#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/96/2209661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209661_Fobs loop_ _publ_author_name 'Zora, Metin' 'Turgut, G\"unseli' 'Odaba\,so\(glu, Mustafa' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; 2-Pyridiniohydrazinium dichloride ; _journal_coeditor_code SJ2084 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2677 _journal_page_last o2679 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.179 _cell_angle_gamma 90.000 _cell_length_a 7.3787 _cell_length_b 8.5682 _cell_length_c 12.6369 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file sj2084Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\OMUS25_DENE\OMUS25' _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.60 6.71 2.19 o 4 0 0 268.59 287.28 6.72 o 6 0 0 418.17 419.50 4.28 o 8 0 0 302.53 295.77 4.21 o 1 1 0 1924.28 1721.98 7.70 o 2 1 0 6981.40 6754.40 200.45 o 3 1 0 298.90 304.78 3.22 o 4 1 0 73.98 69.64 1.52 o 5 1 0 1170.45 1159.37 37.16 o 6 1 0 98.03 91.99 2.65 o 7 1 0 4.18 5.80 1.65 o 8 1 0 24.51 23.27 2.19 o 9 1 0 28.27 28.04 2.45 o 0 2 0 1776.76 1668.39 10.42 o 1 2 0 1092.01 1146.42 12.58 o 2 2 0 342.57 342.15 9.65 o 3 2 0 2147.24 2160.03 39.21 o 4 2 0 38.36 37.65 1.93 o 5 2 0 42.71 36.64 1.83 o 6 2 0 310.41 317.69 10.55 o 7 2 0 382.29 376.36 5.75 o 8 2 0 0.32 1.45 2.34 o 1 3 0 356.07 394.51 8.14 o 2 3 0 698.93 662.65 6.14 o 3 3 0 135.93 125.30 1.81 o 4 3 0 419.71 415.45 5.17 o 5 3 0 189.05 189.01 3.84 o 6 3 0 7.73 8.94 1.66 o 7 3 0 11.80 16.50 2.55 o 8 3 0 45.81 38.88 2.39 o 0 4 0 532.40 468.96 3.10 o 1 4 0 1037.73 1082.13 3.86 o 2 4 0 0.61 1.01 1.16 o 3 4 0 539.12 548.84 2.69 o 4 4 0 12.38 18.65 1.50 o 5 4 0 3.53 4.05 1.39 o 6 4 0 1.68 1.67 1.42 o 7 4 0 28.64 27.31 2.19 o 8 4 0 17.10 17.50 2.34 o 1 5 0 222.10 244.00 2.95 o 2 5 0 50.61 57.18 1.85 o 3 5 0 153.24 165.96 2.34 o 4 5 0 1282.07 1286.58 18.42 o 5 5 0 28.71 29.45 1.58 o 6 5 0 103.74 110.64 8.41 o 7 5 0 10.57 8.59 2.13 o 8 5 0 104.68 97.11 3.16 o 0 6 0 86.65 89.62 1.81 o 1 6 0 310.17 312.12 3.00 o 2 6 0 452.00 479.78 7.38 o 3 6 0 12.94 13.59 2.21 o 4 6 0 7.77 8.63 1.50 o 5 6 0 19.11 19.50 2.20 o 6 6 0 454.58 438.33 3.81 o 7 6 0 0.44 0.04 2.80 o 1 7 0 658.74 641.15 17.99 o 2 7 