#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/97/2209703.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209703_Fobs loop_ _publ_author_name 'Xing, Huan-Ran' 'Li, Xin-Hua' _publ_section_title ; Poly[[diaquacobalt(II)]-\m-2,5-dicarboxybenzene-1,4-dicarboxylato-\m-di-4-pyridylethene] ; _journal_coeditor_code XU2041 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1506 _journal_page_last m1507 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 102.552 _cell_angle_beta 93.594 _cell_angle_gamma 104.500 _cell_length_a 6.8680 _cell_length_b 8.5558 _cell_length_c 8.9769 _exptl_crystal_F_000 270.95 _reflns_d_resolution_high 0.8378 _[local]_cod_data_source_file xu2041Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' l050708m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 230.71 197.78 1.93 o 2 0 0 9739.37 8614.19 210.61 o 3 0 0 5.01 3.11 0.40 o 4 0 0 1397.78 1471.71 15.11 o 5 0 0 429.47 428.46 10.58 o 6 0 0 59.87 55.14 3.99 o 7 0 0 13.15 15.49 2.95 o -8 1 0 33.50 45.08 4.69 o -7 1 0 31.38 33.38 3.73 o -6 1 0 55.31 51.54 3.80 o -5 1 0 131.60 119.01 5.14 o -4 1 0 58.19 77.17 1.70 o -3 1 0 218.88 216.17 4.51 o -2 1 0 2738.20 2897.08 36.66 o -1 1 0 4047.27 4204.50 59.22 o 0 1 0 0.97 1.01 0.16 o 1 1 0 1860.99 1842.79 17.29 o 2 1 0 57.86 63.62 1.80 o 3 1 0 232.46 245.48 6.33 o 4 1 0 366.81 361.02 9.16 o 5 1 0 167.00 150.33 6.20 o 6 1 0 1.99 2.89 1.55 o 7 1 0 27.71 32.42 3.89 o -8 2 0 95.80 104.62 6.70 o -7 2 0 72.17 84.45 5.44 o -6 2 0 65.97 63.04 4.26 o -5 2 0 13.60 11.40 0.87 o -4 2 0 3.54 3.67 0.83 o -3 2 0 453.58 446.45 8.16 o -2 2 0 520.79 578.99 9.57 o -1 2 0 835.36 876.40 7.41 o 0 2 0 30.78 40.39 1.11 o 1 2 0 2447.19 2412.56 22.24 o 2 2 0 595.59 600.96 6.63 o 3 2 0 613.17 628.91 12.45 o 4 2 0 386.07 382.28 9.88 o 5 2 0 146.01 153.06 6.48 o 6 2 0 10.29 11.81 2.59 o 7 2 0 79.51 71.29 5.36 o -8 3 0 28.14 37.28 4.50 o -7 3 0 130.44 169.89 7.84 o -6 3 0 6.39 4.57 0.84 o -5 3 0 53.41 51.64 2.82 o -4 3 0 1032.23 997.45 16.16 o -3 3 0 239.52 260.45 6.23 o -2 3 0 1049.49 1063.60 9.32 o -1 3 0 526.16 556.51 6.76 o 0 3 0 1138.55 1132.68 11.71 o 1 3 0 1265.18 1289.73 13.13 o 2 3 0 1164.14 1259.25 12.95 o 3 3 0 195.67 191.99 6.39 o 4 3 0 295.94 298.98 9.05 o 5 3 0 43.60 48.09 4.00 o 6 3 0 310.95 295.38 10.59 o -7 4 0 15.15 18.99 3.07 o -6 4 0 91.08 88.80 4.23 o -5 