#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/99/2209973.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209973_Fobs loop_ _publ_author_name 'Scheidt, W. Robert' 'Noll, Bruce C.' _publ_section_title ; Dipyridine(2,3,12,13-tetrabromo-5,10,15,20-tetraphenylporphyrin)iron(II) pyridine solvate ; _journal_coeditor_code OM2034 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1892 _journal_page_last m1894 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.688 _cell_angle_gamma 90.000 _cell_length_a 18.4633 _cell_length_b 19.9786 _cell_length_c 14.4636 _exptl_crystal_F_000 2432.00 _reflns_d_resolution_high 0.7436 _[local]_cod_data_source_file om2034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ave01 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 545.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48706.27 48988.88 552.56 o 4 0 0 81057.21 92460.27 1080.08 o 6 0 0 88951.80 99904.18 1165.79 o 8 0 0 208.82 559.34 36.48 o 10 0 0 81242.13 81613.60 1176.70 o 12 0 0 431.56 646.01 49.42 o 14 0 0 3081.66 2847.75 100.30 o 16 0 0 2849.92 2766.63 100.98 o 18 0 0 6706.32 6076.07 273.41 o 20 0 0 12765.94 13167.69 450.13 o 22 0 0 316.82 271.08 217.50 o 1 1 0 47446.96 50279.52 628.00 o 3 1 0 5539.31 5149.23 52.93 o 5 1 0 16635.99 18836.26 170.55 o 7 1 0 21244.34 22891.40 221.58 o 9 1 0 1520.62 2082.58 35.10 o 11 1 0 1401.38 1444.66 36.75 o 13 1 0 3242.56 3312.07 69.78 o 15 1 0 263.52 275.72 59.71 o 17 1 0 40.28 15.55 57.95 o 19 1 0 524.15 684.92 110.04 o 21 1 0 30.65 -107.51 114.50 o 0 2 0 297728.09 284183.22 3162.00 o 2 2 0 19038.14 17657.73 153.29 o 4 2 0 9021.52 10603.90 95.80 o 6 2 0 16239.96 16417.04 155.86 o 8 2 0 1302.59 787.51 20.29 o 10 2 0 42382.84 39541.42 392.77 o 12 2 0 47.67 58.26 25.33 o 14 2 0 1311.37 1417.90 95.40 o 16 2 0 315.76 308.87 66.22 o 18 2 0 2960.62 3061.89 101.57 o 20 2 0 8767.12 8974.54 207.94 o 22 2 0 676.95 708.25 153.47 o 1 3 0 213376.17 229094.94 2010.40 o 3 3 0 24573.46 26138.70 225.53 o 5 3 0 1759.56 1913.71 28.84 o 7 3 0 70427.92 75424.13 709.58 o 9 3 0 958.29 1051.54 40.34 o 11 3 0 1271.45 1306.25 37.91 o 13 3 0 25782.88 25000.05 333.01 o 15 3 0 587.11 490.69 64.56 o 17 3 0 940.23 741.29 73.24 o 19 3 0 1301.52 1289.27 86.29 o 21 3 0 111.25 -16.40 82.00 o 0 4 0 15513.84 26084.13 310.08 o 2 4 0 123186.14 125986.97 1134.77 o 4 4 0 11.23 72.10 12.52 o 6 4 0 3263.22 4016.80 55.49 o 8 4 0 25640.53 24056.93 267.23 o 10 4 0 47690.22 42981.86 515.38 