#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/98/2209881.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209881_Fobs loop_ _publ_author_name 'Rakovsk\'y, Erik' 'Gyepes, Robert' _publ_section_title ; Butane-1,4-diammonium dihydrogendecavanadate(V) ; _journal_coeditor_code HK2073 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1820 _journal_page_last m1822 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.2270 _cell_length_b 16.7200 _cell_length_c 18.2310 _exptl_crystal_F_000 2240.00 _reflns_d_resolution_high 0.7100 _[local]_cod_data_source_file hk2073Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'krDD1,Pbca,150K,analytical absorption correction' _shelx_refln_list_code 4 _shelx_f_calc_maximum 360.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 768.26 1405.16 23.25 o 4 0 0 117804.27 118154.60 2105.69 o 6 0 0 283.89 268.24 8.29 o 8 0 0 2818.35 2698.35 68.40 o 10 0 0 35445.33 36830.35 1013.87 o 12 0 0 6284.91 6114.34 231.52 o 14 0 0 3346.26 3462.68 261.40 o 2 1 0 14176.98 14126.47 156.52 o 4 1 0 1551.24 992.16 13.52 o 6 1 0 2256.53 2396.82 28.86 o 8 1 0 467.97 492.43 11.22 o 10 1 0 820.82 798.59 22.28 o 12 1 0 14545.25 14519.47 387.80 o 14 1 0 2.17 37.91 36.96 o 2 2 0 37331.02 37357.02 427.18 o 4 2 0 12662.73 11259.08 131.69 o 6 2 0 2446.18 2471.99 28.55 o 8 2 0 98.73 112.39 7.11 o 10 2 0 2250.97 2280.76 57.38 o 12 2 0 228.74 193.26 24.48 o 14 2 0 7587.57 7664.28 438.81 o 2 3 0 9963.83 9993.75 111.98 o 4 3 0 6679.99 5926.65 65.88 o 6 3 0 1271.32 1299.55 18.81 o 8 3 0 836.74 859.39 16.91 o 10 3 0 9170.18 9503.38 202.66 o 12 3 0 7586.66 7357.43 296.04 o 14 3 0 302.00 309.13 56.87 o 0 4 0 5422.72 4572.37 82.97 o 4 4 0 9786.09 9040.03 98.05 o 6 4 0 5357.80 5740.46 68.19 o 8 4 0 12329.71 12327.09 163.11 o 10 4 0 52.82 66.66 12.87 o 12 4 0 5037.35 5100.23 154.23 o 14 4 0 218.86 220.98 56.47 o 2 5 0 6202.16 6783.46 82.28 o 4 5 0 860.62 1041.56 13.59 o 6 5 0 2443.01 2299.01 29.10 o 8 5 0 518.31 491.88 11.93 o 10 5 0 4329.24 4318.88 73.79 o 12 5 0 2.60 -32.38 32.38 o 14 5 0 127.67 111.91 33.09 o 0 6 0 25751.01 23857.75 371.73 o 4 6 0 1792.92 1753.52 21.43 o 6 6 0 1057.98 1049.95 16.12 o 8 6 0 8975.05 8931.72 135.68 o 10 6 0 1058.66 1082.49 24.49 o 12 6 0 4882.81 4979.48 172.17 o 4 7 0 6513.09 6323.33 64.45 o 6 7 0 49742.14 49497.75 561.36 o 8 7 0 5628.40 5903.40 81.12 o 10 7 0 6443.63 6716.70 142.06 o 12 7 0 933.08 924.41 45.98 o 0 8 0 39956.49 40747.69 627.65 o 2 8 0 101809.09 102234.75 2023.58 o 4 8 0 3750.10 4112.29 53.73 o 6 8 0 31884.35 31806.82 376.93 o 8 8 0 739.89 745.09 14.61 o 10 8 0 9311.52 9822.32 207.61 o 12 8 0 93.23 162.06 26.30 o 2 9 0 43544.00 44558.03 500.20 o 4 9 0 5990.93 5779.01 73.82 