4 0 54.82 50.30 3.07 o -4 4 0 408.59 393.32 8.97 o -3 4 0 384.08 402.82 5.93 o -2 4 0 162.90 202.62 3.30 o -1 4 0 35.39 46.89 1.70 o 0 4 0 15.22 34.70 1.95 o 1 4 0 356.79 342.35 5.16 o 2 4 0 6.56 1.68 0.48 o 3 4 0 3.74 5.27 1.61 o 4 4 0 11.09 11.14 2.36 o 5 4 0 129.47 120.60 6.46 o 6 4 0 77.90 79.46 5.82 o -6 5 0 148.79 137.25 5.74 o -5 5 0 127.47 113.94 4.99 o -4 5 0 564.45 581.97 12.21 o -3 5 0 123.33 114.72 3.16 o -2 5 0 731.59 788.75 10.09 o -1 5 0 52.37 42.90 1.83 o 0 5 0 596.65 641.64 8.64 o 1 5 0 242.18 233.20 4.47 o 2 5 0 31.15 33.21 3.08 o 3 5 0 126.66 122.41 5.76 o 4 5 0 6.15 10.54 2.31 o 5 5 0 261.56 236.90 9.51 o -7 6 0 189.26 186.77 7.40 o -6 6 0 48.13 45.96 3.57 o -5 6 0 133.51 115.58 5.22 o -4 6 0 33.68 32.50 2.74 o -3 6 0 450.47 478.33 7.73 o -2 6 0 435.95 447.27 7.30 o -1 6 0 466.82 468.31 7.42 o 0 6 0 65.41 74.49 2.62 o 1 6 0 243.89 229.07 7.09 o 2 6 0 113.92 118.27 5.66 o 3 6 0 181.26 167.79 7.38 o 4 6 0 83.26 75.43 5.25 o -7 7 0 76.36 79.36 4.98 o -6 7 0 40.14 37.90 3.57 o -5 7 0 76.05 80.77 4.62 o -4 7 0 13.55 12.21 2.09 o -3 7 0 515.32 539.86 8.79 o -2 7 0 479.04 477.41 8.06 o -1 7 0 35.88 36.72 2.68 o 0 7 0 420.16 409.71 7.40 o 1 7 0 9.75 12.82 2.35 o 2 7 0 1004.18 933.90 19.94 o 3 7 0 74.25 61.87 4.77 o 4 7 0 143.78 125.32 7.27 o -6 8 0 68.13 62.77 4.61 o -5 8 0 4.03 11.01 2.36 o -4 8 0 54.02 49.92 2.64 o -3 8 0 150.85 143.76 4.37 o -2 8 0 1.15 2.58 0.98 o -1 8 0 57.70 52.61 2.66 o 0 8 0 64.74 46.49 4.85 o 1 8 0 128.88 129.19 6.60 o 2 8 0 23.83 32.70 3.89 o -5 9 0 1.78 4.17 1.70 o -4 9 0 129.38 115.74 6.12 o -3 9 0 11.16 18.37 1.90 o -2 9 0 69.83 62.88 3.94 o -1 9 0 73.40 79.02 3.45 o 0 9 0 9.56 15.39 2.82 o 1 9 0 104.70 113.28 6.81 o 1 -10 1 53.31 59.21 4.89 o 2 -10 1 68.00 67.58 3.41 o 3 -10 1 32.03 36.98 2.76 o -1 -9 1 155.11 132.52 7.14 o 0 -9 1 76.94 75.35 5.13 o 1 -9 1 72.07 68.27 3.17 o 2 -9 1 48.20 53.65 2.88 o 3 -9 1 94.13 98.54 3.88 o 4 -9 1 9.93 14.43 1.87 o 5 -9 1 6.25 4.27 1.80 o -3 -8 1 15.21 20.90 3.54 o -2 -8 1 162.51 152.82 7.58 o -1 -8 1 31.02 30.79 3.60 o 0 -8 1 73.21 72.28 3.12 o 1 -8 1 1.01 1.11 0.75 o 2 -8 1 387.11 369.53 7.26 o 3 -8 1 56.52 55.01 2.76 o 4 -8 1 145.68 149.11 6.70 o 5 -8 1 27.31 23.93 3.08 o 6 -8 1 38.02 29.52 3.39 o -4 -7 1 0.93 0.57 1.64 o -3 -7 1 129.40 117.39 6.50 o -2 -7 1 0.87 3.59 1.51 o -1 -7 1 128.23 