#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/96/2209655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209655_Fobs loop_ _publ_author_name 'Jebas, Samuel Robinson' 'Balasubramanian, Thailampillai' 'Peschar, Rene' 'Fraanje, Jan' _publ_section_title ; Bis(2-aminopyridinium) sulfate ; _journal_coeditor_code SJ2069 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2606 _journal_page_last o2607 _journal_volume 62 _journal_year 2006 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.8730 _cell_length_b 16.8350 _cell_length_c 12.0350 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.7995 _[local]_cod_data_source_file sj2069Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nether in F d d 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 249.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/4, y+1/4, z+1/4' 'x+3/4, -y+3/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/4, y+3/4, z+3/4' 'x+3/4, -y+5/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+3/4, y+1/4, z+3/4' 'x+5/4, -y+3/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+3/4, y+3/4, z+1/4' 'x+5/4, -y+5/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11809.98 9061.10 113.93 o 8 0 0 275.21 286.68 7.71 o 12 0 0 10292.12 9104.20 45.54 o 16 0 0 1020.04 1044.06 9.60 o 2 2 0 1066.33 1427.15 7.06 o 4 2 0 866.62 750.88 7.07 o 6 2 0 552.83 625.61 8.49 o 8 2 0 5332.02 4991.06 26.53 o 10 2 0 2487.95 2289.13 21.68 o 12 2 0 22.54 48.80 7.18 o 14 2 0 117.84 107.29 6.88 o 16 2 0 9.82 7.03 3.54 o 0 4 0 14288.07 15810.60 128.38 o 2 4 0 1856.24 1967.37 9.88 o 4 4 0 9751.46 9901.94 133.53 o 6 4 0 3775.99 4013.18 20.44 o 8 4 0 16.05 16.01 5.18 o 10 4 0 41.55 53.58 6.57 o 12 4 0 1777.96 1642.10 19.71 o 14 4 0 1336.53 1411.54 15.62 o 2 6 0 1755.05 1776.38 11.19 o 4 6 0 625.93 612.72 7.93 o 6 6 0 20406.67 22591.34 271.40 o 8 6 0 146.27 124.29 7.03 o 10 6 0 3565.69 3793.13 28.54 o 12 6 0 79.76 81.46 7.08 o 14 6 0 2168.37 2130.72 17.95 o 0 8 0 6900.95 8402.23 27.58 o 2 8 0 6331.35 7522.45 27.05 o 4 8 0 5941.26 6080.36 26.63 o 6 8 0 101.54 110.83 6.52 o 8 8 0 6893.13 7017.85 36.67 o 10 8 0 1950.72 1937.44 20.70 o 12 8 0 1602.68 1731.11 18.98 o 14 8 0 837.59 789.66 10.14 o 2 10 0 3272.84 3472.57 21.45 o 4 10 0 1504.58 1666.73 16.25 o 6 10 0 11229.63 11585.06 46.13 o 8 10 0 13.99 8.83 6.06 o 10 10 0 3299.43 3267.50 26.91 o 12 10 0 482.21 440.77 9.46 o 14 10 0 