#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/99/2209995.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209995_Fobs loop_ _publ_author_name 'Song, Qing-Bao' 'Teng, Ming-Yu' 'Dong, Yu' 'Ma, Chun-An' 'Sun, Jie' _publ_section_title ; (2S,3S)-2,3-Dihydroxysuccinic acid monohydrate ; _journal_coeditor_code SG2032 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3378 _journal_page_last o3379 _journal_volume 62 _journal_year 2006 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6377 _cell_length_b 7.8268 _cell_length_c 11.0427 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.7832 _[local]_cod_data_source_file sg2032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cd2629 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 83.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 136.22 153.81 2.27 o 4 0 0 510.39 496.23 6.23 o 6 0 0 1364.88 1373.19 14.46 o 8 0 0 115.26 118.52 2.91 o 1 1 0 45.46 46.31 0.46 o 2 1 0 0.58 0.56 0.21 o 3 1 0 1940.64 1855.27 141.49 o 4 1 0 3.13 3.66 0.38 o 5 1 0 141.02 119.74 5.01 o 6 1 0 338.74 347.15 7.41 o 7 1 0 196.52 198.00 3.14 o 8 1 0 0.48 0.17 0.34 o 9 1 0 43.80 47.78 2.77 o 0 2 0 1198.41 1040.81 37.36 o 1 2 0 1002.31 1065.92 32.64 o 2 2 0 0.66 0.39 0.17 o 3 2 0 1691.90 1667.22 60.65 o 4 2 0 365.80 395.90 11.87 o 5 2 0 3.45 5.44 0.36 o 6 2 0 399.53 373.37 23.59 o 7 2 0 152.24 123.27 8.52 o 8 2 0 49.02 40.99 1.73 o 9 2 0 1.78 2.59 1.66 o 1 3 0 1455.95 1223.26 34.02 o 2 3 0 1467.15 1543.12 72.50 o 3 3 0 21.98 39.44 2.50 o 4 3 0 205.22 185.20 11.11 o 5 3 0 95.63 89.05 8.18 o 6 3 0 0.61 0.35 0.28 o 7 3 0 27.46 28.39 1.41 o 8 3 0 30.90 28.89 1.52 o 9 3 0 2.85 4.40 0.86 o 0 4 0 1138.54 1151.83 16.10 o 1 4 0 28.46 22.25 2.12 o 2 4 0 0.58 1.01 0.26 o 3 4 0 344.44 305.21 16.34 o 4 4 0 197.03 199.02 13.41 o 5 4 0 45.42 47.26 2.62 o 6 4 0 18.90 19.45 1.48 o 7 4 0 1.78 1.62 0.48 o 8 4 0 94.40 89.36 11.87 o 1 5 0 283.99 237.35 16.28 o 2 5 0 26.67 49.85 4.71 o 3 5 0 6.36 7.48 1.01 o 4 5 0 225.20 215.98 19.36 o 5 5 0 1.08 1.03 0.34 o 6 5 0 84.71 81.00 10.59 o 7 5 0 0.13 0.70 0.43 o 8 5 0 13.54 21.87 4.42 o 0 6 0 10.02 5.13 1.69 o 1 6 0 6.84 9.39 1.24 o 2 6 0 106.49 117.01 11.59 o 3 6 0 750.52 781.26 43.09 o 4 6 0 0.02 0.58 0.31 o 5 6 0 0.29 0.42 0.33 o 6 6 0 29.13 35.35 5.89 o 7 6 0 2.33 1.03 0.58 o 1 7 0 278.11 262.37 28.57 o 2 7 0 23.45 24.36 2.81 o 3 7 0 119.12 127.27 12.02 o 4 7 0 28.25 30.27 2.71 o 5 7 0 0.57 0.49 0.47 o 6 7 0 8.61 8.83 1.14 o 0 8 0 2.47 2.71 0.89 o 1 8 0 108.04 108.32 3.97 o 2 8 0 205.93 230.33 16.19 o 3 8 0 17.58 19.44 1.83 o 4 8 0 0.11 0.95 0.56 o 5 8 0 5.61 6.02 1.41 o 1 9 0 47.18 47.04 2.01 o 2 9 0 2.68 1.72 0.64 o 3 9 0 3.08 3.40 0.84 o 4 9 0 0.41 1.42 1.10 o 1 0 1 121.99 143.98 1.76 o 2 0 1 118.12 101.01 1.29 o 3 0 1 6248.56 5053.47 248.29 o 4 0 1 396.03 353.37 9.60 o 5 0 1 61.79 48.11 2.20 o 6 0 1 14.56 14.01 