#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/97/2209746.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209746_Fobs loop_ _publ_author_name 'Yang, Teng-Jiao' 'Xiao, Hong-Ping' 'Zhu, Long-Guan' _publ_section_title ; catena-Poly[[[cis-diaqua(1,10-phenanthroline-\k^2^N,N')manganese(II)]-\m~2~-3-sulfonatobenzoato-\k^2^O:O'] 0.32-hydrate] ; _journal_coeditor_code BH2034 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1904 _journal_page_last m1905 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.413 _cell_angle_gamma 90.000 _cell_length_a 14.4739 _cell_length_b 7.6406 _cell_length_c 18.9230 _exptl_crystal_F_000 976.80 _reflns_d_resolution_high 0.8380 _[local]_cod_data_source_file bh2034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hp8m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 221.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 27162.91 28937.04 581.46 o 4 0 0 2235.78 2640.01 43.01 o 5 0 0 2857.03 2869.77 47.53 o 6 0 0 1544.38 1683.32 32.08 o 7 0 0 1788.13 1923.84 36.91 o 8 0 0 2191.53 2385.65 51.80 o 9 0 0 8.94 34.07 6.28 o 10 0 0 184.37 192.98 12.26 o 11 0 0 2184.37 2067.33 44.20 o 12 0 0 124.17 121.61 14.77 o 13 0 0 901.09 902.79 35.15 o 14 0 0 2435.59 2359.50 95.40 o 15 0 0 107.06 133.85 24.64 o 16 0 0 351.72 348.75 38.56 o 1 1 0 13253.14 14297.62 196.30 o 2 1 0 601.62 622.07 13.02 o 3 1 0 5319.71 5684.67 65.28 o 4 1 0 2064.67 2145.10 25.60 o 5 1 0 4410.02 5024.85 55.15 o 6 1 0 8055.33 8490.35 90.33 o 7 1 0 325.97 348.85 8.73 o 8 1 0 845.78 958.94 19.96 o 9 1 0 110.74 114.58 6.59 o 10 1 0 956.97 961.76 22.25 o 11 1 0 113.54 142.79 9.16 o 12 1 0 35.61 44.91 6.44 o 13 1 0 135.90 156.24 13.03 o 14 1 0 46.04 46.95 9.51 o 15 1 0 313.92 310.94 50.59 o 16 1 0 11.92 52.37 17.65 o 0 2 0 4237.46 4251.84 74.07 o 1 2 0 15020.14 16472.22 173.10 o 2 2 0 43979.93 46797.41 660.12 o 3 2 0 10039.49 10214.57 148.39 o 4 2 0 48.12 45.58 4.41 o 5 2 0 66.10 48.21 5.95 o 6 2 0 580.50 650.46 12.79 o 7 2 0 72.91 59.06 6.45 o 8 2 0 194.03 219.88 8.39 o 9 2 0 521.03 499.69 14.22 o 10 2 0 625.28 667.01 17.33 o 11 2 0 95.89 120.90 9.07 o 12 2 0 2.55 10.69 6.77 o 13 2 0 746.06 673.06 32.63 o 14 2 0 125.28 133.62 12.56 o 15 2 0 6.44 15.02 10.49 o 16 2 0 247.29 264.65 35.67 o 1 3 0 4293.93 4610.69 58.59 o 2 3 0 1154.31 1219.30 19.90 o 3 3 0 6684.06 7529.07 94.08 o 4 3 0 7120.26 7722.14 146.74 o 5 3 0 2338.87 2574.40 59.44 o 6 3 0 21.31 93.01 