1021.29 966.02 9.39 o 0 12 0 957.76 1097.87 14.21 o 2 12 0 767.20 776.86 12.55 o 4 12 0 36.41 45.32 6.47 o 6 12 0 3045.90 3257.20 26.16 o 8 12 0 4907.41 5141.42 33.30 o 10 12 0 0.69 3.23 5.59 o 12 12 0 348.61 340.49 7.55 o 2 14 0 15628.88 17481.41 61.24 o 4 14 0 4.36 17.29 6.06 o 6 14 0 1451.12 1477.30 18.30 o 8 14 0 660.63 639.52 12.14 o 10 14 0 1453.30 1482.26 15.37 o 12 14 0 296.11 286.13 5.24 o 0 16 0 132.26 131.01 8.37 o 2 16 0 309.58 302.18 10.17 o 4 16 0 6803.89 6622.47 37.54 o 6 16 0 36.36 37.21 5.70 o 8 16 0 2447.27 2186.33 18.28 o 10 16 0 308.78 291.62 6.17 o 2 18 0 1028.18 1029.84 14.37 o 4 18 0 2151.02 2079.30 18.51 o 6 18 0 1233.18 1281.29 13.20 o 8 18 0 103.11 111.41 4.36 o 0 20 0 1738.29 1497.98 13.34 o 2 20 0 210.48 187.52 5.91 o 4 20 0 2099.08 1866.29 12.76 o 1 1 1 10309.56 9830.48 74.77 o 3 1 1 58808.52 58094.29 288.26 o 5 1 1 1074.66 1017.68 9.08 o 7 1 1 1178.41 1112.17 11.91 o 9 1 1 694.54 460.77 10.03 o 11 1 1 646.81 553.58 12.49 o 13 1 1 305.64 326.52 9.81 o 15 1 1 2038.99 2036.65 16.56 o 1 3 1 62013.53 76430.16 305.29 o 3 3 1 2905.85 2616.18 11.93 o 5 3 1 26109.19 27102.92 244.15 o 7 3 1 5568.65 5543.40 25.95 o 9 3 1 1492.45 1377.18 16.14 o 11 3 1 1492.86 1408.83 18.04 o 13 3 1 5075.33 5001.30 31.71 o 15 3 1 912.54 944.08 11.38 o 1 5 1 9960.32 10273.84 119.97 o 3 5 1 7618.31 8005.43 23.30 o 5 5 1 2378.76 1995.40 14.16 o 7 5 1 1775.93 2172.81 17.41 o 9 5 1 3822.71 3828.38 27.12 o 11 5 1 1072.94 1003.08 15.60 o 13 5 1 504.89 509.17 10.95 o 15 5 1 740.29 714.61 9.37 o 1 7 1 234.99 368.15 6.01 o 3 7 1 6232.95 6884.62 25.27 o 5 7 1 2105.48 2000.23 15.52 o 7 7 1 4147.09 4173.33 26.03 o 9 7 1 8048.17 8415.84 41.21 o 11 7 1 3002.71 2945.20 25.54 o 13 7 1 1615.03 1632.50 17.08 o 15 7 1 1163.61 1183.84 9.92 o 1 9 1 3079.21 3661.27 20.11 o 3 9 1 1341.27 1525.69 13.93 o 5 9 1 2960.29 3247.42 22.04 o 7 9 1 7155.47 7492.05 37.18 o 9 9 1 708.77 825.90 14.50 o 11 9 1 779.64 763.98 13.58 o 13 9 1 408.04 430.47 8.99 o 1 11 1 84.40 103.79 6.01 o 3 11 1 12030.33 13136.58 46.21 o 5 11 1 5818.71 6099.78 33.52 o 7 11 1 1337.22 1316.44 17.21 o 9 11 1 3695.79 3745.64 28.71 o 11 11 1 717.11 766.04 12.19 o 13 11 1 402.57 376.67 7.09 o 1 13 1 802.52 795.66 13.53 o 3 13 1 2431.69 2505.60 22.81 o 5 13 1 8053.74 8349.05 42.19 o 7 13 1 3688.33 3918.78 29.02 o 9 13 1 2007.25 1858.91 19.11 o 11 13 1 220.10 196.60 6.52 o 1 15 1 4534.29 4751.57 32.53 