0 153.98 139.02 5.15 o 3 7 0 637.85 682.74 7.00 o 4 7 0 118.76 119.83 5.07 o 5 7 0 33.31 32.60 5.21 o 6 7 0 1.14 0.00 2.22 o 0 8 0 157.44 145.33 3.06 o 1 8 0 427.90 437.52 10.81 o 2 8 0 358.77 377.42 6.97 o 3 8 0 373.78 355.60 7.77 o 4 8 0 51.16 38.61 2.73 o 5 8 0 12.01 10.71 2.29 o 1 9 0 0.01 1.64 1.59 o 2 9 0 3.57 4.70 1.70 o 3 9 0 22.16 21.55 1.89 o 4 9 0 167.33 198.68 11.65 o 0 10 0 52.66 43.35 2.92 o 1 10 0 3.87 4.24 1.81 o 2 10 0 52.62 60.58 2.10 o -9 0 1 65.73 57.54 3.40 o -7 0 1 19.39 21.10 2.46 o -5 0 1 305.90 288.83 15.47 o -3 0 1 92.70 80.23 2.18 o -1 0 1 835.85 779.39 6.87 o 3 0 1 783.15 763.53 6.26 o 5 0 1 42.15 43.70 2.51 o 7 0 1 197.54 188.54 3.37 o 9 0 1 22.39 18.45 3.58 o -9 1 1 14.91 14.75 2.39 o -8 1 1 90.24 89.53 2.36 o -7 1 1 238.58 240.57 9.73 o -6 1 1 234.48 238.59 6.18 o -5 1 1 3.53 6.68 1.14 o -4 1 1 578.03 609.04 8.13 o -3 1 1 149.69 158.68 2.06 o -2 1 1 3110.38 3182.66 49.53 o -1 1 1 64.06 47.64 2.17 o 0 1 1 307.09 301.27 4.54 o 1 1 1 297.47 341.44 4.56 o 2 1 1 6174.49 6041.37 15.84 o 3 1 1 16.60 18.41 1.91 o 4 1 1 194.61 182.43 2.49 o 5 1 1 572.49 542.06 3.33 o 6 1 1 100.20 104.75 2.15 o 7 1 1 62.39 57.38 2.13 o 8 1 1 320.21 317.20 3.41 o -8 2 1 2.84 1.13 1.97 o -7 2 1 11.61 12.66 1.65 o -6 2 1 0.69 0.84 1.37 o -5 2 1 1.30 1.10 1.46 o -4 2 1 1787.90 1781.00 20.61 o -3 2 1 2070.37 1967.27 7.70 o -2 2 1 925.82 899.93 4.90 o -1 2 1 661.21 677.42 3.99 o 0 2 1 599.14 776.92 6.48 o 1 2 1 48.78 61.58 3.76 o 2 2 1 1707.76 1732.55 27.97 o 3 2 1 193.16 199.94 6.99 o 4 2 1 103.44 95.69 1.58 o 5 2 1 291.78 276.46 4.68 o 6 2 1 310.11 307.35 2.84 o 7 2 1 0.21 0.45 2.08 o 8 2 1 14.23 14.24 2.19 o -8 3 1 208.19 198.77 3.47 o -7 3 1 423.07 446.25 17.22 o -6 3 1 8.39 7.18 1.36 o -5 3 1 386.13 377.29 14.31 o -4 3 1 64.69 72.25 1.62 o -3 3 1 8.10 10.88 2.08 o -2 3 1 835.36 864.67 11.46 o -1 3 1 2122.84 2157.58 26.53 o 0 3 1 3950.14 3935.44 7.40 o 1 3 1 9066.41 8604.63 101.83 o 2 3 1 1473.75 1601.46 20.21 o 3 3 1 228.07 260.08 5.05 o 4 3 1 157.67 168.32 4.85 o 5 3 1 566.89 572.78 3.74 o 6 3 1 358.09 349.22 3.23 o 7 3 1 32.46 31.12 2.64 o 8 3 1 0.17 -1.92 2.68 o -8 4 1 46.72 46.25 2.42 o -7 4 1 195.55 210.81 10.54 o -6 4 1 151.06 157.34 5.52 o -5 4 1 165.73 164.85 4.41 o -4 4 