#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210239.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210239_Fobs loop_ _publ_author_name 'Rakovsk\'y, Erik' 'Gyepes, Robert' _publ_section_title ; Butane-1,4-diammonium decavanadate(V) hexahydrate ; _journal_coeditor_code GK2024 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2108 _journal_page_last m2110 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.038 _cell_angle_gamma 90.000 _cell_length_a 10.6504 _cell_length_b 17.6351 _cell_length_c 10.9644 _exptl_crystal_F_000 1340.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file gk2024Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' krD1,P21/n,RT' _shelx_refln_list_code 4 _shelx_f_calc_maximum 305.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9612.14 8999.38 299.89 o 4 0 0 337.16 350.60 29.57 o 6 0 0 93.22 102.85 21.43 o 8 0 0 2916.65 2724.66 123.11 o 10 0 0 11420.25 11746.55 469.02 o 12 0 0 4881.93 5200.59 321.34 o 2 1 0 1321.65 1325.92 33.05 o 3 1 0 20985.08 21208.38 537.14 o 4 1 0 49.48 53.99 11.14 o 5 1 0 828.15 883.13 34.30 o 6 1 0 2846.38 2789.35 82.81 o 7 1 0 51.20 59.14 20.14 o 8 1 0 2286.87 2313.65 75.91 o 9 1 0 100.77 105.85 28.28 o 10 1 0 1289.10 1163.41 55.73 o 11 1 0 5976.21 6420.97 232.19 o 12 1 0 6.79 18.00 62.13 o 13 1 0 134.74 182.12 77.13 o 1 2 0 4641.00 2895.44 142.53 o 2 2 0 4609.65 4906.53 113.72 o 3 2 0 15651.39 15540.95 369.38 o 4 2 0 2462.95 2479.88 71.25 o 5 2 0 1.76 19.71 14.14 o 6 2 0 4267.54 4067.88 111.63 o 7 2 0 19.07 -25.71 25.71 o 8 2 0 49.13 25.28 24.00 o 9 2 0 1092.65 989.77 46.72 o 10 2 0 1286.01 1345.59 66.01 o 11 2 0 338.89 361.27 51.85 o 12 2 0 29.60 -47.99 47.99 o 13 2 0 83.98 85.28 57.85 o 1 3 0 5444.90 5508.00 127.73 o 2 3 0 6870.60 6918.46 161.79 o 3 3 0 531.38 557.29 17.58 o 4 3 0 11732.42 11098.96 268.89 o 5 3 0 16.71 25.28 15.43 o 6 3 0 110.67 125.99 18.43 o 7 3 0 12175.27 12319.52 323.30 o 8 3 0 1876.32 1920.96 62.60 o 9 3 0 0.01 -23.14 25.71 o 10 3 0 136.03 180.84 36.85 o 11 3 0 7.80 38.14 45.85 o 12 3 0 190.56 209.98 71.99 o 13 3 0 344.51 316.27 69.42 o 0 4 0 16703.98 15890.03 378.79 o 1 4 0 1233.28 1193.63 28.32 o 2 4 0 12016.80 12474.22 301.30 o 3 4 0 2280.62 1757.56 43.35 o 4 4 0 968.69 750.75 27.87 o 5 4 0 244.91 211.71 16.71 o 6 4 0 4681.70 4409.54 121.08 o 7 4 0 4308.14 4172.25 122.75 o 8 4 0 1712.68 1733.04 