0.90 o 7 0 1 94.10 76.47 2.02 o 8 0 1 0.62 1.41 0.98 o 0 1 1 435.33 368.14 13.25 o 1 1 1 443.03 511.62 20.03 o 2 1 1 73.65 62.51 2.11 o 3 1 1 1652.37 1616.00 60.77 o 4 1 1 50.27 55.27 0.86 o 5 1 1 35.50 26.88 0.58 o 6 1 1 41.28 33.99 0.82 o 7 1 1 22.76 22.58 0.72 o 8 1 1 0.29 0.39 0.30 o 9 1 1 112.80 117.72 3.92 o 0 2 1 6994.75 5119.94 104.48 o 1 2 1 376.07 396.84 13.07 o 2 2 1 931.59 1000.56 34.26 o 3 2 1 1475.77 1502.55 44.19 o 4 2 1 568.37 537.35 15.85 o 5 2 1 116.33 111.45 4.31 o 6 2 1 141.43 142.62 4.75 o 7 2 1 28.23 28.20 0.95 o 8 2 1 3.96 5.11 0.53 o 9 2 1 0.31 0.34 0.36 o 0 3 1 2.67 1.90 0.31 o 1 3 1 2499.86 2267.48 40.46 o 2 3 1 282.14 307.13 12.06 o 3 3 1 107.02 87.08 3.88 o 4 3 1 413.20 407.97 18.16 o 5 3 1 27.98 25.12 1.32 o 6 3 1 14.14 15.11 1.06 o 7 3 1 44.73 30.45 1.03 o 8 3 1 1.59 1.34 0.42 o 9 3 1 34.76 40.91 2.68 o 0 4 1 223.20 239.30 17.35 o 1 4 1 482.22 498.78 16.53 o 2 4 1 1311.17 1371.71 48.39 o 3 4 1 157.29 176.19 7.79 o 4 4 1 6.77 7.98 0.55 o 5 4 1 215.91 192.28 7.60 o 6 4 1 81.67 84.66 4.72 o 7 4 1 52.00 52.83 3.74 o 8 4 1 32.57 29.37 1.57 o 0 5 1 251.34 363.05 26.58 o 1 5 1 262.47 309.64 13.02 o 2 5 1 109.04 109.79 5.23 o 3 5 1 12.76 11.16 0.58 o 4 5 1 149.75 124.58 5.25 o 5 5 1 204.67 179.56 9.45 o 6 5 1 16.99 14.55 0.68 o 7 5 1 4.00 5.25 0.58 o 8 5 1 35.78 34.84 2.54 o 0 6 1 31.82 25.33 2.60 o 1 6 1 98.56 99.89 6.86 o 2 6 1 685.60 657.78 31.09 o 3 6 1 51.66 47.67 3.77 o 4 6 1 326.63 333.81 13.97 o 5 6 1 56.73 54.22 4.51 o 6 6 1 71.21 69.12 5.40 o 7 6 1 149.20 155.68 13.29 o 0 7 1 299.14 312.38 6.45 o 1 7 1 22.54 22.06 1.14 o 2 7 1 152.89 141.19 9.19 o 3 7 1 68.67 68.41 3.87 o 4 7 1 11.55 10.30 0.61 o 5 7 1 2.33 3.88 0.46 o 6 7 1 90.08 95.13 10.59 o 0 8 1 299.70 318.21 4.93 o 1 8 1 21.87 25.81 0.99 o 2 8 1 29.58 31.24 1.37 o 3 8 1 25.47 23.30 1.49 o 4 8 1 4.49 7.69 0.61 o 5 8 1 3.58 3.69 0.59 o 0 9 1 29.76 38.87 1.83 o 1 9 1 27.53 28.28 1.13 o 2 9 1 13.58 15.33 0.89 o 3 9 1 48.95 58.25 2.59 o 4 9 1 10.86 13.58 1.13 o 0 0 2 4780.26 3811.32 131.50 o 1 0 2 19.21 14.72 0.78 o 2 0 2 10.36 10.80 0.29 o 3 0 2 1698.31 1509.75 41.64 o 4 0 2 415.58 355.89 8.59 o 5 0 2 324.41 282.40 8.70 o 6 0 2 4.91 6.86 0.45 o 7 0 2 34.52 42.51 1.26 o 8 0 2 0.01 0.30 0.41 o 0 1 2 920.64 1008.22 31.11 o 1 1 2 1760.07 1699.67 105.59 o 2 1 2 3291.12 3065.27 130.35 o 3 1 2 279.66 315.26 10.13 o 4 1 2 565.93 513.17 13.68 o 5 1 2 145.79 154.86 3.39 o 6 1 2 84.69 65.65 1.84 o 7 1 2 287.40 265.73 6.59 o 8 1 2 14.24 15.61 0.90 o 9 1 2 6.22 7.25 1.19 o 0 2 2 13.70 8.93 0.54 o 1 2 2 1413.77 1437.46 25.69 o 2 2 2 941.58 1027.32 32.20 o 3 2 2 57.48 53.56 1.68 o 4 2 2 520.78 528.37 22.54 o 5 2 2 280.03 304.35 14.28 o 6 2 2 24.88 25.31 1.09 o 7 2 2 293.12 287.70 14.49 o 8 2 2 8.02 7.54 0.74 o 9 2 2 9.76 11.91 0.83 o 0 3 2 23.75 25.61 1.80 o 1 3 2 1477.87 1572.65 33.09 o 2 3 2 25.29 30.53 1.60 o 