1 152.27 171.06 2.16 o -3 4 1 783.61 808.02 12.54 o -2 4 1 231.21 274.94 3.08 o -1 4 1 800.78 862.84 10.46 o 0 4 1 35.62 23.93 1.25 o 1 4 1 293.85 289.21 2.45 o 2 4 1 381.28 349.39 2.37 o 3 4 1 1682.65 1732.88 99.12 o 4 4 1 975.99 1033.54 16.71 o 5 4 1 329.91 329.74 3.03 o 6 4 1 433.69 434.41 3.52 o 7 4 1 2.26 2.11 2.51 o 8 4 1 11.40 9.89 2.32 o -8 5 1 3.92 4.14 2.83 o -7 5 1 14.20 15.96 1.69 o -6 5 1 82.82 91.59 1.64 o -5 5 1 228.59 218.64 2.53 o -4 5 1 65.49 71.17 1.63 o -3 5 1 192.84 172.35 2.59 o -2 5 1 172.22 167.79 3.95 o -1 5 1 3949.74 3955.79 42.76 o 0 5 1 0.59 0.84 1.01 o 1 5 1 3.75 33.72 13.51 o 2 5 1 198.90 197.34 2.45 o 3 5 1 103.49 123.70 2.98 o 4 5 1 198.35 214.99 3.11 o 5 5 1 25.48 24.15 2.42 o 6 5 1 5.45 3.33 1.97 o 7 5 1 197.71 197.59 2.90 o -7 6 1 20.16 19.70 3.49 o -6 6 1 177.36 198.38 5.78 o -5 6 1 37.72 38.06 2.56 o -4 6 1 8.42 8.38 1.49 o -3 6 1 1511.79 1505.14 33.97 o -2 6 1 32.06 31.91 1.74 o -1 6 1 344.60 333.99 3.23 o 0 6 1 76.50 72.94 1.56 o 1 6 1 549.54 548.98 11.05 o 2 6 1 267.18 258.23 2.47 o 3 6 1 14.84 16.30 1.66 o 4 6 1 122.75 119.45 2.79 o 5 6 1 244.89 249.99 2.86 o 6 6 1 10.54 13.15 2.07 o 7 6 1 1.19 1.81 2.32 o -6 7 1 0.90 1.88 1.58 o -5 7 1 109.42 101.32 8.32 o -4 7 1 246.73 276.31 5.99 o -3 7 1 36.49 36.75 1.33 o -2 7 1 48.85 50.48 1.65 o -1 7 1 625.96 638.12 10.94 o 0 7 1 221.06 217.85 3.05 o 1 7 1 0.91 3.07 1.30 o 2 7 1 488.08 494.81 2.82 o 3 7 1 84.37 84.34 2.13 o 4 7 1 94.13 93.80 2.35 o 5 7 1 0.01 1.65 2.05 o 6 7 1 103.93 93.31 2.57 o -5 8 1 10.84 9.62 1.60 o -4 8 1 304.81 294.86 4.96 o -3 8 1 130.22 131.07 1.74 o -2 8 1 159.34 148.46 5.92 o -1 8 1 219.58 217.40 4.85 o 0 8 1 71.08 67.37 2.55 o 1 8 1 76.82 75.34 1.78 o 2 8 1 28.75 29.34 2.14 o 3 8 1 220.75 225.64 2.39 o 4 8 1 355.29 341.72 3.61 o 5 8 1 28.86 31.23 2.88 o -4 9 1 7.24 9.75 1.60 o -3 9 1 94.53 96.11 2.58 o -2 9 1 269.14 256.40 7.93 o -1 9 1 644.80 654.85 16.49 o 0 9 1 95.04 90.80 2.75 o 1 9 1 14.31 17.03 1.64 o 2 9 1 2.32 3.15 1.91 o 3 9 1 26.02 27.75 1.88 o 4 9 1 16.94 14.93 2.27 o -2 10 1 3.93 6.42 2.09 o -1 10 1 73.74 69.64 2.23 o 0 10 1 134.60 128.96 2.31 o 1 10 1 31.00 29.29 2.11 o 2 10 1 16.93 18.57 2.01 o -8 0 2 72.04 75.51 3.47 o -6 0 2 1374.55 1363.20 30.95 o -4 0 2 