o 6 9 0 1675.34 1801.90 24.58 o 8 9 0 20004.79 20311.29 335.19 o 10 9 0 4995.05 5221.46 116.12 o 12 9 0 93.81 81.19 25.27 o 0 10 0 433.50 545.61 10.35 o 2 10 0 7447.33 8033.99 94.35 o 4 10 0 126.16 108.12 5.45 o 6 10 0 12738.17 13613.79 172.89 o 8 10 0 759.07 778.19 26.70 o 10 10 0 22944.46 23693.28 524.10 o 12 10 0 847.76 795.62 47.00 o 2 11 0 8577.04 8378.64 102.70 o 4 11 0 16909.78 17141.67 218.30 o 6 11 0 67.98 91.53 7.19 o 8 11 0 3499.35 3516.87 75.04 o 10 11 0 1070.92 1053.07 40.05 o 12 11 0 306.25 319.64 33.88 o 0 12 0 52896.57 52886.56 781.32 o 2 12 0 9637.51 9477.99 121.51 o 4 12 0 5007.92 5228.85 78.11 o 6 12 0 369.27 374.31 11.61 o 8 12 0 120.62 98.64 10.58 o 10 12 0 171.88 180.70 21.48 o 12 12 0 1227.54 1170.55 67.39 o 2 13 0 975.41 1024.48 17.38 o 4 13 0 41841.26 42830.63 680.04 o 6 13 0 6023.00 6101.07 122.75 o 8 13 0 2126.94 2125.62 50.89 o 10 13 0 15.90 57.18 23.38 o 12 13 0 3886.18 3839.27 186.65 o 0 14 0 216.46 258.03 10.03 o 2 14 0 7410.23 7253.56 105.18 o 4 14 0 22680.43 24190.18 354.92 o 6 14 0 4130.63 4258.09 79.01 o 8 14 0 38008.54 39372.76 942.26 o 10 14 0 222.96 220.43 27.56 o 2 15 0 2617.04 2609.49 43.72 o 4 15 0 1224.40 1302.85 26.23 o 6 15 0 5890.15 6079.79 120.51 o 8 15 0 513.30 495.64 22.67 o 10 15 0 211.42 245.63 33.01 o 0 16 0 126.05 108.44 9.24 o 2 16 0 3707.49 3824.43 66.03 o 4 16 0 16129.10 17266.79 305.77 o 6 16 0 620.79 547.09 24.25 o 8 16 0 44844.96 46661.16 1274.41 o 10 16 0 7291.14 7782.88 325.06 o 2 17 0 664.01 687.07 16.75 o 4 17 0 3067.45 3159.88 76.76 o 6 17 0 3139.95 3047.83 92.17 o 8 17 0 1415.73 1602.48 61.70 o 0 18 0 3819.27 3862.45 94.02 o 2 18 0 289.00 355.18 12.48 o 4 18 0 1507.71 1517.26 38.87 o 6 18 0 1230.04 1147.05 45.74 o 8 18 0 28.96 91.53 28.98 o 2 19 0 1146.48 1163.15 28.28 o 4 19 0 8085.50 8327.79 252.29 o 6 19 0 4222.62 4447.79 147.78 o 8 19 0 140.20 126.29 27.64 o 0 20 0 382.16 379.60 25.51 o 2 20 0 34.57 69.42 21.80 o 4 20 0 3854.25 4061.64 119.94 o 6 20 0 14844.03 15082.63 545.08 o 2 21 0 895.92 912.86 83.18 o 4 21 0 491.03 343.90 32.31 o 6 21 0 213.39 164.20 69.19 o 2 22 0 321.72 370.58 62.79 o 4 22 0 723.81 581.53 63.74 o 2 1 1 37.02 51.89 1.42 o 3 1 1 3287.87 3710.75 28.13 o 4 1 1 2980.51 2231.06 18.21 o 5 1 1 23.34 149.66 3.40 o 6 1 1 4284.35 4323.39 32.54 o 7 1 1 1766.91 1683.99 17.78 o 8 1 1 28.35 41.07 4.50 o 9 1 1 7694.00 7736.05 94.65 o 10 1 1 639.61 629.33 14.61 o 11 1 1 17461.65 18148.43 301.48 o 12 1 1 4173.38 4106.39 87.30 o 13 1 1 6.96 -16.03 16.03 o 14 1 1 909.08 877.31 47.48 o 1 2 1 13214.29 11527.32 113.48 o 2 2 1 10018.10 10262.47 80.77 o 3 2 1 26929.12 26519.66 221.87 o 4 2 1 2639.75 3060.07 24.30 o 5 2 1 93.96 245.31 4.03 o 6 2 1 1407.99 