59.60 o 9 4 0 66.67 97.27 36.00 o 10 4 0 1985.49 2030.12 81.46 o 11 4 0 220.06 223.70 52.71 o 12 4 0 101.32 -42.85 42.85 o 13 4 0 258.51 287.12 69.85 o 1 5 0 58.22 70.28 3.00 o 2 5 0 13269.57 12786.98 268.29 o 3 5 0 6200.32 5179.99 143.26 o 4 5 0 817.88 757.52 24.01 o 5 5 0 99.25 48.00 12.43 o 6 5 0 51.49 63.42 19.71 o 7 5 0 4950.58 5066.38 138.23 o 8 5 0 2131.11 2272.27 72.90 o 9 5 0 84.19 68.14 23.14 o 10 5 0 1896.83 1884.29 90.46 o 11 5 0 208.08 222.84 40.71 o 12 5 0 360.64 285.41 65.57 o 13 5 0 1172.88 1023.56 137.59 o 0 6 0 1645.30 1719.58 42.47 o 1 6 0 8097.84 8169.95 153.43 o 2 6 0 1404.65 1155.04 27.88 o 3 6 0 278.29 187.29 11.14 o 4 6 0 750.03 938.80 29.58 o 5 6 0 2057.80 2104.20 56.19 o 6 6 0 386.75 421.29 22.71 o 7 6 0 799.26 789.97 33.43 o 8 6 0 2504.55 2597.57 87.06 o 9 6 0 4272.81 4459.07 129.57 o 10 6 0 0.59 27.85 32.57 o 11 6 0 920.91 939.52 70.72 o 12 6 0 8.03 -26.14 65.99 o 13 6 0 414.48 294.84 87.42 o 1 7 0 25.53 21.43 4.29 o 2 7 0 2561.02 2633.68 51.50 o 3 7 0 1865.74 1966.22 45.90 o 4 7 0 97.04 109.70 10.71 o 5 7 0 37.93 34.28 12.86 o 6 7 0 297.82 309.85 21.86 o 7 7 0 1805.69 1974.08 66.03 o 8 7 0 1142.40 1194.26 48.87 o 9 7 0 874.31 864.10 51.01 o 10 7 0 4885.85 5371.90 223.54 o 11 7 0 314.05 281.98 47.14 o 12 7 0 168.75 185.98 62.14 o 13 7 0 8.84 -51.85 90.42 o 0 8 0 2903.01 2698.44 79.40 o 1 8 0 2944.61 2877.83 57.94 o 2 8 0 789.53 909.68 36.01 o 3 8 0 516.49 496.77 16.72 o 4 8 0 11532.08 11218.77 250.65 o 5 8 0 13329.79 13330.06 288.61 o 6 8 0 2630.26 2819.70 78.06 o 7 8 0 4206.35 4534.76 118.43 o 8 8 0 729.67 699.49 39.00 o 9 8 0 870.49 945.96 46.72 o 10 8 0 25.08 38.57 35.14 o 11 8 0 5.06 -37.28 37.28 o 12 8 0 315.02 284.98 72.85 o 1 9 0 2482.95 2487.98 61.35 o 2 9 0 1138.45 1146.03 48.88 o 3 9 0 1744.07 1674.63 39.45 o 4 9 0 15463.20 15855.67 319.95 o 5 9 0 14743.30 15185.50 337.37 o 6 9 0 16166.67 16910.03 391.67 o 7 9 0 8774.76 9268.18 240.63 o 8 9 0 49.00 64.28 22.28 o 9 9 0 764.49 669.05 44.15 o 10 9 0 665.67 616.73 60.00 o 11 9 0 37.46 56.99 40.28 o 12 9 0 111.61 123.84 55.28 o 0 10 0 226.19 191.14 12.43 o 1 10 0 1093.04 1050.80 32.58 o 2 10 0 3001.39 3180.66 96.11 o 3 10 0 331.85 324.86 24.86 o 4 10 0 2772.13 2898.51 72.92 o 5 10 0 34200.35 36703.07 802.28 o 6 10 0 20.32 12.86 15.86 o 7 10 0 4121.51 4245.02 114.13 o 8 10 0 1945.96 2024.98 77.17 o 9 10 0 0.55 -13.28 