#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209778.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209778_Fobs loop_ _publ_author_name 'Bogdanov, Milen G.' 'Todorov, Iliya S.' _publ_section_title ; Methyl trans-6-oxo-11-thiophen-2-yl-11,12-dihydro-6H-dibenzo[c,h]chromene-12-carboxylate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3334 _journal_page_last o3336 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.405 _cell_angle_gamma 90.000 _cell_length_a 10.6396 _cell_length_b 15.3834 _cell_length_c 22.6827 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.8419 _[local]_cod_data_source_file bv2022Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 447.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18861.25 19199.18 238.06 o 4 0 0 21.85 61.75 55.25 o 6 0 0 2384.25 2421.58 82.27 o 8 0 0 8321.17 9763.95 285.78 o 10 0 0 2710.86 3030.75 126.33 o 12 0 0 370.14 372.11 95.11 o 1 1 0 8678.51 10070.04 152.13 o 3 1 0 3898.03 3829.29 115.72 o 5 1 0 20.98 -24.36 54.05 o 7 1 0 1703.21 1716.02 112.93 o 9 1 0 30.88 -10.87 109.83 o 11 1 0 380.46 631.82 93.22 o 0 2 0 3122.59 1873.64 75.06 o 2 2 0 1431.71 1037.27 72.99 o 4 2 0 1690.95 1528.44 66.21 o 6 2 0 246.56 225.93 57.02 o 8 2 0 1546.36 1695.03 94.37 o 10 2 0 417.48 336.77 82.83 o 12 2 0 99.62 49.74 95.25 o 1 3 0 73723.23 73525.34 462.54 o 3 3 0 3388.58 3550.47 100.44 o 5 3 0 6125.01 6309.08 196.43 o 7 3 0 8.82 -29.09 63.10 o 9 3 0 2219.23 2357.10 164.92 o 11 3 0 1.87 198.26 81.24 o 0 4 0 38299.17 33722.75 501.98 o 2 4 0 10921.92 9105.40 233.45 o 4 4 0 647.55 689.69 59.31 o 6 4 0 27.53 -87.38 111.55 o 8 4 0 1716.02 1830.25 97.29 o 10 4 0 1012.44 1226.42 101.17 o 12 4 0 8.97 113.16 102.24 o 1 5 0 2303.45 1431.19 65.24 o 3 5 0 7936.51 7848.78 195.98 o 5 5 0 397.23 510.54 61.83 o 7 5 0 759.09 799.96 76.70 o 9 5 0 647.78 654.21 87.84 o 11 5 0 182.01 287.57 92.22 o 0 6 0 1544.16 1777.24 95.02 o 2 6 0 4316.01 4338.89 121.22 o 4 6 0 456.04 362.84 55.71 o 6 6 0 1600.87 1619.25 83.99 o 8 6 0 69.27 49.71 102.25 o 10 6 0 155.24 36.73 117.75 o 1 7 0 851.22 940.37 72.65 o 3 7 0 2549.94 2975.44 85.97 o 5 7 0 481.79 425.81 69.09 o 7 7 0 235.71 301.76 77.74 o 9 7 0 301.14 263.04 84.90 o 11 7 0 3.46 -35.24 94.22 o 0 8 0 6661.34 6847.98 287.14 o 2 8 0 17448.48 18470.78 393.62 o 4 8 0 20.53 43.00 57.92 o 6 8 0 308.70 136.68 162.16 o 8 8 0 793.07 638.27 92.32 o 10 8 0 30.56 120.17 114.31 o 1 9 0 76.61 -9.11 74.37 o 3 9 0 5174.80 