1312.47 12.65 o 7 2 1 11885.07 11755.13 103.25 o 8 2 1 11095.55 10994.16 111.32 o 9 2 1 677.43 683.94 11.93 o 10 2 1 1363.40 1317.77 22.76 o 11 2 1 7464.96 7627.57 126.74 o 12 2 1 632.74 583.42 19.67 o 13 2 1 3932.75 3859.28 116.85 o 14 2 1 16.52 -27.88 27.88 o 1 3 1 2162.14 2550.18 19.02 o 2 3 1 11133.28 11078.94 82.90 o 3 3 1 47745.79 47654.32 385.29 o 4 3 1 1.64 -2.13 2.13 o 5 3 1 4286.79 4148.10 31.75 o 6 3 1 1441.62 1342.58 13.67 o 7 3 1 24307.92 24651.97 235.54 o 8 3 1 8007.48 8079.79 78.60 o 9 3 1 200.59 220.99 6.79 o 10 3 1 1446.56 1455.28 23.47 o 11 3 1 730.64 716.31 18.17 o 12 3 1 27.93 57.89 15.56 o 13 3 1 17.17 30.33 16.43 o 14 3 1 704.33 658.14 41.86 o 0 4 1 1832.21 1728.97 18.29 o 1 4 1 19210.71 18933.12 145.14 o 2 4 1 2393.93 2220.79 17.58 o 3 4 1 7435.25 7980.69 60.96 o 4 4 1 2630.26 2644.16 23.26 o 5 4 1 392.73 427.67 5.37 o 6 4 1 9741.84 10059.19 80.96 o 7 4 1 102.98 111.20 3.87 o 8 4 1 2939.44 2988.45 29.57 o 9 4 1 3076.22 3124.03 34.79 o 10 4 1 345.30 337.74 11.69 o 11 4 1 1898.18 1924.98 32.08 o 12 4 1 1476.41 1385.98 36.03 o 13 4 1 22.60 77.95 29.62 o 14 4 1 15.01 121.31 35.62 o 1 5 1 10636.65 9761.31 74.24 o 2 5 1 2497.43 1974.04 16.07 o 3 5 1 13314.58 12756.03 94.14 o 4 5 1 14.10 25.75 2.69 o 5 5 1 1661.00 1693.40 13.60 o 6 5 1 6452.83 6440.52 54.03 o 7 5 1 2029.40 2025.01 20.79 o 8 5 1 1483.56 1355.62 15.65 o 9 5 1 4499.33 4657.70 50.15 o 10 5 1 2292.35 2315.67 33.83 o 11 5 1 3654.11 3588.30 64.52 o 12 5 1 68.50 75.03 16.74 o 13 5 1 20382.73 21976.86 665.95 o 14 5 1 708.32 603.32 47.16 o 0 6 1 2308.91 2491.81 26.91 o 1 6 1 542.47 405.49 4.11 o 2 6 1 1710.57 1253.99 10.44 o 3 6 1 16366.92 16650.82 124.76 o 4 6 1 268.01 322.82 4.03 o 5 6 1 1333.43 1326.31 11.78 o 6 6 1 2025.60 2024.83 18.89 o 7 6 1 7711.75 7733.76 72.74 o 8 6 1 28.82 43.91 2.84 o 9 6 1 793.22 837.05 14.61 o 10 6 1 2438.88 2375.27 35.65 o 11 6 1 4.71 34.99 10.11 o 12 6 1 2230.73 2239.60 52.08 o 13 6 1 396.00 382.36 35.15 o 1 7 1 24655.42 23675.25 179.75 o 2 7 1 6167.69 7003.20 54.65 o 3 7 1 63971.37 64527.89 512.91 o 4 7 1 857.72 861.96 8.14 o 5 7 1 11543.61 11804.69 92.47 o 6 7 1 527.89 537.32 6.87 o 7 7 1 1035.52 1023.80 12.25 o 8 7 1 240.80 229.84 5.37 o 9 7 1 17639.74 18196.40 222.50 o 10 7 1 41.63 36.41 7.66 o 11 7 1 1320.78 1311.19 25.60 o 12 7 1 416.31 416.64 22.67 o 13 7 1 16568.50 17072.66 597.05 o 0 8 1 4959.20 4480.48 47.70 o 1 8 1 20178.66 18922.03 140.21 o 2 8 1 32965.02 32861.02 257.76 o 3 8 1 10972.75 11540.10 91.80 o 4 8 1 2419.45 2275.58 19.22 o 5 8 1 62.82 77.71 2.92 o 6 8 1 5024.47 4979.69 46.78 o 7 8 1 1637.26 1688.01 18.10 o 8 8 1 434.18 447.70 7.27 o 9 8 1 15320.48 16052.31 188.15 o 10 8 1 4840.32 5014.84 70.71 o 11 8 