123.44 5.99 o 0 -7 1 6.44 12.31 1.96 o 1 -7 1 144.45 134.44 3.88 o 2 -7 1 263.78 265.75 5.68 o 3 -7 1 359.53 360.01 6.90 o 4 -7 1 36.11 36.43 3.32 o 5 -7 1 119.80 109.78 5.50 o 6 -7 1 6.70 7.24 1.82 o 7 -7 1 147.25 144.62 5.06 o -5 -6 1 65.30 70.81 5.54 o -4 -6 1 560.00 547.60 15.08 o -3 -6 1 43.03 43.64 3.71 o -2 -6 1 233.05 200.81 7.53 o -1 -6 1 655.60 686.64 9.42 o 0 -6 1 112.42 103.91 3.04 o 1 -6 1 1085.55 1061.08 13.01 o 2 -6 1 11.69 11.24 1.27 o 3 -6 1 455.02 429.15 7.27 o 4 -6 1 173.14 168.42 6.26 o 5 -6 1 64.06 55.89 3.68 o 6 -6 1 65.89 55.27 3.82 o 7 -6 1 7.52 12.42 1.80 o -5 -5 1 277.64 258.80 9.74 o -4 -5 1 24.51 28.34 3.33 o -3 -5 1 16.53 16.35 2.49 o -2 -5 1 210.03 217.74 7.26 o -1 -5 1 542.25 592.59 7.97 o 0 -5 1 1123.63 1204.37 13.61 o 1 -5 1 96.79 108.21 2.92 o 2 -5 1 71.61 59.32 2.81 o 3 -5 1 350.08 373.41 6.31 o 4 -5 1 639.94 654.50 13.37 o 5 -5 1 189.95 176.00 6.19 o 6 -5 1 112.59 111.06 4.06 o 7 -5 1 22.49 21.78 2.07 o -6 -4 1 50.41 49.37 4.75 o -5 -4 1 76.97 77.54 5.07 o -4 -4 1 55.98 52.10 3.92 o -3 -4 1 36.08 36.17 3.04 o -2 -4 1 979.87 1000.31 10.99 o -1 -4 1 28.49 15.97 1.01 o 0 -4 1 2549.92 2843.80 37.40 o 1 -4 1 105.27 134.78 2.97 o 2 -4 1 417.41 436.65 6.31 o 3 -4 1 899.29 947.20 16.02 o 4 -4 1 450.44 448.24 9.85 o 6 -4 1 9.33 8.26 1.29 o 8 -4 1 145.33 218.84 10.90 o -6 -3 1 22.86 30.83 3.67 o -5 -3 1 44.33 43.05 3.66 o -4 -3 1 9.85 12.07 2.10 o -3 -3 1 380.84 401.33 9.67 o -2 -3 1 466.23 543.17 10.76 o -1 -3 1 761.08 778.95 14.57 o 0 -3 1 40.04 53.93 1.17 o 1 -3 1 99.08 92.23 2.55 o 2 -3 1 732.98 721.54 8.52 o 3 -3 1 171.86 154.38 4.57 o 5 -3 1 118.95 108.90 6.59 o 6 -3 1 22.22 20.98 2.31 o 7 -3 1 236.76 286.43 11.02 o 8 -3 1 26.03 33.31 4.74 o -7 -2 1 41.13 43.30 4.43 o -6 -2 1 110.29 110.53 5.82 o -5 -2 1 271.78 240.98 8.03 o -4 -2 1 1020.48 930.21 17.21 o -3 -2 1 530.60 572.91 11.46 o -2 -2 1 18.25 12.56 1.39 o -1 -2 1 105.07 110.04 3.29 o 0 -2 1 322.00 300.16 3.63 o 1 -2 1 1807.43 1945.07 18.31 o 2 -2 1 31.68 28.70 1.55 o 3 -2 1 137.96 132.99 3.22 o 4 -2 1 117.63 107.80 5.75 o 5 -2 1 94.70 88.61 4.00 o 6 -2 1 46.68 58.83 4.35 o 7 -2 1 0.37 0.49 1.52 o 8 -2 1 4.81 7.45 2.81 o -7 -1 1 53.74 60.06 4.61 o -6 -1 1 39.69 41.90 3.47 o -5 -1 1 405.68 401.25 10.30 o -4 -1 1 1092.50 1073.33 18.46 o -3 -1 1 183.13 172.45 5.01 o -2 -1 1 30.41 35.10 1.85 