5312.77 148.22 o 5 9 0 61.22 84.07 69.38 o 7 9 0 140.06 239.14 174.90 o 9 9 0 43.03 51.62 89.51 o 0 10 0 3416.73 3189.52 139.78 o 2 10 0 1999.96 1901.91 86.91 o 4 10 0 185.39 278.96 69.61 o 6 10 0 352.63 353.31 76.35 o 8 10 0 32.10 59.94 83.72 o 10 10 0 27.45 28.72 92.50 o 1 11 0 10.26 47.75 64.00 o 3 11 0 1021.84 837.06 80.79 o 5 11 0 0.02 65.60 81.94 o 7 11 0 22.52 152.47 99.50 o 9 11 0 3.46 20.75 207.61 o 0 12 0 420.28 364.95 103.29 o 2 12 0 379.11 574.01 77.15 o 4 12 0 375.03 431.16 85.73 o 6 12 0 6.66 56.30 185.57 o 8 12 0 0.91 -118.78 118.78 o 1 13 0 61.45 23.82 75.71 o 3 13 0 20.23 74.16 78.61 o 5 13 0 61.37 -21.36 80.00 o 7 13 0 191.85 25.75 91.78 o 0 14 0 44.46 78.50 110.17 o 2 14 0 5.81 -84.43 84.43 o 4 14 0 0.50 59.97 83.54 o 6 14 0 312.65 222.65 97.43 o 8 14 0 247.57 250.55 106.35 o 1 15 0 441.23 483.34 88.13 o 3 15 0 322.87 335.01 99.50 o 5 15 0 31.46 -24.42 86.86 o 7 15 0 12.32 -8.41 107.60 o 0 16 0 353.14 112.24 125.32 o 2 16 0 51.92 11.99 89.17 o 4 16 0 0.00 138.31 115.34 o 6 16 0 102.62 95.37 186.95 o 1 17 0 108.31 19.57 116.03 o 3 17 0 18.43 13.20 84.88 o 0 18 0 953.96 866.93 167.33 o 2 18 0 192.67 132.97 106.14 o -11 1 1 110.79 24.79 135.65 o -9 1 1 1152.49 1258.73 126.01 o -7 1 1 0.51 -28.23 88.83 o -5 1 1 193.27 254.78 79.19 o -3 1 1 9634.41 9684.26 326.39 o -1 1 1 47082.00 47389.78 400.07 o 1 1 1 132.54 -32.36 55.09 o 3 1 1 4469.15 5235.31 210.02 o 5 1 1 2032.90 2154.58 103.98 o 7 1 1 1175.80 1341.36 108.80 o 9 1 1 10.66 138.41 103.29 o 11 1 1 17.37 6.20 126.70 o -12 2 1 364.48 190.05 150.80 o -10 2 1 185.27 16.53 120.50 o -8 2 1 1786.83 2023.75 137.72 o -6 2 1 926.17 1099.67 101.22 o -4 2 1 1274.26 1691.16 95.02 o -2 2 1 46513.57 42898.83 531.59 o 0 2 1 19592.00 19766.52 296.09 o 2 2 1 13084.16 13795.80 327.08 o 4 2 1 428.16 413.15 77.12 o 6 2 1 5059.02 5968.65 246.51 o 8 2 1 887.72 968.84 110.17 o 10 2 1 397.67 541.23 128.77 o 12 2 1 395.16 240.32 143.23 o -11 3 1 48.70 139.09 132.90 o -9 3 1 1985.18 2174.55 157.00 o -7 3 1 41.07 81.25 94.34 o -5 3 1 1234.02 1200.89 90.89 o -3 3 1 1758.68 1351.69 92.27 o -1 3 1 1199.51 1713.89 84.70 o 1 3 1 11284.58 9384.03 285.07 o 3 3 1 9472.83 10748.81 359.44 o 5 3 1 24.70 30.99 70.24 o 7 3 1 246.94 203.13 90.20 o 9 3 1 0.96 -98.47 114.31 o 11 3 1 649.54 469.61 138.41 o -12 4 1 2.65 48.20 140.47 o -10 4 1 2.32 -126.01 126.01 o -8 4 1 541.32 550.18 115.68 o -6 4 1 383.86 626.61 95.71 o -4 4 1 279.90 142.54 76.43 o -2 4 1 