21.27 o 7 3 0 128.58 151.31 13.78 o 8 3 0 554.06 469.66 18.64 o 9 3 0 44.00 79.17 8.52 o 10 3 0 521.10 505.19 17.86 o 11 3 0 778.66 720.78 22.27 o 12 3 0 177.13 211.20 14.42 o 13 3 0 766.12 704.28 28.11 o 14 3 0 1.80 11.41 7.79 o 15 3 0 254.82 289.84 21.56 o 0 4 0 20.02 37.19 9.82 o 1 4 0 188.82 181.60 8.78 o 2 4 0 1306.49 1373.31 23.79 o 3 4 0 55.58 78.85 5.38 o 4 4 0 458.91 442.55 17.59 o 5 4 0 87.38 97.14 20.41 o 6 4 0 911.48 822.95 30.15 o 7 4 0 1769.99 1764.78 49.82 o 8 4 0 90.99 81.75 12.73 o 9 4 0 738.28 714.00 42.90 o 10 4 0 243.13 316.76 30.50 o 11 4 0 2.96 23.32 14.13 o 12 4 0 357.74 338.53 21.16 o 13 4 0 2.31 13.10 8.28 o 14 4 0 1.21 8.11 13.05 o 1 5 0 1394.82 1460.55 33.10 o 2 5 0 9.01 25.70 10.97 o 3 5 0 225.22 205.41 11.69 o 4 5 0 171.87 186.74 21.06 o 5 5 0 14.53 12.83 7.14 o 6 5 0 27.89 32.79 10.64 o 7 5 0 248.33 250.49 19.50 o 8 5 0 97.32 109.19 33.86 o 9 5 0 10.54 10.70 8.32 o 10 5 0 150.62 176.39 16.29 o 11 5 0 22.55 27.65 9.28 o 12 5 0 70.35 113.03 13.89 o 13 5 0 240.41 255.06 25.80 o 0 6 0 580.54 507.02 32.20 o 1 6 0 76.94 97.38 10.08 o 2 6 0 282.47 276.16 19.54 o 3 6 0 22.88 30.47 7.76 o 4 6 0 1473.55 1362.26 44.55 o 5 6 0 618.76 588.04 27.97 o 6 6 0 1146.40 1041.94 39.43 o 7 6 0 2011.22 1925.50 58.07 o 8 6 0 19.23 7.63 8.43 o 9 6 0 958.00 927.07 43.34 o 10 6 0 249.97 243.83 19.18 o 11 6 0 49.14 80.07 13.46 o 12 6 0 34.22 51.50 14.22 o 1 7 0 30.01 42.98 9.97 o 2 7 0 158.66 185.90 18.57 o 3 7 0 242.63 283.24 22.31 o 4 7 0 15.59 4.32 8.43 o 5 7 0 422.95 442.09 27.96 o 6 7 0 71.20 101.09 16.18 o 7 7 0 163.33 163.00 43.78 o 8 7 0 411.58 426.23 29.92 o 9 7 0 167.57 231.33 23.62 o 10 7 0 123.11 160.17 20.67 o 0 8 0 23.14 58.83 19.33 o 1 8 0 9.47 4.94 13.34 o 2 8 0 99.99 87.38 25.11 o 3 8 0 9.34 12.81 10.63 o 4 8 0 200.61 225.74 31.39 o 5 8 0 2.67 28.70 12.20 o 6 8 0 135.84 148.51 19.96 o 7 8 0 136.49 155.46 20.02 o 1 9 0 62.83 119.17 31.18 o 2 9 0 2.38 28.31 13.08 o -16 1 1 0.83 31.32 10.96 o -15 1 1 157.71 211.36 21.73 o -14 1 1 17.94 35.71 9.91 o -13 1 1 0.92 8.80 5.50 o -12 1 1 240.97 241.32 19.24 o -11 1 1 457.11 447.76 13.89 o -10 1 1 139.44 155.71 10.49 o -9 1 1 2239.07 2186.96 30.34 o -8 1 1 5933.33 5815.48 65.87 o -7 1 1 542.82 591.61 11.54 o -6 1 1 11591.00 12127.61 125.85 o -5 1 1 5283.42 5271.23 57.28 o -4 1 1 5431.22 5958.93 61.91 o -3 1 1 48942.79 51093.57 607.48 o -1 1 1 23639.17 26130.54 452.16 o 0 1 1 1136.93 1419.52 27.71 