#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209665_Fobs loop_ _publ_author_name 'Kumar, G. Senthil' 'Chinnakali, K.' 'Swaroop, M. Gayatri' 'Rajakumar, P.' 'Fun, Hoong-Kun' _publ_section_title ; 1,9,26-Triazahexacyclo[17.6.1.1^3,7^.1^9,16^.0^10,15^.0^20,25^]pentacosa-3,5,7(26),10(15),11,13,16(27),17,19(28),20(25),21,23-dodecaene ; _journal_coeditor_code SJ2088 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2608 _journal_page_last o2610 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.994 _cell_angle_gamma 90.000 _cell_length_a 19.9027 _cell_length_b 11.3107 _cell_length_c 8.7157 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file sj2088Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' VGS2 in C2/c 100K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 922.27 914.44 21.80 o 4 0 0 22.72 17.05 1.27 o 6 0 0 4047.62 3785.78 63.93 o 8 0 0 310.47 285.34 6.65 o 10 0 0 2241.98 2342.72 23.85 o 12 0 0 99.58 109.35 2.27 o 14 0 0 178.63 220.72 3.28 o 16 0 0 503.86 514.22 7.24 o 18 0 0 1221.23 1273.94 18.23 o 20 0 0 29.31 23.97 3.87 o 22 0 0 19.57 11.53 3.45 o 1 1 0 3158.50 2881.65 32.76 o 3 1 0 461.43 459.79 4.39 o 5 1 0 449.34 400.35 4.59 o 7 1 0 7.50 3.03 0.72 o 9 1 0 1988.63 2001.63 16.79 o 11 1 0 76.35 84.72 2.09 o 13 1 0 135.84 149.06 1.90 o 15 1 0 594.73 603.46 4.75 o 17 1 0 1441.66 1366.25 15.04 o 19 1 0 2010.38 2022.26 20.58 o 21 1 0 1.91 4.47 1.94 o 23 1 0 112.12 129.74 7.01 o 0 2 0 8538.73 8164.62 134.97 o 2 2 0 14160.81 13039.83 349.62 o 4 2 0 240.24 273.31 3.87 o 6 2 0 964.91 946.59 10.11 o 8 2 0 1819.23 1883.03 15.05 o 10 2 0 112.63 123.12 2.03 o 12 2 0 1269.36 1323.13 8.15 o 14 2 0 682.27 685.71 4.85 o 16 2 0 19.69 13.92 1.34 o 18 2 0 151.36 160.70 4.27 o 20 2 0 165.39 179.52 5.24 o 22 2 0 215.55 247.24 7.02 o 1 3 0 38.90 41.28 1.45 o 3 3 0 396.79 455.76 7.80 o 5 3 0 360.91 436.17 6.87 o 7 3 0 502.91 578.28 5.51 o 9 3 0 334.26 388.98 4.27 o 11 3 0 160.48 152.08 2.20 o 13 3 0 1418.05 1510.34 8.80 o 15 3 0 130.46 132.92 2.50 o 17 3 0 6.33 3.13 1.23 o 19 3 0 635.24 655.06 11.71 o 21 3 0 335.89 343.33 7.66 o 23 3 0 4.80 2.59 2.09 o 0 4 0 380.32 455.84 16.49 o 2 4 0 3760.39 3678.15 32.44 o 4 4 0 1020.29 1091.72 12.52 o 6 4 0 177.84 198.76 3.13 o 8 4 0 43.68 48.28 1.35 o 10 4 0 1259.17 1388.36 9.17 o 12 4 0 3.79 11.11 0.73 o 14 4 0 171.92 144.71 2.67 o 16 4 0 18.23 16.76 1.88 o 18 4 0 5.06 9.79 1.64 o 20 4 0 266.81 291.07 10.84 o 22 4 0 168.61 139.76 5.21 o 1 5 0 