3 3 2 74.34 88.10 4.14 o 4 3 2 113.87 134.57 7.18 o 5 3 2 54.91 47.59 3.08 o 6 3 2 47.13 37.36 2.83 o 7 3 2 5.77 6.24 0.55 o 8 3 2 5.51 4.31 0.54 o 9 3 2 20.92 25.63 1.54 o 0 4 2 234.58 333.86 19.04 o 1 4 2 672.46 654.01 19.55 o 2 4 2 10.50 8.65 0.52 o 3 4 2 7.76 5.12 0.33 o 4 4 2 564.91 540.76 22.66 o 5 4 2 276.17 257.20 13.63 o 6 4 2 3.06 2.27 0.37 o 7 4 2 19.64 21.25 1.54 o 8 4 2 45.03 43.57 2.83 o 0 5 2 32.29 40.04 3.83 o 1 5 2 56.10 77.29 3.85 o 2 5 2 612.35 609.45 24.13 o 3 5 2 11.87 10.92 0.52 o 4 5 2 364.53 377.17 20.60 o 5 5 2 230.51 210.63 11.97 o 6 5 2 29.34 28.12 1.47 o 7 5 2 35.18 40.87 2.95 o 8 5 2 36.44 40.59 3.49 o 0 6 2 161.40 147.59 10.47 o 1 6 2 434.71 433.64 17.29 o 2 6 2 154.08 155.00 10.34 o 3 6 2 8.60 10.39 0.70 o 4 6 2 17.88 16.73 0.89 o 5 6 2 143.27 121.33 7.69 o 6 6 2 29.58 30.88 1.62 o 7 6 2 71.28 76.76 6.27 o 0 7 2 13.82 16.44 1.41 o 1 7 2 100.49 102.85 5.33 o 2 7 2 220.79 218.71 11.32 o 3 7 2 136.63 129.51 10.61 o 4 7 2 127.22 126.70 8.16 o 5 7 2 8.61 7.63 0.60 o 6 7 2 0.02 0.41 0.35 o 0 8 2 7.44 13.03 1.05 o 1 8 2 15.58 18.30 0.85 o 2 8 2 66.54 66.90 4.85 o 3 8 2 70.05 70.49 4.77 o 4 8 2 17.32 18.75 1.16 o 5 8 2 7.70 7.50 0.66 o 0 9 2 47.88 52.53 2.12 o 1 9 2 34.74 43.32 1.37 o 2 9 2 13.61 14.09 1.03 o 3 9 2 106.40 100.36 4.85 o 4 9 2 22.84 20.50 1.26 o 1 0 3 2707.90 3087.51 184.10 o 2 0 3 1178.00 1181.33 46.97 o 3 0 3 43.91 40.91 1.08 o 4 0 3 13.18 9.72 0.41 o 5 0 3 307.98 256.68 5.55 o 6 0 3 10.69 8.34 0.59 o 7 0 3 2.61 1.91 0.40 o 8 0 3 43.81 47.75 1.89 o 9 0 3 7.62 8.63 1.47 o 0 1 3 4731.90 4183.27 191.95 o 1 1 3 497.10 466.19 13.58 o 2 1 3 590.71 643.76 23.29 o 3 1 3 701.53 794.79 31.75 o 4 1 3 611.04 628.26 19.65 o 5 1 3 110.44 116.25 3.03 o 6 1 3 126.87 126.14 3.52 o 7 1 3 123.15 121.87 3.25 o 8 1 3 37.99 41.27 1.61 o 9 1 3 34.68 44.53 2.01 o 0 2 3 214.36 189.97 6.53 o 1 2 3 1868.91 1941.06 58.35 o 2 2 3 39.56 29.71 1.09 o 3 2 3 236.78 211.97 11.43 o 4 2 3 87.12 88.32 5.56 o 5 2 3 75.59 75.44 3.88 o 6 2 3 201.59 215.49 12.67 o 7 2 3 232.47 236.33 19.73 o 8 2 3 32.80 31.49 1.13 o 9 2 3 14.44 17.63 0.97 o 0 3 3 3.08 2.07 0.18 o 1 3 3 156.93 160.45 6.66 o 2 3 3 849.08 946.46 31.90 o 3 3 3 65.32 42.40 1.79 o 4 3 3 808.91 819.77 52.14 o 5 3 3 160.06 149.06 9.13 o 6 3 3 127.10 126.57 6.50 o 7 3 3 142.74 133.68 6.40 o 8 3 3 32.46 33.23 1.39 o 9 3 3 15.31 14.96 0.97 o 0 4 3 671.96 657.57 29.64 o 1 4 3 51.89 41.14 2.21 o 2 4 3 496.32 582.53 22.52 o 3 4 3 0.57 0.55 0.17 o 4 4 3 2.14 3.05 0.27 o 5 4 3 21.51 22.34 1.12 o 6 4 3 3.73 4.09 0.47 o 7 4 3 48.21 45.06 3.02 o 8 4 3 20.89 17.68 0.94 o 0 5 3 965.74 1045.21 22.29 o 1 5 3 831.94 881.95 21.29 o 2 5 3 93.93 87.30 4.78 o 3 5 3 422.32 425.93 24.96 o 4 5 3 79.63 81.86 5.06 o 5 5 3 294.86 271.03 16.94 o 6 5 3 140.10 132.78 7.56 o 7 5 3 125.78 135.51 11.44 o 8 5 3 104.42 100.88 5.85 o 0 6 3 51.94 53.03 2.42 