#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:23:40 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181015 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/95/2209585.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209585_Fobs loop_ _publ_author_name 'You, Zhong-Lu' 'Chi, Jing-Yun' _publ_section_title ; {2-[2-(Ethylamino)ethyliminomethyl]phenol}{2-[2-(ethylamino)ethyliminomethyl]phenolato}nickel(II) perchlorate ; _journal_coeditor_code LH2064 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1498 _journal_page_last m1500 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.240 _cell_angle_beta 106.140 _cell_angle_gamma 98.450 _cell_length_a 13.8130 _cell_length_b 13.8500 _cell_length_c 13.9790 _exptl_crystal_F_000 1132.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file lh2064Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 332.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 47.27 102.43 6.97 o 2 0 0 576.49 820.40 23.98 o 3 0 0 1498.52 1338.89 38.53 o 4 0 0 4200.84 4648.12 148.28 o 5 0 0 1339.68 1388.41 43.87 o 6 0 0 6703.13 7143.09 182.50 o 7 0 0 723.48 679.61 40.61 o 8 0 0 318.89 401.15 24.44 o 9 0 0 621.33 541.33 48.01 o 10 0 0 3496.56 3487.74 488.33 o 11 0 0 398.05 421.59 43.91 o 12 0 0 82.20 80.26 22.73 o 13 0 0 64.71 46.02 21.08 o 14 0 0 65.37 76.42 29.24 o 15 0 0 73.51 24.40 23.52 o 16 0 0 85.09 89.72 30.56 o -16 1 0 95.81 65.87 28.73 o -15 1 0 6.68 -6.38 27.42 o -14 1 0 253.67 258.44 53.86 o -13 1 0 1500.63 1396.62 105.86 o -12 1 0 459.66 455.38 49.26 o -11 1 0 6.27 16.06 14.78 o -10 1 0 61.09 102.77 21.77 o -9 1 0 126.86 209.95 30.41 o -8 1 0 308.75 266.05 32.33 o -7 1 0 3592.50 3507.04 96.95 o -6 1 0 257.49 330.89 29.70 o -5 1 0 65.89 67.89 8.44 o -4 1 0 5390.56 5275.89 133.15 o -3 1 0 21282.16 20128.56 482.11 o -2 1 0 1.47 9.42 4.27 o -1 1 0 16737.22 19193.79 570.39 o 0 1 0 478.42 478.47 17.03 o 1 1 0 286.88 330.03 11.52 o 2 1 0 1360.07 1360.69 56.61 o 3 1 0 88475.87 88768.95 2098.71 o 4 1 0 29999.32 30394.47 725.71 o 5 1 0 3017.64 3576.68 96.68 o 6 1 0 323.55 312.31 20.67 o 7 1 0 179.06 149.14 20.75 o 8 1 0 180.27 204.69 19.57 o 9 1 0 1772.78 1817.96 157.17 o 10 1 0 261.78 245.56 33.12 o 11 1 0 822.65 737.05 57.99 o 12 1 0 19.46 7.01 15.87 o 13 1 0 776.37 845.06 68.50 o 14 1 0 15.56 -1.59 18.20 o 15 1 0 31.41 32.76 24.66 o -16 2 0 26.21 5.89 22.61 o -15 2 0 163.17 74.69 56.61 o -14 2 0 129.83 175.64 34.98 o -13 2 0 82.23 48.49 39.54 o -12 2 0 208.10 331.00 42.98 o -11 2 0 101.60 141.98 33.26 o -10 2 0 3543.73 3411.55 