228.60 238.97 3.41 o 3 5 0 1030.78 1184.96 10.66 o 5 5 0 8.46 7.70 1.20 o 7 5 0 1081.81 1083.37 8.61 o 9 5 0 356.56 360.12 3.35 o 11 5 0 1164.55 1185.29 7.34 o 13 5 0 0.00 0.80 0.72 o 15 5 0 14.85 16.63 1.70 o 17 5 0 284.23 261.88 5.81 o 19 5 0 274.50 261.33 6.35 o 21 5 0 62.75 55.64 3.63 o 0 6 0 7224.41 7891.19 77.92 o 2 6 0 202.06 208.65 3.29 o 4 6 0 284.33 265.41 3.42 o 6 6 0 201.31 178.81 2.76 o 8 6 0 116.46 122.24 1.95 o 10 6 0 552.65 451.42 3.98 o 12 6 0 1164.32 1175.95 9.26 o 14 6 0 205.15 203.81 4.61 o 16 6 0 4.87 3.59 1.34 o 18 6 0 0.62 2.36 1.48 o 20 6 0 5.14 3.82 1.78 o 1 7 0 307.94 291.66 3.13 o 3 7 0 1193.92 1395.37 9.57 o 5 7 0 60.41 74.53 1.59 o 7 7 0 3991.86 3909.79 21.35 o 9 7 0 599.24 659.58 5.14 o 11 7 0 1215.50 1256.83 10.77 o 13 7 0 0.06 -0.60 1.00 o 15 7 0 542.55 553.53 8.52 o 17 7 0 18.61 21.46 2.27 o 19 7 0 78.09 65.44 3.76 o 0 8 0 446.10 513.73 5.44 o 2 8 0 845.63 849.71 5.50 o 4 8 0 58.73 61.54 1.32 o 6 8 0 100.87 85.02 1.60 o 8 8 0 9036.09 8719.11 45.57 o 10 8 0 485.48 434.76 5.27 o 12 8 0 29.21 28.86 1.98 o 14 8 0 24.36 16.19 2.09 o 16 8 0 120.59 145.61 6.03 o 18 8 0 22.18 16.03 2.24 o 1 9 0 250.39 258.06 2.55 o 3 9 0 15.78 20.21 0.99 o 5 9 0 41.17 29.52 1.21 o 7 9 0 23.26 23.21 1.34 o 9 9 0 876.79 839.24 8.79 o 11 9 0 1256.88 1211.19 12.88 o 13 9 0 95.36 95.30 4.22 o 15 9 0 10.23 8.30 1.74 o 17 9 0 121.38 128.21 4.55 o 0 10 0 64.12 44.13 3.66 o 2 10 0 76.12 80.62 2.22 o 4 10 0 8.17 11.79 1.24 o 6 10 0 5.83 9.63 1.83 o 8 10 0 33.64 33.08 2.25 o 10 10 0 718.46 745.43 10.61 o 12 10 0 208.57 211.63 7.89 o 14 10 0 390.12 410.00 8.82 o 16 10 0 142.51 136.72 5.44 o 1 11 0 359.22 380.90 5.53 o 3 11 0 129.41 119.00 3.97 o 5 11 0 888.38 873.00 10.79 o 7 11 0 143.27 123.30 4.77 o 9 11 0 83.65 88.10 4.40 o 11 11 0 456.98 442.38 8.84 o 13 11 0 138.17 134.44 4.95 o 15 11 0 44.76 45.50 3.82 o 0 12 0 528.27 517.59 15.19 o 2 12 0 28.80 24.76 2.26 o 4 12 0 139.62 124.98 4.21 o 6 12 0 18.62 22.74 3.09 o 8 12 0 251.35 246.58 6.99 o 10 12 0 37.35 31.04 2.88 o 12 12 0 1343.78 1458.82 18.99 o 1 13 0 0.37 0.15 1.32 o 3 13 0 203.50 181.14 5.22 o 5 13 0 188.80 190.11 6.20 o 7 13 0 186.31 222.66 6.07 o 9 13 0 39.65 41.72 3.34 o 11 13 0 152.98 147.66 5.37 o 0 14 0 184.36 215.83 9.03 o 2 14 0 9.81 19.46 2.64 o 4 14 0 0.35 0.98 1.89 o 6 14 0 310.37 338.73 8.83 o -23 1 1 258.04 260.03 7.21 o -21 1 1 206.27 205.67 5.99 o -19 1 1 12.10 12.38 1.52 o -17 1 1 1.40 2.87 0.79 o -15 1 1 46.69 49.66 1.47 o -13 1 1 634.42 732.44 5.75 o -11 1 1 46.51 56.28 1.20 o -9 1 1 0.45 1.31 0.43 o -7 1 1 1622.84 1654.88 16.96 o -5 1 1 1178.94 1124.79 16.46 o -3 1 1 1849.97 1860.50 24.89 o -1 1 1 21564.88 19166.80 276.77 o 1 1 1 573.69 608.29 6.08 o 3 1 1 47276.52 40311.34 319.75 o 5 1 1 1852.64 1838.71 24.93 o 7 1 1 273.80 286.28 6.85 o 9 1 1 99.67 110.23 1.87 o 11 1 1 880.50 848.55 6.04 o 13 1 1 1259.97 1357.60 8.76 o 15 1 1 426.75 437.32 4.51 o 17 1 1 190.63 195.32 3.59 o 19 1 1 581.53 577.51 8.93 o 21 1 1 178.49 201.45 5.70 o -24 2 1 6.66 3.11 2.02 o -22 2 1 1152.08 1166.64 16.69 o -20 2 1 827.91 835.05 11.19 o -18 2 1 136.72 131.55 2.68 o -16 2 1 756.90 798.11 7.04 o -14 2 1 11.63 9.87 0.75 o -12 2 1 45.56 54.66 1.34 o -10 2 1 5447.56 5836.17 34.62 o -8 2 1 649.72 672.85 6.29 o -6 2 1 1790.75 1730.95 17.91 o -4 2 1 1016.19 1012.80 11.86 o -2 2 1 245.60 277.02 4.22 o 0 2 1 7778.96 7658.13 76.77 o 2 2 1 9743.86 9495.01 86.71 o 4 2 1 13722.05 13816.13 115.75 o 6 2 1 1443.57 1502.08 21.34 o 8 2 1 2747.25 2876.54 16.89 o 10 2 1 317.19 286.39 3.65 o 12 2 1 1043.82 1059.89 7.60 o 14 2 1 21.45 24.69 1.15 o 16 2 1 319.52 315.49 4.29 o 18 2 1 13.98 9.46 1.65 o 20 2 1 6.96 6.53 1.73 o 22 2 1 151.47 145.45 8.69 o -23 3 1 473.24 509.85 10.39 o -21 3 1 0.01 -0.55 1.28 o -19 3 1 125.27 118.18 3.46 o -17 3 1 93.69 90.56 2.84 o -15 3 1 7.17 5.84 0.95 o -13 3 1 75.29 72.32 2.15 o -11 3 1 4640.85 5036.41 26.98 o -9 3 1 844.94 885.62 6.52 o -7 3 1 845.61 893.53 7.94 o -5 3 1 1597.91 1576.86 16.39 o -3 3 1 4.57 3.52 0.88 o -1 3 1 138.61 136.07 2.17 o 1 3 1 533.77 555.39 6.74 o 3 3 1 2035.78 2026.82 20.67 o 5 3 1 2281.46 2394.71 21.40 o 7 3 1 3145.26 3405.86 20.83 o 9 3 1 239.27 292.55 2.94 o 11 3 1 34.69 25.67 1.05 o 13 3 1 114.64 133.22 2.09 o 15 3 1 2.20 1.33 0.76 o 17 3 1 7.33 6.00 1.26 o 19 3 1 7.31 5.94 1.71 o 21 3 1 28.25 33.34 2.96 o -22 4 1 1193.59 1156.91 14.81 o -20 4 1 25.86 20.22 2.08 o -18 4 1 15.13 12.45 1.55 o -16 4 1 469.19 465.98 5.19 o -14 4 1 2082.81 2115.26 16.81 o -12 4 1 351.95 375.13 3.86 o -10 4 1 0.40 -0.12 0.42 o -8 4 1 135.73 127.18 1.96 o -6 4 1 24.00 18.76 1.16 o -4 4 1 2058.08 2071.37 20.35 o -2 4 1 2889.89 2942.37 26.20 o 0 4 1 0.16 1.90 0.97 o 2 4 1 1188.05 1258.23 16.36 o 4 4 1 618.68 700.27 6.58 o 6 4 1 316.76 336.51 3.19 o 8 4 1 518.49 553.88 4.44 o 10 4 1 1707.46 1764.44 10.89 o 12 4 1 13.59 12.76 0.90 o 14 4 1 1757.80 1709.88 12.04 o 16 4 1 13.39 6.87 1.53 o 18 4 1 0.81 2.49 1.46 o 20 4 1 