1 2118.12 2120.24 40.54 o 12 8 1 1648.60 1620.93 46.14 o 13 8 1 642.19 577.41 39.18 o 1 9 1 7646.26 7488.32 57.12 o 2 9 1 11064.08 11056.75 85.99 o 3 9 1 1775.26 1605.58 14.23 o 4 9 1 2436.03 2359.46 21.27 o 5 9 1 67230.59 68195.88 668.84 o 6 9 1 728.99 713.76 8.69 o 7 9 1 3793.46 3737.84 39.07 o 8 9 1 256.92 255.43 6.79 o 9 9 1 9981.08 10462.50 132.80 o 10 9 1 1050.39 1057.50 21.17 o 11 9 1 3860.67 3855.92 74.64 o 12 9 1 925.51 965.56 39.02 o 13 9 1 66.90 99.51 24.40 o 0 10 1 21058.46 21035.70 214.16 o 1 10 1 5637.19 5389.28 40.00 o 2 10 1 2205.88 2290.14 19.29 o 3 10 1 0.78 28.90 3.16 o 4 10 1 3881.05 3848.17 35.05 o 5 10 1 114.43 104.96 4.19 o 6 10 1 563.19 566.38 8.37 o 7 10 1 6697.05 6511.36 64.45 o 8 10 1 0.81 19.03 6.48 o 9 10 1 98.99 112.86 8.92 o 10 10 1 3037.65 3203.99 51.30 o 11 10 1 214.47 207.80 15.87 o 12 10 1 418.68 388.76 22.98 o 13 10 1 1274.04 1200.19 58.86 o 1 11 1 12075.30 12183.06 91.28 o 2 11 1 742.80 685.90 7.98 o 3 11 1 2474.20 2494.02 22.77 o 4 11 1 528.51 496.08 6.79 o 5 11 1 2155.87 2125.59 24.74 o 6 11 1 42.68 48.02 4.66 o 7 11 1 7482.29 7343.97 85.44 o 8 11 1 31.11 55.44 7.90 o 9 11 1 3952.20 4060.84 70.38 o 10 11 1 132.83 135.53 13.35 o 11 11 1 1654.63 1657.20 47.96 o 12 11 1 661.59 689.10 34.44 o 0 12 1 25932.89 26012.00 275.23 o 1 12 1 444.97 519.68 6.16 o 2 12 1 379.41 373.53 5.85 o 3 12 1 4250.06 4215.48 38.53 o 4 12 1 267.31 288.68 5.92 o 5 12 1 4201.27 4240.36 48.81 o 6 12 1 2968.69 2937.50 33.28 o 7 12 1 555.04 548.66 10.51 o 8 12 1 1430.09 1483.44 26.47 o 9 12 1 434.99 454.88 16.98 o 10 12 1 1461.04 1438.35 37.77 o 11 12 1 4311.25 4377.00 117.18 o 12 12 1 214.46 210.16 22.27 o 1 13 1 946.26 963.49 9.88 o 2 13 1 663.84 671.95 8.77 o 3 13 1 105.79 114.91 4.42 o 4 13 1 3569.82 3650.76 38.91 o 5 13 1 936.19 992.35 13.59 o 6 13 1 12.95 16.51 4.98 o 7 13 1 9908.49 10292.56 130.26 o 8 13 1 78.87 86.32 9.79 o 9 13 1 34.55 46.91 10.50 o 10 13 1 846.89 921.39 29.39 o 11 13 1 9315.54 9450.23 301.51 o 0 14 1 5037.15 5269.73 66.63 o 1 14 1 1883.90 1889.63 17.86 o 2 14 1 681.74 649.74 8.61 o 3 14 1 19.90 33.64 4.34 o 4 14 1 3139.09 3172.76 35.18 o 5 14 1 7872.00 8061.96 94.80 o 6 14 1 2435.93 2446.04 31.77 o 7 14 1 3618.93 3729.50 52.58 o 8 14 1 1462.02 1534.77 30.42 o 9 14 1 8052.39 8318.43 162.91 o 10 14 1 1340.12 1312.90 41.24 o 11 14 1 2324.43 2279.69 82.26 o 1 15 1 638.94 681.87 8.93 o 2 15 1 146.87 130.47 5.29 o 3 15 1 23370.93 24235.04 237.41 o 4 15 1 16942.05 17266.73 187.09 o 5 15 1 31.64 37.99 5.21 o 6 15 1 308.09 307.24 9.71 o 7 15 1 28089.06 29476.89 458.85 o 8 15 1 17.07 -16.11 16.11 o 9 15 1 1348.64 1320.18 36.97 o 10 15 1 228.82 245.31 21.80 o 11 15 1 670.37 598.81 34.76 o 0 16 1 1126.86 