199.79 o -9 2 0 31.08 23.15 14.67 o -8 2 0 866.15 933.22 43.88 o -7 2 0 68.42 56.26 8.73 o -6 2 0 638.52 473.77 34.09 o -3 2 0 220.56 267.72 18.97 o -2 2 0 11826.94 12731.52 373.68 o -1 2 0 2443.55 2511.94 64.29 o 0 2 0 15323.40 16317.23 469.97 o 1 2 0 263.11 302.39 12.29 o 2 2 0 10252.15 11291.90 340.81 o 3 2 0 718.43 844.92 29.57 o 4 2 0 9944.75 11004.09 271.31 o 5 2 0 522.98 679.76 28.32 o 6 2 0 8587.07 7887.88 202.73 o 7 2 0 3124.62 2837.39 85.13 o 8 2 0 1513.35 1750.40 60.54 o 9 2 0 43.09 35.49 12.93 o 10 2 0 189.24 250.72 36.15 o 11 2 0 3.03 8.76 14.29 o 12 2 0 1249.78 1179.47 70.26 o 13 2 0 30.71 34.76 20.81 o 14 2 0 3.27 4.89 20.31 o 15 2 0 100.60 116.23 30.21 o -16 3 0 18.30 36.59 27.64 o -15 3 0 1.10 -4.40 28.25 o -14 3 0 228.62 230.61 71.32 o -13 3 0 7.23 -10.03 16.19 o -12 3 0 1.98 13.39 16.23 o -11 3 0 1038.29 1141.83 106.45 o -10 3 0 70.66 35.77 17.58 o -9 3 0 51.26 59.87 18.20 o -8 3 0 3366.59 3233.74 154.71 o -7 3 0 6624.41 6625.28 222.28 o -6 3 0 964.13 1152.84 111.25 o -5 3 0 2875.33 2945.52 106.13 o -4 3 0 418.05 355.41 30.30 o -3 3 0 7577.51 8281.66 203.96 o -2 3 0 891.34 942.68 37.26 o -1 3 0 25323.72 28479.94 678.35 o 0 3 0 378.94 293.42 20.00 o 1 3 0 16156.19 16486.01 396.20 o 2 3 0 6482.90 7884.17 194.82 o 3 3 0 29717.59 30433.03 727.46 o 4 3 0 94.53 75.13 10.77 o 5 3 0 30006.50 32615.46 783.09 o 6 3 0 10.47 20.15 8.76 o 7 3 0 99.99 100.03 15.55 o 8 3 0 454.38 522.76 41.54 o 9 3 0 832.14 931.78 46.63 o 10 3 0 90.99 80.51 21.50 o 11 3 0 1753.76 1706.59 85.57 o 12 3 0 23.38 26.87 33.16 o 13 3 0 168.49 227.17 82.80 o 14 3 0 196.17 162.39 34.09 o 15 3 0 56.43 46.67 33.75 o -16 4 0 19.00 35.84 23.27 o -15 4 0 357.03 373.69 59.01 o -14 4 0 112.47 185.72 60.68 o -13 4 0 54.54 51.39 23.31 o -12 4 0 3.04 8.51 15.11 o -11 4 0 975.66 774.56 96.64 o -10 4 0 13.74 9.98 13.51 o -9 4 0 22.87 26.00 13.76 o -8 4 0 2235.75 2424.43 135.98 o -7 4 0 465.78 495.35 38.87 o -6 4 0 1167.31 1072.26 52.50 o -5 4 0 2059.80 2033.19 59.41 o -4 4 0 21047.51 21594.08 518.67 o -3 4 0 1123.27 1453.08 44.26 o -2 4 0 340.47 399.79 17.71 o -1 4 0 1078.97 1329.84 40.02 o 0 4 0 4178.24 4417.74 113.23 o 1 4 0 483.02 455.15 18.63 o 2 4 0 15878.92 16436.11 398.22 o 3 4 0 2184.21 2395.82 68.50 o 4 4 0 3303.17 3683.50 101.35 o 5 4 0 84.48 97.43 13.54 o 6 4 0 9259.69 8953.68 229.91 o 7 4 0 253.00 280.40 24.83 o 8 4 0 1460.69 1459.81 64.03 o 9 4 0 434.70 420.96 32.41 o 10 4 0 396.32 356.85 32.00 o 11 4 0 2.03 39.35 19.08 o 12 4 0 1341.27 1503.91 89.82 o 13 4 0 25.72 20.49 20.08 o 14 4 0 57.99 