o 12 4 0 18037.09 17849.17 220.48 o 14 4 0 2083.88 1849.00 66.81 o 16 4 0 1056.77 1014.30 76.25 o 18 4 0 120.78 -31.63 71.62 o 20 4 0 1761.71 2194.41 102.00 o 22 4 0 393.08 474.64 93.28 o 1 5 0 95007.13 100240.78 804.82 o 3 5 0 302.11 261.40 13.40 o 5 5 0 149.56 330.12 16.23 o 7 5 0 58841.28 66013.13 674.97 o 9 5 0 12635.66 13190.61 158.19 o 11 5 0 2050.65 1994.21 58.74 o 13 5 0 5484.06 5086.77 110.33 o 15 5 0 355.36 408.79 52.78 o 17 5 0 2655.24 2598.85 134.07 o 19 5 0 900.30 1165.33 90.39 o 21 5 0 720.14 669.84 92.96 o 0 6 0 10197.22 15656.68 205.80 o 2 6 0 7672.87 5721.58 70.52 o 4 6 0 5395.43 5591.22 73.17 o 6 6 0 2411.29 2253.07 39.16 o 8 6 0 18642.89 17066.60 190.30 o 10 6 0 23374.78 21231.47 269.16 o 12 6 0 17628.06 16543.73 219.19 o 14 6 0 2541.85 2513.04 79.45 o 16 6 0 741.29 663.74 91.14 o 18 6 0 13.09 -31.58 77.44 o 20 6 0 1403.96 1449.57 103.36 o 1 7 0 817.09 608.90 29.79 o 3 7 0 13312.20 11471.16 123.82 o 5 7 0 244.16 315.80 21.24 o 7 7 0 265.85 468.47 23.93 o 9 7 0 11335.12 10301.25 147.56 o 11 7 0 13879.58 13351.48 183.34 o 13 7 0 2017.91 1835.91 61.50 o 15 7 0 409.37 302.25 59.50 o 17 7 0 5095.30 4836.41 161.31 o 19 7 0 1141.18 1265.59 97.45 o 21 7 0 610.65 471.87 95.61 o 0 8 0 645.05 298.84 25.91 o 2 8 0 283.93 850.00 27.78 o 4 8 0 4601.37 3850.65 54.32 o 6 8 0 20679.14 19153.11 194.38 o 8 8 0 9249.00 8700.76 119.41 o 10 8 0 13063.08 12575.92 180.47 o 12 8 0 7312.92 6697.73 123.95 o 14 8 0 4385.68 4167.40 132.04 o 16 8 0 390.76 356.94 73.10 o 18 8 0 984.23 1085.42 91.76 o 20 8 0 141.89 89.31 96.75 o 1 9 0 9513.96 12308.29 122.12 o 3 9 0 35242.64 35258.20 355.33 o 5 9 0 56.44 100.63 23.07 o 7 9 0 588.17 858.06 32.15 o 9 9 0 18818.92 18320.87 221.90 o 11 9 0 21116.36 21056.53 251.73 o 13 9 0 57.32 7.59 68.93 o 15 9 0 5874.51 5395.26 162.37 o 17 9 0 4627.22 4066.22 135.20 o 19 9 0 50.84 -37.14 91.18 o 21 9 0 7.18 -102.90 102.90 o 0 10 0 30821.72 31856.46 413.30 o 2 10 0 50822.17 47781.79 443.97 o 4 10 0 24257.16 22478.59 227.28 o 6 10 0 447.10 310.32 29.12 o 8 10 0 2341.03 2078.24 47.05 o 10 10 0 1478.72 1496.79 54.41 o 12 10 0 7861.31 7222.52 141.08 o 14 10 0 6095.33 5585.84 135.47 o 16 10 0 1972.72 2031.45 105.48 o 18 10 0 2013.17 1738.04 112.20 o 20 10 0 6.47 54.16 100.98 o 1 11 0 1281.14 1073.44 31.73 o 3 11 0 1929.12 2085.25 47.19 o 5 11 0 179.44 191.17 43.36 o 7 11 0 964.36 1163.64 46.73 o 9 11 0 6042.64 5898.91 102.96 o 11 11 0 2600.68 2661.87 123.73 o 13 11 0 25.54 -69.93 69.93 o 15 11 0 1171.49 1359.72 109.77 o 17 11 0 137.00 88.60 90.72 o 19 11 0 286.27 311.60 89.86 o 0 12 0 477.95 1028.00 52.81 o 2 12 0 71976.05 69035.23 639.57 o 4 12 0 10739.45 9015.50 113.41 o 6 12 0 2093.10 1728.74 45.91 o 8 12 0 1996.20 1806.06 51.33 o 10 12 0 15155.83 15062.52 249.18 o 12 12 0 4602.41 4595.18 123.10 o 14 12 0 807.61 618.73 95.52 o 16 12 0 6824.00 5964.05 186.17 o 18 12 0 1409.85 1541.31 184.32 o 20 12 0 2.83 -88.30 160.70 o 1 13 0 9937.82 9813.20 113.03 o 3 13 0 4639.47 4379.83 74.66 o 5 13 0 104.12 97.38 35.29 o 7 13 0 1338.93 1346.19 48.69 o 9 13 0 186.63 148.89 38.67 o 11 13 0 150.38 216.54 66.95 o 13 13 0 1317.81 1330.22 101.77 o 15 13 0 525.85 436.92 137.75 o 17 13 0 747.81 1057.92 115.05 o 19 13 0 481.37 556.41 124.49 o 0 14 0 79.86 69.07 43.52 o 2 14 0 17704.05 16459.18 186.55 o 4 14 0 18566.34 17778.10 199.48 o 6 14 0 15975.04 15093.31 200.54 o 8 14 0 4136.55 3850.88 87.21 o 10 14 0 133.02 180.48 69.34 o 12 14 0 8756.13 8966.91 203.17 o 14 14 0 3135.56 3060.69 135.81 o 16 14 0 1041.17 1194.14 118.11 o 18 14 0 12.89 71.21 117.40 o 1 15 0 11722.12 11609.09 143.20 o 3 15 0 16746.70 15678.55 182.05 o 5 15 0 49.58 20.50 40.56 o 7 15 0 3248.29 3301.37 85.76 o 9 15 0 12.07 -20.00 49.20 o 11 15 0 824.12 955.99 95.23 o 13 15 0 8839.10 8357.24 223.34 o 15 15 0 71.15 232.62 117.51 o 17 15 0 80.10 170.24 127.81 o 0 16 0 6.86 -5.51 50.68 o 2 16 0 290.42 279.85 42.25 o 4 16 0 5000.41 4846.35 99.80 o 6 16 0 11604.38 11620.33 268.23 o 8 16 0 9190.33 9335.96 215.23 o 10 16 0 4323.36 4652.47 154.88 o 12 16 0 2857.42 3049.69 168.12 o 14 16 0 1658.01 1619.15 136.83 o 16 16 0 195.80 305.89 129.52 o 18 16 0 105.29 -62.55 140.26 o 1 17 0 71.26 5.58 50.35 o 3 17 0 12918.47 12850.86 237.99 o 5 17 0 17.96 -18.44 56.26 o 7 17 0 20795.06 20212.08 316.26 o 9 17 0 1117.81 1113.21 71.37 o 11 17 0 1454.91 1640.45 118.16 o 13 17 0 5391.87 5571.40 208.72 o 15 17 0 42.97 118.08 125.34 o 17 17 0 739.78 693.21 147.53 o 0 18 0 984.25 816.56 87.34 o 2 18 0 93.65 -21.47 70.50 o 4 18 0 449.92 542.96 74.18 o 6 18 0 1652.37 1728.20 85.87 o 8 18 0 5410.46 5628.53 136.95 o 10 18 0 6260.25 6335.32 159.46 o 12 18 0 887.04 1323.16 134.53 o 14 18 0 1047.49 1430.80 145.00 o 16 18 0 33.67 -80.81 134.99 o 1 19 0 2059.36 2161.24 90.83 o 3 19 0 8978.27 8850.41 273.02 o 5 19 0 1057.79 1276.11 114.72 o 7 19 0 10834.98 10133.89 196.30 o 9 19 0 1945.95 1883.61 89.22 o 11 19 0 1116.73 1269.76 122.85 o 13 19 0 