#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2209930.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209930_Fobs loop_ _publ_author_name 'Besnard, C\'eline' 'Kloc, Christian' 'Siegrist, Theo' 'Svensson, Christer' 'Pluta, Krystian' _publ_section_title ; Diquino[4,3-b;3',4'-e][1,4]thiaselenine ; _journal_coeditor_code LH2116 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3203 _journal_page_last o3205 _journal_volume 62 _journal_year 2006 _space_group_IT_number 31 _symmetry_space_group_name_Hall 'P 2ac -2' _symmetry_space_group_name_H-M 'P m n 21' _audit_creation_date 06-06-09 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 23.625(3) _cell_length_b 7.3299(9) _cell_length_c 4.1297(5) _[local]_cod_data_source_file lh2116Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 0 0 -4 738.96 825.74 39.79 o 1 0 -4 0.17 0.00 10.31 o 2 0 -4 338.71 348.07 20.55 o 3 0 -4 13.62 0.00 9.25 o 1 1 -4 30.20 17.11 10.72 o 2 1 -4 46.21 46.92 10.41 o 3 1 -4 80.72 63.35 11.74 o 1 0 -3 1178.70 1070.31 58.02 o 2 0 -3 3.04 0.00 6.50 o 3 0 -3 1318.33 1285.65 65.86 o 4 0 -3 3.36 0.00 6.89 o 5 0 -3 25.18 18.23 4.65 o 6 0 -3 1.59 0.00 7.48 o 7 0 -3 324.12 274.68 16.95 o 8 0 -3 3.23 0.00 6.54 o 9 0 -3 415.28 372.30 20.77 o 10 0 -3 3.24 0.00 4.52 o 11 0 -3 222.04 201.79 12.25 o 12 0 -3 0.63 0.00 6.45 o 13 0 -3 98.80 110.57 7.11 o 14 0 -3 5.89 0.00 4.98 o 15 0 -3 162.92 212.39 10.45 o 0 1 -3 881.22 870.86 43.55 o 1 1 -3 175.52 184.73 10.08 o 2 1 -3 672.57 642.66 34.61 o 3 1 -3 310.49 274.42 16.41 o 4 1 -3 296.18 265.78 15.70 o 5 1 -3 523.69 509.04 26.47 o 6 1 -3 775.93 767.84 39.35 o 7 1 -3 209.26 224.87 12.25 o 8 1 -3 1103.23 1123.72 55.15 o 9 1 -3 662.74 668.55 33.58 o 10 1 -3 545.10 529.58 27.05 o 11 1 -3 278.71 312.65 15.04 o 12 1 -3 289.31 318.09 15.70 o 13 1 -3 37.01 38.41 5.32 o 14 1 -3 152.36 168.99 9.53 o 15 1 -3 130.63 150.59 9.03 o 1 2 -3 121.85 106.83 8.25 o 2 2 -3 546.84 559.25 28.00 o 3 2 -3 100.25 107.29 7.37 o 4 2 -3 447.34 421.00 22.47 o 5 2 -3 148.88 130.68 9.51 o 6 2 -3 25.66 27.04 5.74 o 7 2 -3 430.10 456.18 22.52 o 8 2 -3 724.70 733.13 37.17 o 9 2 -3 671.41 727.70 33.14 o 10 2 -3 823.75 944.56 41.13 o 11 2 -3 212.05 223.26 11.78 o 12 2 -3 63.97 59.77 6.28 o 13 2 -3 64.63 77.06 6.42 o 14 2 -3 40.37 42.29 6.00 o 0 3 -3 67.09 66.62 6.95 o 1 3 -3 955.15 915.77 48.28 o 2 3 -3 17.84 16.52 6.16 o 3 3 -3 471.03 462.44 24.49 o 4 3 -3 76.41 75.91 7.16 o 5 3 -3 609.44 584.61 30.54 o 6 3 -3 73.97 91.72 7.05 o 7 3 -3 198.49 179.73 12.17 o 8 3 -3 32.71 26.81 6.22 o 9 3 -3 183.15 200.39 11.37 o 10 3 -3 16.85 18.85 6.64 o 11 3 -3 142.14 137.36 9.26 o 12 3 -3 46.84 65.04 6.20 o 1 4 -3 400.23 448.14 22.04 o 2 4 -3 237.92 222.58 13.95 o 3 4 -3 67.12 57.10 7.72 o 4 4 -3 272.46 254.08 15.56 o 5 4 -3 26.30 15.02 7.12 o 6 4 -3 406.44 413.23 22.76 o 7 4 -3 133.45 140.00 10.02 o 8 4 -3 148.69 