o 1 1 1 4.58 7.29 1.45 o 2 1 1 2946.53 2977.32 45.48 o 3 1 1 493.23 493.67 8.29 o 4 1 1 55.15 32.39 2.81 o 5 1 1 7472.77 7685.37 81.83 o 6 1 1 401.15 321.86 8.08 o 7 1 1 1141.62 1106.71 17.84 o 8 1 1 4661.64 4531.72 53.76 o 9 1 1 1219.50 1165.39 20.04 o 10 1 1 1561.07 1393.93 23.46 o 11 1 1 2180.34 2066.53 35.43 o 12 1 1 4.90 13.40 4.99 o 13 1 1 254.15 256.29 14.76 o 14 1 1 156.81 207.37 22.78 o 15 1 1 10.62 47.49 16.91 o -16 2 1 104.73 145.51 19.43 o -15 2 1 41.80 46.10 10.57 o -14 2 1 476.88 446.50 19.30 o -13 2 1 38.76 48.90 8.12 o -12 2 1 194.50 202.28 13.35 o -11 2 1 103.84 88.12 9.31 o -10 2 1 26.27 28.68 5.47 o -9 2 1 1412.43 1364.10 40.44 o -8 2 1 2127.63 2231.53 39.56 o -7 2 1 9844.64 10601.26 123.55 o -6 2 1 0.39 0.90 3.74 o -5 2 1 20426.03 23003.84 331.98 o -4 2 1 374.99 411.97 11.03 o -3 2 1 450.32 443.09 12.35 o -2 2 1 41428.61 46079.43 623.15 o -1 2 1 8253.41 9443.88 136.77 o 0 2 1 230.45 267.96 9.65 o 1 2 1 65.48 59.50 8.64 o 2 2 1 690.93 793.49 16.36 o 3 2 1 56.63 77.07 8.59 o 4 2 1 3935.86 4105.32 64.27 o 5 2 1 909.03 886.29 15.54 o 6 2 1 4261.64 4772.74 59.98 o 7 2 1 2372.53 2269.73 33.20 o 8 2 1 87.55 82.35 6.89 o 9 2 1 781.99 712.66 17.56 o 10 2 1 18.00 25.68 5.45 o 11 2 1 136.28 144.61 9.93 o 12 2 1 141.86 140.11 11.62 o 13 2 1 217.14 212.22 14.41 o 14 2 1 39.56 37.31 9.70 o 15 2 1 14.26 18.97 11.41 o -15 3 1 31.63 57.34 11.91 o -14 3 1 1.32 17.44 7.70 o -13 3 1 267.15 299.60 23.65 o -12 3 1 207.53 232.51 14.91 o -11 3 1 4.73 20.77 6.91 o -10 3 1 3.97 16.04 5.40 o -9 3 1 939.59 934.79 24.15 o -8 3 1 28.86 23.08 8.33 o -7 3 1 102.23 117.47 19.26 o -6 3 1 1899.76 1692.75 91.64 o -5 3 1 2516.45 2386.84 58.68 o -4 3 1 1126.83 1220.33 20.90 o -3 3 1 1123.55 1238.09 21.20 o -2 3 1 69.77 119.78 5.88 o -1 3 1 2578.68 2723.74 38.95 o 0 3 1 306.70 331.51 9.96 o 1 3 1 2178.68 2139.33 45.34 o 2 3 1 883.28 1043.49 21.90 o 3 3 1 841.28 802.12 18.34 o 4 3 1 4612.21 5107.45 79.99 o 5 3 1 97.62 124.24 6.27 o 6 3 1 63.62 73.29 11.07 o 7 3 1 902.99 882.18 25.17 o 8 3 1 479.15 435.32 17.89 o 9 3 1 59.24 63.33 7.83 o 10 3 1 0.24 13.37 5.40 o 11 3 1 53.27 48.55 7.62 o 12 3 1 9.75 21.94 8.26 o 13 3 1 70.89 80.74 12.32 o 14 3 1 118.61 110.99 14.41 o 15 3 1 32.96 62.00 12.36 o -15 4 1 9.16 34.42 12.00 o -14 4 1 125.37 146.07 16.34 o -13 4 1 0.24 6.20 8.18 o -12 4 1 394.70 351.43 25.20 o -11 4 1 802.08 714.58 26.62 o -10 4 1 172.04 147.10 14.00 o -9 4 1 244.65 