5016.66 5925.96 234.12 o 0 4 1 6206.27 5425.36 207.95 o 2 4 1 10868.28 9524.51 342.92 o 4 4 1 462.86 271.30 76.43 o 6 4 1 5.25 68.86 81.94 o 8 4 1 579.50 591.49 112.93 o 10 4 1 2943.87 3173.69 177.65 o 12 4 1 56.33 258.22 127.39 o -11 5 1 523.25 771.90 138.41 o -9 5 1 412.07 503.36 125.32 o -7 5 1 494.24 550.18 99.84 o -5 5 1 2230.37 2306.07 120.50 o -3 5 1 1380.57 1164.40 95.02 o -1 5 1 2008.79 2383.88 103.98 o 1 5 1 7491.74 9763.44 345.67 o 3 5 1 3508.36 3216.38 130.14 o 5 5 1 979.55 1117.57 94.34 o 7 5 1 107.28 -19.97 94.34 o 9 5 1 257.00 192.12 123.26 o 11 5 1 210.49 172.15 122.57 o -10 6 1 165.40 271.99 123.26 o -8 6 1 656.82 689.96 125.32 o -6 6 1 54.79 125.32 92.27 o -4 6 1 67.70 168.70 74.37 o -2 6 1 2808.57 3527.62 148.73 o 0 6 1 3915.99 3599.92 139.09 o 2 6 1 6513.87 7860.20 278.88 o 4 6 1 1844.67 1914.27 114.31 o 6 6 1 299.41 339.47 95.71 o 8 6 1 177.87 281.63 102.60 o 10 6 1 454.57 600.45 121.19 o -11 7 1 0.02 -135.65 135.65 o -9 7 1 1914.87 1942.50 161.13 o -7 7 1 1742.51 1670.51 140.47 o -5 7 1 4725.87 4614.21 183.16 o -3 7 1 4875.58 4807.70 166.64 o -1 7 1 7262.67 7873.97 285.07 o 1 7 1 10819.44 10938.86 406.95 o 3 7 1 24.97 33.05 76.43 o 5 7 1 383.59 363.57 91.58 o 7 7 1 491.35 563.95 108.11 o 9 7 1 418.11 516.44 118.44 o 11 7 1 448.65 553.62 137.72 o -10 8 1 14.38 -103.98 130.14 o -8 8 1 460.04 451.02 134.96 o -6 8 1 258.19 378.72 110.86 o -4 8 1 484.99 419.35 97.78 o -2 8 1 447.92 518.50 92.27 o 0 8 1 1269.53 1200.20 90.89 o 2 8 1 6870.04 7743.83 305.73 o 4 8 1 70.70 71.61 84.01 o 6 8 1 962.54 1164.40 121.19 o 8 8 1 2458.29 2551.21 168.70 o 10 8 1 126.63 183.16 124.63 o -9 9 1 353.95 478.57 124.63 o -7 9 1 860.48 639.70 134.96 o -5 9 1 927.15 1008.09 121.19 o -3 9 1 794.00 791.87 95.71 o -1 9 1 5879.79 6431.38 256.15 o 1 9 1 172.44 227.23 90.89 o 3 9 1 560.40 706.49 101.22 o 5 9 1 219.48 320.19 94.34 o 7 9 1 1.39 -4.82 106.73 o 9 9 1 70.75 61.28 119.13 o -10 10 1 0.08 134.96 128.08 o -8 10 1 180.60 146.67 126.01 o -6 10 1 121.80 130.83 112.24 o -4 10 1 1266.93 1255.29 118.44 o -2 10 1 64.58 -95.71 95.71 o 0 10 1 4626.51 4653.46 181.10 o 2 10 1 1809.47 1448.78 111.55 o 4 10 1 0.02 77.81 88.83 o 6 10 1 38.05 150.80 90.89 o 8 10 1 5.25 17.90 112.24 o 10 10 1 197.70 291.96 132.90 o -9 11 1 0.82 -27.54 126.01 o -7 11 1 3.55 5.51 114.99 o -5 11 1 1188.40 1248.40 130.83 o -3 11 1 1611.60 1371.66 123.26 o -1 11 1 459.30 418.66 101.22 o 1 11 1 65.09 101.91 90.20 o 3 11 1 