0.24 1.55 1.61 o -23 5 1 114.17 108.48 5.45 o -21 5 1 248.43 247.99 8.90 o -19 5 1 589.40 575.07 8.54 o -17 5 1 28.53 27.22 2.11 o -15 5 1 177.09 164.52 2.93 o -13 5 1 2.82 0.28 0.64 o -11 5 1 8.06 12.80 0.87 o -9 5 1 375.86 376.73 3.81 o -7 5 1 884.01 1005.50 6.92 o -5 5 1 1051.53 1144.85 10.54 o -3 5 1 8472.25 8779.76 65.26 o -1 5 1 859.25 822.59 7.47 o 1 5 1 113.09 146.83 2.38 o 3 5 1 1992.10 2260.75 14.78 o 5 5 1 0.00 3.13 0.48 o 7 5 1 209.91 219.86 2.59 o 9 5 1 349.92 342.72 3.43 o 11 5 1 309.09 311.50 3.35 o 13 5 1 158.12 150.40 2.74 o 15 5 1 98.65 67.52 3.18 o 17 5 1 252.10 224.75 5.36 o 19 5 1 18.63 19.92 2.42 o 21 5 1 0.08 1.95 1.76 o -22 6 1 45.27 48.56 3.53 o -20 6 1 193.67 179.68 6.65 o -18 6 1 5.81 1.30 1.31 o -16 6 1 38.27 47.92 2.24 o -14 6 1 231.00 229.88 3.47 o -12 6 1 2388.75 2334.04 15.08 o -10 6 1 1.68 2.53 0.57 o -8 6 1 22.05 29.59 1.30 o -6 6 1 707.05 808.17 6.47 o -4 6 1 333.19 364.11 3.79 o -2 6 1 422.16 443.56 4.41 o 0 6 1 1770.25 1907.05 11.72 o 2 6 1 2042.41 2286.18 13.42 o 4 6 1 488.85 469.34 4.11 o 6 6 1 775.57 795.74 5.99 o 8 6 1 3.56 2.82 0.61 o 10 6 1 464.35 444.16 4.16 o 12 6 1 1856.97 1847.98 12.29 o 14 6 1 126.80 151.41 3.55 o 16 6 1 895.26 815.89 10.68 o 18 6 1 2.34 3.55 1.60 o 20 6 1 8.74 8.82 2.14 o -21 7 1 110.64 120.67 5.07 o -19 7 1 17.24 8.50 1.89 o -17 7 1 66.52 64.01 3.22 o -15 7 1 365.30 321.81 5.65 o -13 7 1 59.54 64.04 2.03 o -11 7 1 603.18 565.45 5.63 o -9 7 1 1308.98 1335.74 9.67 o -7 7 1 59.78 56.75 1.64 o -5 7 1 546.35 517.31 5.58 o -3 7 1 205.35 193.80 3.38 o -1 7 1 1115.83 1224.47 7.87 o 1 7 1 83.66 78.97 1.47 o 3 7 1 354.39 385.40 3.61 o 5 7 1 990.78 989.45 6.76 o 7 7 1 137.13 136.04 2.06 o 9 7 1 79.42 86.64 1.79 o 11 7 1 3162.32 3020.83 18.98 o 13 7 1 2.68 2.42 0.93 o 15 7 1 229.27 219.21 4.73 o 17 7 1 9.59 13.92 2.11 o 19 7 1 61.89 69.77 4.03 o -20 8 1 53.85 63.85 3.67 o -18 8 1 588.92 679.06 11.16 o -16 8 1 274.82 297.95 6.26 o -14 8 1 246.84 230.56 4.64 o -12 8 1 31.30 40.55 1.86 o -10 8 1 1818.75 1695.06 12.57 o -8 8 1 554.05 617.44 5.97 o -6 8 1 58.38 56.60 1.90 o -4 8 1 69.00 68.19 1.62 o -2 8 1 84.98 80.75 1.69 o 0 8 1 968.47 1005.68 7.18 o 2 8 1 0.87 1.19 0.50 o 4 8 1 46.54 44.13 1.42 o 6 8 1 54.62 86.21 1.68 o 8 8 1 144.95 108.78 2.14 o 10 8 1 1332.32 1262.96 10.81 o 12 8 1 6.51 7.00 1.58 o 14 8 1 324.58 359.66 6.20 o 16 8 1 20.83 15.93 2.10 o 18 8 1 33.56 32.90 2.95 o -19 9 1 296.08 312.64 7.52 o -17 9 1 198.39 214.59 7.77 o -15 