32.14 o 10 10 0 61.08 72.85 31.28 o 11 10 0 147.37 55.71 38.14 o 12 10 0 777.61 938.61 188.58 o 1 11 0 131.27 145.70 15.86 o 2 11 0 3082.51 3121.67 109.83 o 3 11 0 2179.40 2367.34 82.77 o 4 11 0 67.84 55.71 3.86 o 5 11 0 1574.70 1684.51 49.73 o 6 11 0 2013.85 1972.83 61.32 o 7 11 0 3586.73 3781.30 102.52 o 8 11 0 624.53 597.45 33.00 o 9 11 0 123.72 100.70 27.00 o 10 11 0 52.34 -12.86 30.00 o 11 11 0 77.12 166.27 50.57 o 12 11 0 2482.27 2587.91 265.39 o 0 12 0 6391.04 6490.98 173.97 o 1 12 0 8398.33 8570.28 197.31 o 2 12 0 314.13 244.71 26.57 o 3 12 0 37.09 25.28 17.14 o 4 12 0 89.09 63.85 21.00 o 5 12 0 939.42 987.16 30.00 o 6 12 0 172.81 194.55 15.43 o 7 12 0 1929.66 1983.81 77.17 o 8 12 0 37.97 50.14 24.85 o 9 12 0 401.76 372.84 42.86 o 10 12 0 1136.95 1231.45 96.44 o 11 12 0 1214.51 1223.31 124.73 o 1 13 0 9497.88 9669.28 241.62 o 2 13 0 10008.77 10381.04 274.76 o 3 13 0 3694.87 3686.72 159.17 o 4 13 0 1040.70 1004.34 54.01 o 5 13 0 74.35 47.14 26.14 o 6 13 0 531.77 528.44 25.71 o 7 13 0 201.42 212.13 22.71 o 8 13 0 0.20 12.43 24.43 o 9 13 0 1132.30 1303.47 81.44 o 10 13 0 1718.93 1931.22 127.32 o 11 13 0 1329.17 1373.36 189.03 o 0 14 0 3128.46 3218.88 88.79 o 1 14 0 4267.87 4512.11 124.01 o 2 14 0 518.08 582.87 33.00 o 3 14 0 1513.54 1538.23 82.31 o 4 14 0 4.47 21.43 21.43 o 5 14 0 0.60 -17.14 25.28 o 6 14 0 169.38 154.70 39.00 o 7 14 0 157.64 149.56 15.86 o 8 14 0 341.06 407.55 32.57 o 9 14 0 3710.07 3679.88 279.21 o 10 14 0 389.09 328.70 90.42 o 1 15 0 1261.41 1247.46 48.87 o 2 15 0 194.60 175.70 24.43 o 3 15 0 24.17 6.43 36.00 o 4 15 0 120.98 89.99 30.00 o 5 15 0 1392.62 1320.32 81.02 o 6 15 0 1425.04 1427.06 99.02 o 7 15 0 444.28 333.42 54.86 o 8 15 0 4.95 -37.71 42.85 o 9 15 0 618.27 480.86 111.86 o 10 15 0 66.10 107.13 102.84 o 0 16 0 548.84 509.58 19.71 o 1 16 0 1217.04 1186.97 46.30 o 2 16 0 47.35 71.99 20.57 o 3 16 0 1936.57 1946.93 86.61 o 4 16 0 2194.59 2179.86 128.20 o 5 16 0 1029.54 966.99 81.44 o 6 16 0 69.41 98.99 46.71 o 7 16 0 67.59 63.85 51.42 o 8 16 0 1496.88 1432.16 213.05 o 9 16 0 780.15 531.02 114.86 o 1 17 0 128.43 111.42 16.28 o 2 17 0 6817.09 7250.61 369.21 o 3 17 0 51.13 41.99 25.28 o 4 17 0 57.62 -32.14 44.99 o 5 17 0 356.06 287.56 46.71 o 6 17 0 395.04 333.42 50.14 o 7 17 0 26.42 -17.14 51.42 o 8 17 0 1713.81 1417.22 197.19 o 9 17 0 1469.04 1658.45 271.76 o 0 18 0 