#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209651.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209651_Fobs loop_ _publ_author_name 'Bolte, Michael' _publ_section_title ; {5-[4'-(2,2,5,5-Tetramethyl-3-pyrroline-1-oxyl-3-carbonyl)biphenyl-4-ylethynyl]-2,3,7,8,12,13,17,18-octaethylporphyrinato}copper(II) benzene solvate ; _journal_coeditor_code SG2037 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1609 _journal_page_last m1610 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.325 _cell_angle_beta 82.552 _cell_angle_gamma 89.157 _cell_length_a 12.7494 _cell_length_b 13.1040 _cell_length_c 17.4594 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.8225 _[local]_cod_data_source_file sg2037Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pr3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 319.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 802.78 870.05 63.10 o 4 0 0 594.37 583.96 52.88 o 5 0 0 543.71 508.12 44.04 o 6 0 0 567.03 591.54 39.41 o 7 0 0 972.19 913.57 46.69 o 8 0 0 4543.70 4717.73 181.75 o 9 0 0 161.83 224.91 35.38 o 10 0 0 1659.72 1632.33 105.99 o 11 0 0 468.18 476.05 36.37 o 12 0 0 212.99 256.23 35.01 o 13 0 0 8.08 6.54 29.02 o 14 0 0 208.86 207.09 32.27 o 15 0 0 488.71 535.53 39.79 o -15 1 0 357.58 361.22 35.80 o -14 1 0 9.24 56.03 34.82 o -13 1 0 122.22 95.34 35.26 o -12 1 0 5.36 -32.16 35.89 o -11 1 0 4.04 17.61 34.01 o 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1235.99 1274.57 71.90 o -7 7 0 18.81 28.95 32.71 o -6 7 0 241.67 357.33 45.84 o -5 7 0 477.71 418.20 91.11 o -4 7 0 7268.98 6221.49 60.15 o -3 7 0 774.98 1025.82 50.30 o -2 7 0 1719.51 1642.18 186.52 o -1 7 0 153.61 234.70 39.37 o 0 7 0 58.29 42.47 38.96 o 1 7 0 50.91 83.11 42.72 o 2 7 0 1287.98 1143.92 46.80 o 3 7 0 2743.34 2982.12 54.05 o 4 7 0 1238.00 1333.79 41.69 o 5 7 0 51.31 76.03 33.78 o 6 7 0 1580.22 1554.83 36.61 o 7 7 0 369.50 381.05 32.28 o 8 7 0 5.26 30.61 35.62 o 9 7 0 840.85 702.31 51.28 o 10 7 0 14.55 50.27 36.25 o 11 7 0 20.95 57.18 35.77 o 12 7 0 33.81 66.50 39.96 o 13 7 0 39.17 25.04 39.98 o -13 8 0 93.08 86.46 41.08 o -12 8 0 164.39 146.35 30.77 o -11 8 0 123.88 135.70 31.78 o -10 8 0 412.95 432.52 33.63 o -9 8 0 208.69 193.75 34.34 o -8 8 0 43.69 14.66 30.16 o -7 8 0 3.62 17.05 33.49 o -6 8 0 711.82 736.34 81.34 o -5 8 0 23.00 -16.91 37.47 o -4 8 0 1178.79 1320.78 87.06 o -3 8 0 189.43 242.51 38.28 o -2 8 0 483.22 387.07 44.56 o -1 8 0 4486.32 4703.62 273.79 o 0 8 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