9 1 580.33 546.22 10.43 o -13 9 1 25.80 28.21 2.52 o -11 9 1 246.29 279.79 6.28 o -9 9 1 1.61 0.45 0.84 o -7 9 1 0.00 2.73 0.83 o -5 9 1 888.24 906.05 7.19 o -3 9 1 92.46 78.29 1.92 o -1 9 1 23.68 29.13 1.29 o 1 9 1 551.33 587.46 4.87 o 3 9 1 1453.18 1312.65 9.08 o 5 9 1 3.71 2.26 0.65 o 7 9 1 40.26 26.24 1.27 o 9 9 1 258.78 303.39 4.31 o 11 9 1 646.19 644.65 8.46 o 13 9 1 39.02 49.62 2.66 o 15 9 1 566.07 657.85 10.00 o 17 9 1 398.11 442.11 9.37 o -18 10 1 270.56 289.03 7.76 o -16 10 1 1.33 -0.99 1.66 o -14 10 1 1028.21 1096.37 15.76 o -12 10 1 65.16 67.86 4.21 o -10 10 1 82.97 89.83 3.39 o -8 10 1 3342.95 3188.95 28.23 o -6 10 1 134.38 121.95 2.73 o -4 10 1 1477.73 1371.12 10.01 o -2 10 1 3975.47 3565.98 29.91 o 0 10 1 480.86 463.51 4.77 o 2 10 1 0.06 1.16 0.73 o 4 10 1 1176.79 1083.72 9.42 o 6 10 1 295.53 269.21 3.77 o 8 10 1 189.79 194.76 3.79 o 10 10 1 73.14 85.92 3.75 o 12 10 1 8.35 7.58 1.75 o 14 10 1 0.00 2.29 1.53 o 16 10 1 169.83 187.80 6.02 o -15 11 1 245.10 245.07 8.77 o -13 11 1 6.99 5.21 2.15 o -11 11 1 0.17 2.21 1.32 o -9 11 1 450.28 445.36 9.03 o -7 11 1 99.04 118.33 3.97 o -5 11 1 5.08 2.65 1.02 o -3 11 1 134.56 97.36 2.99 o -1 11 1 62.69 39.07 1.94 o 1 11 1 154.65 142.14 3.22 o 3 11 1 3.29 2.36 0.99 o 5 11 1 11.11 9.98 1.26 o 7 11 1 33.97 26.50 2.07 o 9 11 1 444.47 463.87 8.19 o 11 11 1 246.64 271.87 6.43 o 13 11 1 131.65 166.68 5.14 o -14 12 1 16.98 16.79 3.58 o -12 12 1 3.17 0.88 1.48 o -10 12 1 46.35 60.53 3.51 o -8 12 1 105.82 108.46 5.14 o -6 12 1 489.81 503.70 9.10 o -4 12 1 193.08 192.25 4.61 o -2 12 1 54.30 66.76 2.75 o 0 12 1 648.94 538.48 7.53 o 2 12 1 17.79 25.85 2.13 o 4 12 1 814.83 886.21 10.46 o 6 12 1 447.07 511.15 11.23 o 8 12 1 0.10 -0.12 1.37 o 10 12 1 87.68 70.64 4.99 o 12 12 1 194.42 245.77 6.64 o -11 13 1 455.82 504.17 9.77 o -9 13 1 142.03 141.64 5.63 o -7 13 1 85.90 84.03 5.56 o -5 13 1 19.94 16.77 2.36 o -3 13 1 0.38 0.21 1.37 o -1 13 1 67.84 68.93 3.22 o 1 13 1 42.73 57.02 5.30 o 3 13 1 27.06 27.51 2.62 o 5 13 1 1.23 3.00 1.68 o 7 13 1 4.26 2.74 1.56 o 9 13 1 32.04 29.17 2.92 o -6 14 1 27.26 20.93 3.21 o -4 14 1 18.78 17.64 2.94 o -2 14 1 315.86 325.95 7.83 o 0 14 1 12.85 21.53 2.43 o 2 14 1 9.76 18.87 2.46 o 4 14 1 0.07 0.39 1.44 o -24 0 2 177.30 181.12 9.96 o -22 0 2 581.96 601.10 13.03 o -20 0 2 1570.58 1636.32 24.67 o -18 0 2 535.18 504.95 7.41 o -16 0 2 17.26 18.97 1.86 o -14 0 2 94.69 83.24 2.45 o -12 0 2 16.54 17.72 1.35 o -10 0 2 2800.91 3070.34 