23.59 -84.70 99.16 o 5 11 1 54.17 81.94 103.98 o 7 11 1 54.63 137.03 110.86 o 9 11 1 9.77 81.94 115.68 o -8 12 1 107.53 125.32 134.27 o -6 12 1 87.51 -129.45 142.54 o -4 12 1 738.30 758.82 127.39 o -2 12 1 2122.23 2109.82 143.23 o 0 12 1 507.46 550.18 107.42 o 2 12 1 151.71 254.09 108.80 o 4 12 1 276.50 230.68 112.93 o 6 12 1 1501.32 1614.04 144.60 o 8 12 1 58.34 165.26 129.45 o -7 13 1 0.00 77.81 126.01 o -5 13 1 929.67 757.44 132.90 o -3 13 1 529.08 624.55 122.57 o -1 13 1 70.94 -106.04 106.04 o 1 13 1 171.20 86.07 114.31 o 3 13 1 310.74 192.80 111.55 o 5 13 1 942.95 791.87 142.54 o 7 13 1 267.51 305.73 132.90 o -8 14 1 28.37 -145.98 145.98 o -6 14 1 139.60 174.90 127.39 o -4 14 1 485.92 532.96 125.32 o -2 14 1 232.69 246.51 114.99 o 0 14 1 107.00 218.97 98.47 o 2 14 1 19.46 117.75 108.11 o 4 14 1 1096.77 700.98 138.41 o 6 14 1 156.34 58.53 132.90 o 8 14 1 108.26 364.95 133.59 o -7 15 1 83.57 0.00 148.05 o -5 15 1 523.53 784.30 145.29 o -3 15 1 1810.35 1731.10 163.88 o -1 15 1 33.18 -17.21 119.81 o 1 15 1 148.87 212.77 123.26 o 3 15 1 166.43 277.50 114.99 o 5 15 1 1.01 -6.89 117.75 o 7 15 1 121.87 8.26 141.85 o -6 16 1 23.88 -83.32 152.87 o -4 16 1 53.57 20.66 129.45 o -2 16 1 510.59 516.44 146.67 o 0 16 1 178.80 68.86 128.77 o 2 16 1 49.37 19.28 128.08 o 4 16 1 0.29 33.74 118.44 o 6 16 1 370.30 565.33 141.85 o -3 17 1 46.09 70.92 127.39 o -1 17 1 530.40 518.50 140.47 o 1 17 1 25.46 116.37 121.88 o 3 17 1 39.56 -35.81 128.08 o -2 18 1 34.57 66.79 143.23 o 0 18 1 26.11 187.98 137.03 o 2 18 1 3.47 -140.47 140.47 o -12 0 2 403.92 363.57 128.77 o -10 0 2 770.37 524.01 128.77 o -8 0 2 2951.66 3201.23 152.18 o -6 0 2 1936.43 1945.94 109.48 o -4 0 2 152.93 144.60 77.81 o -2 0 2 16159.30 16228.57 331.21 o 2 0 2 2789.83 1486.65 81.25 o 4 0 2 265.87 163.88 76.43 o 6 0 2 3160.74 3009.12 127.39 o 8 0 2 1.28 -45.45 95.02 o 10 0 2 1788.51 1777.93 150.80 o 12 0 2 7.89 56.46 121.19 o -11 1 2 37.97 -111.55 130.14 o -9 1 2 256.76 511.62 109.48 o -7 1 2 469.18 461.35 99.16 o -5 1 2 371.63 250.64 79.88 o -3 1 2 322.86 574.97 81.25 o -1 1 2 609.53 517.82 61.28 o 1 1 2 10832.20 11772.73 257.53 o 3 1 2 8132.68 7190.89 245.14 o 5 1 2 2196.73 2112.58 101.22 o 7 1 2 1091.12 1297.29 110.86 o 9 1 2 67.62 -14.46 103.98 o 11 1 2 268.90 256.15 130.83 o -12 2 2 52.88 225.86 132.21 o -10 2 2 155.66 314.68 117.75 o -8 2 2 235.87 310.55 101.22 o -6 2 2 1736.64 1618.17 112.93 o -4 2 2 1008.41 1090.72 88.14 o -2 2 