o 3 15 1 61.47 64.57 7.08 o 5 15 1 4871.70 4834.12 32.30 o 7 15 1 1011.45 1028.07 15.03 o 9 15 1 833.39 857.39 11.94 o 11 15 1 149.70 144.41 4.78 o 1 17 1 1111.53 1156.97 16.22 o 3 17 1 4447.93 4437.30 29.88 o 5 17 1 989.44 947.44 13.90 o 7 17 1 1237.32 1123.13 12.94 o 9 17 1 1697.20 1612.64 12.06 o 1 19 1 1773.30 1639.89 16.17 o 3 19 1 1504.17 1373.35 14.45 o 5 19 1 301.54 269.50 6.89 o 2 0 2 48059.05 46412.02 241.31 o 6 0 2 10080.88 8846.54 29.63 o 10 0 2 1506.57 1458.43 17.84 o 14 0 2 3269.95 2999.90 22.99 o 0 2 2 19912.52 20099.64 138.05 o 2 2 2 46053.21 46413.02 251.20 o 4 2 2 20714.17 18051.72 180.22 o 6 2 2 1190.79 1046.16 10.47 o 8 2 2 6060.53 5437.01 28.57 o 10 2 2 430.53 377.12 9.97 o 12 2 2 3441.67 3259.15 26.92 o 14 2 2 753.45 746.86 12.25 o 2 4 2 54425.95 59294.89 325.08 o 4 4 2 11303.66 11994.53 155.27 o 6 4 2 280.70 299.51 6.58 o 8 4 2 3097.56 3154.66 22.30 o 10 4 2 3694.43 3518.34 27.21 o 12 4 2 166.87 151.66 8.01 o 14 4 2 1672.20 1735.45 16.62 o 0 6 2 22986.91 25452.77 219.52 o 2 6 2 8194.26 8985.62 26.18 o 4 6 2 1253.73 1290.78 11.30 o 6 6 2 1720.23 1971.13 16.48 o 8 6 2 7652.77 7737.68 37.00 o 10 6 2 900.05 822.75 14.10 o 12 6 2 2610.88 2642.24 23.75 o 14 6 2 11.64 12.06 4.82 o 2 8 2 2449.63 2977.84 17.78 o 4 8 2 670.49 653.85 9.78 o 6 8 2 3321.87 3493.52 23.62 o 8 8 2 421.27 456.19 11.20 o 10 8 2 5647.70 5733.60 35.72 o 12 8 2 118.30 125.26 6.57 o 14 8 2 868.64 905.08 10.15 o 0 10 2 7293.15 8436.23 33.10 o 2 10 2 1622.17 1835.01 16.26 o 4 10 2 6196.13 6481.13 32.18 o 6 10 2 873.80 876.44 14.00 o 8 10 2 2399.69 2666.74 24.40 o 10 10 2 454.86 431.51 11.20 o 12 10 2 2577.70 2531.48 20.30 o 14 10 2 65.00 59.80 3.85 o 2 12 2 1338.65 1498.79 16.70 o 4 12 2 5502.77 5737.14 33.48 o 6 12 2 18408.52 19661.45 65.19 o 8 12 2 175.85 185.91 8.37 o 10 12 2 1543.60 1499.45 16.82 o 12 12 2 237.27 253.59 6.52 o 0 14 2 5379.30 5658.76 34.50 o 2 14 2 510.21 534.07 12.13 o 4 14 2 4191.90 4340.97 31.04 o 6 14 2 572.64 575.66 12.54 o 8 14 2 280.37 279.10 8.78 o 10 14 2 224.42 197.11 6.98 o 2 16 2 1819.14 1828.36 20.64 o 4 16 2 268.23 261.26 8.99 o 6 16 2 2092.90 2086.20 19.48 o 8 16 2 504.04 487.14 9.51 o 10 16 2 1275.21 1127.54 9.56 o 0 18 2 9278.15 9095.98 41.23 o 2 18 2 1051.32 970.39 14.32 o 4 18 2 1497.95 1482.78 15.68 o 6 18 2 373.77 362.17 7.76 o 8 18 2 1661.29 1468.06 10.31 o 2 20 2 1426.89 1309.17 12.14 o 4 20 2 172.93 152.09 