#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209787_Fobs loop_ _publ_author_name 'Suresh, J.' 'Krishnakumar, R. V.' 'Rajagopal, K.' 'Natarajan, S.' _publ_section_title ; Pyridinium (2R,3R)-tartrate ; _journal_coeditor_code CI2080 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3220 _journal_page_last o3222 _journal_volume 62 _journal_year 2006 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.0390 _cell_length_b 13.2204 _cell_length_c 15.3183 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file ci2080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PYRIDINE TARTRATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1509.25 1717.39 8.81 o 4 0 0 27.90 35.24 2.63 o 1 1 0 4813.57 5875.16 15.04 o 2 1 0 129.05 112.97 2.40 o 3 1 0 90.87 128.58 3.72 o 4 1 0 30.50 45.21 2.61 o 5 1 0 53.49 55.63 2.38 o 0 2 0 2282.41 2665.53 7.61 o 1 2 0 2.78 1.92 1.18 o 2 2 0 554.63 598.97 5.13 o 3 2 0 84.24 129.43 4.05 o 4 2 0 63.54 116.20 3.44 o 5 2 0 6.62 4.87 2.00 o 1 3 0 3197.77 3381.84 12.03 o 2 3 0 723.24 635.26 5.54 o 3 3 0 2.45 2.58 3.86 o 4 3 0 20.87 23.76 1.60 o 5 3 0 0.08 -2.62 3.84 o 0 4 0 3804.13 3786.16 12.50 o 1 4 0 2524.41 2580.82 10.91 o 2 4 0 35.01 27.43 0.78 o 3 4 0 109.72 172.08 5.16 o 4 4 0 7.54 5.31 3.44 o 5 4 0 0.83 -2.99 4.05 o 1 5 0 726.80 733.18 5.74 o 2 5 0 109.01 124.18 3.88 o 3 5 0 9.75 16.23 1.98 o 4 5 0 52.44 46.33 1.84 o 5 5 0 31.66 34.15 2.15 o 0 6 0 4871.30 4517.12 16.58 o 1 6 0 1350.64 1228.27 8.23 o 2 6 0 330.44 389.31 8.30 o 3 6 0 28.92 40.88 2.27 o 4 6 0 20.36 13.74 1.70 o 5 6 0 2.45 2.02 1.86 o 1 7 0 91.64 105.10 2.66 o 2 7 0 14.45 13.48 1.82 o 3 7 0 7.09 12.66 2.05 o 4 7 0 26.38 21.77 1.86 o 5 7 0 2.61 0.83 4.07 o 0 8 0 901.93 651.93 6.26 o 1 8 0 4.86 3.79 0.61 o 2 8 0 6.31 8.99 1.93 o 3 8 0 30.26 25.85 1.86 o 4 8 0 11.67 3.12 4.06 o 5 8 0 6.82 3.50 4.32 o 1 9 0 107.09 81.42 2.44 o 2 9 0 100.42 107.03 3.37 o 3 9 0 14.58 14.96 1.78 o 4 9 0 8.23 4.68 4.25 o 0 10 0 306.29 210.37 4.21 o 1 10 0 503.97 342.30 5.42 o 2 10 0 226.30 210.56 6.05 o 3 10 0 28.53 22.35 2.04 o 4 10 0 17.58 16.57 2.01 o 1 11 0 913.85 