o -1 -1 1 30.75 35.73 0.77 o 0 -1 1 387.68 420.36 3.76 o 1 -1 1 344.83 341.43 6.62 o 2 -1 1 172.39 159.32 2.54 o 3 -1 1 7.00 8.15 0.91 o 4 -1 1 826.52 810.08 9.83 o 5 -1 1 240.47 250.31 7.82 o 6 -1 1 368.16 407.43 11.58 o 7 -1 1 0.92 1.25 1.68 o -7 0 1 11.72 11.99 2.51 o -6 0 1 38.98 43.32 3.54 o -5 0 1 318.96 315.42 8.38 o -4 0 1 196.82 172.73 5.30 o -3 0 1 978.11 973.85 9.99 o -2 0 1 5.86 9.20 0.54 o -1 0 1 918.73 907.36 8.61 o 0 0 1 746.31 728.94 7.47 o 1 0 1 28.20 23.52 1.03 o 2 0 1 25.22 38.12 1.20 o 3 0 1 57.80 54.27 1.64 o 4 0 1 492.40 496.18 6.74 o 5 0 1 548.59 531.59 12.51 o 6 0 1 34.38 31.26 3.38 o 7 0 1 20.93 23.71 3.46 o -8 1 1 160.20 160.35 7.92 o -7 1 1 44.26 48.62 3.89 o -6 1 1 732.88 752.49 15.59 o -5 1 1 1.07 1.77 0.54 o -4 1 1 4603.85 4886.02 44.39 o -3 1 1 1068.74 1049.25 12.47 o -2 1 1 14799.00 13128.32 178.16 o -1 1 1 1980.03 2052.76 19.73 o 0 1 1 4236.75 3864.07 36.34 o 1 1 1 2101.47 2024.46 18.79 o 2 1 1 9.24 9.59 0.68 o 3 1 1 850.89 895.33 9.96 o 4 1 1 21.48 15.46 2.03 o 5 1 1 282.45 278.50 8.86 o 6 1 1 14.50 17.29 2.87 o 7 1 1 44.44 37.08 4.19 o -7 2 1 221.70 232.15 8.36 o -6 2 1 516.85 505.44 12.06 o -5 2 1 109.49 126.49 7.50 o -4 2 1 562.70 625.55 11.02 o -3 2 1 2391.78 2572.74 34.38 o -2 2 1 54.37 66.09 1.73 o -1 2 1 80.90 79.45 1.35 o 0 2 1 42.10 36.64 1.13 o 1 2 1 747.47 730.33 8.07 o 2 2 1 940.35 988.82 10.63 o 3 2 1 16.69 16.54 1.02 o 4 2 1 113.40 98.52 4.84 o 5 2 1 122.87 128.76 6.16 o 6 2 1 289.08 262.34 9.79 o 7 2 1 224.29 237.62 10.12 o -6 3 1 0.59 0.72 0.63 o -5 3 1 20.62 21.44 1.96 o -4 3 1 62.25 61.09 2.54 o -3 3 1 835.15 851.92 11.48 o -2 3 1 337.47 314.78 3.68 o -1 3 1 2.02 2.42 0.47 o 0 3 1 2196.51 2220.52 21.27 o 1 3 1 853.44 912.88 10.17 o 2 3 1 1203.25 1239.34 13.23 o 3 3 1 0.78 1.01 0.87 o 4 3 1 3.87 3.90 1.34 o 5 3 1 94.04 102.89 5.78 o 6 3 1 107.88 108.92 6.52 o -8 4 1 135.66 124.29 6.85 o -7 4 1 1.51 2.71 1.36 o -6 4 1 633.11 598.16 9.63 o -5 4 1 19.87 23.35 3.36 o -4 4 1 760.36 807.72 10.63 o -3 4 1 41.94 36.21 2.03 o -2 4 1 215.42 210.24 3.01 o -1 4 1 526.37 503.57 6.78 o 0 4 1 405.40 414.17 6.00 o 1 4 1 775.63 780.85 9.50 o 2 4 1 450.70 451.69 6.53 o 3 4 1 0.62 0.73 1.10 o 4 4 1 138.06 124.56 6.13 o 5 4 1 34.44 29.67 3.55 o 6 4 1 21.35 26.33 3.88 o -7 5 1 208.78 207.35 7.54 o -6 5 1 6.15 6.38 1.61 o -5 5 1 90.87 86.90 4.39 