#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209562.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209562_Fobs loop_ _publ_author_name 'Kooijman, Huub' 'van Leijen, Monique M.' 'Akkerman, Otto S.' 'Bickelhaupt, Friedrich' 'Spek, Anthony L.' _publ_section_title ; [\h^2^-8-(tert-Butylimino)-1-naphthyl]bis(\h^5^-cyclopentadienyl)titanium(IV) ; _journal_coeditor_code IS2052 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1545 _journal_page_last m1547 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.200 _cell_angle_gamma 90.000 _cell_length_a 15.0891 _cell_length_b 8.4475 _cell_length_c 15.6025 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file is2052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S756A 051092 CD3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 141.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 202.11 226.80 5.96 o 2 0 0 16394.32 16472.39 62.80 o 3 0 0 18726.27 17277.99 82.55 o 4 0 0 64.61 -66.38 66.38 o 5 0 0 671.35 597.85 16.91 o 6 0 0 2224.15 2165.25 29.87 o 7 0 0 2360.67 2452.72 107.36 o 8 0 0 4271.82 4074.27 56.95 o 9 0 0 179.83 144.85 25.13 o 10 0 0 1657.12 1587.81 31.61 o 11 0 0 1113.25 1092.82 31.56 o 12 0 0 1043.50 978.05 32.03 o 13 0 0 1687.88 1589.88 38.61 o 14 0 0 3.67 -0.58 49.72 o 15 0 0 1063.60 993.13 52.75 o 16 0 0 72.79 55.88 35.25 o 17 0 0 149.16 165.53 28.87 o 18 0 0 243.36 278.03 40.46 o 19 0 0 18.31 1.42 37.55 o 1 1 0 12514.78 11900.58 54.05 o 2 1 0 726.88 697.24 9.63 o 3 1 0 6910.84 6819.61 54.11 o 4 1 0 28.13 14.60 12.64 o 5 1 0 34.55 39.23 12.37 o 6 1 0 1459.49 1323.84 20.12 o 7 1 0 2935.98 3005.01 43.56 o 8 1 0 775.10 807.51 26.60 o 9 1 0 22.17 -17.32 29.98 o 10 1 0 81.67 69.24 17.96 o 11 1 0 330.89 262.35 21.32 o 12 1 0 1.35 -27.20 37.71 o 13 1 0 140.88 169.50 22.90 o 14 1 0 342.77 352.66 25.43 o 15 1 0 40.08 31.11 74.13 o 16 1 0 95.71 108.83 31.74 o 17 1 0 181.57 192.69 26.54 o 18 1 0 1.51 36.61 20.36 o 19 1 0 66.57 36.53 29.80 o 0 2 0 362.69 420.66 14.45 o 1 2 0 1595.93 1515.63 20.97 o 2 2 0 3619.85 3398.24 84.41 o 3 2 0 1759.54 1791.14 27.72 o 4 2 0 227.02 256.40 23.17 o 5 2 0 2102.27 2299.39 31.13 o 6 2 0 143.92 150.38 12.27 o 7 2 0 1855.79 1952.35 47.83 o 8 2 0 54.91 83.40 40.38 o 9 2 0 3.91 5.81 15.70 o 10 2 0 0.99 -0.51 32.69 o 11 2 0 30.58 -17.22 35.12 o 