#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/99/2209980.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209980_Fobs loop_ _publ_author_name 'da Silva, Luiz Everson' 'Joussef, Antonio Carlos' 'Foro, Sabine' 'Schmidt, Boris' _publ_section_title ; Bis[N-(5,7-dibromoquinolin-8-yl)-3,5-bis(trifluoromethyl)benzenesulfonamidato-\k^2^N,N']zinc(II) ; _journal_coeditor_code RZ2053 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1901 _journal_page_last m1903 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.091 _cell_angle_beta 100.293 _cell_angle_gamma 100.519 _cell_length_a 11.7057 _cell_length_b 12.4768 _cell_length_c 14.0759 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file rz2053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LD955 (LE92) P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 332.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 27091.34 26369.69 262.10 o 4 0 0 563.63 512.34 12.72 o 5 0 0 927.63 698.69 26.91 o 6 0 0 8249.10 8719.17 96.18 o 7 0 0 266.14 239.70 14.56 o 8 0 0 1107.08 883.16 24.54 o 9 0 0 832.02 715.69 36.98 o 10 0 0 328.25 293.99 40.29 o 11 0 0 1757.00 1754.52 38.26 o 12 0 0 2786.44 2787.43 68.83 o 13 0 0 145.20 108.45 25.33 o 14 0 0 1603.34 1781.89 75.20 o -14 1 0 11.10 29.89 23.82 o -13 1 0 52.73 41.81 17.26 o -12 1 0 1570.53 1629.30 126.09 o -11 1 0 405.69 385.17 27.22 o -10 1 0 8122.73 8252.23 159.45 o 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8 3 0 20879.94 22079.30 357.64 o 9 3 0 277.55 250.29 20.88 o 10 3 0 667.79 545.33 65.14 o 11 3 0 6588.09 7117.56 291.06 o 12 3 0 944.09 1037.03 44.33 o 13 3 0 28.67 14.02 16.35 o -14 4 0 4.61 7.36 16.59 o -13 4 0 526.75 387.03 38.72 o -12 4 0 418.14 447.36 44.88 o -11 4 0 5931.13 6135.31 112.12 o -10 4 0 2037.29 1950.51 36.94 o -9 4 0 1563.21 1483.75 28.92 o -8 4 0 5609.93 5602.72 40.59 o -7 4 0 1789.12 1799.05 76.51 o -6 4 0 69.07 57.27 11.23 o -5 4 0 333.39 238.65 10.35 o -4 4 0 3196.54 3374.85 70.83 o -3 4 0 978.49 1015.02 13.09 o -2 4 0 4244.57 4328.90 19.67 o -1 4 0 17632.48 18167.66 62.40 o 0 4 0 1427.52 1630.70 18.18 o 1 4 0 2301.76 2478.31 77.82 o 2 4 0 18397.49 18486.74 411.30 o 3 4 0 2221.79 2606.58 26.03 o 4 4 0 10284.64 11153.61 89.83 o 5 4 0 494.58 475.45 17.59 o 6 4 0 511.35 582.12 48.56 o 7 4 0 334.76 320.60 22.17 o 8 4 0 36.09 38.96 13.60 o 9 4 0 718.27 671.27 39.08 o 10 4 0 1704.71 1801.44 49.43 o 11 4 0 231.41 141.96 34.75 o 12 4 0 392.12 349.23 94.61 o -14 5 0 357.90 318.20 46.18 o -13 5 0 183.03 133.66 32.40 o -12 5 0 865.78 848.91 51.09 o -11 5 0 483.78 420.95 22.39 o -10 5 0 229.05 154.06 18.48 o -9 5 0 28473.51 29686.29 342.17 o -8 5 0 4399.31 4494.50 39.54 o -7 5 0 1703.48 1576.53 76.91 o -6 5 0 17379.99 18290.79 161.33 o -5 5 0 1179.70 1232.27 19.55 o -4 