2 554.79 469.61 81.94 o 0 2 2 467.73 475.12 64.04 o 2 2 2 0.84 -1.38 74.37 o 4 2 2 9.65 141.16 72.99 o 6 2 2 171.81 310.55 81.94 o 8 2 2 379.55 541.23 100.53 o 10 2 2 50.90 27.54 116.37 o 12 2 2 46.72 35.81 130.14 o -11 3 2 795.92 767.77 149.42 o -9 3 2 13.50 -24.79 112.93 o -7 3 2 1902.67 1996.21 126.01 o -5 3 2 58.14 -14.46 75.74 o -3 3 2 1170.70 1008.09 90.89 o -1 3 2 6774.21 6890.67 265.79 o 1 3 2 31462.99 33804.01 475.81 o 3 3 2 2333.91 2171.11 98.47 o 5 3 2 3683.01 3544.83 123.95 o 7 3 2 135.50 208.64 89.52 o 9 3 2 164.10 79.19 114.31 o 11 3 2 520.33 421.41 157.00 o -12 4 2 13.71 -40.63 145.29 o -10 4 2 53.54 114.31 123.26 o -8 4 2 909.33 883.45 127.39 o -6 4 2 611.12 641.07 95.02 o -4 4 2 801.38 926.15 88.14 o -2 4 2 8020.72 8462.71 323.63 o 0 4 2 1757.36 1775.86 90.89 o 2 4 2 11806.01 12306.39 375.28 o 4 4 2 763.34 1152.69 86.07 o 6 4 2 1166.06 1251.16 99.16 o 8 4 2 144.09 53.02 108.11 o 10 4 2 1108.80 1083.14 132.90 o 12 4 2 220.77 259.60 145.29 o -11 5 2 115.57 139.09 130.14 o -9 5 2 1485.20 1587.19 149.42 o -7 5 2 540.92 232.74 109.48 o -5 5 2 3934.00 4301.59 188.67 o -3 5 2 2027.15 1746.94 96.40 o -1 5 2 5530.65 5592.00 235.50 o 1 5 2 10037.91 10252.34 353.93 o 3 5 2 1086.49 819.42 83.32 o 5 5 2 2620.50 2664.82 119.81 o 7 5 2 91.37 -94.34 94.34 o 9 5 2 2604.52 2856.94 163.88 o 11 5 2 242.44 152.87 132.90 o -10 6 2 0.51 72.99 124.63 o -8 6 2 851.73 902.73 128.77 o -6 6 2 14.36 0.00 94.34 o -4 6 2 2307.40 2591.83 121.88 o -2 6 2 2400.68 2306.76 103.29 o 0 6 2 4618.43 4910.30 212.08 o 2 6 2 7825.07 7029.76 275.43 o 4 6 2 151.62 0.00 81.25 o 6 6 2 29.64 22.03 90.89 o 8 6 2 1068.22 1162.33 126.01 o 10 6 2 618.78 822.86 128.08 o -11 7 2 90.47 -145.29 145.29 o -9 7 2 1223.63 1212.60 152.18 o -7 7 2 1047.65 1366.15 126.70 o -5 7 2 1128.98 1231.19 116.37 o -3 7 2 1954.71 2079.53 104.66 o -1 7 2 1981.56 2045.79 102.60 o 1 7 2 551.70 785.68 82.63 o 3 7 2 3971.70 4586.66 185.23 o 5 7 2 192.54 246.51 88.83 o 7 7 2 2446.69 2693.06 149.42 o 9 7 2 463.42 389.74 122.57 o 11 7 2 931.91 922.70 143.91 o -10 8 2 113.28 235.50 128.08 o -8 8 2 4839.30 4332.58 197.62 o -6 8 2 2841.07 2681.35 149.42 o -4 8 2 3.18 55.09 88.14 o -2 8 2 522.67 431.05 86.07 o 0 8 2 1825.94 1772.42 104.66 o 2 8 2 75.25 17.21 81.25 o 4 8 2 721.66 706.49 99.84 o 6 8 2 1782.14 1815.11 136.34 o 8 8 2 2014.93 2052.67 152.87 o 10 8 2 138.61 170.77 110.86 o -9 9 2 71.28 98.47 123.95 o -7 9 2 587.72 656.91 130.14 o -5 9 2 