o -4 5 1 88.50 88.67 4.29 o -3 5 1 63.57 61.62 2.99 o -2 5 1 1.28 5.87 0.88 o -1 5 1 242.71 229.81 4.46 o 0 5 1 89.38 109.27 4.15 o 1 5 1 217.12 215.25 4.39 o 2 5 1 21.14 19.11 2.45 o 3 5 1 194.08 186.16 7.25 o 4 5 1 70.43 63.48 4.68 o 5 5 1 6.15 9.76 2.64 o -7 6 1 183.20 166.75 7.05 o -6 6 1 168.29 170.15 6.79 o -5 6 1 71.81 72.78 4.26 o -4 6 1 153.22 150.14 6.09 o -3 6 1 189.12 187.34 4.36 o -2 6 1 829.06 851.30 11.18 o -1 6 1 111.89 104.37 3.18 o 0 6 1 3.02 4.62 1.26 o 1 6 1 259.23 260.07 5.28 o 2 6 1 40.82 42.70 3.58 o 3 6 1 490.19 471.49 13.11 o 4 6 1 2.15 2.38 1.68 o -7 7 1 41.45 40.30 3.95 o -6 7 1 92.30 96.19 5.41 o -5 7 1 65.62 52.64 3.96 o -4 7 1 100.07 96.87 5.15 o -3 7 1 293.07 293.75 6.03 o -2 7 1 392.33 386.84 7.08 o -1 7 1 13.47 9.75 1.34 o 0 7 1 301.39 286.67 6.03 o 1 7 1 4.72 5.00 1.69 o 2 7 1 591.70 592.95 15.16 o 3 7 1 28.88 34.56 3.96 o -6 8 1 86.17 94.56 5.69 o -5 8 1 38.54 39.47 3.77 o -4 8 1 166.97 175.49 7.43 o -3 8 1 38.53 39.83 3.77 o -2 8 1 225.71 223.00 17.24 o -1 8 1 98.88 98.18 3.59 o 0 8 1 226.21 198.12 5.22 o 1 8 1 122.12 122.24 6.48 o 2 8 1 152.40 136.77 7.27 o -5 9 1 97.45 85.73 5.58 o -4 9 1 35.60 40.99 4.10 o -3 9 1 24.89 30.79 3.62 o -2 9 1 23.71 17.97 2.86 o -1 9 1 184.83 186.17 6.84 o 0 9 1 0.94 0.72 1.45 o 1 -10 2 49.20 42.82 4.34 o 2 -10 2 5.78 5.95 1.37 o 3 -10 2 125.13 115.86 4.51 o -1 -9 2 35.88 36.99 4.15 o 0 -9 2 148.96 144.68 7.21 o 1 -9 2 4.82 5.81 1.27 o 2 -9 2 90.56 81.18 7.16 o 3 -9 2 436.26 432.69 8.65 o 4 -9 2 110.73 114.70 4.34 o -3 -8 2 93.02 98.08 6.42 o -2 -8 2 176.90 174.09 8.00 o -1 -8 2 32.66 34.75 3.72 o 0 -8 2 97.65 99.98 5.50 o 1 -8 2 62.40 52.60 2.61 o 2 -8 2 46.09 44.37 2.50 o 3 -8 2 32.98 32.48 2.34 o 4 -8 2 0.94 1.77 1.45 o 6 -8 2 16.27 14.63 1.98 o -4 -7 2 47.04 56.13 5.01 o -3 -7 2 84.64 85.21 5.55 o -2 -7 2 8.81 10.73 2.36 o -1 -7 2 291.79 294.24 9.54 o 0 -7 2 284.71 247.53 13.26 o 1 -7 2 125.98 131.06 3.86 o 2 -7 2 160.05 162.88 7.17 o 3 -7 2 26.74 20.77 1.83 o 4 -7 2 35.37 36.07 3.29 o 5 -7 2 164.34 156.40 4.89 o 6 -7 2 1.16 1.70 0.99 o 7 -7 2 233.16 214.83 6.20 o -5 -6 2 148.92 143.04 7.66 o -4 -6 2 31.55 28.14 3.60 o -3 -6 2 31.93 30.41 3.45 o -2 -6 2 5.30 4.62 1.66 o -1 -6 2 1000.79 1000.05 12.23 o 0 -6 2 266.03 245.80 4.97 o 1 -6 2 1036.34 1066.89 13.18 o 2 -6 2 0.82 1.40 1.01 o 3 -6 2 313.24 313.17 