140.98 9.86 o 9 4 -3 142.21 185.94 9.71 o 0 0 -2 2752.67 2792.58 137.65 o 1 0 -2 -2.55 0.00 4.17 o 2 0 -2 820.48 798.82 40.78 o 3 0 -2 2.08 0.00 3.83 o 4 0 -2 2333.05 2384.87 116.74 o 5 0 -2 1.17 0.00 5.14 o 6 0 -2 169.33 216.50 9.82 o 7 0 -2 0.25 0.00 4.72 o 8 0 -2 894.24 828.68 43.37 o 9 0 -2 -1.00 0.00 3.81 o 10 0 -2 1050.22 1015.78 52.76 o 11 0 -2 0.50 0.00 4.38 o 12 0 -2 72.97 75.37 5.75 o 13 0 -2 1.25 0.00 5.58 o 14 0 -2 343.02 369.08 17.71 o 15 0 -2 -1.05 0.00 5.44 o 16 0 -2 571.99 618.20 29.57 o 17 0 -2 -0.23 0.00 3.95 o 18 0 -2 326.89 349.67 17.50 o 19 0 -2 2.85 0.00 4.88 o 20 0 -2 107.21 119.89 8.05 o 1 1 -2 2129.85 2242.54 105.92 o 2 1 -2 545.58 546.96 26.29 o 3 1 -2 2343.19 2352.17 118.14 o 4 1 -2 608.57 664.45 32.20 o 5 1 -2 6765.57 6467.90 340.11 o 6 1 -2 5416.18 5300.39 271.69 o 7 1 -2 1834.11 1859.28 88.39 o 8 1 -2 2445.33 2427.26 121.75 o 9 1 -2 944.96 977.99 46.53 o 10 1 -2 265.98 257.85 13.95 o 11 1 -2 764.65 756.89 38.14 o 12 1 -2 1458.82 1474.78 72.96 o 13 1 -2 1250.44 1276.08 63.26 o 14 1 -2 606.22 641.31 31.23 o 15 1 -2 1715.80 1749.65 85.54 o 16 1 -2 48.89 48.53 4.88 o 17 1 -2 288.74 277.85 15.56 o 18 1 -2 158.88 157.35 9.61 o 19 1 -2 289.88 284.44 15.96 o 20 1 -2 103.62 115.06 8.08 o 0 2 -2 233.44 245.16 13.10 o 1 2 -2 593.25 613.90 30.16 o 2 2 -2 198.42 205.52 11.07 o 3 2 -2 941.50 925.06 46.04 o 4 2 -2 1102.22 1094.97 55.08 o 5 2 -2 129.03 164.38 8.22 o 6 2 -2 1473.18 1438.15 72.77 o 7 2 -2 501.62 508.28 25.86 o 8 2 -2 658.28 666.11 32.80 o 9 2 -2 432.94 441.26 22.48 o 10 2 -2 464.12 481.80 23.57 o 11 2 -2 404.08 419.25 20.87 o 12 2 -2 390.48 408.90 19.64 o 13 2 -2 157.99 167.96 9.42 o 14 2 -2 666.11 697.50 33.93 o 15 2 -2 33.77 42.31 4.55 o 16 2 -2 46.79 45.96 5.09 o 17 2 -2 391.11 380.32 20.10 o 18 2 -2 3.37 4.71 6.04 o 19 2 -2 132.29 146.46 9.04 o 1 3 -2 533.44 507.79 26.43 o 2 3 -2 2676.05 2569.11 131.49 o 3 3 -2 612.59 602.88 31.89 o 4 3 -2 1787.53 1775.51 89.42 o 5 3 -2 403.90 407.97 21.07 o 6 3 -2 957.02 955.30 49.16 o 7 3 -2 293.42 301.58 15.23 o 8 3 -2 1205.27 1160.10 60.24 o 9 3 -2 134.93 137.91 8.40 o 10 3 -2 742.45 688.69 37.56 o 11 3 -2 196.30 201.58 11.09 o 12 3 -2 556.30 576.77 28.47 o 13 3 -2 65.00 63.45 6.15 o 14 3 -2 589.53 610.99 30.48 o 15 3 -2 41.43 47.16 6.54 o 16 3 -2 632.39 606.82 31.69 o 17 3 -2 90.64 96.28 7.13 o 0 4 -2 77.04 77.86 6.14 o 1 4 -2 1086.58 1037.59 53.20 o 2 4 -2 54.56 55.84 5.38 o 3 4 -2 1059.66 1071.32 53.49 o 4 4 -2 15.55 17.99 4.44 o 5 4 -2 669.35 671.57 34.34 o 6 4 -2 46.29 57.48 5.32 o 7 4 -2 1019.74 985.38 49.93 o 8 4 -2 61.34 53.37 5.60 o 9 4 -2 1249.60 1269.09 63.33 o 10 4 -2 446.48 462.96 22.82 o 11 4 -2 631.86 611.83 31.92 o 12 4 -2 4.11 5.22 6.18 o 13 4 -2 496.22 519.83 26.34 o 14 4 -2 18.76 28.12 6.54 o 15 4 -2 235.65 229.50 14.12 o 1 5 -2 463.10 488.19 24.44 o 2 5 -2 97.75 104.61 7.15 o 3 5 -2 