448.92 215.14 69.00 o 1 18 0 2350.41 2530.65 120.92 o 2 18 0 6419.53 6256.43 380.73 o 3 18 0 815.84 669.05 47.57 o 4 18 0 4.74 38.99 33.00 o 5 18 0 423.97 278.56 48.86 o 6 18 0 291.56 347.98 80.57 o 7 18 0 90.05 128.13 97.70 o 8 18 0 1075.54 814.80 183.02 o 1 19 0 939.11 770.65 87.44 o 2 19 0 2604.00 2458.26 195.10 o 3 19 0 1327.08 1429.13 111.88 o 4 19 0 186.36 102.85 49.28 o 5 19 0 87.56 68.99 51.42 o 6 19 0 5.31 38.57 89.13 o 7 19 0 19.58 30.42 73.28 o 0 20 0 29.06 59.56 72.85 o 1 20 0 304.80 360.41 101.99 o 2 20 0 1558.14 1663.68 224.20 o 3 20 0 20.93 -21.43 68.56 o 4 20 0 31.05 42.85 81.42 o 5 20 0 350.23 317.12 118.71 o 6 20 0 111.78 68.14 106.70 o 1 21 0 137.52 30.43 124.70 o 2 21 0 251.83 300.83 90.85 o 3 21 0 78.11 166.27 80.99 o 4 21 0 428.68 398.56 114.85 o 5 21 0 146.41 158.13 90.42 o 0 22 0 506.04 307.71 103.28 o 1 22 0 183.23 123.85 192.41 o 2 22 0 7.84 -68.13 136.27 o 3 22 0 19.84 -98.13 98.13 o -13 0 1 270.48 269.98 98.99 o -11 0 1 1353.24 1291.99 126.88 o -9 0 1 872.67 926.70 60.01 o -7 0 1 2418.08 2543.05 105.51 o -5 0 1 296.81 287.58 31.29 o -3 0 1 5996.95 5845.75 210.62 o 3 0 1 19994.25 19710.86 630.00 o 5 0 1 3080.00 3255.99 119.75 o 7 0 1 263.84 296.56 29.14 o 9 0 1 754.07 825.94 67.72 o 11 0 1 15000.99 15155.66 839.71 o 13 0 1 2456.49 2989.26 286.41 o -13 1 1 1323.82 1198.91 104.16 o -12 1 1 24.50 77.99 39.85 o -11 1 1 0.95 -37.28 37.28 o -10 1 1 586.37 739.74 51.43 o -9 1 1 2248.52 2281.71 77.19 o -8 1 1 2.23 -10.28 20.14 o -7 1 1 12434.13 12700.53 296.67 o -6 1 1 1265.65 1264.83 44.16 o -5 1 1 1859.37 1804.11 53.19 o -4 1 1 89.00 127.70 13.71 o -3 1 1 5201.04 4951.69 127.40 o -2 1 1 4528.79 4870.15 126.22 o 1 1 1 41.24 27.43 6.43 o 2 1 1 2332.00 2292.66 53.28 o 3 1 1 20861.36 20063.78 475.97 o 4 1 1 1436.51 1272.14 37.74 o 5 1 1 10264.13 10132.87 242.55 o 6 1 1 331.23 348.86 22.71 o 7 1 1 630.77 661.78 33.43 o 8 1 1 549.52 483.88 31.29 o 9 1 1 466.37 468.43 37.71 o 10 1 1 6456.17 6257.76 186.74 o 11 1 1 2354.28 2280.22 114.05 o 12 1 1 4782.23 5009.95 259.12 o 13 1 1 424.23 415.70 71.57 o -13 2 1 1272.15 1230.62 117.88 o -12 2 1 65.65 90.42 47.14 o -11 2 1 9.76 11.14 35.57 o -10 2 1 72.83 52.28 36.85 o -9 2 1 12.92 45.85 30.85 o -8 2 1 8477.77 8396.97 211.87 o -7 2 1 17751.75 17884.84 457.76 o -6 2 1 10351.61 10117.45 266.03 o -5 2 1 3996.66 3959.55 110.36 o -4 2 1 3296.98 