1614.20 19.12 o 2 11 0 93.32 73.01 2.67 o 3 11 0 116.21 96.82 2.82 o 4 11 0 0.50 3.11 4.08 o 0 12 0 11.76 3.49 5.77 o 1 12 0 77.44 118.83 3.51 o 2 12 0 49.43 38.11 2.53 o 3 12 0 16.00 8.57 4.59 o 1 13 0 18.77 9.88 6.47 o 2 13 0 23.42 6.92 5.36 o 3 13 0 2.88 -2.92 5.06 o 0 14 0 24.92 24.40 3.00 o 1 14 0 105.11 125.73 4.06 o 2 14 0 11.45 -3.27 5.58 o 1 15 0 81.52 84.00 3.75 o 1 0 1 1020.60 987.03 20.81 o 2 0 1 1.61 1.51 0.50 o 3 0 1 32.33 31.55 1.40 o 4 0 1 46.80 86.88 6.45 o 5 0 1 3.44 3.04 1.78 o 0 1 1 713.50 788.58 55.62 o 1 1 1 2057.63 2254.97 20.06 o 2 1 1 258.42 248.86 2.92 o 3 1 1 755.19 1256.03 16.75 o 4 1 1 52.87 88.30 2.08 o 5 1 1 4.80 0.78 2.90 o 0 2 1 73.73 58.64 0.86 o 1 2 1 4398.17 4838.68 77.17 o 2 2 1 430.20 454.49 6.34 o 3 2 1 114.10 174.65 3.62 o 4 2 1 12.37 22.27 1.93 o 5 2 1 2.12 6.26 2.95 o 0 3 1 1997.37 1865.32 91.75 o 1 3 1 3785.56 4019.07 43.04 o 2 3 1 690.14 701.33 4.11 o 3 3 1 268.37 413.56 6.24 o 4 3 1 25.69 26.60 1.17 o 5 3 1 21.35 16.26 1.38 o 0 4 1 522.54 380.74 3.57 o 1 4 1 1893.03 1857.21 6.38 o 2 4 1 383.86 330.54 3.37 o 3 4 1 71.64 87.75 1.85 o 4 4 1 7.49 9.93 1.06 o 5 4 1 17.52 16.59 1.39 o 0 5 1 845.78 741.13 6.01 o 1 5 1 121.90 99.96 3.09 o 2 5 1 289.35 390.43 5.51 o 3 5 1 165.41 234.48 4.62 o 4 5 1 19.55 20.21 1.72 o 5 5 1 14.12 12.24 1.39 o 0 6 1 80.72 50.48 1.09 o 1 6 1 372.58 295.36 2.79 o 2 6 1 106.81 127.27 6.36 o 3 6 1 102.98 127.82 6.59 o 4 6 1 33.34 27.61 1.31 o 5 6 1 1.35 -0.31 5.22 o 0 7 1 19.94 14.03 0.72 o 1 7 1 173.53 137.96 2.14 o 2 7 1 117.99 154.64 3.22 o 3 7 1 47.56 65.00 1.86 o 4 7 1 37.35 32.81 3.31 o 5 7 1 8.30 10.59 2.00 o 0 8 1 34.77 33.93 0.71 o 1 8 1 163.19 146.05 7.40 o 2 8 1 286.03 315.09 9.76 o 3 8 1 10.55 12.91 1.21 o 4 8 1 15.05 10.63 4.13 o 5 8 1 3.82 0.51 5.97 o 0 9 1 58.55 51.72 1.08 o 1 9 1 386.51 278.07 3.18 o 2 9 1 10.18 7.52 1.93 o 3 9 1 95.48 79.65 1.70 o 4 9 1 14.78 6.86 1.76 o 0 10 1 8.85 7.85 0.55 o 1 10 1 56.40 39.19 0.79 o 2 10 1 181.75 165.41 3.36 o 3 10 1 38.93 30.50 1.48 o 4 10 1 5.86 4.78 2.99 o 0 11 1 35.06 39.15 1.80 o 1 11 1 244.87 428.68 7.52 o 2 11 1 20.74 