832.35 754.00 119.81 o -3 9 2 510.33 550.18 95.02 o -1 9 2 1586.81 1618.86 110.86 o 1 9 2 154.35 172.83 83.32 o 3 9 2 4939.28 4531.58 173.52 o 5 9 2 381.96 401.44 106.04 o 7 9 2 598.18 519.19 121.19 o 9 9 2 303.25 234.81 119.81 o -10 10 2 69.29 71.61 128.77 o -8 10 2 340.99 499.91 123.95 o -6 10 2 840.73 1150.63 130.14 o -4 10 2 1817.90 1703.56 128.08 o -2 10 2 1112.77 949.56 114.31 o 0 10 2 261.69 433.12 86.76 o 2 10 2 640.41 647.96 106.04 o 4 10 2 1960.88 1920.46 132.90 o 6 10 2 1581.83 1766.91 140.47 o 8 10 2 712.13 601.82 131.52 o 10 10 2 50.98 100.53 132.90 o -9 11 2 26.32 -102.60 128.08 o -7 11 2 1095.20 747.11 140.47 o -5 11 2 66.89 38.56 117.06 o -3 11 2 405.08 433.12 110.17 o -1 11 2 382.26 307.11 103.29 o 1 11 2 369.37 453.09 97.09 o 3 11 2 11.05 -42.69 96.40 o 5 11 2 13.63 82.63 100.53 o 7 11 2 423.83 417.97 122.57 o 9 11 2 29.00 61.97 119.13 o -8 12 2 15.77 -33.05 124.63 o -6 12 2 474.83 309.86 124.63 o -4 12 2 3.01 9.64 117.75 o -2 12 2 162.37 259.60 103.98 o 0 12 2 237.88 216.22 105.35 o 2 12 2 847.89 918.57 117.06 o 4 12 2 310.18 418.66 111.55 o 6 12 2 42.57 -39.25 115.68 o 8 12 2 357.98 325.01 131.52 o -7 13 2 54.95 6.20 136.34 o -5 13 2 2457.53 2160.09 169.39 o -3 13 2 3553.52 3360.29 174.90 o -1 13 2 239.10 312.62 107.42 o 1 13 2 1964.61 1756.58 139.78 o 3 13 2 2978.41 3003.61 163.88 o 5 13 2 1619.88 1700.12 151.49 o 7 13 2 3.62 45.45 119.81 o -8 14 2 3.30 49.58 148.05 o -6 14 2 64.31 364.26 114.31 o -4 14 2 39.59 40.63 127.39 o -2 14 2 978.26 689.27 136.34 o 0 14 2 150.94 230.68 116.37 o 2 14 2 75.50 21.35 112.93 o 4 14 2 35.01 -64.04 128.77 o 6 14 2 186.64 -52.33 135.65 o 8 14 2 29.16 191.43 132.21 o -7 15 2 0.04 0.00 154.24 o -5 15 2 70.04 231.36 131.52 o -3 15 2 2038.04 2602.85 175.59 o -1 15 2 79.86 0.00 121.19 o 1 15 2 0.37 109.48 112.24 o 3 15 2 167.28 236.18 121.88 o 5 15 2 1039.65 1099.67 153.55 o 7 15 2 122.08 123.95 156.31 o -6 16 2 0.23 207.95 137.03 o -4 16 2 271.09 -68.17 137.72 o -2 16 2 69.87 -57.84 128.77 o 0 16 2 13.83 156.31 109.48 o 2 16 2 23.59 57.84 119.13 o 4 16 2 399.09 272.68 132.21 o 6 16 2 237.06 158.37 153.55 o -3 17 2 0.46 -133.59 133.59 o -1 17 2 5.73 102.60 133.59 o 1 17 2 132.71 294.71 126.01 o 3 17 2 13.56 -136.34 136.34 o 0 18 2 35.64 270.61 134.27 o -11 1 3 0.37 280.94 113.62 o -9 1 3 1.69 67.48 108.80 o -7 1 3 51.61 172.15 87.45 o -5 1 3 9982.89 8977.08 310.55 o -3 1 3 618.86 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