5.03 o 1 1 3 55996.55 52093.78 278.62 o 3 1 3 27336.76 22977.40 198.32 o 5 1 3 450.04 387.32 6.68 o 7 1 3 606.75 450.51 8.64 o 9 1 3 1964.06 1725.06 18.34 o 11 1 3 8279.07 7657.89 41.43 o 13 1 3 615.48 585.03 12.08 o 15 1 3 245.32 245.13 6.27 o 1 3 3 4608.54 4459.70 15.44 o 3 3 3 32104.93 32586.59 251.81 o 5 3 3 15017.93 14005.45 187.59 o 7 3 3 1904.24 1764.25 15.71 o 9 3 3 117.29 113.86 7.08 o 11 3 3 1526.14 1497.99 18.61 o 13 3 3 300.00 291.86 9.19 o 15 3 3 200.10 188.39 5.86 o 1 5 3 5987.48 5822.18 20.23 o 3 5 3 46783.39 50548.58 354.23 o 5 5 3 3138.69 2991.39 18.55 o 7 5 3 4098.30 4122.89 25.25 o 9 5 3 2969.46 2667.05 23.26 o 11 5 3 101.41 112.05 7.08 o 13 5 3 1353.36 1281.88 15.72 o 15 5 3 852.12 918.75 9.38 o 1 7 3 2617.18 3110.70 16.92 o 3 7 3 1510.76 1730.99 13.63 o 5 7 3 8264.96 8630.62 34.22 o 7 7 3 2057.77 1968.84 18.86 o 9 7 3 711.48 759.01 13.63 o 11 7 3 3337.75 3494.15 27.48 o 13 7 3 902.86 936.45 12.77 o 1 9 3 4741.77 5522.22 26.44 o 3 9 3 4565.15 5019.14 26.50 o 5 9 3 3650.64 3554.44 24.52 o 7 9 3 4561.73 4551.23 29.89 o 9 9 3 2283.01 2237.76 22.64 o 11 9 3 461.67 530.36 11.25 o 13 9 3 552.33 535.94 8.95 o 1 11 3 659.99 697.61 11.62 o 3 11 3 2685.60 2739.91 22.01 o 5 11 3 52.50 86.02 6.98 o 7 11 3 4111.59 4218.31 30.20 o 9 11 3 904.47 956.63 14.92 o 11 11 3 1580.43 1487.57 16.00 o 13 11 3 579.73 530.79 7.51 o 1 13 3 2559.26 2669.14 23.38 o 3 13 3 517.28 566.36 12.08 o 5 13 3 444.22 465.30 11.61 o 7 13 3 82.93 87.36 6.98 o 9 13 3 2715.14 2676.99 22.06 o 11 13 3 1156.33 1141.49 12.17 o 1 15 3 6839.44 6743.23 38.57 o 3 15 3 6538.93 6532.63 37.60 o 5 15 3 546.67 536.61 11.67 o 7 15 3 2113.43 2046.21 19.17 o 9 15 3 1710.16 1547.59 14.67 o 1 17 3 585.32 605.18 12.13 o 3 17 3 626.00 663.34 12.08 o 5 17 3 1034.80 938.64 12.93 o 7 17 3 1393.10 1291.03 13.06 o 1 19 3 670.51 651.03 10.65 o 3 19 3 2320.91 2147.34 16.63 o 5 19 3 1008.17 990.36 10.42 o 0 0 4 10675.02 8286.07 113.66 o 4 0 4 4770.64 3630.24 17.95 o 8 0 4 6992.18 5712.49 31.42 o 12 0 4 1450.25 1398.03 18.09 o 2 2 4 7662.60 6181.90 20.80 o 4 2 4 96.09 97.13 4.26 o 6 2 4 19404.81 18608.63 49.14 o 8 2 4 823.20 745.23 12.45 o 10 2 4 7969.98 7434.94 40.08 o 12 2 4 2147.34 2207.98 22.27 o 14 2 4 1546.40 1543.06 15.38 o 0 4 4 3803.43 3664.89 16.33 o 2 4 4 821.61 953.39 8.97 o 4 4 4 2003.98 1933.30 14.29 o 6 4 4 7859.31 8643.00 34.49 o 8 4 4 730.19 784.97 12.81 o 10 4 4 66.78 