94.28 35.22 o -16 5 0 2.77 -0.18 23.40 o -15 5 0 142.01 154.17 35.13 o -14 5 0 60.48 32.54 37.28 o -13 5 0 213.01 204.26 36.02 o -12 5 0 378.42 458.04 73.14 o -11 5 0 720.76 709.82 59.31 o -10 5 0 88.95 165.51 28.83 o -9 5 0 645.28 580.75 48.34 o -8 5 0 1815.30 1683.09 78.62 o -7 5 0 3158.50 3596.99 134.90 o -6 5 0 70.49 75.28 9.60 o -5 5 0 2067.86 2057.10 61.32 o -4 5 0 10.11 13.36 8.84 o -3 5 0 629.24 715.00 27.95 o -2 5 0 6648.04 7394.65 186.44 o -1 5 0 20235.20 20028.28 483.10 o 0 5 0 418.22 450.00 19.96 o 1 5 0 2325.55 2908.30 79.84 o 2 5 0 583.28 606.36 25.16 o 3 5 0 250.11 171.80 15.17 o 4 5 0 9.64 14.95 8.36 o 5 5 0 4481.93 3977.52 112.18 o 6 5 0 22.43 49.53 11.82 o 7 5 0 30.23 32.33 11.68 o 8 5 0 33.34 22.89 14.94 o 9 5 0 1599.68 1606.94 62.69 o 10 5 0 14.93 3.37 12.38 o 11 5 0 1343.23 1353.51 95.07 o 12 5 0 11.57 55.23 32.57 o 13 5 0 86.44 70.44 36.01 o -16 6 0 52.15 85.11 32.78 o -15 6 0 305.22 263.52 43.48 o -14 6 0 19.86 31.61 21.61 o -13 6 0 39.47 22.50 19.33 o -12 6 0 47.29 19.85 20.01 o -11 6 0 19.38 42.32 18.73 o -10 6 0 1251.55 1272.60 81.58 o -9 6 0 2447.41 2298.16 144.66 o -8 6 0 4901.99 4553.02 167.93 o -7 6 0 1544.35 1600.49 74.92 o -6 6 0 159.77 174.25 16.93 o -5 6 0 428.52 407.72 27.33 o -4 6 0 6652.26 7307.82 187.68 o -3 6 0 2835.24 3204.66 90.30 o -2 6 0 8506.60 9227.31 231.86 o -1 6 0 886.46 927.92 33.79 o 0 6 0 86.07 72.15 14.33 o 1 6 0 566.67 700.43 28.34 o 2 6 0 5470.66 5199.28 137.18 o 3 6 0 893.38 723.68 30.39 o 4 6 0 1502.54 1421.00 49.54 o 5 6 0 1201.54 1213.61 46.70 o 6 6 0 109.24 123.98 17.39 o 7 6 0 1.36 11.98 10.62 o 8 6 0 2133.95 2343.13 80.20 o 9 6 0 22.10 15.78 13.17 o 10 6 0 75.07 129.20 27.66 o 11 6 0 17.16 11.25 32.08 o 12 6 0 357.09 362.11 68.87 o 13 6 0 12.65 17.07 30.71 o -15 7 0 119.76 153.35 34.62 o -14 7 0 29.49 37.67 22.45 o -13 7 0 20.81 22.87 19.55 o -12 7 0 397.74 320.84 44.38 o -11 7 0 18.60 4.01 15.81 o -10 7 0 745.70 780.79 61.68 o -9 7 0 409.01 408.75 42.72 o -8 7 0 551.94 499.29 45.70 o -7 7 0 2636.14 2585.18 108.06 o -6 7 0 154.38 185.85 26.93 o -5 7 0 7232.29 7735.60 201.23 o -4 7 0 551.94 618.70 29.83 o -3 7 0 1360.13 1516.65 51.35 o -2 7 0 43.64 64.91 12.96 o -1 7 0 3117.63 3251.52 92.41 o 0 7 0 882.88 821.84 33.19 o 1 7 0 10955.16 10903.13 273.25 o 2 7 0 281.01 302.45 26.89 o 3 7 0 180.87 218.79 18.90 o 4 7 0 946.41 1098.90 43.14 o 5 7 0 1455.21 1514.16 55.40 o 6 7 0 49.52 76.98 15.08 o 7 7 0 644.06 771.23 55.67 o 8 7 0 10.67 47.42 18.17 o 9 7 0 182.97 151.44 29.55 o 10 7 0 1.08 14.11 28.16 o 11 7 0 956.68 1019.57 