247.05 19.89 o -8 4 1 167.49 165.60 17.70 o -7 4 1 882.90 876.82 32.43 o -6 4 1 115.63 113.37 13.10 o -5 4 1 3513.83 3628.52 81.35 o -4 4 1 10597.89 11496.07 171.25 o -3 4 1 5471.40 6250.99 83.46 o -2 4 1 3945.59 4168.15 58.46 o -1 4 1 109.23 93.21 8.55 o 0 4 1 5584.67 6054.74 90.79 o 1 4 1 16.61 12.42 4.56 o 2 4 1 2971.71 3083.14 44.58 o 3 4 1 154.62 175.06 13.68 o 4 4 1 1298.64 1228.94 29.02 o 5 4 1 98.45 107.01 12.27 o 6 4 1 1460.14 1387.54 56.73 o 7 4 1 180.89 197.17 16.74 o 8 4 1 32.96 42.26 8.34 o 9 4 1 323.69 289.80 17.73 o 10 4 1 75.97 65.62 10.31 o 11 4 1 882.31 766.36 42.06 o 12 4 1 65.59 52.19 13.87 o 13 4 1 105.07 96.00 17.21 o 14 4 1 190.43 174.06 22.72 o -13 5 1 326.43 343.37 23.28 o -12 5 1 225.53 220.82 18.77 o -11 5 1 42.23 44.51 10.26 o -10 5 1 1508.34 1354.32 75.20 o -9 5 1 780.17 653.24 55.31 o -8 5 1 85.52 87.72 29.02 o -7 5 1 10.53 2.84 6.01 o -6 5 1 75.59 67.53 11.20 o -5 5 1 133.58 127.88 14.30 o -4 5 1 2778.50 2486.26 63.24 o -3 5 1 578.52 612.65 18.96 o -2 5 1 1142.42 1097.60 27.34 o -1 5 1 2297.24 2282.05 38.14 o 0 5 1 73.05 78.27 9.06 o 1 5 1 3082.03 3120.58 47.66 o 2 5 1 1607.04 1634.80 28.93 o 3 5 1 2497.60 2333.24 37.46 o 4 5 1 3069.35 2959.77 100.33 o 5 5 1 4.83 11.38 6.79 o 6 5 1 483.88 502.37 24.25 o 7 5 1 1.76 -0.51 9.09 o 8 5 1 125.25 173.19 17.80 o 9 5 1 84.50 92.63 11.84 o 10 5 1 471.71 445.98 22.86 o 11 5 1 13.86 47.87 10.69 o 12 5 1 629.72 586.42 33.29 o 13 5 1 77.99 94.48 33.38 o -12 6 1 15.44 27.71 9.04 o -11 6 1 156.80 169.89 17.64 o -10 6 1 49.78 77.84 14.65 o -9 6 1 79.18 112.43 16.34 o -8 6 1 0.01 14.94 9.45 o -7 6 1 100.17 111.33 15.94 o -6 6 1 207.48 192.57 19.12 o -5 6 1 213.27 267.92 21.32 o -4 6 1 355.33 385.71 29.84 o -3 6 1 10.08 5.84 6.31 o -2 6 1 863.97 900.63 49.59 o -1 6 1 1403.48 1359.34 39.93 o 0 6 1 328.73 298.90 18.04 o 1 6 1 178.00 161.46 12.01 o 2 6 1 132.14 139.06 14.92 o 3 6 1 480.61 475.68 23.49 o 4 6 1 378.05 372.11 21.36 o 5 6 1 40.49 59.00 25.87 o 6 6 1 0.27 13.00 10.51 o 7 6 1 8.65 21.35 21.43 o 8 6 1 98.05 95.13 14.67 o 9 6 1 65.86 75.84 12.06 o 10 6 1 10.91 12.42 8.42 o 11 6 1 13.47 19.34 11.69 o 12 6 1 146.45 137.77 21.43 o -10 7 1 57.49 89.61 16.97 o -9 7 1 14.62 49.66 14.84 o -8 7 1 48.72 61.08 12.90 o -7 7 1 176.29 182.67 21.29 o -6 7 1 7.00 17.96 18.70 o -5 7 1 149.55 159.13 18.37 o -4 7 1 218.69 297.91 33.46 o -3 7 1 0.69 9.80 7.72 o -2 7 1 764.87 776.68 49.59 o -1 7 1 722.44 