5 0 8333.91 8264.16 32.44 o -3 5 0 1405.37 1315.32 74.94 o -2 5 0 426.73 430.10 26.91 o -1 5 0 10735.19 11210.14 57.53 o 0 5 0 3856.92 4319.24 15.62 o 1 5 0 1567.54 1577.35 34.33 o 2 5 0 4279.42 3860.84 107.48 o 3 5 0 10400.88 10418.84 42.35 o 4 5 0 4257.63 4666.68 58.74 o 5 5 0 10493.48 10703.52 104.41 o 6 5 0 8294.92 9165.39 476.48 o 7 5 0 5441.66 5959.76 329.94 o 8 5 0 2509.54 2589.04 45.81 o 9 5 0 452.75 374.42 71.05 o 10 5 0 4018.14 4246.33 116.52 o 11 5 0 2269.60 2287.49 124.10 o 12 5 0 27.80 42.58 45.71 o -14 6 0 8.55 17.69 20.78 o -13 6 0 1101.32 1002.01 58.68 o -12 6 0 1366.19 1189.65 55.71 o -11 6 0 54.51 30.43 11.19 o -10 6 0 954.95 898.13 27.73 o -9 6 0 1292.71 1274.52 116.42 o -8 6 0 526.56 507.02 22.22 o -7 6 0 659.52 603.56 21.53 o -6 6 0 6710.73 6913.98 38.83 o -5 6 0 4410.31 4012.93 29.27 o -4 6 0 306.99 324.22 16.41 o -3 6 0 9379.33 8456.00 385.52 o -2 6 0 2878.14 3018.99 107.17 o -1 6 0 2020.31 2234.66 109.22 o 0 6 0 17610.51 17333.66 200.56 o 1 6 0 922.08 889.88 17.83 o 2 6 0 2271.28 2352.95 45.41 o 3 6 0 913.49 834.92 22.14 o 4 6 0 801.01 698.49 32.40 o 5 6 0 486.15 524.58 23.80 o 6 6 0 1093.55 986.14 54.65 o 7 6 0 2379.91 2642.54 243.66 o 8 6 0 832.47 792.90 106.36 o 9 6 0 604.26 605.29 68.83 o 10 6 0 41.89 15.78 18.30 o 11 6 0 653.51 572.05 35.43 o -13 7 0 8.14 21.42 22.48 o -12 7 0 3694.23 3798.59 73.02 o -11 7 0 19.29 37.02 37.90 o -10 7 0 2362.04 2193.10 119.48 o -9 7 0 5352.17 5298.37 101.11 o -8 7 0 3569.22 3577.98 109.92 o -7 7 0 5771.77 6002.33 53.91 o -6 7 0 1550.62 1579.97 120.70 o -5 7 0 1001.16 1032.84 45.23 o -4 7 0 637.60 800.15 88.29 o -3 7 0 5631.72 5765.34 242.02 o -2 7 0 2698.51 2618.85 52.88 o -1 7 0 3812.66 4153.40 377.83 o 0 7 0 3232.61 3227.19 51.71 o 1 7 0 2010.90 2043.78 49.25 o 2 7 0 4607.51 4963.85 105.15 o 3 7 0 3459.59 3184.32 37.98 o 4 7 0 1423.00 1313.92 28.76 o 5 7 0 2915.25 2880.07 63.75 o 6 7 0 761.95 766.87 55.80 o 7 7 0 948.34 1050.30 108.82 o 8 7 0 2737.27 2898.54 314.41 o 9 7 0 1253.91 1410.17 162.56 o 10 7 0 748.12 792.31 176.48 o 11 7 0 753.26 688.65 98.72 o -13 8 0 29.63 30.64 23.99 o -12 8 0 45.49 65.56 28.55 o -11 8 0 410.48 364.51 32.10 o -10 8 0 809.58 704.76 34.96 o -9 8 0 4.01 36.43 12.83 o -8 8 0 1912.16 1967.38 60.65 o -7 8 0 2267.09 2212.42 50.06 o -6 8 0 3226.31 3051.09 48.02 o -5 8 0 2176.90 2019.99 117.36 o -4 8 0 1306.25 1238.37 98.20 o -3 8 0 697.67 619.35 31.11 o -2 8 0 2864.02 2705.48 73.55 o -1 8 0 18645.39 19203.48 501.96 o 0 8 0 6931.25 7210.31 251.24 o 1 8 0 804.13 752.42 30.07 o 2 8 0 21937.65 22443.50 559.03 o 3 8 0 3056.12 3032.25 39.81 o 4 8 0 1161.94 1180.41 30.27 o 5 8 0 680.21 549.87 44.28 o 6 8 0 2136.00 2073.63 73.32 o 7 8 0 325.16 271.65 42.51 o 8 8 0 94.52 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