4054.52 3986.22 48.64 o -2 0 2 4768.29 4429.91 72.76 o 0 0 2 116.58 121.19 3.89 o 4 0 2 80.52 74.02 2.86 o 6 0 2 879.40 891.72 5.69 o 8 0 2 42.02 37.52 3.28 o -9 1 2 15.24 16.44 2.80 o -8 1 2 1.07 2.64 1.68 o -7 1 2 39.36 40.31 1.45 o -6 1 2 508.82 520.39 6.96 o -5 1 2 79.52 84.78 1.90 o -4 1 2 1061.25 1044.13 9.56 o -3 1 2 935.78 950.92 4.64 o -2 1 2 210.73 208.12 2.57 o -1 1 2 699.45 777.70 3.71 o 0 1 2 616.34 578.62 5.05 o 1 1 2 33.47 16.65 3.72 o 2 1 2 2510.16 2396.53 13.91 o 3 1 2 1985.13 2043.49 8.27 o 4 1 2 1636.59 1726.10 6.82 o 5 1 2 74.32 73.29 4.75 o 6 1 2 6.91 8.40 1.76 o 7 1 2 79.79 80.56 2.21 o 8 1 2 19.53 20.62 2.25 o -8 2 2 9.55 9.39 1.64 o -7 2 2 26.05 25.01 1.63 o -6 2 2 146.99 150.15 1.69 o -5 2 2 16.67 19.38 1.19 o -4 2 2 156.67 160.01 1.82 o -3 2 2 230.27 257.47 2.92 o -2 2 2 67.87 77.51 2.24 o -1 2 2 5740.04 5567.87 28.74 o 0 2 2 4217.09 3983.97 34.77 o 1 2 2 3941.49 3690.92 77.92 o 2 2 2 1090.99 1054.93 10.99 o 3 2 2 1164.13 1141.83 37.35 o 4 2 2 653.07 697.13 4.78 o 5 2 2 10.41 10.67 1.70 o 6 2 2 17.55 19.25 1.59 o 7 2 2 1.57 0.47 1.62 o 8 2 2 42.97 40.22 2.00 o -8 3 2 61.20 61.80 1.79 o -7 3 2 5.67 7.21 1.64 o -6 3 2 93.90 96.70 1.83 o -5 3 2 643.88 653.08 9.12 o -4 3 2 254.55 265.78 7.21 o -3 3 2 554.70 541.90 16.62 o -2 3 2 2687.84 2630.91 23.72 o -1 3 2 1397.19 1464.09 32.50 o 0 3 2 2.73 6.15 1.59 o 1 3 2 1016.57 1042.31 3.89 o 2 3 2 345.96 358.94 3.79 o 3 3 2 845.16 867.87 18.70 o 4 3 2 289.04 268.51 2.88 o 5 3 2 13.63 13.87 2.22 o 6 3 2 0.44 3.76 2.32 o 7 3 2 20.32 20.46 2.61 o 8 3 2 98.20 94.55 2.70 o -8 4 2 22.61 21.41 2.04 o -7 4 2 404.23 420.91 14.95 o -6 4 2 34.73 35.46 3.60 o -5 4 2 267.50 273.05 2.42 o -4 4 2 351.49 377.02 3.84 o -3 4 2 1371.88 1355.38 14.90 o -2 4 2 1631.07 1703.20 28.66 o -1 4 2 5.46 8.31 1.24 o 0 4 2 4.76 12.99 1.20 o 1 4 2 103.03 125.14 5.93 o 2 4 2 2.11 8.20 1.48 o 3 4 2 432.82 451.92 5.56 o 4 4 2 127.29 138.94 2.45 o 5 4 2 339.38 351.63 3.15 o 6 4 2 84.80 83.19 2.82 o 7 4 2 161.05 153.79 2.74 o 8 4 2 11.60 13.96 2.36 o -7 5 2 10.34 12.13 1.70 o -6 5 2 2.81 5.06 1.52 o -5 5 2 242.55 241.32 2.55 o -4 5 2 70.28 68.90 1.51 o -3 5 2 0.29 1.06 1.18 o -2 5 2 1164.22 1129.62 6.45 o -1 5 2 0.64 1.85 1.17 o 0 5 2 721.20 765.64 4.85 o 