17.73 2.01 o 3 11 1 41.55 36.86 1.63 o 4 11 1 8.62 2.64 3.98 o 0 12 1 4.05 6.36 3.88 o 1 12 1 242.94 371.83 11.16 o 2 12 1 241.20 175.67 3.81 o 3 12 1 11.01 8.01 3.80 o 0 13 1 288.44 417.36 8.05 o 1 13 1 0.94 5.49 2.46 o 2 13 1 166.04 114.04 2.45 o 3 13 1 1.99 -0.64 3.72 o 0 14 1 208.50 270.20 5.76 o 1 14 1 6.08 6.32 4.30 o 2 14 1 13.54 12.36 2.35 o 0 15 1 4.14 9.43 2.76 o 1 15 1 38.65 54.92 5.15 o 0 0 2 78.03 55.29 1.09 o 1 0 2 96.59 81.82 1.76 o 2 0 2 2.48 1.63 0.55 o 3 0 2 172.54 254.58 7.10 o 4 0 2 0.75 -5.03 5.20 o 5 0 2 59.60 67.03 2.49 o 0 1 2 14.18 25.10 0.70 o 1 1 2 2162.08 2298.44 8.78 o 2 1 2 148.77 159.63 2.80 o 3 1 2 161.26 213.08 5.96 o 4 1 2 56.08 84.08 2.91 o 5 1 2 0.37 -2.05 4.23 o 0 2 2 3279.61 3704.79 10.44 o 1 2 2 1756.18 1737.88 7.81 o 2 2 2 1299.02 1373.26 8.20 o 3 2 2 12.83 15.27 1.88 o 4 2 2 57.11 97.83 2.99 o 5 2 2 27.72 28.90 2.18 o 0 3 2 5418.29 5987.70 15.88 o 1 3 2 2447.01 2426.31 10.16 o 2 3 2 379.93 381.17 4.33 o 3 3 2 538.23 744.51 11.69 o 4 3 2 40.42 31.14 1.70 o 5 3 2 10.12 11.01 1.91 o 0 4 2 446.33 353.58 3.37 o 1 4 2 334.65 323.16 3.62 o 2 4 2 186.85 215.43 3.42 o 3 4 2 17.02 24.73 1.99 o 4 4 2 7.03 6.49 1.49 o 5 4 2 54.82 60.39 2.31 o 0 5 2 3421.91 3408.92 12.99 o 1 5 2 7.88 8.00 0.58 o 2 5 2 124.47 191.69 5.18 o 3 5 2 40.00 65.43 2.40 o 4 5 2 36.86 35.12 1.74 o 5 5 2 7.99 6.01 1.89 o 0 6 2 87.01 65.51 1.71 o 1 6 2 407.47 346.30 4.30 o 2 6 2 391.64 500.12 9.20 o 3 6 2 302.85 401.15 9.91 o 4 6 2 36.51 38.03 1.89 o 5 6 2 9.69 14.15 1.87 o 0 7 2 7.89 6.62 0.56 o 1 7 2 104.79 75.51 2.07 o 2 7 2 553.57 599.73 10.91 o 3 7 2 4.39 5.42 4.83 o 4 7 2 69.26 56.42 2.15 o 5 7 2 3.14 2.87 4.09 o 0 8 2 241.73 175.62 3.36 o 1 8 2 91.97 82.17 2.20 o 2 8 2 162.73 206.80 6.21 o 3 8 2 18.22 17.07 1.74 o 4 8 2 43.02 34.58 2.08 o 5 8 2 10.72 12.17 2.05 o 0 9 2 305.37 174.03 3.58 o 1 9 2 86.63 56.38 1.60 o 2 9 2 121.56 129.77 3.72 o 3 9 2 86.63 61.75 2.25 o 4 9 2 21.42 14.77 1.97 o 0 10 2 301.59 182.91 4.01 o 1 10 2 50.26 37.69 1.10 o 2 10 2 154.47 139.02 4.22 o 3 10 2 26.71 19.99 2.03 o 4 10 2 25.88 21.16 2.07 o 0 11 2 5.25 8.02 