57.74 7.08 o 12 4 4 1193.03 1187.00 16.17 o 14 4 4 222.91 225.16 6.78 o 2 6 4 6295.84 6307.92 25.03 o 4 6 4 18380.49 18967.03 246.50 o 6 6 4 7761.96 7420.97 33.84 o 8 6 4 572.21 520.83 11.31 o 10 6 4 1155.08 1162.22 16.53 o 12 6 4 252.46 259.81 8.47 o 14 6 4 1139.75 1152.59 12.02 o 0 8 4 7126.08 7868.46 30.54 o 2 8 4 7999.36 8535.33 33.15 o 4 8 4 12260.33 13237.61 44.44 o 6 8 4 596.49 547.43 11.31 o 8 8 4 5873.30 6050.97 35.91 o 10 8 4 198.52 223.51 8.93 o 12 8 4 2375.31 2401.48 20.39 o 14 8 4 172.41 188.29 5.29 o 2 10 4 4641.60 4526.43 26.90 o 4 10 4 1552.03 1753.67 18.26 o 6 10 4 151.30 158.02 8.42 o 8 10 4 4414.49 4270.10 30.80 o 10 10 4 447.88 470.93 10.79 o 12 10 4 45.20 55.48 5.18 o 0 12 4 5424.48 5522.59 32.64 o 2 12 4 391.42 371.16 10.22 o 4 12 4 3251.67 3517.13 27.22 o 6 12 4 1068.69 1087.20 16.32 o 8 12 4 4485.14 4499.52 30.71 o 10 12 4 58.97 70.52 6.06 o 12 12 4 2380.72 2350.27 14.69 o 2 14 4 4112.36 4034.42 29.73 o 4 14 4 510.63 516.74 11.67 o 6 14 4 4736.36 4754.34 31.20 o 8 14 4 450.04 419.32 9.82 o 10 14 4 452.79 489.09 8.43 o 0 16 4 2663.27 2914.48 25.10 o 2 16 4 3218.45 2961.55 24.89 o 4 16 4 1483.63 1447.59 17.07 o 6 16 4 95.48 97.73 6.16 o 8 16 4 1609.29 1546.70 13.85 o 2 18 4 2946.07 2713.15 20.64 o 4 18 4 15.92 17.65 4.41 o 6 18 4 1303.75 1210.50 11.41 o 0 20 4 605.84 574.27 7.72 o 2 20 4 251.77 189.32 5.14 o 1 1 5 2045.21 2127.35 13.17 o 3 1 5 527.14 403.48 6.79 o 5 1 5 11877.87 10485.74 36.03 o 7 1 5 5560.67 4816.42 28.51 o 9 1 5 878.48 876.76 14.82 o 11 1 5 687.38 686.22 13.63 o 13 1 5 1291.56 1226.50 14.79 o 15 1 5 459.29 449.11 6.58 o 1 3 5 844.16 957.76 9.58 o 3 3 5 18454.51 18426.14 222.00 o 5 3 5 1818.51 1607.94 14.88 o 7 3 5 8554.38 7886.25 36.33 o 9 3 5 8691.86 8470.23 42.60 o 11 3 5 82.37 82.84 7.70 o 13 3 5 1147.77 1213.56 15.04 o 15 3 5 173.89 178.45 4.37 o 1 5 5 18045.88 18394.90 223.57 o 3 5 5 5229.23 4933.93 24.15 o 5 5 5 4486.48 4403.40 25.09 o 7 5 5 795.98 746.09 12.86 o 9 5 5 2897.19 2815.57 24.96 o 11 5 5 1297.75 1237.43 16.69 o 13 5 5 437.03 439.49 9.25 o 1 7 5 6530.14 7148.79 29.77 o 3 7 5 7102.05 6909.52 30.85 o 5 7 5 450.13 437.77 9.92 o 7 7 5 545.55 621.48 12.34 o 9 7 5 3512.52 3683.40 28.74 o 11 7 5 836.04 870.97 13.79 o 13 7 5 237.34 237.40 7.24 o 1 9 5 11284.13 11726.84 43.14 o 3 9 5 1643.14 1625.68 16.98 o 5 9 5 830.67 948.96 14.56 o 7 9 5 849.60 922.02 15.08 o 9 9 5 2100.07 2065.57 