12 2 0 7.34 53.75 33.38 o 13 2 0 0.37 -59.77 86.87 o 14 2 0 131.75 92.60 48.80 o 15 2 0 50.82 -28.39 49.47 o 16 2 0 123.10 134.14 27.57 o 17 2 0 0.99 17.53 45.04 o 18 2 0 9.61 59.25 17.79 o 19 2 0 4.06 -17.32 28.28 o 1 3 0 2937.68 2940.61 44.33 o 2 3 0 17.46 -9.19 15.50 o 3 3 0 1191.51 1052.19 29.58 o 4 3 0 366.41 321.32 15.27 o 5 3 0 60.77 45.39 22.95 o 6 3 0 51.99 76.93 13.49 o 7 3 0 99.41 97.81 15.59 o 8 3 0 5.27 37.77 19.56 o 9 3 0 74.52 71.18 40.75 o 10 3 0 8.11 24.44 18.78 o 11 3 0 82.71 30.58 40.93 o 12 3 0 783.40 786.28 42.32 o 13 3 0 1.16 21.99 26.00 o 14 3 0 525.34 498.62 34.12 o 15 3 0 7.25 0.05 42.14 o 16 3 0 164.39 198.50 26.37 o 17 3 0 4.03 3.17 46.57 o 18 3 0 0.50 -34.61 34.61 o 0 4 0 3602.07 3773.24 73.16 o 1 4 0 209.12 193.42 22.72 o 2 4 0 2947.06 2802.39 49.17 o 3 4 0 2346.78 2335.02 39.34 o 4 4 0 3.74 -26.08 26.08 o 5 4 0 4189.41 4103.44 66.16 o 6 4 0 1795.35 1697.60 46.94 o 7 4 0 570.86 561.77 31.44 o 8 4 0 1200.01 1145.75 26.76 o 9 4 0 1.04 -23.07 35.99 o 10 4 0 670.80 685.41 25.55 o 11 4 0 176.90 164.54 23.24 o 12 4 0 69.32 78.22 22.13 o 13 4 0 1153.38 1130.20 33.60 o 14 4 0 1.95 22.57 38.44 o 15 4 0 274.89 300.61 27.49 o 16 4 0 227.75 251.41 38.74 o 17 4 0 50.99 26.70 23.82 o 18 4 0 32.20 -37.98 37.98 o 1 5 0 2554.26 2350.54 33.92 o 2 5 0 884.02 846.99 21.81 o 3 5 0 8.84 -6.23 30.19 o 4 5 0 1375.80 1320.51 26.28 o 5 5 0 78.51 103.28 17.54 o 6 5 0 243.12 221.32 22.70 o 7 5 0 131.62 118.96 19.28 o 8 5 0 24.94 12.96 24.11 o 9 5 0 332.57 351.49 39.71 o 10 5 0 52.87 30.44 51.04 o 11 5 0 172.76 163.49 23.49 o 12 5 0 177.34 175.31 25.27 o 13 5 0 22.10 37.83 27.93 o 14 5 0 197.00 251.61 44.33 o 15 5 0 2.20 15.63 30.09 o 16 5 0 51.88 44.36 27.94 o 17 5 0 10.96 20.33 28.84 o 0 6 0 21.51 50.81 27.42 o 1 6 0 2.25 -7.22 33.90 o 2 6 0 351.93 346.04 30.55 o 3 6 0 375.26 361.22 30.62 o 4 6 0 2.29 -25.48 36.74 o 5 6 0 316.15 304.63 37.10 o 6 6 0 135.93 135.74 34.57 o 7 6 0 268.27 243.49 25.41 o 8 6 0 152.48 132.63 22.65 o 9 6 0 62.01 61.88 34.05 o 10 6 0 33.99 64.68 35.69 o 11 6 0 123.96 95.46 45.00 o 12 6 0 2.02 25.62 39.04 o 13 6 0 4.16 18.70 65.49 o 14 6 0 0.37 -23.82 44.03 o 15 6 0 1.64 -15.85 26.96 o 16 6 0 5.60 -19.48 29.65 o 1 7 0 433.23 413.78 26.15 o 2 7 0 21.08 -25.28 38.08 o 3 7 0 24.13 22.50 26.19 o 4 7 0 1068.76 1006.45 31.01 o 