5.38 o 1 11 2 27.88 41.86 2.60 o 2 11 2 26.75 22.12 2.31 o 3 11 2 15.16 12.35 1.98 o 4 11 2 2.76 -0.52 4.23 o 0 12 2 104.50 164.02 4.83 o 1 12 2 26.69 46.91 3.01 o 2 12 2 45.35 34.55 2.41 o 3 12 2 6.61 4.75 4.25 o 0 13 2 127.49 232.45 7.19 o 1 13 2 3.45 6.15 5.67 o 2 13 2 4.88 2.26 4.75 o 3 13 2 1.53 5.27 5.09 o 0 14 2 261.59 365.23 10.24 o 1 14 2 151.73 194.89 5.83 o 2 14 2 1.02 -2.47 5.27 o 0 15 2 29.08 38.26 3.25 o 1 15 2 40.88 60.85 3.51 o 1 0 3 2036.49 2142.75 8.79 o 2 0 3 93.48 84.47 2.25 o 3 0 3 163.30 214.37 6.00 o 4 0 3 1.35 5.13 5.03 o 5 0 3 0.04 1.60 4.03 o 0 1 3 949.52 876.13 4.45 o 1 1 3 418.00 415.83 3.63 o 2 1 3 754.81 843.25 6.28 o 3 1 3 36.18 47.78 2.06 o 4 1 3 92.62 154.02 4.65 o 5 1 3 9.62 14.14 2.06 o 0 2 3 1657.06 1615.04 6.78 o 1 2 3 415.32 362.51 3.52 o 2 2 3 101.65 102.26 2.39 o 3 2 3 153.86 204.68 6.02 o 4 2 3 94.58 96.67 2.87 o 5 2 3 34.75 37.74 2.29 o 0 3 3 4026.16 4349.23 13.45 o 1 3 3 4014.02 4015.34 14.47 o 2 3 3 104.97 109.27 2.55 o 3 3 3 52.77 84.46 2.48 o 4 3 3 13.00 16.11 1.53 o 5 3 3 6.91 7.16 3.97 o 0 4 3 297.87 252.86 2.97 o 1 4 3 647.06 590.37 5.02 o 2 4 3 342.35 480.09 8.40 o 3 4 3 55.79 81.69 2.46 o 4 4 3 68.71 55.88 1.89 o 5 4 3 9.69 11.45 1.96 o 0 5 3 732.46 586.54 4.90 o 1 5 3 629.28 588.74 5.36 o 2 5 3 499.66 612.28 9.89 o 3 5 3 106.23 151.38 4.80 o 4 5 3 12.43 9.83 1.52 o 5 5 3 6.41 9.71 1.91 o 0 6 3 2141.02 2013.72 10.38 o 1 6 3 363.36 303.00 4.12 o 2 6 3 418.60 532.62 9.70 o 3 6 3 222.78 305.62 7.82 o 4 6 3 28.99 24.27 1.84 o 5 6 3 3.31 3.28 3.96 o 0 7 3 654.22 544.16 5.47 o 1 7 3 35.77 33.83 0.97 o 2 7 3 562.15 609.14 11.19 o 3 7 3 36.27 52.29 2.62 o 4 7 3 121.65 92.16 2.82 o 5 7 3 3.88 1.54 4.32 o 0 8 3 239.01 171.15 3.40 o 1 8 3 41.66 24.11 0.82 o 2 8 3 25.86 25.74 2.15 o 3 8 3 163.04 144.58 4.41 o 4 8 3 4.43 0.73 4.04 o 5 8 3 1.05 2.32 4.38 o 0 9 3 726.54 517.63 6.21 o 1 9 3 337.08 225.58 4.26 o 2 9 3 7.70 5.28 4.74 o 3 9 3 39.89 33.35 2.07 o 4 9 3 6.49 0.77 4.02 o 0 10 3 3.96 5.64 0.74 o 1 10 3 183.09 133.21 3.52 o 2 10 3 122.20 110.72 3.37 o 3 10 3 44.01 33.30 2.09 o 4 10 3 37.73 26.72 2.15 o 