74.76 o 12 7 0 23.64 86.53 41.11 o -15 8 0 83.76 108.70 41.16 o -14 8 0 15.53 23.06 21.96 o -13 8 0 173.84 200.00 37.22 o -12 8 0 37.72 35.13 21.04 o -11 8 0 40.15 41.07 19.63 o -10 8 0 367.04 447.33 48.50 o -9 8 0 1189.27 1070.90 63.79 o -8 8 0 273.84 225.70 32.54 o -7 8 0 5.18 15.22 14.75 o -6 8 0 2232.40 2096.73 68.90 o -5 8 0 1061.77 1115.05 77.84 o -4 8 0 800.87 899.25 37.85 o -3 8 0 647.86 650.27 41.70 o -2 8 0 2054.24 2050.01 65.87 o -1 8 0 20.19 45.25 12.31 o 0 8 0 181.67 218.77 22.59 o 1 8 0 3153.38 3232.58 93.97 o 2 8 0 302.19 355.71 45.77 o 3 8 0 1944.59 1821.70 102.36 o 4 8 0 4363.59 4594.04 164.81 o 5 8 0 31.52 32.17 16.96 o 6 8 0 640.15 760.94 55.75 o 7 8 0 425.00 432.21 45.15 o 8 8 0 779.19 826.51 62.43 o 9 8 0 2.59 29.51 21.19 o 10 8 0 279.54 352.06 105.27 o 11 8 0 4.06 -3.76 28.45 o -15 9 0 24.04 23.12 22.63 o -14 9 0 0.26 24.27 21.34 o -13 9 0 6.50 33.34 22.01 o -12 9 0 12.58 0.73 18.76 o -11 9 0 878.04 862.81 130.19 o -10 9 0 624.84 650.54 86.33 o -9 9 0 1284.81 1454.95 94.04 o -8 9 0 1631.80 1722.67 151.04 o -7 9 0 609.53 729.77 56.27 o -6 9 0 1429.92 1673.21 60.44 o -5 9 0 48.87 75.43 16.40 o -4 9 0 144.23 123.52 16.67 o -3 9 0 927.48 874.68 38.68 o -2 9 0 557.76 518.49 34.32 o -1 9 0 114.61 158.83 17.84 o 0 9 0 389.35 379.19 30.62 o 1 9 0 1934.21 1820.50 75.31 o 2 9 0 1996.57 1787.38 80.51 o 3 9 0 1027.60 1025.62 57.68 o 4 9 0 1509.85 1415.13 71.69 o 5 9 0 267.31 280.12 36.30 o 6 9 0 8.72 9.36 17.13 o 7 9 0 1821.80 1849.69 143.04 o 8 9 0 2.26 -4.83 48.86 o 9 9 0 144.23 191.58 37.28 o 10 9 0 2.21 3.48 23.17 o 11 9 0 185.01 228.10 57.78 o -14 10 0 69.35 89.84 27.52 o -13 10 0 242.91 236.80 41.78 o -12 10 0 205.37 233.23 40.06 o -11 10 0 1.91 -6.54 17.44 o -10 10 0 52.41 26.38 51.95 o -9 10 0 332.68 338.33 43.81 o -8 10 0 425.26 387.18 44.33 o -7 10 0 338.49 310.01 38.18 o -6 10 0 2318.13 2268.58 81.83 o -5 10 0 7.54 -8.69 9.94 o -4 10 0 1043.05 1016.95 44.54 o -3 10 0 1305.19 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282.83 61.07 o 7 11 0 630.54 719.97 65.64 o 8 11 0 52.04 168.45 51.21 o 9 11 0 153.73 115.57 47.09 o -13 12 0 227.57 284.99 46.70 o -12 12 0 82.46 56.18 27.68 o -11 12 0 700.68 799.28 73.67 o -10 12 0 705.42 613.30 61.43 o -9 12 0 0.17 -2.46 18.27 o -8 12 0 7.23 18.58 19.11 o -7 12 0 25.89 13.35 17.93 o -6 12 0 9.00 13.34 29.04 o -5 12 0 323.23 363.53 55.87 o -4 12 0 592.05 631.26 58.18 o -3 12 0 1386.53 1431.11 75.02 o -2 12 0 445.97 372.61 41.78 o -1 12 0 206.27 204.45 32.30 o 0 12 0 83.38 74.20 22.78 o 1 12 0 97.45 60.26 29.14 