503.76 510.68 25.91 o 4 5 -2 166.19 198.68 10.03 o 5 5 -2 338.52 350.99 18.15 o 6 5 -2 88.28 84.67 6.93 o 7 5 -2 67.53 51.80 6.49 o 8 5 -2 54.69 51.59 6.62 o 9 5 -2 333.78 318.23 17.92 o 10 5 -2 197.46 220.76 11.83 o 11 5 -2 123.86 121.45 8.74 o 12 5 -2 118.83 131.15 9.08 o 0 6 -2 1239.38 1314.69 62.55 o 1 6 -2 118.64 102.40 9.08 o 2 6 -2 500.75 492.55 26.29 o 3 6 -2 28.49 27.74 6.21 o 4 6 -2 291.94 306.58 16.23 o 5 6 -2 22.78 33.23 7.27 o 6 6 -2 359.34 368.15 19.56 o 2 0 -1 -5.55 0.00 4.54 o 4 0 -1 -2.21 0.00 6.70 o 6 0 -1 -0.01 0.00 5.06 o 7 0 -1 2365.79 2508.46 118.88 o 8 0 -1 -0.39 0.00 6.49 o 9 0 -1 1482.86 1617.92 72.82 o 10 0 -1 -0.62 0.00 4.65 o 11 0 -1 2832.65 2922.31 140.69 o 12 0 -1 -2.21 0.00 6.10 o 13 0 -1 2686.03 2756.74 134.09 o 14 0 -1 0.44 0.00 4.79 o 15 0 -1 1802.68 1979.93 92.77 o 16 0 -1 0.96 0.00 5.87 o 17 0 -1 2314.96 2396.18 116.87 o 18 0 -1 2.41 0.00 6.12 o 19 0 -1 588.54 642.54 30.01 o 20 0 -1 0.68 0.00 5.49 o 21 0 -1 1110.18 1241.17 58.20 o 22 0 -1 -11.65 0.00 7.11 o 0 1 -1 2046.42 2070.25 106.83 o 1 1 -1 1279.24 1112.00 65.71 o 4 1 -1 6032.12 5981.64 289.65 o 5 1 -1 3643.36 3482.11 177.04 o 6 1 -1 2244.41 2344.05 110.60 o 7 1 -1 1186.64 1146.84 58.78 o 8 1 -1 1704.93 1780.93 85.58 o 9 1 -1 3577.25 3443.98 178.43 o 10 1 -1 281.51 367.21 16.03 o 11 1 -1 1296.09 1334.19 64.91 o 12 1 -1 2641.34 2646.92 130.74 o 13 1 -1 460.42 451.18 22.77 o 14 1 -1 1182.73 1173.11 58.88 o 15 1 -1 554.40 534.86 27.68 o 16 1 -1 1631.39 1589.74 80.49 o 17 1 -1 346.18 365.92 18.37 o 18 1 -1 708.30 717.44 36.48 o 19 1 -1 7.05 17.45 5.28 o 20 1 -1 156.71 154.42 10.11 o 21 1 -1 206.17 195.56 12.37 o 22 1 -1 465.84 544.82 24.81 o 1 2 -1 1134.83 1133.95 57.89 o 2 2 -1 2550.29 2781.80 127.19 o 3 2 -1 574.37 615.75 30.12 o 4 2 -1 4385.59 4330.46 214.92 o 5 2 -1 475.07 522.83 23.22 o 6 2 -1 3419.14 3563.26 170.65 o 7 2 -1 2520.59 2539.56 123.48 o 8 2 -1 2660.80 2671.26 134.05 o 9 2 -1 523.45 529.72 27.06 o 10 2 -1 2823.90 2905.45 141.51 o 11 2 -1 1159.19 1174.83 58.06 o 12 2 -1 1873.19 1896.07 93.78 o 13 2 -1 806.62 781.79 40.11 o 14 2 -1 1139.66 1186.68 57.18 o 15 2 -1 24.70 25.13 4.63 o 16 2 -1 360.45 351.39 18.54 o 17 2 -1 426.60 421.53 22.83 o 18 2 -1 257.61 243.04 14.20 o 19 2 -1 70.75 70.32 7.23 o 20 2 -1 796.73 772.32 41.19 o 21 2 -1 52.02 48.30 7.03 o 0 3 -1 2130.66 2017.23 109.19 o 1 3 -1 2683.35 2674.65 132.24 o 2 3 -1 588.75 550.12 29.34 o 3 3 -1 1979.40 2060.97 99.76 o 4 3 -1 1582.89 1529.38 77.15 o 5 3 -1 4005.22 3979.64 198.03 o 6 3 -1 786.06 719.11 39.64 o 7 3 -1 2743.86 2679.71 136.64 o 8 3 -1 282.93 319.51 15.44 o 9 3 -1 527.32 576.70 26.55 o 10 3 -1 230.39 250.66 12.35 o 11 3 -1 1257.66 1249.83 63.21 o 12 3 -1 179.49 201.03 10.12 o 13 3 -1 1201.10 1207.31 60.00 o 14 3 -1 253.15 252.45 13.48 o 15 3 -1 802.48 773.73 41.06 o 16 3 -1 162.87 162.23 9.85 o 17 3 -1 510.42 