21.33 o 11 9 5 1002.46 978.81 13.80 o 13 9 5 914.93 994.57 10.15 o 1 11 5 4438.54 4476.49 29.31 o 3 11 5 1052.36 1124.72 15.91 o 5 11 5 7111.37 7138.80 39.08 o 7 11 5 2164.71 2316.32 22.58 o 9 11 5 293.71 314.81 8.94 o 11 11 5 1557.02 1544.20 14.71 o 1 13 5 809.71 822.10 14.04 o 3 13 5 2510.36 2501.93 23.48 o 5 13 5 2095.60 2208.42 22.06 o 7 13 5 1106.65 1102.92 15.50 o 9 13 5 294.00 305.28 7.96 o 11 13 5 428.40 375.87 6.63 o 1 15 5 2745.87 2661.74 24.28 o 3 15 5 616.99 572.67 12.19 o 5 15 5 885.23 911.04 13.64 o 7 15 5 175.09 167.85 7.03 o 9 15 5 281.34 303.09 6.63 o 1 17 5 1004.25 930.74 13.23 o 3 17 5 439.30 425.35 9.15 o 5 17 5 364.65 390.54 8.22 o 7 17 5 752.00 685.62 8.76 o 1 19 5 2854.67 2702.49 17.15 o 3 19 5 494.28 456.14 7.61 o 2 0 6 9446.44 8391.38 30.30 o 6 0 6 12254.92 10773.18 42.68 o 10 0 6 8186.91 7754.34 41.78 o 14 0 6 779.08 786.93 9.37 o 0 2 6 5602.20 5113.17 23.23 o 2 2 6 4728.00 4534.61 22.66 o 4 2 6 2131.41 1964.80 16.61 o 6 2 6 1334.91 1103.59 14.23 o 8 2 6 5040.84 4956.56 32.54 o 10 2 6 107.14 129.15 7.90 o 12 2 6 1549.70 1519.83 17.38 o 14 2 6 348.65 347.43 7.20 o 2 4 6 5009.01 4512.85 23.29 o 4 4 6 8351.94 8272.52 34.42 o 6 4 6 14479.14 14193.58 50.51 o 8 4 6 3745.24 3424.20 27.42 o 10 4 6 1436.56 1406.72 18.71 o 12 4 6 127.81 137.79 7.24 o 14 4 6 302.88 307.47 6.22 o 0 6 6 11146.98 10539.34 37.84 o 2 6 6 1487.48 1581.48 15.22 o 4 6 6 4933.46 4957.64 28.55 o 6 6 6 1602.24 1520.78 17.69 o 8 6 6 1661.66 1766.85 20.12 o 10 6 6 1053.39 1037.25 15.91 o 12 6 6 906.99 998.48 13.54 o 14 6 6 853.83 962.13 8.56 o 2 8 6 4121.48 4192.96 26.80 o 4 8 6 1803.12 1728.19 18.53 o 6 8 6 1002.90 1085.53 15.70 o 8 8 6 1013.92 1132.21 16.68 o 10 8 6 1653.62 1685.63 18.73 o 12 8 6 1134.16 1206.30 13.14 o 0 10 6 19788.41 21590.48 64.65 o 2 10 6 469.59 504.21 11.25 o 4 10 6 7057.08 7405.29 39.45 o 6 10 6 158.04 171.17 8.06 o 8 10 6 942.94 1001.43 15.18 o 10 10 6 80.82 84.85 6.62 o 12 10 6 1086.24 1102.02 10.57 o 2 12 6 1962.28 2068.53 21.69 o 4 12 6 3463.51 3365.23 27.49 o 6 12 6 22.63 36.69 6.11 o 8 12 6 206.65 192.41 8.01 o 10 12 6 1658.21 1692.66 14.88 o 0 14 6 8559.29 8147.35 42.15 o 2 14 6 190.91 195.83 8.47 o 4 14 6 1130.32 1174.40 16.02 o 6 14 6 170.49 145.35 7.03 o 8 14 6 1278.36 1259.98 13.25 o 10 14 6 67.13 51.44 3.90 o 2 16 6 1011.47 993.59 13.90 o 4 16 6 117.01 104.31 6.21 o 6 16 6 1036.30 982.04 11.54 o 8 16 6 2.44 -3.44 