o 1 6 3 83.65 80.75 3.81 o 2 6 3 218.72 228.52 14.00 o 3 6 3 36.71 35.49 2.20 o 4 6 3 292.26 276.76 17.07 o 5 6 3 78.16 78.91 5.61 o 6 6 3 3.71 4.00 0.48 o 7 6 3 126.16 129.75 11.47 o 0 7 3 81.41 84.57 5.37 o 1 7 3 95.47 105.65 4.17 o 2 7 3 171.17 166.63 9.95 o 3 7 3 42.59 44.34 2.81 o 4 7 3 72.58 71.48 4.31 o 5 7 3 42.56 42.22 2.96 o 6 7 3 3.97 5.36 0.59 o 0 8 3 29.15 31.85 1.92 o 1 8 3 4.90 5.68 0.68 o 2 8 3 81.64 83.51 5.99 o 3 8 3 81.52 90.47 6.83 o 4 8 3 17.21 20.09 1.09 o 5 8 3 4.19 4.81 0.59 o 0 9 3 82.20 87.75 3.34 o 1 9 3 3.87 3.92 0.67 o 2 9 3 2.85 1.99 0.59 o 3 9 3 16.68 16.44 1.23 o 0 0 4 6998.05 5942.96 246.08 o 1 0 4 48.67 40.01 1.79 o 2 0 4 753.82 1030.59 56.24 o 3 0 4 2.36 4.94 0.28 o 4 0 4 10.07 6.70 0.36 o 5 0 4 382.48 348.77 12.08 o 6 0 4 344.35 345.44 28.16 o 7 0 4 15.21 14.76 1.05 o 8 0 4 32.60 39.32 1.74 o 9 0 4 4.73 6.88 1.39 o 0 1 4 246.44 263.34 4.82 o 1 1 4 1121.93 1272.17 41.41 o 2 1 4 633.98 709.22 30.10 o 3 1 4 542.29 595.01 21.40 o 4 1 4 13.22 13.89 0.45 o 5 1 4 1070.94 1021.36 33.23 o 6 1 4 425.33 436.87 17.47 o 7 1 4 211.21 210.42 6.37 o 8 1 4 52.01 56.88 1.71 o 9 1 4 96.75 120.17 7.20 o 0 2 4 5.46 4.43 0.25 o 1 2 4 78.91 75.63 2.34 o 2 2 4 1227.81 1267.18 65.32 o 3 2 4 36.29 44.23 2.11 o 4 2 4 392.09 405.31 28.06 o 5 2 4 51.05 48.15 2.65 o 6 2 4 145.06 141.84 9.15 o 7 2 4 29.87 29.75 1.72 o 8 2 4 74.81 73.17 4.00 o 9 2 4 25.03 28.12 1.42 o 0 3 4 12.52 9.41 0.34 o 1 3 4 354.83 389.99 9.60 o 2 3 4 613.52 725.62 26.56 o 3 3 4 69.84 73.79 3.54 o 4 3 4 69.96 69.27 4.44 o 5 3 4 177.96 157.50 10.47 o 6 3 4 92.27 89.63 6.37 o 7 3 4 13.25 13.31 0.76 o 8 3 4 4.57 3.84 0.55 o 0 4 4 2.45 2.17 0.22 o 1 4 4 119.39 148.67 4.65 o 2 4 4 31.25 27.21 1.43 o 3 4 4 64.75 64.97 4.52 o 4 4 4 89.46 97.87 6.54 o 5 4 4 113.27 105.27 5.03 o 6 4 4 17.69 15.00 1.38 o 7 4 4 13.42 10.40 0.87 o 8 4 4 40.75 42.12 1.99 o 0 5 4 6.88 3.02 0.32 o 1 5 4 52.66 55.64 1.87 o 2 5 4 507.75 516.79 24.06 o 3 5 4 231.41 226.65 13.31 o 4 5 4 216.11 201.44 11.55 o 5 5 4 90.53 83.80 5.06 o 6 5 4 49.77 52.73 3.19 o 7 5 4 37.02 39.90 3.49 o 0 6 4 6.32 3.31 0.44 o 1 6 4 82.24 91.34 4.23 o 2 6 4 4.91 5.41 0.40 o 3 6 4 329.22 337.33 17.02 o 4 6 4 69.25 56.23 3.68 o 5 6 4 6.90 4.87 0.49 o 6 6 4 12.45 15.30 1.11 o 7 6 4 46.63 44.28 4.25 o 0 7 4 3.88 2.93 0.48 o 1 7 4 46.99 44.03 2.98 o 2 7 4 167.24 169.52 10.87 o 3 7 4 34.01 33.24 2.07 o 4 7 4 18.99 22.91 1.75 o 5 7 4 31.54 27.63 1.78 o 6 7 4 2.61 2.14 0.47 o 0 8 4 38.81 44.06 2.72 o 1 8 4 51.49 57.38 3.88 o 2 8 4 2.05 1.90 0.42 o 3 8 4 46.38 55.38 3.83 o 4 8 4 14.76 15.99 1.26 o 5 8 4 23.36 31.13 2.20 o 0 9 4 0.01 0.58 0.83 o 1 9 4 19.65 24.14 1.30 o 2 9 4 4.49 7.45 0.88 o 3 9 4 65.75 53.86 4.45 o 1 0 5 370.12 396.92 16.64 o 2 0 5 8.87 3.57 0.25 o 3 0 5 1380.03 1703.54 118.90 o 4 0 5 0.75 0.52 0.25 o 5 0 5 179.50 184.77 4.92 o 6 0 5 11.53 10.80 0.84 o 7 