1 5 2 254.94 276.58 1.98 o 2 5 2 1454.06 1385.49 8.92 o 3 5 2 2.65 3.86 1.45 o 4 5 2 28.58 26.13 1.93 o 5 5 2 150.46 151.71 2.50 o 6 5 2 17.47 15.80 2.05 o 7 5 2 8.24 6.59 2.20 o -7 6 2 19.72 31.15 5.02 o -6 6 2 4.08 4.93 2.32 o -5 6 2 4.52 4.94 1.55 o -4 6 2 159.38 154.92 5.18 o -3 6 2 23.55 24.85 1.26 o -2 6 2 1.21 1.49 1.21 o -1 6 2 233.21 236.16 3.73 o 0 6 2 1582.36 1551.17 12.38 o 1 6 2 71.57 63.96 1.37 o 2 6 2 219.24 222.37 2.80 o 3 6 2 29.48 34.50 1.75 o 4 6 2 271.85 264.63 2.85 o 5 6 2 23.66 26.31 2.12 o 6 6 2 0.78 1.26 2.51 o 7 6 2 40.26 44.49 2.49 o -6 7 2 0.26 2.89 1.57 o -5 7 2 468.22 480.91 2.66 o -4 7 2 59.05 56.50 1.45 o -3 7 2 0.04 1.59 2.14 o -2 7 2 221.01 221.63 3.65 o -1 7 2 12.44 10.76 1.37 o 0 7 2 3.88 3.68 1.38 o 1 7 2 15.82 15.98 1.41 o 2 7 2 30.57 37.12 2.05 o 3 7 2 313.53 313.49 2.80 o 4 7 2 68.29 61.21 2.25 o 5 7 2 394.63 400.26 3.76 o 6 7 2 157.96 146.21 3.25 o -5 8 2 9.23 11.04 2.22 o -4 8 2 85.31 81.67 1.74 o -3 8 2 310.62 320.33 3.91 o -2 8 2 0.88 0.88 1.40 o -1 8 2 19.93 18.65 1.26 o 0 8 2 640.26 652.86 15.75 o 1 8 2 35.63 39.19 1.42 o 2 8 2 62.19 59.86 2.28 o 3 8 2 15.41 17.69 1.84 o 4 8 2 15.46 11.89 2.68 o 5 8 2 481.41 430.42 3.59 o -4 9 2 0.28 0.17 1.53 o -3 9 2 6.11 7.01 1.42 o -2 9 2 106.82 121.06 1.87 o -1 9 2 40.93 39.31 1.31 o 0 9 2 108.23 111.78 3.54 o 1 9 2 227.37 237.20 6.62 o 2 9 2 238.48 239.36 2.41 o 3 9 2 97.76 91.68 3.44 o 4 9 2 11.92 8.55 2.80 o -2 10 2 112.49 115.98 2.33 o -1 10 2 42.51 45.78 1.76 o 0 10 2 103.47 100.76 4.62 o 1 10 2 86.91 87.60 2.60 o 2 10 2 0.65 0.07 2.39 o -9 0 3 90.35 85.00 3.55 o -7 0 3 14.99 17.69 1.79 o -5 0 3 62.55 53.32 1.82 o -3 0 3 1499.98 1414.38 20.15 o -1 0 3 6031.58 4793.49 2547.59 o 5 0 3 4.72 3.59 2.21 o 7 0 3 0.12 -0.69 2.45 o -8 1 3 215.00 213.02 2.00 o -7 1 3 0.01 0.88 1.29 o -6 1 3 197.05 203.55 4.11 o -5 1 3 278.21 273.04 1.78 o -4 1 3 650.85 628.20 2.43 o -3 1 3 352.48 314.52 2.02 o -2 1 3 533.77 609.31 3.54 o -1 1 3 3113.14 3092.19 6.01 o 0 1 3 768.34 862.32 9.46 o 1 1 3 2501.20 2467.13 8.76 o 2 1 3 127.63 105.42 3.71 o 3 1 3 737.64 803.02 16.45 o 4 1 3 4543.98 4437.07 41.86 o 5 1 3 16.83 16.81 1.80 o 6 1 3 84.63 87.93 3.70 o 7 1 3 195.77 187.98 5.15 o 8 1 3 13.63 14.24 2.07 o -8 2 3 47.97 51.39 