1246.96 20.70 o 1 16 1 2588.93 2580.03 27.43 o 2 16 1 4998.33 5196.24 55.30 o 3 16 1 8134.38 8252.55 91.23 o 4 16 1 582.13 585.63 10.98 o 5 16 1 352.77 374.07 9.32 o 6 16 1 81.88 102.67 9.24 o 7 16 1 259.57 281.57 14.30 o 8 16 1 120.99 226.51 20.38 o 9 16 1 2071.44 1993.13 56.74 o 10 16 1 67.08 61.84 26.06 o 1 17 1 1353.73 1329.44 18.41 o 2 17 1 547.23 563.43 10.11 o 3 17 1 2436.63 2557.11 32.09 o 4 17 1 565.72 583.97 11.77 o 5 17 1 46.15 39.80 8.77 o 6 17 1 773.10 814.58 22.36 o 7 17 1 8509.00 8692.69 166.42 o 8 17 1 62.54 82.92 16.27 o 9 17 1 1579.00 1795.55 55.07 o 0 18 1 1489.41 1481.09 30.97 o 1 18 1 613.85 626.08 11.85 o 2 18 1 2669.40 2553.37 35.09 o 3 18 1 3447.89 3516.84 49.33 o 4 18 1 275.61 258.90 10.43 o 5 18 1 8.24 26.46 12.32 o 6 18 1 134.41 147.21 15.48 o 7 18 1 1475.76 1477.13 36.90 o 8 18 1 254.73 216.56 20.61 o 9 18 1 2199.33 2021.51 80.92 o 1 19 1 794.70 812.38 17.77 o 2 19 1 4011.67 4011.62 64.44 o 3 19 1 657.95 633.66 15.09 o 4 19 1 522.69 535.22 17.85 o 5 19 1 3675.85 3768.26 80.09 o 6 19 1 2629.63 2507.49 62.99 o 7 19 1 33.21 -15.64 15.64 o 8 19 1 171.27 187.02 30.41 o 0 20 1 13.75 63.81 19.59 o 1 20 1 65.46 65.95 12.40 o 2 20 1 658.80 636.98 20.62 o 3 20 1 93.07 118.86 12.24 o 4 20 1 263.62 272.80 14.77 o 5 20 1 2594.92 2484.61 62.44 o 6 20 1 828.52 797.12 30.97 o 7 20 1 2692.59 2492.58 92.23 o 1 21 1 4634.36 4847.40 171.68 o 2 21 1 3092.13 3018.45 110.58 o 3 21 1 581.20 582.06 32.38 o 4 21 1 620.55 617.93 33.10 o 5 21 1 17841.57 17859.97 657.55 o 6 21 1 879.85 763.31 48.58 o 1 22 1 11796.53 11903.29 823.06 o 2 22 1 1744.92 1744.76 152.65 o 3 22 1 322.92 333.14 32.70 o 4 22 1 93.25 40.28 27.56 o 5 22 1 1169.00 1189.02 71.49 o 3 23 1 1302.40 1306.53 97.57 o 2 0 2 49850.50 49513.96 594.08 o 3 0 2 77805.70 78938.31 935.13 o 4 0 2 7216.40 6373.47 70.45 o 5 0 2 25.49 132.44 5.21 o 6 0 2 251.13 209.47 6.87 o 7 0 2 5122.51 5054.51 64.60 o 8 0 2 22.27 63.97 7.42 o 9 0 2 3327.91 3258.93 51.64 o 10 0 2 297.18 299.42 12.40 o 11 0 2 8088.88 8300.19 181.24 o 12 0 2 3448.32 3442.92 106.57 o 13 0 2 392.35 382.75 41.55 o 14 0 2 669.12 616.90 53.71 o 1 1 2 14588.51 12572.98 131.92 o 2 1 2 300.58 360.91 3.40 o 3 1 2 6226.36 5962.95 46.97 o 4 1 2 2303.31 2057.09 17.41 o 5 1 2 4236.60 4606.41 37.77 o 6 1 2 6588.38 6488.71 51.76 o 7 1 2 9086.44 8815.99 81.38 o 8 1 2 146.50 136.63 5.13 o 9 1 2 6607.28 6511.81 74.90 o 10 1 2 993.64 988.71 16.43 o 11 1 2 126.00 145.32 11.77 o 12 1 2 2385.78 2411.17 51.77 o 13 1 2 1573.70 1526.23 47.33 o 14 1 2 6.37 134.49 28.98 o 1 2 2 6744.74 6770.87 48.09 o 2 2 2 7311.90 7436.99 54.44 o 3 2 2 8255.39 8093.25 60.10 o 4 2 2 43.75 69.66 2.13 o 5 2 2 40.47 -2.29 2.29 o 6 2 2 1221.23 1146.13 