6.14 o 4 -6 2 275.77 258.75 8.01 o 5 -6 2 67.05 71.43 4.52 o 6 -6 2 38.96 34.97 6.03 o 7 -6 2 1.96 1.69 1.14 o -5 -5 2 150.11 157.34 7.40 o -4 -5 2 198.81 213.77 8.28 o -3 -5 2 64.47 60.38 4.05 o -2 -5 2 277.56 273.58 8.17 o -1 -5 2 739.27 772.86 10.21 o 0 -5 2 862.72 901.78 8.61 o 1 -5 2 74.29 62.50 2.23 o 2 -5 2 213.56 195.97 8.28 o 3 -5 2 58.85 46.22 2.92 o 4 -5 2 701.22 673.34 14.20 o 5 -5 2 8.17 8.27 1.28 o 6 -5 2 36.31 39.87 2.34 o 7 -5 2 54.91 52.20 2.96 o -6 -4 2 23.40 28.39 3.61 o -5 -4 2 26.42 26.37 3.25 o -4 -4 2 234.35 223.30 7.73 o -3 -4 2 53.72 55.96 3.63 o -2 -4 2 772.86 776.38 8.90 o -1 -4 2 69.80 67.54 1.76 o 0 -4 2 1050.55 1118.24 20.73 o 1 -4 2 323.91 315.20 5.07 o 2 -4 2 597.55 624.53 11.89 o 3 -4 2 1423.43 1538.47 17.14 o 4 -4 2 277.92 284.28 5.47 o 5 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1.44 o -3 0 7 114.68 112.04 5.49 o -2 0 7 35.63 34.96 3.60 o -1 0 7 506.70 523.06 9.25 o 0 0 7 630.74 624.82 13.66 o 1 0 7 57.29 54.40 3.82 o 2 0 7 26.32 28.06 2.58 o 3 0 7 9.06 11.33 1.56 o 4 0 7 54.08 59.21 3.98 o 5 0 7 19.19 19.70 3.22 o -6 1 7 112.30 129.55 7.53 o -5 1 7 38.25 35.43 4.11 o -4 1 7 116.92 119.89 4.21 o -3 1 7 21.08 19.59 2.30 o -2 1 7 113.26 105.62 3.87 o -1 1 7 493.79 469.63 11.91 o 0 1 7 192.00 188.89 7.10 o 1 1 7 174.06 165.48 6.71 o 2 1 7 60.63 57.59 2.63 o 3 1 7 134.22 135.36 4.32 o 4 1 7 122.69 131.90 4.55 o -6 2 7 8.51 14.75 3.22 o -5 2 7 32.68 34.93 2.61 o -4 2 7 76.53 68.08 5.05 o -3 2 7 78.04 78.93 5.29 o -2 2 7 223.56 206.69 5.90 o -1 2 7 17.34 13.00 2.23 o 0 2 7 488.72 430.76 11.50 o 1 2 7 55.12 66.69 4.42 o 2 2 7 481.20 406.58 11.38 o 3 2 7 148.66 154.36 4.87 o 4 2 7 160.54 151.59 7.48 o -6 3 7 1.74 2.68 1.75 o -5 3 7 15.14 15.79 2.02 o -4 3 7 50.07 47.97 2.87 o -3 3 7 181.06 163.90 5.13 o -2 3 7 40.02 33.51 3.27 o -1 3 7 137.03 120.22 5.81 o 0 3 7 3.76 0.96 1.23 o 1 3 7 361.71 338.16 10.31 o 2 3 7 6.42 11.24 2.32 o -5 4 7 47.06 55.17 3.28 o -4 4 7 130.55 126.93 4.75 o -3 4 7 56.41 61.77 4.00 o -2 4 7 5.93 4.10 1.61 o -1 4 7 44.48 46.12 3.82 o 0 4 7 95.69 90.13 5.20 o 1 4 7 75.03 73.22 4.77 o 2 4 7 21.11 24.80 3.22 o -4 5 7 84.72 102.24 6.11 o -3 5 7 7.11 9.22 2.34 o -2 5 7 125.29 132.82 6.79 o -1 5 7 0.36 1.45 1.28 o 0 5 7 94.13 86.17 5.36 o 1 5 7 35.68 50.14 4.14 o -2 6 7 125.44 140.65 7.25 o 0 -8 8 26.42 37.29 4.02 o 