0 5 0.08 0.39 0.41 o 8 0 5 4.22 7.29 0.96 o 9 0 5 9.03 9.56 1.15 o 0 1 5 481.30 474.55 12.90 o 1 1 5 596.10 681.70 12.42 o 2 1 5 474.56 571.04 20.06 o 3 1 5 517.14 575.33 24.29 o 4 1 5 33.41 33.57 1.73 o 5 1 5 552.99 524.20 23.52 o 6 1 5 170.24 175.71 7.16 o 7 1 5 18.90 14.98 0.68 o 8 1 5 2.96 2.51 0.49 o 9 1 5 197.04 228.69 4.71 o 0 2 5 181.12 206.97 6.15 o 1 2 5 36.85 34.77 0.95 o 2 2 5 447.48 504.95 20.95 o 3 2 5 163.00 176.86 7.52 o 4 2 5 290.99 319.72 16.96 o 5 2 5 264.46 265.27 18.38 o 6 2 5 72.60 76.54 3.42 o 7 2 5 35.43 37.40 2.32 o 8 2 5 45.78 42.77 1.56 o 0 3 5 237.51 246.48 5.31 o 1 3 5 217.12 254.00 6.14 o 2 3 5 101.34 100.57 4.52 o 3 3 5 389.05 382.92 23.31 o 4 3 5 135.30 147.54 7.68 o 5 3 5 311.41 316.15 17.34 o 6 3 5 46.03 42.16 2.56 o 7 3 5 7.25 8.49 0.69 o 8 3 5 66.16 69.99 1.79 o 0 4 5 5.11 11.48 0.43 o 1 4 5 3.41 4.11 0.24 o 2 4 5 91.08 95.07 4.08 o 3 4 5 112.29 105.50 5.10 o 4 4 5 127.09 122.41 7.11 o 5 4 5 184.48 172.47 11.51 o 6 4 5 28.84 25.13 0.99 o 7 4 5 62.02 61.73 1.63 o 8 4 5 53.88 57.15 1.70 o 0 5 5 57.85 55.76 2.40 o 1 5 5 120.78 117.39 3.30 o 2 5 5 50.44 60.18 3.22 o 3 5 5 71.92 82.21 4.79 o 4 5 5 32.80 29.14 1.75 o 5 5 5 322.21 283.82 15.05 o 6 5 5 9.48 8.51 0.55 o 7 5 5 31.23 30.15 1.23 o 0 6 5 58.26 58.25 2.91 o 1 6 5 12.84 10.99 0.60 o 2 6 5 88.73 78.53 3.47 o 3 6 5 156.59 151.82 7.58 o 4 6 5 48.98 52.22 2.84 o 5 6 5 66.09 66.55 3.96 o 6 6 5 59.50 55.75 4.51 o 0 7 5 5.57 4.52 0.72 o 1 7 5 117.25 122.96 5.64 o 2 7 5 99.20 102.39 7.52 o 3 7 5 65.57 63.65 3.82 o 4 7 5 172.04 153.70 9.12 o 5 7 5 3.03 4.00 0.47 o 6 7 5 38.41 40.43 2.43 o 0 8 5 226.62 242.53 6.54 o 1 8 5 38.34 35.80 2.83 o 2 8 5 13.23 13.71 1.00 o 3 8 5 14.82 13.05 0.98 o 4 8 5 26.85 29.12 2.78 o 0 9 5 48.73 44.22 3.02 o 1 9 5 12.81 19.21 1.50 o 2 9 5 37.85 40.81 2.45 o 0 0 6 2473.97 2737.29 190.94 o 1 0 6 1264.38 1403.91 51.33 o 2 0 6 172.65 191.05 6.51 o 3 0 6 308.86 332.21 11.82 o 4 0 6 60.38 60.03 1.37 o 5 0 6 409.63 399.03 27.48 o 6 0 6 529.08 573.13 18.36 o 7 0 6 176.89 198.99 3.90 o 8 0 6 10.08 14.65 1.20 o 0 1 6 595.49 665.20 24.75 o 1 1 6 67.93 77.71 2.24 o 2 1 6 708.01 894.18 32.56 o 3 1 6 524.75 492.77 23.25 o 4 1 6 3.67 3.05 0.29 o 5 1 6 51.71 42.56 1.31 o 6 1 6 325.84 335.21 12.71 o 7 1 6 57.56 64.26 2.32 o 8 1 6 20.72 23.14 1.05 o 0 2 6 645.91 717.86 14.86 o 1 2 6 19.43 21.43 0.68 o 2 2 6 134.65 160.15 5.23 o 3 2 6 49.44 51.90 2.39 o 4 2 6 156.00 141.00 8.10 o 5 2 6 100.01 95.03 4.82 o 6 2 6 123.83 120.61 4.79 o 7 2 6 6.63 8.47 0.60 o 8 2 6 23.63 24.22 1.82 o 0 3 6 535.27 549.18 10.09 o 1 3 6 381.94 413.19 11.08 o 2 3 6 405.95 429.90 18.06 o 3 3 6 149.64 167.68 10.62 o 4 3 6 231.88 244.99 16.61 o 5 3 6 47.79 42.49 3.34 o 6 3 6 131.17 141.57 9.87 o 7 3 6 140.33 132.44 3.37 o 8 3 6 0.35 0.20 0.38 o 0 4 6 30.66 35.14 0.74 o 1 4 6 78.12 86.89 1.64 o 2 4 6 55.25 47.84 1.94 o 3 