3.44 o 0 18 6 71.85 76.53 5.54 o 2 18 6 94.15 86.40 5.49 o 4 18 6 1154.68 1102.82 10.58 o 1 1 7 420.48 394.38 8.38 o 3 1 7 174.03 242.15 7.39 o 5 1 7 4546.57 4303.05 27.26 o 7 1 7 4327.74 3978.64 29.40 o 9 1 7 3670.13 3633.24 28.76 o 11 1 7 1227.17 1226.70 16.38 o 13 1 7 428.24 412.86 8.07 o 1 3 7 7.51 13.50 4.82 o 3 3 7 1297.82 1218.00 14.07 o 5 3 7 3436.03 3466.13 25.18 o 7 3 7 2507.90 2453.25 23.33 o 9 3 7 4550.63 4780.75 33.47 o 11 3 7 1825.19 1901.05 19.46 o 13 3 7 233.23 244.29 6.68 o 1 5 7 798.54 667.00 11.06 o 3 5 7 1249.47 1303.90 15.05 o 5 5 7 2070.48 1846.24 18.96 o 7 5 7 158.09 233.08 9.19 o 9 5 7 931.03 1071.04 16.67 o 11 5 7 326.57 312.90 9.35 o 13 5 7 227.16 225.04 6.22 o 1 7 7 2319.80 2360.18 20.48 o 3 7 7 5990.75 5525.02 32.03 o 5 7 7 8725.38 9223.41 43.93 o 7 7 7 7561.87 7704.28 41.55 o 9 7 7 1790.32 1843.46 20.44 o 11 7 7 224.40 283.79 8.47 o 13 7 7 491.39 497.24 7.15 o 1 9 7 7969.82 8050.83 40.16 o 3 9 7 8181.57 8541.45 42.12 o 5 9 7 1088.08 1070.08 16.17 o 7 9 7 356.77 356.11 10.07 o 9 9 7 187.56 201.99 7.70 o 11 9 7 243.74 296.52 7.45 o 1 11 7 2445.70 2621.92 24.20 o 3 11 7 949.59 930.02 15.08 o 5 11 7 163.12 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9 832.38 805.70 14.05 o 11 1 9 493.31 501.34 9.41 o 1 3 9 102.92 101.28 7.39 o 3 3 9 455.28 496.53 11.87 o 5 3 9 4284.07 4128.93 30.95 o 7 3 9 2516.49 2494.96 24.26 o 9 3 9 966.52 1002.36 14.77 o 11 3 9 1129.04 1140.81 12.88 o 1 5 9 5967.47 5943.69 35.41 o 3 5 9 3974.05 3848.24 29.20 o 5 5 9 903.64 950.63 15.85 o 7 5 9 4688.71 4812.33 33.22 o 9 5 9 154.86 188.06 7.96 o 11 5 9 481.40 517.70 9.15 o 1 7 9 1906.49 1838.71 20.86 o 3 7 9 1271.17 1248.43 17.62 o 5 7 9 1380.84 1385.33 18.61 o 7 7 9 677.15 735.55 13.83 o 9 7 9 290.96 272.24 8.53 o 11 7 9 652.28 730.93 9.11 o 1 9 9 3167.54 3166.66 27.00 o 3 9 9 5170.41 5388.41 34.99 o 5 9 9 574.23 643.63 12.65 o 7 9 9 255.09 248.01 8.78 o 9 9 9 1224.46 1318.19 13.92 o 1 11 9 1524.39 1531.36 18.72 o 3 11 9 935.89 1019.67 15.29 o 5 11 9 1576.70 1546.76 17.54 o 7 11 9 1406.08 1579.97 15.73 o 9 11 9 318.84 340.06 6.94 o 1 13 9 1654.81 1621.42 17.91 o 3 13 9 180.61 183.15 7.29 o 5 13 9 488.21 567.24 10.18 o 7 13 9 197.57 207.80 5.91 o 1 15 9 406.28 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12 10 342.13 349.90 8.32 o 6 12 10 936.71 1036.30 11.44 o 0 14 10 1813.26 1881.33 15.82 o 2 14 10 41.26 43.57 4.93 o 4 14 