0 11 3 28.67 50.09 2.54 o 1 11 3 79.47 130.16 4.07 o 2 11 3 37.98 32.45 2.39 o 3 11 3 34.97 28.36 2.16 o 4 11 3 0.72 2.46 3.84 o 0 12 3 37.93 62.71 2.95 o 1 12 3 36.34 53.98 2.98 o 2 12 3 64.33 60.28 2.63 o 3 12 3 2.04 1.03 4.23 o 0 13 3 16.81 27.31 2.90 o 1 13 3 177.01 276.07 8.86 o 2 13 3 7.99 1.91 4.83 o 3 13 3 17.10 13.87 2.54 o 0 14 3 6.59 13.93 2.82 o 1 14 3 54.07 71.02 3.36 o 2 14 3 19.65 13.82 2.49 o 0 15 3 28.05 44.70 3.37 o 1 15 3 6.19 7.79 6.70 o 0 0 4 1.25 1.51 0.47 o 1 0 4 7.12 8.06 0.57 o 2 0 4 34.50 34.52 1.02 o 3 0 4 209.00 311.01 7.98 o 4 0 4 70.78 84.06 2.55 o 5 0 4 0.22 -4.23 4.25 o 0 1 4 699.51 671.02 4.27 o 1 1 4 164.72 160.39 2.52 o 2 1 4 27.42 26.33 0.82 o 3 1 4 75.08 99.18 2.88 o 4 1 4 10.88 11.88 1.57 o 5 1 4 28.62 26.57 2.27 o 0 2 4 336.58 309.49 3.01 o 1 2 4 136.64 173.75 2.68 o 2 2 4 918.42 964.91 7.13 o 3 2 4 83.88 107.51 3.12 o 4 2 4 14.40 18.10 1.62 o 5 2 4 3.85 4.62 4.35 o 0 3 4 337.98 298.18 3.18 o 1 3 4 34.93 30.34 0.89 o 2 3 4 1002.80 1065.36 7.76 o 3 3 4 391.48 537.42 10.57 o 4 3 4 105.53 101.15 3.02 o 5 3 4 30.18 30.36 2.09 o 0 4 4 235.58 181.44 2.70 o 1 4 4 275.37 252.52 3.46 o 2 4 4 364.32 439.91 8.41 o 3 4 4 49.61 64.30 2.36 o 4 4 4 2.97 4.80 3.58 o 5 4 4 16.73 16.08 1.98 o 0 5 4 0.86 0.47 1.12 o 1 5 4 1241.09 1060.81 7.64 o 2 5 4 18.66 24.97 1.74 o 3 5 4 134.85 201.30 5.87 o 4 5 4 59.95 59.29 2.02 o 5 5 4 1.59 4.98 3.78 o 0 6 4 43.48 44.85 1.29 o 1 6 4 76.92 57.30 1.74 o 2 6 4 595.19 717.33 11.48 o 3 6 4 133.01 162.40 5.08 o 4 6 4 21.51 19.60 1.79 o 5 6 4 10.78 6.84 4.41 o 0 7 4 770.64 623.27 5.98 o 1 7 4 441.46 411.77 5.32 o 2 7 4 154.98 180.97 5.44 o 3 7 4 64.49 69.50 2.07 o 4 7 4 27.92 21.98 2.02 o 5 7 4 15.30 15.37 2.07 o 0 8 4 200.84 159.54 3.30 o 1 8 4 143.15 93.77 2.44 o 2 8 4 4.43 -2.38 4.66 o 3 8 4 411.34 334.58 8.18 o 4 8 4 49.00 31.41 2.08 o 0 9 4 499.24 304.79 4.80 o 1 9 4 81.87 58.56 1.83 o 2 9 4 109.53 106.68 2.96 o 3 9 4 139.00 116.41 3.47 o 4 9 4 1.17 -0.31 4.13 o 0 10 4 37.62 24.26 0.92 o 1 10 4 30.24 45.63 2.48 o 2 10 4 113.95 86.43 2.74 o 3 10 4 10.88 10.07 1.91 o 4 10 4 7.89 3.69 4.04 