4 6 13.84 11.43 0.65 o 4 4 6 2.63 3.37 0.29 o 5 4 6 223.40 222.94 14.98 o 6 4 6 11.88 8.52 0.68 o 7 4 6 46.71 47.52 1.48 o 0 5 6 193.93 177.71 3.20 o 1 5 6 87.06 86.90 2.51 o 2 5 6 217.48 208.48 8.55 o 3 5 6 24.65 30.96 1.53 o 4 5 6 31.45 34.24 2.10 o 5 5 6 59.30 59.34 3.51 o 6 5 6 18.68 18.46 0.83 o 7 5 6 2.36 2.69 0.57 o 0 6 6 20.46 19.89 1.17 o 1 6 6 40.02 33.79 1.01 o 2 6 6 15.66 15.53 0.62 o 3 6 6 245.55 234.96 10.48 o 4 6 6 6.33 5.29 0.46 o 5 6 6 5.17 4.34 0.46 o 6 6 6 8.67 8.13 0.69 o 0 7 6 11.67 12.17 1.33 o 1 7 6 39.76 35.41 1.46 o 2 7 6 2.46 2.84 0.46 o 3 7 6 72.38 77.83 5.14 o 4 7 6 38.10 35.35 2.30 o 5 7 6 4.68 5.81 0.56 o 0 8 6 3.02 2.82 0.73 o 1 8 6 7.12 6.79 0.79 o 2 8 6 23.99 19.47 1.75 o 3 8 6 193.98 184.56 13.20 o 4 8 6 14.73 17.47 2.15 o 0 9 6 22.71 18.31 2.11 o 1 0 7 7.99 10.47 0.87 o 2 0 7 2.90 5.78 0.49 o 3 0 7 1317.92 1410.57 94.82 o 4 0 7 11.92 10.81 0.68 o 5 0 7 21.07 16.92 0.86 o 6 0 7 104.44 101.68 2.79 o 7 0 7 24.92 27.04 1.93 o 8 0 7 0.03 0.54 0.58 o 0 1 7 388.18 478.88 17.30 o 1 1 7 21.16 13.97 0.63 o 2 1 7 27.07 41.17 1.65 o 3 1 7 91.88 113.46 2.72 o 4 1 7 186.18 187.10 4.24 o 5 1 7 0.69 1.27 0.29 o 6 1 7 185.93 184.05 6.51 o 7 1 7 9.47 13.05 0.81 o 8 1 7 5.73 4.59 0.63 o 0 2 7 5.08 6.42 0.42 o 1 2 7 334.84 396.26 5.90 o 2 2 7 3.80 5.60 0.33 o 3 2 7 15.59 14.97 1.36 o 4 2 7 32.83 33.24 1.10 o 5 2 7 195.19 185.82 10.19 o 6 2 7 33.03 34.31 1.62 o 7 2 7 61.23 65.35 3.87 o 8 2 7 4.30 4.49 0.75 o 0 3 7 175.25 201.17 4.92 o 1 3 7 154.69 143.83 3.93 o 2 3 7 571.32 580.35 21.63 o 3 3 7 0.40 0.86 0.20 o 4 3 7 159.84 157.05 9.01 o 5 3 7 67.24 65.66 3.87 o 6 3 7 2.02 1.95 0.36 o 7 3 7 80.73 80.07 4.87 o 0 4 7 0.44 0.21 0.23 o 1 4 7 370.24 370.34 7.73 o 2 4 7 135.75 145.17 5.16 o 3 4 7 54.35 52.46 2.34 o 4 4 7 4.41 5.16 0.39 o 5 4 7 61.60 56.44 3.48 o 6 4 7 3.09 3.68 0.52 o 7 4 7 19.38 18.37 1.01 o 0 5 7 87.63 91.83 2.36 o 1 5 7 53.68 50.25 1.49 o 2 5 7 34.49 33.75 1.15 o 3 5 7 85.95 78.12 3.60 o 4 5 7 149.38 151.93 10.33 o 5 5 7 23.53 22.80 0.89 o 6 5 7 7.50 6.34 0.69 o 0 6 7 585.24 607.03 14.21 o 1 6 7 14.98 13.08 0.73 o 2 6 7 212.52 214.11 7.11 o 3 6 7 38.47 38.90 2.16 o 4 6 7 88.79 78.36 3.80 o 5 6 7 35.46 32.16 1.89 o 6 6 7 45.30 43.97 1.40 o 0 7 7 21.15 24.54 1.78 o 1 7 7 43.89 48.62 1.97 o 2 7 7 87.10 80.36 4.72 o 3 7 7 59.14 61.90 5.92 o 4 7 7 71.22 65.60 5.44 o 5 7 7 3.54 1.11 0.42 o 0 8 7 9.29 7.18 1.01 o 1 8 7 37.55 30.25 1.71 o 2 8 7 3.53 3.12 0.67 o 3 8 7 6.66 10.32 1.49 o 0 0 8 530.16 574.37 9.82 o 1 0 8 42.99 63.33 1.94 o 2 0 8 231.18 273.82 7.32 o 3 0 8 9.40 6.03 0.55 o 4 0 8 13.86 12.42 0.74 o 5 0 8 45.55 39.33 1.69 o 6 0 8 0.25 1.03 0.89 o 7 0 8 32.11 37.37 1.85 o 8 0 8 8.86 12.06 1.31 o 0 1 8 836.71 856.95 41.65 o 1 1 8 166.58 185.52 6.07 o 2 1 8 97.34 105.14 2.56 o 3 1 8 82.09 75.03 1.42 o 4 1 8 39.78 40.15 1.16 o 5 1 8 81.39 78.55 2.34 o 6 1 