10.51 o 7 2 2 2036.90 2099.43 22.61 o 8 2 2 15146.04 15250.83 149.81 o 9 2 2 14272.38 14453.14 155.47 o 10 2 2 611.56 563.37 12.01 o 11 2 2 2340.39 2300.29 40.94 o 12 2 2 1288.79 1277.75 36.11 o 13 2 2 533.63 524.16 35.94 o 14 2 2 2344.07 2284.51 106.84 o 1 3 2 5597.13 5538.48 39.16 o 2 3 2 7.80 -2.53 2.53 o 3 3 2 7343.96 7010.90 54.30 o 4 3 2 2906.02 3120.14 24.93 o 5 3 2 40.52 109.78 2.45 o 6 3 2 1217.85 1308.74 12.33 o 7 3 2 26720.19 26708.84 241.61 o 8 3 2 2060.58 2072.73 24.50 o 9 3 2 9717.65 9890.01 107.40 o 10 3 2 769.43 743.74 13.67 o 11 3 2 143.88 144.69 10.82 o 12 3 2 493.53 470.28 22.67 o 13 3 2 372.49 373.51 22.35 o 14 3 2 1466.91 1333.22 65.97 o 0 4 2 3.73 24.72 1.82 o 1 4 2 18384.81 17869.23 126.99 o 2 4 2 2549.11 2490.09 18.29 o 3 4 2 6335.13 6033.54 45.65 o 4 4 2 15106.03 14936.14 115.31 o 5 4 2 8767.46 8773.06 70.17 o 6 4 2 15625.58 15289.99 118.38 o 7 4 2 8056.53 8284.48 75.14 o 8 4 2 10304.39 10602.69 96.75 o 9 4 2 17597.00 17772.79 184.18 o 10 4 2 4496.66 4575.29 63.75 o 11 4 2 223.53 206.77 11.14 o 12 4 2 116.89 120.99 14.85 o 13 4 2 1019.25 1041.58 44.87 o 14 4 2 33.59 -40.20 40.20 o 1 5 2 20246.02 19883.52 149.28 o 2 5 2 1120.96 1023.48 8.06 o 3 5 2 9335.11 8902.26 62.99 o 4 5 2 16194.09 15990.28 123.85 o 5 5 2 1630.83 1624.27 13.99 o 6 5 2 5358.66 5358.82 45.37 o 7 5 2 10965.21 11041.62 100.55 o 8 5 2 127.32 124.23 5.45 o 9 5 2 1353.23 1314.47 18.33 o 10 5 2 3300.36 3438.11 47.28 o 11 5 2 3056.47 3004.38 52.81 o 12 5 2 1914.56 1953.51 55.87 o 13 5 2 1403.48 1447.78 57.52 o 14 5 2 3480.41 3290.90 145.37 o 0 6 2 10187.01 9352.76 97.59 o 1 6 2 6822.46 6076.51 45.35 o 2 6 2 13862.25 11374.27 81.09 o 3 6 2 460.30 636.50 6.08 o 4 6 2 47.13 91.69 2.37 o 5 6 2 1040.53 1072.28 10.19 o 6 6 2 1900.91 1915.69 18.34 o 7 6 2 10515.08 10627.45 95.20 o 8 6 2 4834.56 4894.98 52.62 o 9 6 2 7526.04 7757.26 89.16 o 10 6 2 100.58 116.10 8.13 o 11 6 2 754.85 747.83 18.80 o 12 6 2 543.39 481.58 24.33 o 13 6 2 116.23 97.77 27.88 o 1 7 2 1492.82 1233.28 9.96 o 2 7 2 57249.41 59501.83 496.92 o 3 7 2 23710.51 22811.59 164.77 o 4 7 2 3702.89 3653.80 27.86 o 5 7 2 46939.50 47446.05 384.76 o 6 7 2 3076.96 2999.65 27.92 o 7 7 2 41.90 64.92 4.26 o 8 7 2 1089.91 1089.83 14.85 o 9 7 2 1337.61 1363.51 19.44 o 10 7 2 540.96 546.52 12.64 o 11 7 2 1189.48 1171.22 28.44 o 12 7 2 235.26 203.69 20.53 o 13 7 2 8803.56 9081.57 291.32 o 0 8 2 4091.63 4189.69 45.93 o 1 8 2 1029.54 1046.17 8.85 o 2 8 2 42387.20 42074.39 317.22 o 3 8 2 21351.44 22601.53 167.87 o 4 8 2 247.78 243.12 3.63 o 5 8 2 527.08 519.55 6.71 o 6 8 2 19914.96 20658.05 190.15 o 7 8 2 1939.26 1983.88 21.50 o 8 8 2 36.42 61.44 4.66 o 9 8 2 823.55 790.44 14.22 o 10 8 2 13759.30 