478.24 25.97 o 18 3 -1 78.21 91.46 7.58 o 19 3 -1 393.63 379.47 21.23 o 20 3 -1 33.17 35.38 8.28 o 1 4 -1 314.10 356.30 16.96 o 2 4 -1 879.24 932.33 44.00 o 3 4 -1 843.36 864.00 42.42 o 4 4 -1 936.05 930.73 48.35 o 5 4 -1 136.53 138.41 8.09 o 6 4 -1 1704.48 1680.78 85.35 o 7 4 -1 588.17 635.13 30.39 o 8 4 -1 1384.60 1416.00 69.12 o 9 4 -1 578.80 584.00 29.15 o 10 4 -1 1301.58 1278.08 64.77 o 11 4 -1 564.49 539.99 28.01 o 12 4 -1 792.87 782.07 40.24 o 13 4 -1 256.92 254.53 14.19 o 14 4 -1 191.73 159.36 11.18 o 15 4 -1 15.59 12.63 6.23 o 16 4 -1 271.72 231.49 15.53 o 17 4 -1 116.55 118.00 9.58 o 18 4 -1 256.05 230.54 15.34 o 0 5 -1 841.88 856.31 42.83 o 1 5 -1 528.74 548.17 27.17 o 2 5 -1 1121.94 1086.78 56.51 o 3 5 -1 677.97 676.07 33.57 o 4 5 -1 441.33 428.83 23.08 o 5 5 -1 204.03 216.21 11.60 o 6 5 -1 673.43 688.37 34.40 o 7 5 -1 625.26 650.80 32.94 o 8 5 -1 351.85 341.64 17.99 o 9 5 -1 1257.46 1253.38 62.59 o 10 5 -1 98.59 93.51 6.80 o 11 5 -1 507.74 531.54 26.40 o 12 5 -1 558.65 534.36 28.33 o 13 5 -1 32.72 33.31 5.93 o 14 5 -1 263.04 258.34 15.11 o 15 5 -1 96.22 102.18 8.41 o 16 5 -1 261.40 277.93 15.09 o 1 6 -1 1017.16 986.11 50.68 o 2 6 -1 29.24 25.44 4.77 o 3 6 -1 945.42 922.39 48.07 o 4 6 -1 66.54 65.44 5.76 o 5 6 -1 187.88 186.66 11.16 o 6 6 -1 41.31 36.15 5.28 o 7 6 -1 313.67 320.50 16.55 o 8 6 -1 10.70 11.07 5.22 o 9 6 -1 138.69 124.68 9.35 o 10 6 -1 24.31 28.97 5.62 o 11 6 -1 217.78 206.80 13.59 o 0 7 -1 371.80 391.17 19.68 o 1 7 -1 17.44 16.33 5.76 o 2 7 -1 316.34 321.77 16.03 o 3 0 0 3.31 0.00 3.61 x 4 0 0 38.52 0.00 4.60 x 5 0 0 -9.52 0.00 4.01 o 7 0 0 -3.30 0.00 4.38 o 8 0 0 6540.76 6600.49 324.42 o 9 0 0 -10.10 0.00 3.82 o 10 0 0 6210.33 6316.27 308.18 o 11 0 0 -0.68 0.00 5.25 o 12 0 0 3128.81 3079.53 155.13 o 13 0 0 -0.73 0.00 5.13 o 14 0 0 4836.18 4795.04 239.78 o 15 0 0 2.54 0.00 3.78 o 16 0 0 1799.34 1762.11 89.42 o 17 0 0 -1.14 0.00 4.57 o 18 0 0 5112.10 4942.48 253.46 o 19 0 0 3.93 0.00 5.05 o 20 0 0 3662.45 3598.95 181.66 o 21 0 0 8.73 0.00 6.56 o 22 0 0 4.36 7.49 8.06 o 23 0 0 12.54 0.00 9.88 o 2 1 0 450.41 0.00 22.98 x 3 1 0 1.69 0.00 4.63 x 4 1 0 546.11 646.02 27.52 o 6 1 0 307.28 414.56 15.90 o 7 1 0 4.21 57.73 4.15 o 8 1 0 825.43 931.38 41.20 o 9 1 0 2806.11 2828.24 139.14 o 10 1 0 1987.62 1965.23 98.57 o 11 1 0 591.43 727.02 29.78 o 12 1 0 188.45 179.11 10.43 o 13 1 0 222.21 297.04 11.93 o 14 1 0 178.28 140.86 9.98 o 15 1 0 1668.02 1642.84 82.90 o 16 1 0 85.92 77.83 6.26 o 17 1 0 759.80 736.98 38.21 o 18 1 0 78.74 58.33 6.58 o 19 1 0 1270.85 1217.27 63.56 o 20 1 0 178.36 222.12 11.02 o 21 1 0 25.25 23.19 7.06 o 22 1 0 37.45 27.31 8.70 o 23 1 0 27.25 19.33 10.26 o 0 2 0 19.11 36.77 5.32 o 2 2 0 587.77 722.90 29.73 o 3 2 0 3473.05 3746.88 172.31 o 4 2 0 2159.49 2348.44 107.17 o 5 2 0 3271.83 3399.10 162.29 o 6 2 0 120.44 75.29 7.67 o 8 2 0 1015.19 1029.10 