10 929.47 940.83 10.05 o 1 1 11 1898.39 1766.46 20.65 o 3 1 11 983.59 965.33 15.54 o 5 1 11 1753.54 1714.27 20.18 o 7 1 11 614.65 536.36 11.06 o 9 1 11 901.49 832.48 11.28 o 1 3 11 30.55 25.04 7.03 o 3 3 11 4077.12 4132.38 31.08 o 5 3 11 180.61 171.54 8.52 o 7 3 11 644.32 631.37 11.67 o 9 3 11 637.25 689.51 10.39 o 1 5 11 4886.08 4924.09 33.40 o 3 5 11 944.33 1010.59 16.01 o 5 5 11 1686.56 1720.83 19.14 o 7 5 11 804.36 781.26 12.40 o 9 5 11 109.01 102.06 5.24 o 1 7 11 1731.52 1799.81 20.38 o 3 7 11 1412.77 1427.28 17.94 o 5 7 11 58.79 76.83 6.47 o 7 7 11 372.66 420.18 9.40 o 9 7 11 1103.57 1184.14 10.53 o 1 9 11 1215.63 1336.25 16.85 o 3 9 11 1665.54 1772.71 18.42 o 5 9 11 606.60 640.02 10.95 o 7 9 11 229.93 257.85 6.93 o 1 11 11 127.01 140.97 6.93 o 3 11 11 255.36 253.89 7.96 o 5 11 11 1283.35 1372.01 13.00 o 7 11 11 494.53 498.51 6.43 o 1 13 11 437.67 457.38 8.02 o 3 13 11 527.40 565.14 7.97 o 0 0 12 3098.77 2810.58 25.39 o 4 0 12 3001.90 2915.19 23.94 o 8 0 12 18.26 20.83 4.62 o 2 2 12 1427.39 1346.56 17.94 o 4 2 12 790.35 778.16 13.22 o 6 2 12 1108.27 1108.10 14.01 o 8 2 12 96.87 84.70 5.13 o 0 4 12 6297.46 5991.86 35.87 o 2 4 12 169.43 184.88 8.47 o 4 4 12 2030.25 2021.33 20.05 o 6 4 12 7.31 15.91 4.82 o 8 4 12 774.97 792.09 9.37 o 2 6 12 1005.73 1039.76 15.03 o 4 6 12 1042.25 1062.08 14.47 o 6 6 12 562.20 553.61 9.77 o 8 6 12 60.49 61.44 4.26 o 0 8 12 414.58 371.18 9.46 o 2 8 12 372.93 373.04 8.99 o 4 8 12 411.84 446.67 9.46 o 6 8 12 129.94 128.98 5.39 o 2 10 12 1150.88 1272.75 13.56 o 4 10 12 658.06 694.28 9.47 o 6 10 12 2227.74 2403.26 12.80 o 0 12 12 152.87 162.28 5.49 o 2 12 12 498.11 527.18 7.51 o 1 1 13 1973.26 1790.43 18.39 o 3 1 13 620.62 575.26 10.44 o 5 1 13 480.20 421.14 8.48 o 7 1 13 82.76 80.44 4.62 o 1 3 13 2322.08 2223.86 19.92 o 3 3 13 1608.50 1654.27 16.67 o 5 3 13 501.74 507.42 9.00 o 7 3 13 164.64 135.22 5.08 o 1 5 13 520.22 486.04 9.87 o 3 5 13 514.05 497.74 9.82 o 5 5 13 159.96 167.24 5.75 o 7 5 13 491.00 477.51 6.54 o 1 7 13 478.28 445.99 8.95 o 3 7 13 217.18 222.96 6.42 o 5 7 13 1666.08 1671.10 12.62 o 1 9 13 372.70 404.95 7.50 o 3 9 13 73.15 80.90 4.41 o 2 0 14 6179.90 5582.39 25.83 o 0 2 14 977.09 880.00 11.08 o 2 2 14 180.58 174.75 6.16 o 4 2 14 495.36 468.71 7.41 o 2 4 14 1069.28 1058.16 11.08 o 4 4 14 46.68 39.62 3.80 o 0 6 14 443.48 437.88 7.35 o 2 6 14 71.07 66.06 4.31 o 1 1 15 772.38 650.49 7.42 o