5 7 0 40.85 40.52 49.10 o 6 7 0 168.53 165.33 25.85 o 7 7 0 42.74 41.43 38.37 o 8 7 0 6.93 11.25 54.76 o 9 7 0 124.43 124.36 23.76 o 10 7 0 0.26 39.09 28.77 o 11 7 0 46.68 48.23 24.10 o 12 7 0 15.83 47.35 32.63 o 13 7 0 79.89 89.96 58.71 o 14 7 0 18.69 -54.37 54.37 o 15 7 0 0.24 38.67 23.51 o 0 8 0 739.10 820.45 43.96 o 1 8 0 3.26 31.64 21.15 o 2 8 0 88.53 60.06 29.05 o 3 8 0 1225.00 1244.28 37.55 o 4 8 0 7.13 -3.32 77.93 o 5 8 0 1061.76 976.80 33.55 o 6 8 0 46.88 26.93 55.73 o 7 8 0 156.15 190.49 24.64 o 8 8 0 149.51 142.27 25.34 o 9 8 0 89.35 50.95 30.55 o 10 8 0 165.57 170.47 27.71 o 11 8 0 99.78 127.87 47.24 o 12 8 0 86.82 105.95 32.89 o 13 8 0 91.17 122.07 21.47 o 1 9 0 2.70 29.16 30.92 o 2 9 0 3.67 4.52 30.14 o 3 9 0 1.00 -45.75 45.75 o 4 9 0 305.30 297.97 28.98 o 5 9 0 26.26 -6.55 46.08 o 6 9 0 76.45 29.21 32.95 o 7 9 0 61.80 78.05 26.39 o 8 9 0 38.35 59.01 32.37 o 9 9 0 29.48 28.96 36.34 o 10 9 0 33.63 37.80 21.45 o 11 9 0 33.12 -8.41 32.50 o 0 10 0 13.89 58.26 37.40 o 1 10 0 0.01 -30.20 44.48 o 2 10 0 71.25 73.28 27.39 o 3 10 0 27.10 1.02 32.44 o 4 10 0 3.53 3.13 20.55 o 5 10 0 29.63 23.64 24.27 o 6 10 0 24.94 51.17 25.83 o 7 10 0 12.87 -18.41 29.32 o 8 10 0 0.11 18.98 35.68 o -19 1 1 43.93 70.94 28.75 o -18 1 1 28.86 32.93 60.65 o -17 1 1 30.88 87.47 34.72 o -16 1 1 42.03 54.69 32.04 o -15 1 1 55.27 35.17 59.46 o -14 1 1 659.93 627.04 40.23 o -13 1 1 441.67 456.87 37.25 o -12 1 1 795.78 789.31 36.81 o -11 1 1 1294.64 1212.05 39.93 o -10 1 1 178.72 170.62 24.74 o -9 1 1 1845.89 1874.85 39.34 o -8 1 1 57.33 34.57 18.33 o -7 1 1 4.10 6.71 31.74 o -6 1 1 3870.47 3872.48 70.33 o -5 1 1 3099.32 3077.21 58.86 o -4 1 1 1493.51 1406.81 27.27 o -3 1 1 11406.08 10616.39 95.37 o -2 1 1 2199.42 2185.98 41.13 o -1 1 1 12525.06 12328.07 81.81 o 0 1 1 932.77 1016.40 19.22 o 1 1 1 6287.62 6476.14 59.75 o 2 1 1 11258.21 11396.16 88.21 o 3 1 1 17307.08 16890.61 120.25 o 4 1 1 59.66 35.46 14.75 o 5 1 1 2019.52 2008.96 40.38 o 6 1 1 4667.72 4803.05 87.62 o 7 1 1 2799.93 2813.91 56.03 o 8 1 1 261.86 277.90 22.80 o 9 1 1 1395.19 1433.03 35.17 o 10 1 1 893.57 904.64 34.12 o 11 1 1 597.51 578.01 34.12 o 12 1 1 433.78 400.99 33.23 o 13 1 1 26.95 13.41 56.33 o 14 1 1 141.24 148.27 32.48 o 15 1 1 65.75 19.37 60.35 o 16 1 1 137.04 105.20 35.02 o 17 1 1 19.04 7.15 