6688.16 7057.38 500.67 o 15 19 0 899.51 818.68 162.14 o 0 20 0 10029.25 9205.89 254.18 o 2 20 0 467.08 426.81 80.87 o 4 20 0 10.87 -79.84 79.84 o 6 20 0 1874.07 1650.23 101.37 o 8 20 0 624.21 687.15 88.27 o 10 20 0 550.20 566.04 115.79 o 12 20 0 0.40 81.33 144.38 o 14 20 0 306.79 22.26 161.44 o 1 21 0 666.47 538.88 102.82 o 3 21 0 954.34 1013.28 99.33 o 5 21 0 877.92 680.99 94.70 o 7 21 0 2463.59 2749.82 138.32 o 9 21 0 3556.00 3332.81 169.47 o 11 21 0 484.23 520.20 161.56 o 13 21 0 1993.99 2310.40 202.31 o 0 22 0 14562.51 15531.51 427.56 o 2 22 0 917.97 962.57 103.34 o 4 22 0 4.29 54.26 95.76 o 6 22 0 2860.14 2537.74 131.17 o 8 22 0 1041.69 729.44 98.13 o 10 22 0 488.84 771.68 138.86 o 12 22 0 624.14 530.93 172.34 o 1 23 0 1411.92 1465.61 127.93 o 3 23 0 1006.94 872.35 117.69 o 5 23 0 162.07 -14.97 106.68 o 7 23 0 40.42 152.03 105.10 o 9 23 0 19.47 -28.91 92.68 o 11 23 0 44.00 284.80 169.38 o 0 24 0 3918.06 5210.07 948.46 o 2 24 0 703.65 906.58 140.76 o 4 24 0 67.86 10.70 111.66 o 6 24 0 326.81 462.23 118.97 o 8 24 0 479.62 295.79 112.14 o 10 24 0 1419.23 1839.13 126.76 o 1 25 0 3091.46 3039.57 349.33 o 3 25 0 969.95 1047.05 271.90 o 5 25 0 599.64 825.03 160.44 o 7 25 0 353.26 253.61 125.28 o 0 26 0 360.83 1125.82 307.10 o 2 26 0 1.84 97.23 160.54 o 4 26 0 535.32 625.24 170.36 o -23 1 1 86.86 69.69 135.49 o -21 1 1 3275.90 3762.19 168.07 o -19 1 1 30.30 85.57 82.50 o -17 1 1 1016.27 959.23 55.37 o -15 1 1 20630.49 19038.90 263.34 o -13 1 1 7417.71 7866.36 108.26 o -11 1 1 64025.80 60858.25 719.83 o -9 1 1 51904.94 54044.98 577.64 o -7 1 1 9266.09 8955.97 95.29 o -5 1 1 164199.28 172258.28 1456.16 o -3 1 1 8495.01 9947.79 91.49 o -1 1 1 5946.02 4006.74 37.34 o 1 1 1 10664.30 14185.57 136.75 o 3 1 1 180.58 1052.39 17.89 o 5 1 1 62203.71 59590.16 542.67 o 7 1 1 6031.68 5441.65 63.70 o 9 1 1 43928.83 42078.21 433.44 o 11 1 1 4705.67 4373.93 67.17 o 13 1 1 13045.78 12736.47 171.32 o 15 1 1 44491.82 42652.78 632.36 o 17 1 1 2287.10 2044.32 132.10 o 19 1 1 331.03 357.85 109.71 o 21 1 1 158.79 207.42 121.15 o -22 2 1 75.39 127.32 136.85 o -20 2 1 78.18 42.95 76.10 o -18 2 1 2836.73 2555.60 98.06 o -16 2 1 1224.50 904.24 51.15 o -14 2 1 34.68 -32.78 37.39 o -12 2 1 10951.31 10592.81 139.60 o -10 2 1 14423.43 15477.60 199.87 o -8 2 1 8595.80 10348.08 128.54 o -6 2 1 6483.32 7022.94 77.44 o -4 2 1 5367.14 7002.98 73.62 o -2 2 1 385.81 766.28 20.67 o 0 2 1 22973.42 26810.63 208.84 o 2 2 1 134.32 176.77 