13896.28 184.74 o 11 8 2 1136.60 1168.43 28.12 o 12 8 2 709.90 673.00 27.73 o 13 8 2 572.53 533.32 35.39 o 1 9 2 1477.32 1401.12 11.70 o 2 9 2 1503.23 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929.68 o 3 0 4 13801.58 14586.00 145.96 o 4 0 4 204.48 123.46 3.32 o 5 0 4 5057.33 4716.85 47.14 o 6 0 4 755.66 940.17 13.98 o 7 0 4 9001.18 8967.65 115.23 o 8 0 4 18644.95 18808.69 254.42 o 9 0 4 858.31 873.74 18.33 o 10 0 4 431.69 418.23 14.85 o 11 0 4 50.09 66.50 13.74 o 12 0 4 0.93 44.38 19.35 o 13 0 4 1318.77 1230.80 62.41 o 14 0 4 3754.68 3679.25 236.45 o 1 1 4 2867.56 2608.30 21.01 o 2 1 4 23281.91 23573.20 185.59 o 3 1 4 1628.81 1400.64 10.99 o 4 1 4 2991.05 3121.56 23.59 o 5 1 4 4636.41 5029.19 36.83 o 6 1 4 797.18 743.94 8.14 o 7 1 4 1286.95 1238.27 14.22 o 8 1 4 4597.08 4489.84 43.91 o 9 1 4 2954.10 2987.75 33.44 o 10 1 4 5384.71 5388.04 66.94 o 11 1 4 380.03 398.16 13.43 o 12 1 4 21.20 35.14 16.51 o 13 1 4 797.35 696.87 32.23 o 14 1 4 59.09 54.81 24.32 o 0 2 4 12520.40 12647.44 148.37 o 1 2 4 76482.66 75736.80 709.18 o 2 2 4 926.95 954.21 7.90 o 3 2 4 8762.06 8614.78 64.12 o 4 2 4 19764.53 19758.41 150.12 o 5 2 4 3469.82 3506.55 27.86 o 6 2 4 6159.29 5897.31 47.06 o 7 2 4 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14 2714.87 2671.07 54.38 o 10 6 14 3623.28 3572.10 108.15 o 11 6 14 1056.96 965.35 42.18 o 1 7 14 3109.18 3198.83 38.11 o 2 7 14 1577.33 1610.70 21.41 o 3 7 14 72.68 91.38 4.66 o 4 7 14 4792.35 4890.10 61.47 o 5 7 14 95.24 106.22 5.61 o 6 7 14 570.54 588.63 12.56 o 7 7 14 556.64 547.31 15.48 o 8 7 14 79.29 79.77 11.14 o 9 7 14 49.34 78.19 15.72 o 10 7 14 7858.13 7914.84 250.42 o 11 7 14 568.68 486.16 33.49 o 0 8 14 2400.60 2390.98 38.50 o 1 8 14 3769.91 3768.05 42.63 o 2 8 14 23178.57 23522.84 302.34 o 3 8 14 1517.21 1492.25 24.50 o 4 8 14 928.10 900.52 17.38 o 5 8 14 829.27 819.28 16.12 o 6 8 14 39.49 48.49 9.16 o 7 8 14 1169.17 1194.61 25.52 o 8 8 14 3965.10 4033.49 82.07 o 9 8 14 4243.47 4014.01 102.55 o 10 8 14 273.43 236.07 27.64 o 11 8 14 73.12 54.02 30.80 o 1 9 14 154.06 171.46 6.00 o 2 9 14 90.95 101.88 7.74 o 3 9 14 4227.04 4300.68 58.92 o 4 9 14 6766.16 6696.37 92.77 o 5 9 14 244.03 243.18 10.50 o 6 9 14 762.82 758.58 20.38 o 7 9 14 2561.97 2520.15 59.59 o 8 9 14 783.80 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12 22 6620.70 6207.11 341.45 o 1 1 23 3955.14 3671.56 121.05 o 2 1 23 254.23 225.41 21.09 o 3 1 23 887.23 886.32 47.16 o 4 1 23 9.17 36.33 28.43 o 5 1 23 3231.66 3325.06 222.35 o 6 1 23 2757.12 2669.09 209.36 o 0 2 23 4466.62 4331.73 191.05 o 1 2 23 1069.38 1014.58 44.40 o 2 2 23 116.38 128.73 17.69 o 3 2 23 1080.28 1066.24 53.80 o 4 2 23 18.91 75.18 22.59 o 5 2 23 1038.61 