8 23.63 27.18 0.94 o 7 1 8 32.10 35.15 1.76 o 0 2 8 34.44 36.53 2.04 o 1 2 8 102.88 100.60 3.18 o 2 2 8 137.49 129.02 4.98 o 3 2 8 135.73 125.98 6.14 o 4 2 8 126.08 124.63 5.60 o 5 2 8 34.75 32.72 1.56 o 6 2 8 5.03 6.96 0.57 o 7 2 8 53.65 62.94 3.78 o 0 3 8 20.27 16.97 0.68 o 1 3 8 75.28 80.09 2.10 o 2 3 8 4.32 3.67 0.32 o 3 3 8 47.72 51.52 2.30 o 4 3 8 73.06 66.10 3.17 o 5 3 8 3.96 4.27 0.47 o 6 3 8 19.85 23.94 1.89 o 7 3 8 56.10 52.46 3.67 o 0 4 8 80.17 78.38 3.38 o 1 4 8 123.06 120.18 1.72 o 2 4 8 262.34 268.37 8.28 o 3 4 8 18.75 19.85 1.19 o 4 4 8 132.58 129.10 6.49 o 5 4 8 225.86 220.15 14.95 o 6 4 8 4.99 4.00 0.51 o 7 4 8 13.30 12.63 1.09 o 0 5 8 12.36 11.81 0.98 o 1 5 8 6.93 7.78 0.61 o 2 5 8 218.92 204.49 7.45 o 3 5 8 15.61 14.13 0.71 o 4 5 8 39.72 37.15 1.80 o 5 5 8 28.66 20.12 1.00 o 6 5 8 22.49 20.08 1.07 o 0 6 8 2.94 2.75 0.68 o 1 6 8 327.39 328.31 7.13 o 2 6 8 5.55 6.45 0.63 o 3 6 8 13.18 12.98 0.89 o 4 6 8 85.86 73.69 2.45 o 5 6 8 10.28 13.05 0.81 o 0 7 8 0.07 0.61 0.52 o 1 7 8 7.86 6.23 0.65 o 2 7 8 45.44 45.58 2.11 o 3 7 8 28.39 29.74 2.59 o 4 7 8 42.32 41.38 2.46 o 0 8 8 19.24 19.04 1.47 o 1 8 8 35.72 29.27 1.44 o 1 0 9 75.56 70.96 1.61 o 2 0 9 5.17 9.90 0.67 o 3 0 9 306.48 293.45 10.08 o 4 0 9 16.41 13.00 0.81 o 5 0 9 65.30 77.28 2.44 o 6 0 9 66.01 69.63 2.45 o 7 0 9 97.72 115.59 3.32 o 0 1 9 163.01 158.38 9.98 o 1 1 9 57.80 55.92 1.04 o 2 1 9 97.75 103.40 1.61 o 3 1 9 72.67 68.80 1.17 o 4 1 9 120.62 125.84 3.27 o 5 1 9 22.84 23.01 0.86 o 6 1 9 5.72 6.35 0.66 o 7 1 9 0.35 0.44 0.43 o 0 2 9 759.80 826.05 33.72 o 1 2 9 373.05 388.77 7.13 o 2 2 9 39.60 41.91 1.46 o 3 2 9 90.37 87.70 2.49 o 4 2 9 76.16 68.24 2.09 o 5 2 9 9.60 8.90 0.62 o 6 2 9 62.36 65.61 2.96 o 7 2 9 43.91 48.07 1.56 o 0 3 9 81.26 81.28 3.10 o 1 3 9 143.63 138.62 3.75 o 2 3 9 97.98 97.52 3.66 o 3 3 9 217.14 197.34 7.94 o 4 3 9 3.06 1.89 0.36 o 5 3 9 42.27 40.77 2.64 o 6 3 9 4.93 4.43 0.55 o 0 4 9 42.55 42.49 4.55 o 1 4 9 120.10 120.24 2.55 o 2 4 9 37.00 31.67 1.37 o 3 4 9 6.82 7.40 0.50 o 4 4 9 65.76 65.78 3.82 o 5 4 9 46.15 48.18 3.04 o 6 4 9 29.89 36.15 2.59 o 0 5 9 2.37 3.27 0.70 o 1 5 9 10.97 12.61 0.76 o 2 5 9 271.86 265.50 12.25 o 3 5 9 3.24 2.54 0.41 o 4 5 9 0.31 0.20 0.27 o 5 5 9 35.54 28.52 1.68 o 0 6 9 23.19 20.66 1.35 o 1 6 9 1.24 1.03 0.40 o 2 6 9 197.35 189.27 10.57 o 3 6 9 17.38 19.03 1.38 o 4 6 9 77.74 66.82 2.14 o 0 7 9 6.83 5.92 0.96 o 1 7 9 12.48 10.21 0.81 o 2 7 9 8.15 9.40 0.81 o 3 7 9 12.66 11.68 1.04 o 0 0 10 607.65 729.89 33.52 o 1 0 10 78.29 69.83 1.71 o 2 0 10 44.68 46.20 1.41 o 3 0 10 136.27 127.75 3.71 o 4 0 10 20.03 23.73 1.10 o 5 0 10 97.54 109.75 3.05 o 6 0 10 103.32 110.73 3.22 o 0 1 10 766.82 847.17 22.67 o 1 1 10 151.55 151.95 1.79 o 2 1 10 23.46 25.25 0.75 o 3 1 10 24.66 19.63 0.93 o 4 1 10 128.47 125.39 3.31 o 5 1 10 24.79 24.41 0.92 o 6 1 10 17.70 19.61 1.02 o 0 2 