34.87 o 18 1 1 7.95 -36.73 56.03 o 19 1 1 88.29 101.05 76.52 o -19 2 1 10.25 31.60 33.28 o -18 2 1 220.88 222.47 77.04 o -17 2 1 17.38 -15.50 59.60 o -16 2 1 0.31 -3.58 59.31 o -15 2 1 210.06 247.66 35.76 o -14 2 1 4.92 30.10 52.00 o -13 2 1 1224.70 1199.83 45.60 o -12 2 1 126.77 162.57 29.06 o -11 2 1 760.42 770.09 34.57 o -10 2 1 1191.81 1213.84 38.59 o -9 2 1 612.56 608.71 29.50 o -8 2 1 1833.65 1743.27 36.66 o -7 2 1 194.94 115.33 18.92 o -6 2 1 61.49 105.65 16.99 o -5 2 1 4667.50 4665.96 82.40 o -4 2 1 44.50 69.29 15.50 o -3 2 1 588.10 508.87 18.63 o -2 2 1 83.38 94.47 13.86 o -1 2 1 1245.33 1250.64 26.52 o 0 2 1 51.37 60.35 12.07 o 1 2 1 329.25 368.65 15.20 o 2 2 1 8691.33 8254.13 91.94 o 3 2 1 26.74 14.01 14.75 o 4 2 1 7637.17 7723.65 101.92 o 5 2 1 8407.43 7749.88 106.54 o 6 2 1 329.09 284.46 19.52 o 7 2 1 2550.31 2553.29 50.66 o 8 2 1 1169.11 986.45 31.29 o 9 2 1 118.47 113.69 24.44 o 10 2 1 683.06 650.73 32.93 o 11 2 1 312.21 308.30 30.25 o 12 2 1 176.44 124.13 30.25 o 13 2 1 646.34 625.84 40.08 o 14 2 1 225.18 172.55 35.46 o 15 2 1 349.55 304.73 38.89 o 16 2 1 80.32 121.29 33.23 o 17 2 1 50.80 27.42 64.52 o 18 2 1 75.63 140.68 53.72 o 19 2 1 17.95 57.37 72.72 o -18 3 1 0.99 -50.20 50.20 o -17 3 1 90.23 144.84 38.00 o -16 3 1 10.59 62.88 32.78 o -15 3 1 0.33 51.71 32.93 o -14 3 1 1012.37 1035.92 47.09 o -13 3 1 38.70 -37.70 60.35 o -12 3 1 507.08 519.15 36.81 o -11 3 1 557.58 550.44 34.87 o -10 3 1 143.42 154.08 27.86 o -9 3 1 1104.89 1071.23 37.70 o -8 3 1 725.90 678.74 30.70 o -7 3 1 1324.30 1204.75 32.93 o -6 3 1 4683.81 4688.61 85.98 o -5 3 1 418.31 454.78 21.76 o -4 3 1 5387.48 5019.41 90.60 o -3 3 1 80.80 81.96 16.39 o -2 3 1 449.44 438.54 19.07 o -1 3 1 1121.57 1107.00 24.44 o 0 3 1 88.49 113.99 16.24 o 1 3 1 278.15 251.38 17.88 o 2 3 1 1.73 16.54 15.05 o 3 3 1 925.01 901.96 23.84 o 4 3 1 1605.20 1426.48 28.61 o 5 3 1 68.22 61.39 17.88 o 6 3 1 3492.35 3567.45 70.48 o 7 3 1 2271.14 2246.18 44.85 o 8 3 1 28.28 28.01 22.20 o 9 3 1 417.35 368.65 29.80 o 10 3 1 68.63 75.25 26.67 o 11 3 1 32.68 26.82 28.46 o 12 3 1 445.86 491.73 38.15 o 13 3 1 27.14 -23.54 54.24 o 14 3 1 278.09 262.85 36.95 o 15 3 1 165.90 177.32 36.66 o 16 3 1 67.32 41.42 63.78 o 17 3 1 10.17 36.66 60.20 o 18 3 1 57.26 -0.04 51.84 o -18 4 1 12.66 -29.56 49.42 o -17 4 1 