -11 9 0 20.89 25.97 58.22 o -10 9 0 104.59 120.92 64.03 o -9 9 0 208.82 458.65 84.58 o -8 9 0 269.40 311.10 67.74 o -7 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