1.63 o -7 2 3 23.57 21.30 1.31 o -6 2 3 408.94 412.07 7.70 o -5 2 3 55.87 54.03 1.32 o -4 2 3 1.34 2.14 1.06 o -3 2 3 299.00 293.10 1.88 o -2 2 3 33.14 42.59 3.83 o -1 2 3 1259.48 1181.06 3.96 o 0 2 3 11.05 19.84 5.56 o 1 2 3 78.02 78.90 2.97 o 2 2 3 1929.17 1867.28 50.25 o 3 2 3 0.87 9.83 8.83 o 4 2 3 784.42 781.36 4.72 o 5 2 3 56.02 57.43 1.71 o 6 2 3 218.92 217.00 2.37 o 7 2 3 1.20 1.83 1.58 o 8 2 3 8.26 8.33 2.10 o -8 3 3 123.09 116.53 2.12 o -7 3 3 26.20 26.70 1.54 o -6 3 3 118.48 123.67 2.33 o -5 3 3 1034.60 1022.24 6.56 o -4 3 3 284.54 290.29 3.15 o -3 3 3 296.82 260.18 1.90 o -2 3 3 168.37 136.67 1.75 o -1 3 3 1457.14 1445.66 5.74 o 0 3 3 984.66 992.45 5.96 o 1 3 3 2532.73 2394.50 27.40 o 2 3 3 19.28 22.76 2.45 o 3 3 3 558.29 582.74 8.13 o 4 3 3 10.26 6.85 1.66 o 5 3 3 0.04 -0.30 1.50 o 6 3 3 163.67 164.19 2.96 o 7 3 3 208.52 225.88 2.98 o 8 3 3 45.97 47.05 2.51 o -8 4 3 20.42 19.00 1.85 o -7 4 3 23.16 26.52 2.09 o -6 4 3 91.82 86.27 3.54 o -5 4 3 565.15 576.22 24.36 o -4 4 3 336.63 330.85 3.35 o -3 4 3 114.89 109.02 3.55 o -2 4 3 17.14 26.82 1.37 o -1 4 3 4.60 11.50 1.36 o 0 4 3 994.80 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3.37 2.02 1.32 o 1 2 13 0.39 2.43 1.59 o 2 2 13 239.85 236.61 2.43 o 3 2 13 10.12 12.47 1.71 o 4 2 13 0.37 2.19 3.37 o -4 3 13 11.37 7.36 1.49 o -3 3 13 201.99 186.80 7.57 o -2 3 13 75.83 75.79 1.50 o -1 3 13 4.65 6.80 1.48 o 0 3 13 18.96 20.16 1.37 o 1 3 13 20.11 21.42 1.49 o 2 3 13 22.68 22.59 1.77 o 3 3 13 53.86 54.63 2.11 o -4 4 13 238.87 239.58 3.98 o -3 4 13 15.02 14.30 1.50 o -2 4 13 56.92 54.69 1.47 o -1 4 13 13.13 11.90 1.43 o 0 4 13 0.22 -0.12 1.46 o 1 4 13 31.07 33.54 1.63 o 2 4 13 0.60 3.08 1.90 o 3 4 13 0.27 1.94 1.95 o -3 5 13 3.77 4.06 1.55 o -2 5 13 12.82 16.60 2.66 o -1 5 13 126.46 122.34 1.97 o 0 5 13 37.33 40.21 1.54 o 1 5 13 116.58 113.28 2.30 o 2 5 13 27.60 25.33 1.61 o -4 0 14 44.83 54.00 1.94 o -2 0 14 311.24 309.10 7.63 o 0 0 14 101.84 102.78 2.72 o 2 0 14 372.63 353.11 4.00 o -4 1 14 17.79 18.73 1.43 o -3 1 14 57.47 51.64 1.51 o -2 1 14 37.58 43.04 1.46 o -1 1 14 5.84 7.32 1.62 o 0 1 14 120.05 116.66 2.13 o 1 1 14 45.33 47.43 1.79 o 2 1 14 132.72 135.88 3.25 o 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