o 0 11 4 11.64 16.81 2.29 o 1 11 4 91.78 135.08 4.31 o 2 11 4 37.63 32.47 2.32 o 3 11 4 2.66 -1.13 4.30 o 4 11 4 9.08 3.40 4.21 o 0 12 4 51.96 79.58 3.11 o 1 12 4 3.89 8.57 5.57 o 2 12 4 43.93 36.46 2.47 o 3 12 4 6.27 5.24 4.19 o 0 13 4 0.01 7.91 5.29 o 1 13 4 106.55 172.01 5.06 o 2 13 4 10.34 13.54 2.27 o 3 13 4 21.62 15.56 2.30 o 0 14 4 14.93 33.99 3.05 o 1 14 4 4.71 4.58 5.97 o 2 14 4 11.02 7.63 5.42 o 0 15 4 0.00 5.04 2.84 o 1 15 4 9.65 8.97 6.67 o 1 0 5 1261.83 1229.72 7.23 o 2 0 5 744.37 885.98 6.91 o 3 0 5 52.06 99.74 3.06 o 4 0 5 492.86 503.87 8.92 o 5 0 5 4.05 1.83 4.10 o 0 1 5 854.83 761.34 5.02 o 1 1 5 1196.82 1209.22 7.21 o 2 1 5 42.80 37.93 1.06 o 3 1 5 26.12 39.87 2.18 o 4 1 5 31.55 29.18 1.72 o 5 1 5 49.56 47.21 2.47 o 0 2 5 1046.10 1078.03 6.20 o 1 2 5 467.48 440.50 4.34 o 2 2 5 126.49 120.71 2.80 o 3 2 5 17.72 27.79 2.04 o 4 2 5 299.89 273.31 6.79 o 5 2 5 3.75 7.57 2.00 o 0 3 5 1248.29 1255.04 7.08 o 1 3 5 8.40 9.47 0.60 o 2 3 5 96.23 95.08 2.55 o 3 3 5 204.53 312.05 8.50 o 4 3 5 69.14 73.35 2.30 o 5 3 5 22.45 28.63 2.03 o 0 4 5 101.40 86.75 2.15 o 1 4 5 985.98 925.01 6.94 o 2 4 5 319.63 400.08 8.23 o 3 4 5 40.25 56.11 2.47 o 4 4 5 91.23 85.02 2.66 o 5 4 5 58.95 61.77 2.37 o 0 5 5 562.57 549.85 5.09 o 1 5 5 495.47 464.40 5.10 o 2 5 5 135.77 169.16 5.31 o 3 5 5 22.63 33.67 2.31 o 4 5 5 10.10 3.77 3.64 o 5 5 5 13.30 15.15 2.01 o 0 6 5 5.07 5.27 0.55 o 1 6 5 324.51 273.63 4.22 o 2 6 5 49.30 53.82 2.19 o 3 6 5 22.20 36.27 2.41 o 4 6 5 89.92 73.39 2.20 o 5 6 5 19.72 17.27 2.08 o 0 7 5 69.49 62.39 1.96 o 1 7 5 133.87 112.79 2.99 o 2 7 5 320.32 360.08 9.36 o 3 7 5 20.30 18.63 1.76 o 4 7 5 41.07 32.37 2.02 o 5 7 5 5.31 6.20 4.36 o 0 8 5 258.05 220.51 3.97 o 1 8 5 219.17 143.60 3.45 o 2 8 5 116.15 91.68 2.72 o 3 8 5 308.94 239.07 7.10 o 4 8 5 70.60 57.83 2.37 o 0 9 5 440.66 336.94 5.20 o 1 9 5 4.22 2.88 1.65 o 2 9 5 2.68 6.57 3.92 o 3 9 5 67.81 57.62 2.29 o 4 9 5 32.07 20.41 2.03 o 0 10 5 43.36 60.64 2.52 o 1 10 5 12.40 19.24 2.33 o 2 10 5 25.20 19.80 2.20 o 3 10 5 3.24 5.52 4.10 o 4 10 5 9.49 7.03 4.40 o 0 11 5 2.24 -0.54 5.08 o 1 11 