10 112.18 123.77 2.24 o 1 2 10 0.92 1.29 0.25 o 2 2 10 128.40 128.17 2.49 o 3 2 10 76.29 74.27 1.61 o 4 2 10 68.84 66.79 2.73 o 5 2 10 19.47 22.60 0.92 o 6 2 10 12.72 15.55 0.85 o 0 3 10 200.67 199.49 8.04 o 1 3 10 17.95 19.95 1.08 o 2 3 10 138.47 135.23 5.39 o 3 3 10 15.07 15.12 0.66 o 4 3 10 83.51 88.00 4.18 o 5 3 10 4.30 3.01 0.47 o 6 3 10 39.80 32.68 2.66 o 0 4 10 126.06 103.76 9.87 o 1 4 10 1.62 1.79 0.41 o 2 4 10 64.84 62.97 2.92 o 3 4 10 17.22 17.30 0.89 o 4 4 10 82.38 79.50 3.99 o 5 4 10 9.06 9.05 0.74 o 0 5 10 57.45 59.12 2.16 o 1 5 10 8.86 9.96 0.74 o 2 5 10 27.07 24.30 1.06 o 3 5 10 29.77 32.57 1.45 o 4 5 10 5.05 4.22 0.55 o 0 6 10 3.95 3.23 0.77 o 1 6 10 70.40 59.82 1.63 o 2 6 10 10.06 10.40 0.97 o 3 6 10 33.24 33.66 2.47 o 0 7 10 0.01 0.02 0.57 o 1 0 11 27.41 28.27 1.18 o 2 0 11 10.21 10.97 0.82 o 3 0 11 253.23 250.94 7.09 o 4 0 11 0.47 0.37 0.50 o 5 0 11 2.54 3.45 0.85 o 6 0 11 0.52 1.28 0.74 o 0 1 11 404.49 433.09 9.97 o 1 1 11 56.76 57.42 1.16 o 2 1 11 130.08 130.59 1.77 o 3 1 11 22.36 17.31 0.78 o 4 1 11 55.52 51.54 1.33 o 5 1 11 0.16 0.99 0.46 o 6 1 11 43.05 38.47 2.40 o 0 2 11 1.97 2.87 0.51 o 1 2 11 85.98 84.20 1.74 o 2 2 11 12.86 14.25 0.71 o 3 2 11 59.89 56.88 2.49 o 4 2 11 14.06 14.92 0.79 o 5 2 11 53.02 58.12 1.83 o 0 3 11 37.69 35.03 1.63 o 1 3 11 64.69 62.93 2.36 o 2 3 11 22.07 18.41 0.90 o 3 3 11 49.22 40.89 1.46 o 4 3 11 54.21 55.64 3.11 o 5 3 11 18.94 17.31 1.22 o 0 4 11 46.26 54.69 3.07 o 1 4 11 1.56 2.11 0.50 o 2 4 11 18.30 17.50 0.81 o 3 4 11 15.00 12.91 0.76 o 4 4 11 2.05 2.70 0.57 o 0 5 11 0.13 0.32 0.53 o 1 5 11 20.03 19.35 1.15 o 2 5 11 85.58 76.63 4.99 o 3 5 11 56.30 48.15 3.08 o 0 6 11 77.64 70.89 2.63 o 1 6 11 29.73 28.29 1.50 o 0 0 12 3.76 4.64 1.08 o 1 0 12 0.26 0.21 0.35 o 2 0 12 24.00 22.65 1.15 o 3 0 12 5.15 5.98 0.96 o 4 0 12 1.01 0.86 0.66 o 5 0 12 26.72 30.03 4.04 o 0 1 12 44.67 45.77 1.54 o 1 1 12 5.34 6.61 0.52 o 2 1 12 5.68 6.58 0.66 o 3 1 12 98.36 96.94 3.53 o 4 1 12 30.26 33.14 1.27 o 5 1 12 17.80 16.15 2.14 o 0 2 12 0.29 0.32 0.37 o 1 2 12 36.37 35.61 1.22 o 2 2 12 48.28 49.19 1.31 o 3 2 12 4.05 3.52 0.52 o 4 2 12 17.42 19.90 1.02 o 0 3 12 228.29 230.64 6.49 o 1 3 12 14.74 13.98 0.99 o 2 3 12 50.14 43.30 1.40 o 3 3 12 71.32 73.84 4.47 o 4 3 12 74.14 74.50 2.99 o 0 4 12 3.68 2.63 1.15 o 1 4 12 72.03 69.39 3.82 o 2 4 12 51.12 45.91 3.46 o 3 4 12 23.00 26.58 1.63 o 0 5 12 0.09 -0.56 0.74 o 1 5 12 16.10 14.90 1.15 o 1 0 13 10.01 9.31 0.88 o 2 0 13 34.85 41.48 1.61 o 3 0 13 33.81 34.95 1.95 o 0 1 13 74.49 77.82 2.58 o 1 1 13 43.34 40.89 1.21 o 2 1 13 6.63 8.66 0.71 o 3 1 13 6.81 6.82 0.68 o 0 2 13 82.95 69.45 2.52 o 1 2 13 50.54 49.01 2.15 o 2 2 13 7.20 7.56 0.75 o 3 2 13 0.63 0.94 0.46 o 0 3 13 0.74 2.12 1.08 o 1 3 13 14.69 14.78 1.15 o 2 3 13 25.80 31.04 1.30 o 0 0 14 0.76 0.44 0.91 o 1 0 14 1.26 2.39 0.81 o 0 1 14 47.27 47.85 3.11 o