1 -8 8 10.05 12.77 1.86 o 2 -8 8 147.19 140.31 7.22 o -2 -7 8 170.26 176.06 7.75 o -1 -7 8 33.33 32.23 3.54 o 0 -7 8 36.63 44.48 2.69 o 1 -7 8 48.57 57.73 3.61 o 2 -7 8 136.76 142.81 7.03 o 3 -7 8 9.05 15.78 2.88 o -1 -6 8 250.85 221.04 8.06 o 0 -6 8 62.12 64.33 3.07 o 1 -6 8 346.97 305.54 9.97 o 2 -6 8 3.66 6.53 1.83 o 3 -6 8 173.49 157.74 7.40 o 4 -6 8 33.37 41.94 4.32 o -4 -5 8 14.60 18.21 3.31 o -3 -5 8 39.32 48.14 4.34 o -2 -5 8 324.48 302.83 10.67 o -1 -5 8 225.83 224.39 5.38 o 0 -5 8 589.88 530.06 9.16 o 1 -5 8 28.99 35.02 3.43 o 2 -5 8 112.90 96.64 5.42 o 3 -5 8 232.42 215.52 8.42 o 4 -5 8 22.22 23.61 3.29 o -4 -4 8 31.10 23.98 3.66 o -3 -4 8 16.77 19.73 3.16 o -2 -4 8 6.85 12.62 2.31 o -1 -4 8 257.26 262.15 6.37 o 0 -4 8 20.94 28.93 3.12 o 1 -4 8 59.27 52.30 3.92 o 2 -4 8 130.67 125.17 6.11 o 3 -4 8 221.75 209.82 8.27 o 4 -4 8 165.80 171.00 7.65 o 5 -4 8 17.75 19.70 3.21 o -5 -3 8 19.73 22.54 3.80 o -4 -3 8 119.64 119.40 6.95 o -3 -3 8 35.22 37.95 4.05 o -2 -3 8 160.07 166.10 4.93 o -1 -3 8 98.40 96.82 3.75 o 0 -3 8 310.12 317.74 9.73 o 1 -3 8 147.28 140.33 6.41 o 2 -3 8 633.22 641.30 15.38 o 3 -3 8 168.07 173.72 7.45 o 4 -3 8 230.66 227.24 8.88 o 5 -3 8 5.55 10.34 2.54 o -5 -2 8 93.96 87.81 6.36 o -4 -2 8 182.37 176.40 8.55 o -3 -2 8 0.68 0.52 1.42 o -2 -2 8 49.39 44.59 2.52 o -1 -2 8 40.96 40.54 2.50 o 0 -2 8 230.50 213.03 7.75 o 1 -2 8 19.99 13.21 2.38 o 2 -2 8 96.25 94.28 5.28 o 3 -2 8 86.25 78.73 4.98 o 4 -2 8 62.89 71.42 4.88 o -5 -1 8 234.31 214.32 9.85 o -4 -1 8 18.35 22.75 3.50 o 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197.17 10.54 o -3 3 8 81.75 85.29 5.64 o -2 3 8 81.41 63.33 4.38 o -1 3 8 81.87 89.64 5.30 o 0 3 8 311.50 271.32 9.54 o 1 3 8 225.42 221.93 8.64 o 2 3 8 154.33 136.04 6.84 o -4 4 8 3.66 5.37 1.48 o -3 4 8 26.51 28.51 3.62 o -2 4 8 1.53 1.31 1.27 o -1 4 8 63.93 71.31 4.93 o 0 4 8 22.16 28.99 3.51 o 1 4 8 51.51 60.41 4.66 o 0 -7 9 99.94 101.48 4.11 o 1 -7 9 8.56 8.86 2.35 o 2 -7 9 43.59 54.15 4.61 o 0 -6 9 60.04 68.23 4.65 o 1 -6 9 39.64 46.60 4.31 o 2 -6 9 1.40 2.90 1.61 o 3 -6 9 62.97 44.75 4.38 o -3 -5 9 205.53 194.53 9.21 o -2 -5 9 22.34 30.10 3.86 o -1 -5 9 500.15 479.56 9.50 o 0 -5 9 58.48 65.44 4.68 o 1 -5 9 31.61 43.15 4.07 o 2 -5 9 81.31 85.75 5.46 o 3 -5 9 68.04 70.53 5.11 o -3 -4 9 8.71 9.32 2.67 o -2 -4 9 331.29 319.20 