28.79 o -8 0 2 206.39 190.64 5.46 o -6 0 2 11454.23 11295.45 173.69 o -4 0 2 80048.41 67583.18 1186.67 o -2 0 2 15877.22 15506.25 207.04 o 0 0 2 21117.82 20346.74 188.91 o 2 0 2 31512.69 29353.02 297.93 o 4 0 2 143.72 112.71 3.33 o 6 0 2 195.44 197.33 3.38 o 8 0 2 6.10 6.63 0.98 o 10 0 2 294.41 309.53 4.34 o 12 0 2 4438.38 4320.29 34.29 o 14 0 2 1600.55 1600.91 14.68 o 16 0 2 478.00 498.13 7.35 o 18 0 2 25.43 18.07 2.35 o 20 0 2 22.04 20.85 2.99 o -25 1 2 37.39 25.84 4.36 o -23 1 2 230.06 233.72 6.80 o -21 1 2 571.04 564.61 6.55 o -19 1 2 1580.80 1546.35 12.22 o -17 1 2 404.89 418.64 4.40 o -15 1 2 2.14 1.02 0.58 o -13 1 2 94.73 94.25 1.61 o -11 1 2 88.10 90.00 1.65 o -9 1 2 407.37 400.80 5.02 o -7 1 2 817.28 827.77 11.72 o -5 1 2 7016.99 6974.27 59.31 o -3 1 2 2437.73 2418.39 20.39 o -1 1 2 20.12 12.46 0.66 o 1 1 2 15850.46 15058.17 106.56 o 3 1 2 3924.53 3817.19 30.71 o 5 1 2 759.67 753.22 6.09 o 7 1 2 559.29 589.41 4.57 o 9 1 2 13.35 19.55 0.87 o 11 1 2 546.10 517.42 4.39 o 13 1 2 2139.60 2037.51 13.02 o 15 1 2 1374.21 1350.58 9.32 o 17 1 2 300.00 280.99 5.02 o 19 1 2 47.60 56.30 3.44 o 21 1 2 23.80 30.98 2.84 o -24 2 2 313.75 370.48 9.83 o -22 2 2 322.35 365.97 6.83 o -20 2 2 711.41 721.43 8.08 o -18 2 2 5.12 2.54 0.88 o -16 2 2 462.36 470.80 4.96 o -14 2 2 207.17 221.56 3.07 o -12 2 2 691.66 715.99 5.92 o -10 2 2 953.53 1049.01 7.69 o -8 2 2 2594.26 2747.76 23.20 o -6 2 2 4922.68 5046.57 52.17 o -4 2 2 1366.91 1378.40 15.21 o -2 2 2 1533.20 1584.36 16.65 o 0 2 2 234.49 257.74 3.66 o 2 2 2 18973.59 18393.29 155.81 o 4 2 2 620.00 679.50 5.93 o 6 2 2 1584.45 1642.26 10.31 o 8 2 2 954.20 937.98 6.17 o 10 2 2 105.32 99.20 1.76 o 12 2 2 133.24 133.88 2.44 o 14 2 2 113.63 114.20 2.29 o 16 2 2 180.72 198.24 3.33 o 18 2 2 13.34 15.12 1.71 o 20 2 2 2.15 5.19 1.84 o -23 3 2 102.72 83.58 4.53 o -21 3 2 85.17 77.81 2.72 o -19 3 2 1512.45 1452.86 12.64 o -17 3 2 1627.99 1610.42 12.28 o -15 3 2 374.47 385.74 4.35 o -13 3 2 45.60 33.83 1.28 o -11 3 2 735.63 833.05 6.86 o -9 3 2 7.66 13.25 0.85 o -7 3 2 526.39 532.00 5.72 o -5 3 2 465.14 473.63 6.57 o -3 3 2 67.84 61.49 1.81 o -1 3 2 2917.33 2909.31 30.87 o 1 3 2 4814.57 4782.20 53.40 o 3 3 2 7773.58 8100.88 52.78 o 5 3 2 1696.34 1862.06 11.90 o 7 3 2 561.40 640.26 4.80 o 9 3 2 674.97 721.33 5.33 o 11 3 2 425.24 433.40 4.22 o 13 3 2 41.17 38.38 1.82 o 15 3 2 45.98 42.37 1.61 o 17 3 2 313.95 306.95 5.32 o 19 3 2 34.50 29.72 2.41 o -24 4 2 10.23 7.29 2.75 o -22 4 2 7.20 4.77 1.71 o -20 4 2 505.79 521.54 6.31 o -18 4 2 18.60 11.84 1.16 o -16 4 2 298.09 263.13 3.70 o -14 4 2 495.00 477.14 4.90 o -12 4 2 33.57 30.11 1.25 o -10 4 2 902.41 996.25 7.48 o -8 4 2 5879.83 6274.78 36.65 o -6 4 2 98.91 104.67 1.91 o -4 4 2 653.06 651.63 6.95 o -2 4 2 1268.02 1237.01 11.57 o 0 4 2 524.20 602.40 5.76 o 2 4 2 165.83 182.48 2.38 o 4 4 2 960.92 1048.92 6.83 o 6 4 2 2.99 5.08 0.54 o 8 4 2 98.16 83.77 1.81 o 10 4 2 24.37 39.31 1.50 o 12 4 2 127.78 120.49 2.32 o 14 4 2 462.70 489.95 5.01 o 16 4 2 346.13 356.44 5.37 o 18 4 2 7.64 2.40 1.25 o 20 4 2 103.18 113.06 4.43 o -23 5 2 1.95 1.61 1.76 o -21 5 2 2.91 7.51 1.61 o -19 5 2 280.31 275.67 4.39 o -17 5 2 40.41 22.00 1.43 o -15 5 2 17.94 10.87 1.06 o -13 5 2 205.03 185.06 2.86 o -11 5 2 1934.00 1995.83 12.91 o -9 5 2 76.67 81.06 1.59 o -7 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341.09 339.53 4.06 o 0 2 9 18.84 21.23 1.46 o 2 2 9 31.92 34.07 2.04 o 4 2 9 379.41 366.55 5.21 o -21 3 9 106.36 126.82 4.00 o -19 3 9 1.62 1.89 1.13 o -17 3 9 0.77 2.24 0.96 o -15 3 9 2.26 0.85 0.94 o -13 3 9 389.88 416.64 5.74 o -11 3 9 93.83 75.30 3.72 o -9 3 9 782.98 803.01 13.71 o -7 3 9 31.64 26.03 2.83 o -5 3 9 206.05 201.77 3.69 o -3 3 9 373.78 393.44 4.44 o -1 3 9 110.64 107.77 2.58 o 1 3 9 84.76 81.80 2.76 o 3 3 9 57.98 59.48 2.27 o 5 3 9 12.49 15.81 1.68 o -20 4 9 93.10 87.31 3.77 o -18 4 9 398.91 417.44 6.21 o -16 4 9 68.07 62.54 1.98 o -14 4 9 3.48 1.60 0.81 o -12 4 9 197.61 175.60 3.82 o -10 4 9 2275.80 2282.81 19.14 o -8 4 9 0.10 1.14 1.35 o -6 4 9 106.76 101.18 3.51 o -4 4 9 12.01 11.24 1.04 o -2 4 9 1054.22 1091.10 9.82 o 0 4 9 0.99 1.87 1.08 o 2 4 9 262.45 274.72 4.49 o 4 4 9 435.62 477.85 6.33 o -19 5 9 231.60 248.72 5.25 o -17 5 9 0.28 0.64 1.09 o -15 5 9 15.63 15.43 1.49 o -13 5 9 0.68 0.57 0.95 o -11 5 9 433.01 468.01 5.63 o -9 5 9 22.77 19.85 1.45 o -7 5 9 6.66 6.90 1.02 o -5 5 9 464.47 461.69 5.80 o -3 5 9 43.84 39.10 1.87 o -1 5 9 207.90 206.28 4.13 o 1 5 9 13.22 8.37 1.36 o 3 5 9 289.02 304.83 4.75 o -18 6 9 0.34 0.10 1.09 o -16 6 9 0.20 0.21 1.05 o -14 6 9 4.37 5.00 1.29 o -12 6 9 27.97 27.18 1.87 o -10 6 9 167.89 174.59 3.53 o -8 6 9 16.94 18.91 1.46 o -6 6 9 13.19 6.92 1.17 o -4 6 9 12.72 11.32 1.37 o -2 6 9 2.75 2.89 1.18 o 0 6 9 152.46 142.14 3.15 o 2 6 9 81.73 68.28 2.52 o -17 7 9 25.45 28.72 1.97 o -15 7 9 94.14 112.22 3.34 o -13 7 9 0.33 0.68 1.23 o -11 7 9 15.28 16.55 1.67 o -9 7 9 8.63 7.59 1.42 