723.55 48.33 o 0 7 1 21.03 26.83 6.14 o 1 7 1 855.71 820.82 33.71 o 2 7 1 56.75 54.39 11.74 o 3 7 1 365.39 370.29 24.85 o 4 7 1 265.81 280.13 22.57 o 5 7 1 17.34 40.11 11.77 o 6 7 1 210.17 209.02 21.22 o 7 7 1 5.15 29.06 13.79 o 8 7 1 14.24 22.84 11.30 o 9 7 1 61.24 115.03 16.72 o 10 7 1 182.09 190.87 32.02 o -8 8 1 4.57 9.91 10.49 o -7 8 1 2.67 26.71 17.81 o -6 8 1 1.69 29.74 11.76 o -5 8 1 20.37 34.87 13.05 o -4 8 1 225.82 249.98 34.20 o -3 8 1 597.04 573.00 31.28 o -2 8 1 102.46 118.46 17.03 o -1 8 1 827.50 790.21 54.26 o 0 8 1 1666.86 1474.35 54.81 o 1 8 1 0.42 17.62 9.97 o 2 8 1 552.42 472.68 37.22 o 3 8 1 36.26 53.25 20.59 o 4 8 1 77.23 116.44 30.86 o 5 8 1 34.24 65.66 13.90 o 6 8 1 30.69 44.73 17.07 o 7 8 1 72.06 80.07 15.45 o -2 9 1 34.79 57.21 21.17 o -1 9 1 3.31 44.89 12.52 o 0 9 1 59.13 111.54 18.89 o 1 9 1 92.18 127.97 20.39 o 2 9 1 77.33 83.80 20.01 o -16 0 2 391.44 426.97 42.97 o -15 0 2 725.23 700.96 47.70 o -14 0 2 1540.17 1496.38 71.28 o -13 0 2 120.98 121.19 22.85 o -12 0 2 2064.97 2120.53 57.32 o -11 0 2 1124.79 1046.29 27.67 o -10 0 2 2475.73 2696.94 51.25 o -9 0 2 3858.20 4041.48 68.96 o -8 0 2 48.79 62.29 7.49 o -7 0 2 10133.47 11272.45 166.98 o -6 0 2 1072.06 1036.78 21.90 o -5 0 2 170.45 170.20 5.70 o -4 0 2 682.86 747.24 19.11 o -3 0 2 810.12 782.61 18.77 o -1 0 2 38327.70 36990.46 649.84 o 2 0 2 28760.55 31232.54 439.86 o 3 0 2 7707.21 8385.89 122.87 o 4 0 2 1046.87 1133.95 22.57 o 5 0 2 109.18 83.22 6.78 o 6 0 2 603.10 641.03 17.29 o 7 0 2 110.64 102.76 8.11 o 8 0 2 680.83 722.41 20.53 o 9 0 2 6.64 4.98 5.14 o 10 0 2 101.90 116.58 10.59 o 11 0 2 452.24 491.75 19.26 o 12 0 2 230.16 241.39 29.92 o 13 0 2 1562.12 1549.50 49.87 o 14 0 2 50.55 29.68 15.08 o -16 1 2 78.04 111.87 17.83 o -15 1 2 105.42 118.91 17.96 o -14 1 2 8.36 14.48 9.46 o -13 1 2 12.77 19.33 6.28 o -12 1 2 5.55 9.79 8.65 o -11 1 2 364.33 424.46 13.35 o -10 1 2 573.06 570.35 15.07 o -9 1 2 4.52 3.62 3.06 o -8 1 2 5236.11 5702.19 64.42 o -7 1 2 20.03 38.45 5.53 o -6 1 2 136.78 129.29 4.85 o -5 1 2 2730.99 3018.31 34.12 o -4 1 2 14883.12 15968.32 144.38 o -3 1 2 1497.71 1741.72 25.25 o -2 1 2 445.09 399.22 7.74 o -1 1 2 2004.38 2241.73 30.32 o 0 1 2 9676.45 10661.42 185.07 o 1 1 2 840.06 902.36 14.23 o 2 1 2 92.40 93.71 4.51 o 3 1 2 1659.28 1803.13 22.10 o 4 1 2 9110.69 9843.17 102.50 o 5 1 2 423.59 380.72 8.46 o 6 1 2 325.55 294.85 7.98 o 7 1 2 15.21 33.17 3.88 o 8 1 2 