50.64 o 9 2 0 9762.39 9519.66 484.02 o 10 2 0 4795.40 4518.10 237.76 o 11 2 0 3799.43 3914.52 188.38 o 12 2 0 10.10 5.31 4.27 o 13 2 0 1820.64 1889.08 90.41 o 14 2 0 99.63 134.47 6.76 o 15 2 0 846.70 861.34 42.47 o 16 2 0 285.64 290.56 15.29 o 17 2 0 1366.68 1248.79 68.19 o 18 2 0 85.52 70.70 7.25 o 19 2 0 1000.54 945.08 50.37 o 20 2 0 109.95 96.30 8.95 o 21 2 0 335.69 330.50 18.93 o 22 2 0 29.53 39.96 10.11 o 1 3 0 1152.11 1005.77 57.47 o 2 3 0 2283.54 2501.01 113.33 o 3 3 0 1194.73 1109.74 59.53 o 4 3 0 5834.32 5638.77 289.26 o 5 3 0 51.32 50.08 5.23 o 6 3 0 2075.83 2183.93 103.01 o 7 3 0 263.68 299.55 14.00 o 8 3 0 2121.52 2083.81 105.27 o 9 3 0 758.00 738.43 38.02 o 10 3 0 929.43 987.91 46.48 o 11 3 0 250.31 258.75 13.43 o 12 3 0 635.48 665.72 32.09 o 13 3 0 115.26 143.56 7.65 o 14 3 0 1355.77 1340.35 67.61 o 15 3 0 100.41 107.29 7.05 o 16 3 0 797.99 822.05 40.24 o 17 3 0 34.40 38.23 6.00 o 18 3 0 364.39 316.76 19.49 o 19 3 0 110.71 102.74 8.86 o 20 3 0 186.77 164.46 12.50 o 21 3 0 111.89 123.62 12.03 o 0 4 0 3658.57 3512.01 181.39 o 1 4 0 4.39 29.00 5.29 o 2 4 0 369.89 448.95 19.18 o 3 4 0 1903.04 1922.88 94.53 o 4 4 0 502.56 562.70 25.62 o 5 4 0 1898.89 1755.54 94.35 o 6 4 0 1577.93 1491.17 78.51 o 7 4 0 537.61 560.95 27.35 o 8 4 0 1313.28 1279.11 65.45 o 9 4 0 1251.03 1291.37 62.40 o 10 4 0 967.19 979.68 48.44 o 11 4 0 636.03 628.68 32.18 o 12 4 0 308.57 280.28 16.42 o 13 4 0 499.10 460.39 25.63 o 14 4 0 565.80 563.52 28.93 o 15 4 0 306.14 313.73 16.57 o 16 4 0 190.40 170.14 11.97 o 17 4 0 41.57 26.95 7.49 o 18 4 0 90.64 79.19 9.53 o 19 4 0 42.54 27.01 10.73 o 1 5 0 924.91 879.10 46.32 o 2 5 0 317.32 326.97 16.59 o 3 5 0 957.59 989.13 47.94 o 4 5 0 730.82 740.88 36.80 o 5 5 0 1712.10 1714.19 85.17 o 6 5 0 2132.92 2140.86 105.96 o 7 5 0 156.71 142.01 9.21 o 8 5 0 965.88 1001.07 48.40 o 9 5 0 141.85 144.86 8.65 o 10 5 0 359.52 376.05 18.83 o 11 5 0 121.36 122.00 8.06 o 12 5 0 834.08 839.38 42.11 o 13 5 0 452.27 429.27 23.55 o 14 5 0 609.94 631.09 31.28 o 15 5 0 910.90 931.69 46.14 o 16 5 0 6.54 3.54 8.42 o 17 5 0 103.08 93.60 12.18 o 0 6 0 271.24 236.91 14.44 o 1 6 0 24.97 23.32 4.16 o 2 6 0 528.11 504.41 26.93 o 3 6 0 25.15 32.07 4.35 o 4 6 0 1004.56 1114.73 50.34 o 5 6 0 104.53 100.93 7.05 o 6 6 0 38.00 34.84 4.98 o 7 6 0 4.15 4.28 5.75 o 8 6 0 7.78 18.22 5.21 o 9 6 0 286.52 315.68 15.71 o 10 6 0 215.07 219.37 12.57 o 11 6 0 18.83 24.84 6.55 o 12 6 0 86.50 61.31 8.49 o 13 6 0 30.97 32.88 7.25 o 1 7 0 477.46 459.50 24.73 o 2 7 0 14.91 17.80 5.11 o 3 7 0 412.72 389.26 21.66 o 4 7 0 30.64 36.08 5.54 o 5 7 0 511.38 519.73 26.49 o 6 7 0 142.23 166.14 9.71 o 2 0 1 -8.03 0.00 4.29 o 4 0 1 -6.01 0.00 4.23 o 6 0 1 -5.69 0.00 4.70 o 7 0 1 2459.85 2541.98 118.90 o 8 0 1 -1.79 0.00 4.79 o 9 0 1 1425.41 1553.80 72.78 o 10 0 1 7.36 0.00 4.66 o 11 0 1 2847.52 2844.44 140.69 o 12 0 