o 2 12 0 404.26 422.10 52.78 o 3 12 0 687.95 737.41 61.57 o 4 12 0 153.73 144.70 30.38 o 5 12 0 54.76 75.37 24.63 o 6 12 0 342.30 413.00 68.48 o 7 12 0 16.36 -10.99 30.31 o 8 12 0 38.28 59.94 37.18 o -12 13 0 28.75 10.24 27.41 o -11 13 0 0.17 8.46 24.00 o -10 13 0 168.33 206.82 36.87 o -9 13 0 16.42 29.24 38.65 o -8 13 0 321.69 370.35 70.83 o -7 13 0 915.74 867.26 104.19 o -6 13 0 25.86 31.79 32.77 o -5 13 0 122.62 177.63 32.52 o -4 13 0 652.60 678.18 94.08 o -3 13 0 2.64 15.65 18.26 o -2 13 0 198.98 296.29 40.13 o -1 13 0 790.18 760.55 62.50 o 0 13 0 646.61 777.39 107.57 o 1 13 0 22.26 21.40 19.88 o 2 13 0 87.84 105.03 30.66 o 3 13 0 146.35 260.78 40.23 o 4 13 0 10.31 -19.71 18.63 o 5 13 0 219.00 240.96 39.13 o 6 13 0 11.24 30.02 33.26 o 7 13 0 29.83 15.99 36.69 o -11 14 0 251.73 137.25 56.22 o -10 14 0 16.41 -44.15 30.81 o -9 14 0 160.54 133.23 51.51 o -8 14 0 36.25 34.24 39.14 o -7 14 0 153.61 156.38 53.57 o -6 14 0 12.11 13.83 32.08 o -4 14 0 180.54 183.05 34.56 o -3 14 0 150.26 157.98 33.60 o -2 14 0 664.91 718.15 157.51 o -1 14 0 703.81 748.28 64.33 o 0 14 0 19.87 -10.79 18.34 o 1 14 0 67.23 57.33 35.02 o 2 14 0 247.51 297.18 43.95 o 3 14 0 196.47 245.31 41.21 o 4 14 0 15.00 14.47 43.02 o 5 14 0 8.21 -20.21 25.51 o 6 14 0 46.30 -2.85 33.26 o -10 15 0 78.43 70.73 52.39 o -9 15 0 26.59 3.34 37.08 o -8 15 0 155.99 208.67 60.83 o -7 15 0 134.08 108.60 46.01 o -5 15 0 69.85 159.23 47.78 o -4 15 0 186.44 178.18 36.02 o -3 15 0 52.38 51.81 25.40 o -2 15 0 246.42 286.09 43.70 o -1 15 0 117.47 94.62 27.65 o 0 15 0 11.10 32.84 23.52 o 1 15 0 587.35 547.80 132.44 o 2 15 0 208.51 112.01 47.78 o 3 15 0 61.72 16.61 28.06 o 4 15 0 5.91 37.28 42.77 o -8 16 0 60.12 87.02 52.29 o -6 16 0 20.07 30.90 37.28 o -5 16 0 190.41 149.12 53.96 o -4 16 0 66.45 56.92 59.21 o -3 16 0 176.49 166.33 36.09 o -2 16 0 114.96 104.43 33.09 o -1 16 0 7.39 35.70 24.96 o 0 16 0 103.44 100.07 34.88 o 1 16 0 169.44 121.28 35.57 o -2 -16 1 93.17 103.99 56.12 o -1 -16 1 238.21 144.51 52.88 o 0 -16 1 325.56 412.74 94.87 o 1 -16 1 25.00 25.11 23.77 o 2 -16 1 76.17 59.61 37.97 o 3 -16 1 5.10 7.81 23.49 o 4 -16 1 3.71 26.59 31.10 o 5 -16 1 58.24 123.61 50.72 o 7 -16 1 64.03 108.31 50.23 o 8 -16 1 53.48 100.36 48.86 o -4 -15 1 4.49 5.10 42.77 o -3 -15 1 9.35 27.37 41.89 o -2 -15 1 479.74 449.33 79.66 o -1 -15 1 90.63 144.47 33.13 o 0 -15 1 178.14 151.43 44.00 o 1 -15 1 68.12 62.51 25.11 o 2 -15 1 92.57 79.23 27.05 o 3 -15 1 587.57 639.28 61.51 o 4 -15 1 207.54 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