902.78 57.67 o 6 2 23 85.49 94.46 39.25 o 1 3 23 654.04 643.53 36.26 o 2 3 23 1874.29 1807.81 70.17 o 3 3 23 1792.54 1785.01 73.64 o 4 3 23 2489.24 2318.86 106.85 o 5 3 23 9213.35 9605.64 375.43 o 6 3 23 2803.75 2694.01 158.94 o 0 4 23 1387.92 1237.94 75.37 o 1 4 23 2984.05 3048.69 133.74 o 2 4 23 1411.47 1440.36 59.57 o 3 4 23 2381.96 2386.21 102.34 o 4 4 23 20.38 62.23 22.90 o 5 4 23 876.66 861.90 45.26 o 1 5 23 3949.67 3768.09 189.43 o 2 5 23 782.44 758.24 36.81 o 3 5 23 3728.34 3695.30 166.73 o 4 5 23 1420.51 1349.65 67.87 o 5 5 23 242.00 183.71 27.41 o 0 6 23 1768.87 1866.77 122.39 o 1 6 23 2535.72 2663.16 179.16 o 2 6 23 1538.03 1580.24 72.06 o 3 6 23 47.62 74.95 20.22 o 4 6 23 121.70 139.24 27.25 o 5 6 23 528.26 478.10 34.44 o 1 7 23 1724.36 1671.66 101.61 o 2 7 23 1286.66 1194.12 66.05 o 3 7 23 1879.76 2051.54 104.38 o 4 7 23 401.74 355.50 38.07 o 0 8 23 442.44 443.34 55.05 o 1 8 23 75.14 65.55 25.98 o 2 8 23 22.24 57.65 27.96 o 3 8 23 212.27 130.47 28.51 o 4 8 23 1366.53 1221.39 69.84 o 1 9 23 75.12 90.74 32.38 o 2 9 23 1111.03 1036.77 65.49 o 3 9 23 1633.72 1434.01 92.99 o 0 10 23 4358.42 4362.39 327.18 o 1 10 23 2526.05 2525.49 143.44 o 0 0 24 10727.04 11210.12 1072.73 o 1 0 24 8043.47 8120.79 572.81 o 2 0 24 3269.58 3415.25 184.73 o 3 0 24 7268.50 7448.26 684.64 o 4 0 24 6540.96 6969.10 723.18 o 5 0 24 306.77 330.62 122.66 o 1 1 24 1572.21 1556.08 60.44 o 2 1 24 1060.20 1030.60 71.89 o 3 1 24 138.62 124.94 40.04 o 4 1 24 339.33 330.07 53.23 o 5 1 24 36.24 -33.96 33.96 o 0 2 24 12753.86 12929.93 744.97 o 1 2 24 2394.58 2427.31 128.02 o 2 2 24 183.03 168.62 26.62 o 3 2 24 2280.27 2429.97 117.75 o 4 2 24 3356.89 3220.17 214.85 o 1 3 24 2090.20 1881.39 105.97 o 2 3 24 3.38 -21.88 21.88 o 3 3 24 2.38 30.01 33.49 o 4 3 24 423.87 451.47 37.12 o 0 4 24 27.52 30.41 27.88 o 1 4 24 4034.63 4272.49 200.97 o 2 4 24 10719.54 10443.25 506.19 o 3 4 24 153.61 108.99 20.61 o 4 4 24 446.93 431.73 32.70 o 1 5 24 845.72 792.38 63.83 o 2 5 24 352.40 263.88 29.30 o 3 5 24 705.06 744.32 49.68 o 4 5 24 3636.81 3719.10 146.16 o 0 6 24 1987.86 1854.85 161.67 o 1 6 24 6010.14 6160.50 379.61 o 2 6 24 2866.76 2720.40 169.29 o 3 6 24 231.79 133.00 24.33 o 1 7 24 16.27 68.95 32.62 o 2 7 24 77.67 77.71 23.53 o 0 8 24 54.52 43.52 33.25 o 1 8 24 1613.21 1440.56 94.49 o 1 1 25 482.32 468.78 38.78 o 2 1 25 46.93 33.56 35.30 o 3 1 25 2846.37 2841.75 217.82 o 0 2 25 1405.30 1156.47 123.01 o 1 2 25 506.14 404.56 36.73 o 2 2 25 394.66 317.59 41.70 o 3 2 25 588.33 691.22 81.04 o 1 3 25 1271.00 1202.96 72.13 o 2 3 25 816.54 763.30 64.77 o 0 4 25 263.26 231.49 47.86 o 1 4 25 1144.24 914.81 65.96 o 2 4 25 300.19 250.13 37.44 o 1 5 25 716.46 641.48 47.16 o