20.90 -4.58 46.10 o -16 4 1 35.83 3.87 71.38 o -15 4 1 1.29 -21.90 62.44 o -14 4 1 10.72 33.23 30.55 o -13 4 1 38.87 57.52 31.14 o -12 4 1 20.63 -31.74 53.79 o -11 4 1 10.11 62.88 28.31 o -10 4 1 120.23 30.85 29.50 o -9 4 1 38.37 31.59 49.77 o -8 4 1 8.60 60.50 24.29 o -7 4 1 404.85 405.16 28.31 o -6 4 1 6.06 26.23 21.76 o -5 4 1 16.89 35.46 20.12 o -4 4 1 108.72 98.20 20.41 o -3 4 1 22.09 16.54 17.58 o -2 4 1 40.26 59.75 17.29 o -1 4 1 55.98 87.92 16.99 o 0 4 1 4.04 -23.84 33.08 o 1 4 1 483.78 486.37 22.20 o 2 4 1 18.48 15.50 16.39 o 3 4 1 14.80 -9.69 17.58 o 4 4 1 18.18 -7.75 36.21 o 5 4 1 538.42 559.38 26.08 o 6 4 1 686.21 647.60 29.50 o 7 4 1 24.78 38.15 23.54 o 8 4 1 104.73 97.75 26.67 o 9 4 1 0.22 -18.33 49.32 o 10 4 1 168.60 181.20 29.95 o 11 4 1 49.59 8.05 56.77 o 12 4 1 70.87 34.87 54.39 o 13 4 1 92.23 78.53 33.23 o 14 4 1 0.32 -27.27 56.47 o 15 4 1 34.64 32.78 35.32 o 16 4 1 35.88 23.84 64.37 o 17 4 1 0.38 -34.16 34.16 o 18 4 1 7.70 4.82 49.41 o -17 5 1 93.16 88.75 28.60 o -16 5 1 79.95 99.48 27.50 o -15 5 1 16.19 -31.29 60.20 o -14 5 1 136.79 156.61 36.95 o -13 5 1 2.06 -32.78 32.78 o -12 5 1 207.92 263.75 35.61 o -11 5 1 317.47 286.10 35.17 o -10 5 1 313.60 315.90 35.61 o -9 5 1 1314.87 1384.90 44.55 o -8 5 1 20.33 -49.92 53.49 o -7 5 1 252.71 281.03 28.91 o -6 5 1 188.40 141.71 28.16 o -5 5 1 63.89 102.22 25.03 o -4 5 1 936.07 927.74 32.63 o -3 5 1 221.72 241.10 25.03 o -2 5 1 230.21 268.52 25.63 o -1 5 1 1075.78 1046.95 31.74 o 0 5 1 31.67 -5.07 42.32 o 1 5 1 2002.11 2070.94 40.83 o 2 5 1 6.63 35.32 20.41 o 3 5 1 1015.17 1077.05 33.53 o 4 5 1 161.69 167.49 25.18 o 5 5 1 8.50 -47.09 47.09 o 6 5 1 33.75 45.00 25.03 o 7 5 1 2.87 29.06 49.77 o 8 5 1 330.01 355.84 31.44 o 9 5 1 283.76 255.85 31.59 o 10 5 1 279.75 300.40 34.57 o 11 5 1 243.19 233.50 33.68 o 12 5 1 38.23 12.67 57.67 o 13 5 1 39.70 5.22 33.23 o 14 5 1 10.43 -66.01 66.01 o 15 5 1 24.12 43.66 35.46 o 16 5 1 3.83 -10.22 54.39 o 17 5 1 79.59 87.04 29.03 o -16 6 1 69.39 109.55 48.13 o -15 6 1 75.40 94.17 84.94 o -14 6 1 0.21 -7.30 35.61 o -13 6 1 81.03 118.76 35.46 o -12 6 1 96.55 100.73 35.17 o -11 6 1 16.61 -55.58 57.82 o -10 6 1 612.72 613.48 39.49 o -9 6 1 163.83 172.26 32.93 o -8 6 1 333.75 371.04 35.46 o -7 6 1 451.00 458.21 33.83 o -6 6 1 17.35 -46.49 57.82 o -5 6 1 1319.06 