11.76 o -1 -4 9 96.15 100.69 10.18 o 0 -4 9 75.26 73.39 4.88 o 1 -4 9 127.29 126.24 6.49 o 2 -4 9 18.34 19.75 3.16 o 3 -4 9 112.98 106.83 6.25 o -4 -3 9 59.76 61.79 5.31 o -3 -3 9 16.61 18.04 3.41 o -2 -3 9 106.23 109.94 4.27 o -1 -3 9 29.84 29.07 2.44 o 0 -3 9 355.62 374.91 11.32 o 1 -3 9 192.06 208.64 8.35 o 2 -3 9 120.96 117.09 6.31 o 3 -3 9 89.32 101.67 6.05 o 4 -3 9 60.72 68.59 5.07 o -4 -2 9 33.13 33.85 4.43 o -3 -2 9 119.27 118.98 5.13 o -2 -2 9 30.31 31.00 2.57 o -1 -2 9 118.87 125.25 4.64 o 0 -2 9 580.56 584.40 14.71 o 1 -2 9 96.61 91.43 5.39 o 2 -2 9 45.50 49.77 4.24 o 3 -2 9 4.78 8.62 2.20 o -4 -1 9 18.52 25.90 4.05 o -3 -1 9 0.73 1.91 1.32 o -2 -1 9 14.71 18.44 2.10 o -1 -1 9 184.57 201.83 8.11 o 0 -1 9 47.92 48.87 3.90 o 1 -1 9 157.56 154.19 7.16 o 2 -1 9 42.34 41.73 4.00 o 3 -1 9 34.29 35.40 3.83 o -4 0 9 10.24 10.17 2.32 o -3 0 9 32.61 36.84 3.26 o -2 0 9 0.44 2.04 1.13 o -1 0 9 12.44 13.07 2.52 o 0 0 9 40.84 44.58 4.06 o 1 0 9 33.61 33.63 3.67 o 2 0 9 188.42 184.39 7.82 o 3 0 9 33.19 31.45 3.60 o -4 1 9 531.51 511.55 10.44 o -3 1 9 93.84 90.31 4.09 o -2 1 9 254.89 263.28 7.16 o -1 1 9 3.21 4.45 1.61 o 0 1 9 31.48 26.81 3.43 o 1 1 9 170.08 177.27 7.86 o 2 1 9 34.10 38.20 4.06 o -4 2 9 42.79 48.27 3.39 o -3 2 9 123.75 120.25 4.82 o -2 2 9 0.93 1.19 1.39 o -1 2 9 12.31 11.85 2.51 o 0 2 9 7.73 12.19 2.60 o 1 2 9 112.31 122.24 6.63 o -3 3 9 86.72 77.57 5.37 o -2 3 9 68.30 60.05 4.59 o -1 3 9 35.13 37.98 4.05 o 0 3 9 74.49 61.13 4.66 o -1 -5 10 127.00 129.54 4.95 o 0 -5 10 13.64 16.79 3.09 o 1 -5 10 0.52 4.12 1.92 o -2 -4 10 135.09 123.46 7.45 o -1 -4 10 18.76 24.41 2.47 o 0 -4 10 136.30 135.96 6.99 o 1 -4 10 148.18 156.73 7.70 o 2 -4 10 48.24 50.69 4.77 o -3 -3 10 57.06 54.50 5.63 o -2 -3 10 8.23 12.78 1.87 o -1 -3 10 64.30 72.78 5.03 o 0 -3 10 68.51 74.12 5.11 o 1 -3 10 214.85 221.52 9.17 o 2 -3 10 12.97 14.70 2.90 o -3 -2 10 107.24 116.86 7.63 o -2 -2 10 47.70 48.66 3.22 o -1 -2 10 162.18 167.49 7.56 o 0 -2 10 175.22 185.70 8.24 o 1 -2 10 123.29 108.08 6.27 o 2 -2 10 39.23 42.58 4.30 o -3 -1 10 20.58 28.37 3.36 o -2 -1 10 165.56 169.16 7.68 o -1 -1 10 11.18 12.49 2.67 o 0 -1 10 25.14 26.80 3.51 o 1 -1 10 0.44 0.38 1.26 o -3 0 10 118.24 120.34 6.26 o -2 0 10 68.74 72.26 5.09 o -1 0 10 34.63 30.72 3.79 o 0 0 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