1 3.89 0.00 4.52 o 13 0 1 2738.90 2731.21 134.06 o 14 0 1 5.71 0.00 4.69 o 15 0 1 1995.46 1942.44 92.81 o 16 0 1 5.23 0.00 4.35 o 17 0 1 2431.37 2385.07 116.92 o 18 0 1 4.24 0.00 4.75 o 20 0 1 3.73 0.00 5.61 o 21 0 1 1259.80 1237.81 58.29 o 0 1 1 2263.49 2211.36 106.89 o 1 1 1 1366.50 1114.81 65.72 o 4 1 1 5743.99 5950.75 289.57 o 5 1 1 3508.35 3486.74 177.00 o 6 1 1 2207.88 2339.98 110.60 o 7 1 1 1170.39 1142.55 58.80 o 8 1 1 1752.76 1827.40 85.61 o 9 1 1 3631.55 3498.02 178.45 o 10 1 1 347.14 405.10 16.12 o 11 1 1 1317.55 1363.87 64.95 o 12 1 1 2629.33 2662.99 130.75 o 13 1 1 425.94 440.18 22.72 o 14 1 1 1177.52 1165.89 58.88 o 15 1 1 532.20 545.75 27.65 o 16 1 1 1600.80 1611.31 80.47 o 17 1 1 357.29 384.90 18.36 o 18 1 1 748.68 740.94 36.49 o 20 1 1 160.49 161.55 10.24 o 21 1 1 197.76 196.28 12.43 o 1 2 1 1186.54 1154.16 57.88 o 2 2 1 2578.50 2736.08 127.20 o 3 2 1 617.54 646.43 30.11 o 4 2 1 4282.96 4214.85 214.88 o 5 2 1 439.99 510.69 23.16 o 6 2 1 3465.14 3514.94 170.67 o 7 2 1 2459.88 2535.85 123.47 o 8 2 1 2739.55 2679.72 134.07 o 9 2 1 543.81 545.99 26.98 o 10 2 1 2889.85 2878.84 141.53 o 11 2 1 1172.46 1193.02 58.04 o 12 2 1 1909.56 1865.30 93.79 o 13 2 1 787.69 772.13 40.15 o 14 2 1 1155.57 1155.32 57.23 o 15 2 1 19.86 22.23 4.87 o 16 2 1 344.86 338.16 18.63 o 17 2 1 462.55 435.12 22.96 o 18 2 1 249.04 231.09 14.36 o 19 2 1 71.02 73.10 7.89 o 20 2 1 822.32 761.59 41.37 o 21 2 1 56.58 47.90 8.42 o 0 3 1 2250.99 2033.99 109.20 o 1 3 1 2653.48 2647.00 132.24 o 2 3 1 573.29 546.05 29.31 o 3 3 1 2034.98 2086.59 99.75 o 4 3 1 1524.95 1517.16 77.13 o 5 3 1 3984.60 4007.10 198.03 o 6 3 1 794.64 719.87 39.62 o 7 3 1 2767.80 2727.41 136.65 o 8 3 1 303.22 320.76 15.42 o 9 3 1 519.69 576.18 26.52 o 10 3 1 226.01 249.21 12.34 o 11 3 1 1282.40 1261.92 63.22 o 12 3 1 180.22 201.33 10.14 o 13 3 1 1203.64 1221.03 59.98 o 14 3 1 244.44 250.46 13.51 o 15 3 1 836.34 771.97 41.11 o 16 3 1 160.91 161.00 10.01 o 17 3 1 487.00 481.40 26.08 o 18 3 1 84.37 92.51 8.10 o 19 3 1 398.24 373.42 21.96 o 20 3 1 29.36 35.90 7.97 o 1 4 1 329.37 352.80 16.95 o 2 4 1 876.41 946.10 43.99 o 3 4 1 847.97 839.26 42.42 o 4 4 1 989.11 965.82 48.36 o 5 4 1 128.11 128.66 8.05 o 6 4 1 1726.75 1707.42 85.35 o 7 4 1 611.15 633.60 30.38 o 8 4 1 1389.85 1427.02 69.12 o 9 4 1 570.60 567.01 29.14 o 10 4 1 1294.91 1285.93 64.77 o 11 4 1 535.03 527.01 27.96 o 12 4 1 804.04 799.59 40.27 o 13 4 1 256.85 252.84 14.26 o 14 4 1 178.31 163.27 11.23 o 15 4 1 10.38 10.41 5.91 o 16 4 1 274.09 233.55 15.49 o 17 4 1 107.90 114.11 9.21 o 18 4 1 255.07 229.01 15.57 o 0 5 1 862.47 855.29 42.84 o 1 5 1 537.99 535.18 27.17 o 2 5 1 1136.94 1085.73 56.49 o 3 5 1 651.60 655.24 33.57 o 4 5 1 456.41 433.56 23.11 o 5 5 1 212.55 209.68 11.68 o 6 5 1 687.91 699.36 34.43 o 7 5 1 673.46 655.32 32.98 o 8 5 1 333.97 331.72 17.97 o 9 5 1 1247.93 