o -7 7 9 1.51 2.11 1.18 o -5 7 9 165.65 173.23 4.33 o -3 7 9 6.27 5.96 1.24 o -1 7 9 32.61 24.72 1.72 o -14 8 9 26.67 43.69 2.36 o -12 8 9 0.68 0.99 1.18 o -10 8 9 32.58 25.27 1.88 o -8 8 9 246.06 274.52 4.86 o -6 8 9 0.74 3.45 1.23 o -4 8 9 0.49 -0.14 1.13 o -20 0 10 0.02 3.28 1.71 o -18 0 10 54.55 63.69 2.96 o -16 0 10 294.31 339.92 9.57 o -14 0 10 15.66 16.45 3.97 o -12 0 10 20.14 17.91 4.08 o -10 0 10 2.11 1.61 2.11 o -8 0 10 1094.56 1101.42 21.39 o -6 0 10 125.80 110.25 8.08 o -4 0 10 181.40 187.75 8.65 o -2 0 10 36.58 40.28 2.99 o 0 0 10 185.54 195.03 5.30 o -19 1 10 59.40 54.77 2.16 o -17 1 10 66.44 68.63 2.54 o -15 1 10 0.16 -0.96 1.66 o -13 1 10 28.21 24.07 3.18 o -11 1 10 163.87 153.92 6.10 o -9 1 10 520.65 500.88 10.15 o -7 1 10 156.42 164.91 5.91 o -5 1 10 601.78 627.02 12.75 o -3 1 10 426.50 447.86 5.79 o -1 1 10 0.08 0.29 1.04 o 1 1 10 272.53 266.24 4.78 o -18 2 10 20.71 30.55 1.69 o -16 2 10 2.12 2.37 1.40 o -14 2 10 0.62 4.19 2.45 o -12 2 10 15.01 10.62 2.32 o -10 2 10 24.44 30.34 4.43 o -8 2 10 62.83 64.51 4.24 o -6 2 10 144.83 152.48 5.91 o -4 2 10 579.81 624.73 8.33 o -2 2 10 300.79 322.20 4.94 o 0 2 10 242.60 249.41 4.48 o -19 3 10 10.73 7.69 1.37 o -17 3 10 73.90 73.66 2.30 o -15 3 10 68.33 69.20 3.06 o -13 3 10 12.87 7.42 1.45 o -11 3 10 0.23 -0.73 1.83 o -9 3 10 238.31 226.97 9.02 o -7 3 10 847.32 849.69 12.62 o -5 3 10 0.30 -1.13 1.01 o -3 3 10 0.99 2.95 1.07 o -1 3 10 287.50 284.34 4.69 o -18 4 10 3.19 5.19 1.29 o -16 4 10 21.96 24.80 2.38 o -14 4 10 2.26 3.65 1.09 o -12 4 10 95.02 99.40 3.02 o -10 4 10 22.92 26.29 2.14 o -8 4 10 103.61 107.83 3.09 o -6 4 10 355.90 356.61 5.08 o -4 4 10 0.12 -0.44 1.01 o -2 4 10 32.64 28.67 1.77 o -15 5 10 23.40 28.19 2.07 o -13 5 10 45.99 54.01 2.01 o -11 5 10 47.43 47.68 2.06 o -9 5 10 264.64 261.78 4.54 o -7 5 10 719.77 781.50 8.78 o -5 5 10 162.36 161.08 3.20 o -3 5 10 10.97 10.09 1.38 o -14 6 10 159.21 161.82 4.04 o -12 6 10 353.22 410.11 5.81 o -10 6 10 2.71 5.52 1.34 o -8 6 10 226.71 234.12 4.02 o -6 6 10 23.01 19.95 1.64 o -4 6 10 57.35 61.51 2.40 o -15 1 11 0.38 6.83 2.82 o -13 1 11 167.75 176.00 8.49 o -11 1 11 9.43 9.30 2.89 o -9 1 11 61.56 65.09 4.86 o -7 1 11 29.16 40.08 4.17 o -5 1 11 750.54 808.87 11.80 o -14 2 11 1.00 -0.16 2.77 o -12 2 11 19.31 15.84 3.10 o -10 2 11 182.83 200.78 8.05 o -8 2 11 7.86 5.47 2.87 o -6 2 11 17.85 19.57 2.21 o -13 3 11 89.97 95.71 3.91 o -11 3 11 23.87 32.96 3.88 o -9 3 11 74.81 78.05 3.97 o