5 36.09 67.44 2.99 o 2 11 5 89.81 72.91 2.77 o 3 11 5 48.85 42.71 2.36 o 0 12 5 52.50 80.24 3.13 o 1 12 5 5.26 6.34 5.47 o 2 12 5 46.22 28.00 2.46 o 3 12 5 23.16 15.41 2.20 o 0 13 5 2.07 0.00 5.83 o 1 13 5 27.71 34.51 3.01 o 2 13 5 41.12 27.60 2.52 o 0 14 5 43.53 53.57 3.29 o 1 14 5 9.23 5.67 6.55 o 2 14 5 8.74 6.27 5.43 o 0 15 5 24.53 29.87 3.21 o 0 0 6 5753.52 6057.16 18.61 o 1 0 6 219.10 222.15 3.26 o 2 0 6 237.28 257.55 3.89 o 3 0 6 93.62 135.90 3.92 o 4 0 6 78.32 92.67 2.98 o 5 0 6 4.45 7.21 4.66 o 0 1 6 832.69 847.66 5.72 o 1 1 6 5064.86 5163.65 18.54 o 2 1 6 83.03 83.11 2.14 o 3 1 6 16.02 20.05 2.01 o 4 1 6 62.66 75.34 2.29 o 5 1 6 23.99 31.57 2.23 o 0 2 6 1060.60 1055.02 6.60 o 1 2 6 37.90 27.34 0.79 o 2 2 6 93.11 96.14 2.64 o 3 2 6 54.68 67.87 2.48 o 4 2 6 8.98 6.06 3.46 o 5 2 6 5.34 3.83 4.68 o 0 3 6 3087.95 3297.92 13.24 o 1 3 6 398.30 377.03 4.44 o 2 3 6 71.35 72.75 2.11 o 3 3 6 277.43 398.13 9.68 o 4 3 6 1.29 -0.85 3.45 o 5 3 6 7.43 8.47 1.88 o 0 4 6 314.18 311.24 3.82 o 1 4 6 395.02 395.14 4.69 o 2 4 6 226.83 272.93 7.36 o 3 4 6 6.26 8.92 4.48 o 4 4 6 18.97 21.09 1.81 o 5 4 6 51.22 47.19 2.32 o 0 5 6 1.90 1.98 1.21 o 1 5 6 1421.26 1294.80 9.16 o 2 5 6 842.77 1199.15 14.90 o 3 5 6 111.98 138.28 4.10 o 4 5 6 7.61 6.88 1.68 o 5 5 6 0.50 5.06 3.92 o 0 6 6 1064.40 821.36 7.02 o 1 6 6 229.30 200.32 3.82 o 2 6 6 234.64 270.84 7.03 o 3 6 6 109.86 88.53 2.89 o 4 6 6 44.64 33.98 2.00 o 5 6 6 10.02 11.87 2.01 o 0 7 6 337.92 231.62 3.90 o 1 7 6 242.92 186.99 3.91 o 2 7 6 199.07 234.28 6.83 o 3 7 6 4.07 5.65 3.87 o 4 7 6 5.57 3.71 3.64 o 0 8 6 0.20 0.68 0.64 o 1 8 6 7.65 6.10 0.72 o 2 8 6 77.93 112.34 3.43 o 3 8 6 92.38 70.97 2.29 o 4 8 6 8.93 7.98 1.96 o 0 9 6 16.01 9.12 0.83 o 1 9 6 40.89 23.18 0.92 o 2 9 6 20.53 21.34 2.00 o 3 9 6 91.03 78.46 2.51 o 4 9 6 0.77 2.65 4.01 o 0 10 6 4.08 1.86 4.96 o 1 10 6 88.99 147.92 4.76 o 2 10 6 296.61 264.10 7.18 o 3 10 6 7.48 5.22 4.29 o 4 10 6 17.09 8.44 4.29 o 0 11 6 7.08 15.59 2.50 o 1 11 6 117.46 171.36 5.29 o 2 11 6 82.73 64.96 2.63 o 3 11 6 166.80 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