1241.36 62.61 o 10 5 1 75.68 81.29 6.86 o 11 5 1 516.96 523.16 26.44 o 12 5 1 543.89 539.59 28.35 o 13 5 1 36.93 34.68 6.51 o 14 5 1 265.25 264.23 15.13 o 15 5 1 93.18 97.23 9.10 o 1 6 1 1003.38 984.80 50.68 o 2 6 1 28.41 26.50 4.82 o 3 6 1 969.05 949.14 48.09 o 4 6 1 61.72 67.56 5.76 o 5 6 1 202.81 198.78 11.26 o 6 6 1 36.47 36.25 5.27 o 7 6 1 299.92 314.69 16.62 o 8 6 1 9.17 10.73 5.62 o 9 6 1 133.18 127.13 9.65 o 10 6 1 23.15 27.89 6.77 o 11 6 1 227.40 215.18 13.59 o 0 7 1 365.17 382.84 19.80 o 1 7 1 21.90 17.70 5.76 o 2 7 1 266.04 320.03 16.03 o 0 0 2 2820.31 2823.85 137.67 o 1 0 2 -1.96 0.00 3.52 o 2 0 2 807.34 777.63 40.72 o 3 0 2 2.45 0.00 3.42 o 4 0 2 2396.83 2400.82 116.74 o 5 0 2 0.28 0.00 6.09 o 6 0 2 155.71 195.04 9.57 o 7 0 2 -0.95 0.00 8.71 o 8 0 2 805.22 768.88 43.28 o 9 0 2 0.38 0.00 4.96 o 10 0 2 1067.72 996.00 52.73 o 11 0 2 2.88 0.00 3.93 o 12 0 2 69.04 73.70 5.71 o 13 0 2 3.45 0.00 4.47 o 14 0 2 335.26 379.85 17.69 o 15 0 2 0.93 0.00 7.85 o 16 0 2 603.24 613.13 29.63 o 17 0 2 1.20 0.00 3.99 o 18 0 2 342.12 352.11 17.59 o 20 0 2 111.65 121.44 8.33 o 1 1 2 2143.48 2238.74 105.93 o 2 1 2 486.62 525.90 26.28 o 3 1 2 2434.81 2397.69 118.15 o 4 1 2 685.68 691.27 32.22 o 5 1 2 6955.23 6512.81 340.17 o 6 1 2 5557.24 5323.29 271.74 o 7 1 2 1714.04 1813.72 88.34 o 8 1 2 2468.17 2412.95 121.77 o 9 1 2 908.55 962.05 46.53 o 10 1 2 254.52 256.36 13.93 o 11 1 2 750.61 755.40 38.14 o 12 1 2 1474.99 1482.51 72.93 o 13 1 2 1302.91 1288.73 63.28 o 14 1 2 642.55 646.24 31.28 o 15 1 2 1724.30 1766.46 85.54 o 16 1 2 40.93 43.61 4.95 o 17 1 2 294.07 278.82 15.58 o 18 1 2 160.40 155.03 9.78 o 19 1 2 302.33 285.80 16.08 o 20 1 2 111.48 116.47 8.66 o 0 2 2 257.20 251.18 13.12 o 1 2 2 603.28 608.72 30.15 o 2 2 2 205.18 208.57 11.03 o 3 2 2 894.42 872.61 46.03 o 4 2 2 1108.06 1106.37 55.06 o 5 2 2 147.33 187.71 8.11 o 6 2 2 1448.67 1430.80 72.75 o 7 2 2 516.64 513.76 25.84 o 8 2 2 639.82 664.08 32.82 o 9 2 2 451.30 437.33 22.51 o 10 2 2 460.24 485.41 23.61 o 11 2 2 409.28 418.40 20.95 o 12 2 2 364.26 403.38 19.69 o 13 2 2 173.08 174.39 9.51 o 14 2 2 679.44 704.70 33.97 o 15 2 2 28.48 34.79 4.71 o 16 2 2 47.32 47.29 5.41 o 17 2 2 369.02 362.51 20.15 o 18 2 2 5.27 3.62 5.20 o 19 2 2 133.62 150.28 9.19 o 1 3 2 507.29 497.70 26.39 o 2 3 2 2628.93 2542.87 131.47 o 3 3 2 648.78 603.42 31.89 o 4 3 2 1809.09 1798.78 89.40 o 5 3 2 415.80 404.21 21.03 o 6 3 2 1006.23 972.35 49.15 o 7 3 2 285.55 294.62 15.15 o 8 3 2 1208.12 1165.02 60.26 o 9 3 2 131.21 133.84 8.39 o 10 3 2 748.92 704.65 37.56 o 11 3 2 198.91 198.58 11.21 o 12 3 2 561.98 574.24 28.55 o 13 3 2 67.45 61.80 6.68 o 14 3 2 608.30 619.75 30.65 o 15 3 2 38.07 46.15 7.12 o 16 3 2 599.05 600.53 31.74 o 17 3 2 79.21 94.43 7.30 o 0 4 2 75.06 79.06 6.11 o 1 4 2 1045.58 1030.21 53.17 o 2 4 2 57.90 61.16 5.52 o 3 4 2 1076.74 1074.75 53.49 o 4 4 