1285.36 43.21 o -4 6 1 1.91 15.80 52.00 o -3 6 1 161.01 145.29 27.12 o -2 6 1 1050.90 1017.29 36.66 o -1 6 1 0.08 54.39 24.29 o 0 6 1 1093.51 1144.99 37.25 o 1 6 1 263.94 246.31 28.16 o 2 6 1 1504.64 1581.59 42.91 o 3 6 1 251.49 251.83 29.21 o 4 6 1 7.38 6.71 46.79 o 5 6 1 81.41 36.36 28.76 o 6 6 1 1339.94 1217.86 44.26 o 7 6 1 1111.55 1112.96 41.28 o 8 6 1 633.35 616.46 38.89 o 9 6 1 19.45 66.31 30.85 o 10 6 1 905.58 852.34 43.96 o 11 6 1 385.63 314.41 40.23 o 12 6 1 24.72 63.78 33.08 o 13 6 1 44.98 15.05 64.67 o 14 6 1 4.69 -66.16 66.16 o 15 6 1 102.48 116.03 61.91 o 16 6 1 48.44 36.36 55.21 o -15 7 1 23.95 20.84 31.81 o -14 7 1 77.71 21.78 50.94 o -13 7 1 41.84 94.47 36.36 o -12 7 1 24.98 34.72 63.18 o -11 7 1 121.94 131.43 35.91 o -10 7 1 52.99 102.07 33.23 o -9 7 1 405.66 402.77 38.15 o -8 7 1 404.30 407.99 38.59 o -7 7 1 176.14 182.39 34.12 o -6 7 1 1450.00 1339.45 50.37 o -5 7 1 65.74 99.84 31.44 o -4 7 1 551.38 529.73 38.59 o -3 7 1 45.91 35.61 29.36 o -2 7 1 34.06 91.05 27.57 o -1 7 1 724.67 701.09 37.25 o 0 7 1 21.61 -40.23 57.82 o 1 7 1 704.14 717.78 38.44 o 2 7 1 837.32 796.16 39.04 o 3 7 1 560.15 571.01 35.91 o 4 7 1 141.23 111.91 35.17 o 5 7 1 1648.79 1482.35 50.07 o 6 7 1 1029.31 1027.43 47.24 o 7 7 1 467.14 525.86 37.40 o 8 7 1 163.23 76.44 33.53 o 9 7 1 327.63 350.77 38.30 o 10 7 1 30.93 54.69 33.23 o 11 7 1 48.42 104.16 33.83 o 12 7 1 158.55 91.05 40.53 o 13 7 1 21.04 -4.17 70.63 o 14 7 1 92.12 28.70 57.90 o -13 8 1 3.42 -14.92 51.17 o -12 8 1 7.43 -54.77 54.77 o -11 8 1 19.72 -72.42 72.42 o -10 8 1 13.64 15.65 69.29 o -9 8 1 12.53 -34.42 34.42 o -8 8 1 10.27 -63.18 63.18 o -7 8 1 0.18 14.75 33.38 o -6 8 1 13.49 -59.60 61.24 o -5 8 1 191.99 196.25 36.06 o -4 8 1 371.69 343.92 36.51 o -3 8 1 1.96 78.98 29.95 o -2 8 1 1.82 -39.19 56.47 o -1 8 1 4.91 56.03 31.89 o 0 8 1 92.95 53.05 31.74 o 1 8 1 37.95 29.80 57.37 o 2 8 1 49.80 38.00 32.63 o 3 8 1 194.03 181.05 34.12 o 4 8 1 37.60 -6.26 62.58 o 5 8 1 18.68 -22.50 58.86 o 6 8 1 61.05 26.52 61.69 o 7 8 1 39.36 31.89 33.53 o 8 8 1 18.12 62.88 33.38 o 9 8 1 17.76 37.55 61.39 o 10 8 1 9.82 -68.25 68.25 o 11 8 1 0.02 46.94 36.66 o 12 8 1 8.52 -28.42 48.87 o 13 8 1 11.88 42.78 50.43 o -11 9 1 2.76 -49.09 51.26 o -10 9 1 32.27 -8.63 51.63 o 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