21.09 o 4 2 1 1436.23 1874.05 33.61 o 6 2 1 5667.11 6722.39 79.57 o 8 2 1 16685.46 17409.13 187.37 o 10 2 1 797.64 639.15 32.58 o 12 2 1 1114.55 1217.90 40.06 o 14 2 1 3173.79 3059.92 78.08 o 16 2 1 4582.46 4114.01 108.35 o 18 2 1 368.15 406.33 83.82 o 20 2 1 290.17 290.54 118.40 o -21 3 1 4150.10 4334.42 133.51 o -19 3 1 597.90 887.68 84.61 o -17 3 1 2788.40 2432.26 135.63 o -15 3 1 3444.41 3176.77 83.22 o -13 3 1 63.69 98.44 30.00 o -11 3 1 44635.02 44159.49 478.87 o -9 3 1 2900.83 2069.12 40.47 o -7 3 1 16111.11 15149.46 158.39 o -5 3 1 67419.06 70955.90 663.88 o -3 3 1 13407.96 15661.26 152.55 o -1 3 1 55135.65 53470.49 430.36 o 1 3 1 21407.31 17314.14 147.69 o 3 3 1 31227.75 29566.12 294.39 o 5 3 1 74987.80 75223.00 839.65 o 7 3 1 23.59 41.66 13.70 o 9 3 1 16082.84 14243.11 164.97 o 11 3 1 234.68 174.59 28.13 o 13 3 1 4557.52 4169.32 88.27 o 15 3 1 11839.09 11003.53 206.99 o 17 3 1 319.85 350.40 65.13 o 19 3 1 1191.91 1115.37 75.48 o 21 3 1 51.33 8.81 120.12 o -22 4 1 790.62 639.70 93.42 o -20 4 1 304.55 345.26 85.61 o -18 4 1 2369.36 2416.53 101.18 o -16 4 1 389.27 333.56 67.98 o -14 4 1 5397.62 4977.77 100.65 o -12 4 1 20384.78 20031.90 229.67 o -10 4 1 36367.88 38579.79 419.87 o -8 4 1 3068.33 2612.87 46.12 o -6 4 1 31476.19 35631.18 339.70 o -4 4 1 1145.95 892.86 22.86 o -2 4 1 182.55 288.88 20.24 o 0 4 1 1759.18 1908.77 27.84 o 2 4 1 91899.45 95100.90 747.51 o 4 4 1 3717.20 3396.77 52.14 o 6 4 1 1430.68 1189.29 33.14 o 8 4 1 33090.20 31099.12 357.08 o 10 4 1 2227.34 2258.55 49.44 o 12 4 1 1707.08 1746.24 49.77 o 14 4 1 13472.85 12460.08 199.81 o 16 4 1 5155.87 4819.44 124.51 o 18 4 1 586.60 607.06 77.33 o 20 4 1 152.46 9.83 72.23 o -21 5 1 2330.81 2620.56 118.74 o -19 5 1 4201.12 4126.61 129.44 o -17 5 1 4137.93 4061.99 121.51 o -15 5 1 97.00 98.44 46.07 o -13 5 1 243.28 190.61 37.93 o -11 5 1 16470.07 15971.93 179.48 o -9 5 1 811.06 439.21 29.97 o -7 5 1 3908.39 3515.04 69.36 o -5 5 1 16239.95 15921.24 153.27 o -3 5 1 1322.54 1180.88 33.59 o -1 5 1 285548.81 291747.88 2409.87 o 1 5 1 39394.63 36622.93 368.78 o 3 5 1 54596.66 50541.36 434.05 o 5 5 1 55312.95 55253.74 596.04 o 7 5 1 2356.68 2343.70 51.64 o 9 5 1 9872.37 10166.08 138.82 o 11 5 1 2113.93 2024.11 49.24 o 13 5 1 1226.32 1027.05 45.62 o 15 5 1 2283.14 2327.09 76.19 o 17 5 1 1240.37 1259.43 82.27 o 19 5 1 1225.95 1383.05 91.65 o 21 5 1 572.74 713.54 122.66 o -22 6 1 799.03 650.31 102.19 o -20 6 1 1425.18 1472.55 103.20 o -18 6 1 1945.07 1871.69 101.92 o -16 6 1 790.73 767.44 77.49 o -14 6 1 5770.77 5340.34 106.12 o -12 6 1 8869.13 9248.88 132.75 o -10 6 1 10724.40 10413.42 120.97 o -8 6 1 26415.34 26740.69 300.08 o -6 6 1 7430.06 8041.47 114.75 o -4 6 1 32164.07 33149.49 396.37 o -2 6 1 43628.34 43973.95 389.93 o 0 6 1 51185.46 53176.77 433.34 o 2 6 1 60606.24 63332.55 543.12 o 4 6 1 28118.91 28391.29 275.48 o 6 6 1 20524.76 21426.76 231.52 o 8 6 1 10769.26 9665.51 127.17 o 10 6 1 596.98 660.07 35.38 o 12 6 1 11330.18 10901.89 155.54 o 14 6 1 5329.84 5001.48 147.64 o 16 6 1 1304.15 1184.54 83.82 o 18 6 1 2115.75 2279.34 103.90 o 20 6 1 125.84 97.62 88.87 o -21 7 1 156.69 172.33 96.50 o -19 7 1 5288.78 5206.02 152.23 o -17 7 1 741.33 795.10 131.13 o -15 7 1 357.60 243.51 105.51 o -13 7 1 1645.83 1633.34 51.59 o -11 7 1 65.77 152.91 34.07 o -9 7 1 6249.72 5402.45 79.19 o -7 7 1 5227.04 4167.24 68.10 o -5 7 1 4189.39 4469.71 80.52 o -3 7 1 5235.10 5225.93 57.48 o -1 7 1 23168.11 20762.04 191.71 o 1 7 1 138354.08 134093.91 1050.63 o 3 7 1 30152.67 26881.76 262.03 o 5 7 1 19504.58 19039.75 208.31 o 7 7 1 1455.87 1354.37 38.30 o 9 7 1 1152.10 1292.40 48.11 o 11 7 1 13010.50 12881.71 177.55 o 13 7 1 2234.85 2017.24 63.49 o 15 7 1 834.04 697.13 62.37 o 17 7 1 234.67 264.51 83.40 o 19 7 1 1204.21 1020.92 90.43 o 21 7 1 1610.91 1946.25 116.24 o -22 8 1 449.03 492.84 136.50 o -20 8 1 4143.68 4205.26 157.08 o -18 8 1 19.37 -39.94 81.48 o -16 8 1 425.53 463.13 77.59 o -14 8 1 5711.15 5658.95 140.64 o -12 8 1 2972.98 3118.87 77.25 o -10 8 1 442.18 583.62 27.94 o -8 8 1 23779.82 24086.86 242.14 o -6 8 1 1342.07 1425.15 35.69 o -4 8 1 8243.65 8832.01 134.95 o -2 8 1 112559.38 115604.75 1012.55 o 0 8 1 130329.76 137672.53 1108.56 o 2 8 1 3917.76 4306.93 63.23 o 4 8 1 52111.50 53025.43 699.16 o 6 8 1 46551.25 46673.72 487.32 o 8 8 1 285.23 267.21 36.48 o 10 8 1 750.53 719.77 42.59 o 12 8 1 13008.50 12563.82 194.12 o 14 8 1 42.17 -33.58 58.08 o 16 8 1 19.31 -12.00 93.57 o 18 8 1 2988.92 3264.70 125.25 o 20 8 1 907.27 852.47 101.70 o -21 9 1 6.67 20.99 103.52 o -19 9 1 1400.09 1655.98 132.69 o -17 9 1 1753.68 1949.96 115.95 o -15 9 1 53.81 37.13 78.30 o -13 9 1 6434.53 5900.04 121.72 o -11 9 1 4.61 -21.94 36.60 o -9 9 1 27568.60 25875.25 261.26 o -7 9 1 56656.98 54687.38 508.60 o -5 9 1 312.46 333.33 26.57 o -3 9 1 16.28 32.44 19.84 o -1 9 1 11180.98 13703.58 126.54 o 1 9 1 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