2 16.46 21.03 4.33 o 5 4 2 687.70 674.30 34.32 o 6 4 2 44.78 55.05 5.32 o 7 4 2 971.85 983.83 49.87 o 8 4 2 56.30 52.20 5.69 o 9 4 2 1287.41 1295.94 63.39 o 10 4 2 432.24 459.48 22.85 o 11 4 2 615.99 616.88 31.92 o 12 4 2 6.78 4.81 6.90 o 13 4 2 529.26 509.23 26.79 o 14 4 2 26.09 30.11 7.51 o 15 4 2 221.88 230.38 13.19 o 1 5 2 481.64 493.37 24.44 o 2 5 2 102.42 97.98 7.26 o 3 5 2 504.44 513.47 25.94 o 4 5 2 164.93 190.24 10.04 o 5 5 2 345.35 350.68 18.18 o 6 5 2 80.97 77.31 6.95 o 7 5 2 61.24 49.92 6.52 o 8 5 2 62.41 54.62 6.90 o 9 5 2 326.21 316.69 18.01 o 10 5 2 197.14 225.68 11.75 o 11 5 2 117.48 117.68 8.89 o 12 5 2 115.50 125.16 8.28 o 0 6 2 1258.43 1327.77 62.54 o 1 6 2 107.25 105.50 8.30 o 2 6 2 509.72 495.76 26.27 o 3 6 2 27.74 28.92 6.11 o 4 6 2 284.55 303.20 16.47 o 5 6 2 30.34 35.06 7.64 o 6 6 2 347.51 364.57 19.71 o 1 0 3 1126.46 1089.97 57.94 o 2 0 3 1.81 0.00 5.48 o 3 0 3 1323.79 1326.46 65.79 o 4 0 3 2.40 0.00 3.10 o 5 0 3 14.43 19.34 3.83 o 6 0 3 1.85 0.00 4.38 o 7 0 3 306.59 274.95 16.77 o 8 0 3 -4.33 0.00 4.24 o 9 0 3 370.76 387.29 20.54 o 10 0 3 3.11 0.00 3.94 o 11 0 3 213.77 211.34 11.92 o 12 0 3 2.78 0.00 3.88 o 13 0 3 92.25 109.49 6.71 o 14 0 3 -1.80 0.00 4.41 o 15 0 3 179.31 225.42 10.24 o 0 1 3 847.72 856.21 43.51 o 1 1 3 164.93 175.81 10.02 o 2 1 3 700.61 641.56 34.59 o 3 1 3 304.96 266.66 16.36 o 4 1 3 293.07 262.14 15.56 o 5 1 3 506.14 497.29 26.32 o 6 1 3 791.73 764.81 39.26 o 7 1 3 232.79 228.13 12.05 o 8 1 3 1095.41 1110.20 55.04 o 9 1 3 663.26 665.79 33.47 o 10 1 3 495.50 508.67 26.87 o 11 1 3 281.10 305.02 14.84 o 12 1 3 300.82 315.11 15.52 o 13 1 3 34.92 35.77 4.69 o 14 1 3 149.51 171.44 9.09 o 15 1 3 136.21 148.03 8.61 o 1 2 3 118.17 103.14 8.14 o 2 2 3 547.56 577.94 27.93 o 3 2 3 93.97 102.59 7.16 o 4 2 3 415.03 417.48 22.37 o 5 2 3 159.02 133.31 9.41 o 6 2 3 33.37 33.26 5.70 o 7 2 3 435.64 460.32 22.50 o 8 2 3 748.97 760.80 37.18 o 9 2 3 628.26 716.54 33.08 o 10 2 3 804.22 957.91 41.05 o 11 2 3 195.79 221.10 11.55 o 12 2 3 69.10 66.57 5.62 o 13 2 3 65.59 81.04 5.72 o 14 2 3 24.17 38.51 5.04 o 0 3 3 74.55 64.36 6.64 o 1 3 3 963.19 904.37 48.24 o 2 3 3 13.84 16.17 5.72 o 3 3 3 468.39 458.30 24.42 o 4 3 3 72.97 76.48 7.05 o 5 3 3 579.37 578.26 30.48 o 6 3 3 71.32 89.66 7.00 o 7 3 3 210.58 189.49 12.20 o 8 3 3 26.85 25.50 6.18 o 9 3 3 181.93 199.14 11.71 o 10 3 3 18.34 19.93 7.51 o 11 3 3 134.23 138.93 8.93 o 12 3 3 43.48 64.41 6.08 o 1 4 3 421.42 458.51 21.98 o 2 4 3 230.72 215.20 13.77 o 3 4 3 71.20 60.43 7.58 o 4 4 3 271.36 245.45 15.43 o 5 4 3 18.17 15.33 6.89 o 6 4 3 429.10 415.77 22.65 o 7 4 3 116.59 140.22 8.49 o 8 4 3 143.77 140.79 9.30 o 9 4 3 147.71 190.00 12.01 o 0 0 4 812.20 839.97 39.38 o 1 0 4 6.80 0.00 7.95 o 2 0 4 354.76 351.70 19.74 o 3 0 4 4.83 0.00 7.03 o 1 1 4 15.90 17.82 9.15 o 2 1 4 33.41 44.67 9.00 o 3 1 4 54.14 58.84 9.43 o