14.08 15.33 3.44 o 9 1 2 587.72 538.98 12.95 o 10 1 2 182.85 183.46 9.38 o 11 1 2 87.28 101.31 8.65 o 12 1 2 340.42 379.59 16.35 o 13 1 2 126.27 127.91 10.37 o 14 1 2 86.60 89.49 14.96 o 15 1 2 29.67 25.58 16.49 o -16 2 2 18.08 52.05 19.44 o -15 2 2 177.79 212.33 18.04 o -14 2 2 577.81 547.06 20.51 o -13 2 2 6.56 16.12 6.18 o -12 2 2 805.10 778.25 22.97 o -11 2 2 1240.79 1147.97 27.75 o -10 2 2 345.94 371.51 14.71 o -9 2 2 1486.23 1438.91 30.05 o -8 2 2 575.38 666.83 20.15 o -7 2 2 3817.06 4113.95 71.63 o -6 2 2 1082.77 1164.63 22.85 o -5 2 2 482.31 539.26 13.58 o -4 2 2 1121.75 1293.58 22.78 o -3 2 2 3913.98 4201.95 56.53 o -2 2 2 35057.37 38201.42 536.67 o -1 2 2 4303.42 4461.57 68.10 o 0 2 2 1843.28 2009.38 47.15 o 1 2 2 177.19 170.80 7.93 o 2 2 2 46.76 37.59 3.82 o 3 2 2 14.74 10.08 3.34 o 4 2 2 1576.63 1652.73 26.88 o 5 2 2 0.77 9.71 2.95 o 6 2 2 253.49 307.34 10.72 o 7 2 2 508.89 546.87 13.07 o 8 2 2 26.10 38.09 4.53 o 9 2 2 76.26 69.09 7.12 o 10 2 2 38.32 69.22 7.40 o 11 2 2 2.61 16.54 5.07 o 12 2 2 748.35 730.57 19.95 o 13 2 2 331.35 328.75 24.96 o 14 2 2 0.10 13.16 10.01 o 15 2 2 105.47 132.16 19.03 o -15 3 2 126.92 151.16 16.66 o -14 3 2 2.83 11.04 7.06 o -13 3 2 359.18 356.90 18.42 o -12 3 2 0.30 5.76 6.01 o -11 3 2 658.70 647.16 21.56 o -10 3 2 1875.76 1896.16 38.67 o -9 3 2 622.82 549.37 27.97 o -8 3 2 1167.97 1107.33 72.69 o -7 3 2 89.44 80.28 9.41 o -6 3 2 3937.89 4035.07 59.71 o -5 3 2 3268.33 3447.44 59.18 o -4 3 2 7342.42 7761.68 99.13 o -3 3 2 2547.63 2728.56 39.63 o -2 3 2 5827.32 5927.76 111.06 o -1 3 2 608.22 558.83 14.86 o 0 3 2 23.58 22.60 4.83 o 1 3 2 162.25 129.90 8.65 o 2 3 2 298.17 318.28 16.80 o 3 3 2 15484.47 16773.74 242.03 o 4 3 2 10.13 12.33 4.29 o 5 3 2 437.64 416.93 26.51 o 6 3 2 2380.10 2450.56 39.35 o 7 3 2 85.82 107.90 10.50 o 8 3 2 151.30 134.04 11.83 o 9 3 2 255.93 239.16 15.49 o 10 3 2 1168.55 1063.78 56.80 o 11 3 2 12.76 11.06 6.35 o 12 3 2 928.94 941.47 39.79 o 13 3 2 6.35 18.88 10.68 o 14 3 2 208.40 239.88 24.78 o 15 3 2 104.08 133.09 19.84 o -15 4 2 81.64 72.48 15.00 o -14 4 2 0.36 25.35 7.79 o -13 4 2 3.52 20.91 10.74 o -12 4 2 146.32 131.83 12.37 o -11 4 2 63.67 74.36 12.05 o -10 4 2 24.70 22.04 10.66 o -9 4 2 404.39 341.68 23.43 o -8 4 2 1536.07 1420.47 44.60 o -7 4 2 1023.86 1051.13 50.74 o -6 4 2 389.29 313.14 18.22 o -5 4 2 437.79 355.53 15.27 o -4 4 2 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