2734.04 75.15 o -3 2 1 1841.13 1665.52 45.49 o -2 2 1 111.41 52.71 11.57 o -1 2 1 7205.81 6811.00 149.83 o 0 2 1 7501.48 5587.31 260.42 o 1 2 1 269.83 231.49 9.00 o 2 2 1 4676.34 4728.54 105.07 o 3 2 1 1955.29 2102.95 51.07 o 4 2 1 3867.37 3624.09 91.92 o 5 2 1 7193.86 7402.01 179.35 o 6 2 1 199.79 218.99 19.71 o 7 2 1 266.42 228.85 25.28 o 8 2 1 6314.38 6321.65 169.20 o 9 2 1 301.80 288.84 30.43 o 10 2 1 718.54 722.19 56.15 o 11 2 1 521.51 453.43 51.86 o 12 2 1 602.60 551.15 61.29 o 13 2 1 510.06 578.99 91.28 o -13 3 1 53.73 39.00 71.56 o -12 3 1 34.55 174.83 140.98 o -11 3 1 422.58 359.13 42.86 o -10 3 1 750.45 822.06 47.57 o -9 3 1 165.05 195.41 29.57 o -8 3 1 8129.47 8176.55 248.36 o -7 3 1 5429.37 5357.56 135.69 o -6 3 1 9239.90 9033.46 233.61 o -5 3 1 10.53 15.43 13.71 o -4 3 1 86.49 79.28 12.00 o -3 3 1 26976.10 25311.01 654.28 o -2 3 1 7459.84 7455.42 157.94 o -1 3 1 2512.39 2621.68 57.16 o 0 3 1 4219.66 4112.18 86.17 o 1 3 1 62.52 55.28 6.00 o 2 3 1 5723.80 5804.41 130.53 o 3 3 1 4972.86 5375.53 128.59 o 4 3 1 16750.23 16574.63 380.85 o 5 3 1 4225.67 4091.06 103.49 o 6 3 1 852.99 810.61 36.44 o 7 3 1 25831.46 26057.31 697.01 o 8 3 1 388.14 355.28 28.71 o 9 3 1 3.40 36.85 29.57 o 10 3 1 8.12 10.71 26.14 o 11 3 1 67.20 46.71 47.14 o 12 3 1 549.76 403.71 99.86 o 13 3 1 204.08 224.98 82.71 o -13 4 1 2.15 69.85 59.99 o -12 4 1 113.20 99.85 52.28 o -11 4 1 341.69 341.13 47.14 o -10 4 1 104.37 65.56 35.57 o -9 4 1 512.10 489.01 36.86 o -8 4 1 5743.33 6015.77 154.56 o -7 4 1 3934.86 4065.23 114.15 o -6 4 1 465.90 536.17 27.43 o -5 4 1 10.83 22.71 15.43 o -4 4 1 25.70 26.57 10.71 o -3 4 1 1953.49 1992.67 53.64 o -2 4 1 8339.43 8270.48 183.37 o -1 4 1 1052.45 1002.88 22.73 o 0 4 1 1422.54 1235.07 26.18 o 1 4 1 173.29 192.43 16.29 o 2 4 1 25159.33 25099.20 533.39 o 3 4 1 1041.25 965.69 25.73 o 4 4 1 474.36 426.91 18.86 o 5 4 1 1411.04 1313.85 43.74 o 6 4 1 2940.22 2917.89 79.80 o 7 4 1 6471.84 6408.63 165.80 o 8 4 1 5731.99 5888.59 148.97 o 9 4 1 52.59 120.84 26.14 o 10 4 1 125.78 119.56 30.00 o 11 4 1 44.04 75.85 44.99 o 12 4 1 7.56 128.13 59.13 o 13 4 1 50.13 107.56 82.28 o -13 5 1 88.84 73.28 65.99 o -12 5 1 46.68 -55.28 55.28 o -11 5 1 2888.14 2931.46 134.22 o -10 5 1 111.59 179.98 33.42 o -9 5 1 839.23 878.67 45.43 o -8 5 1 1358.97 1182.79 47.59 o -7 5 1 2277.40 2347.61 68.62 o -6 5 1 419.48 406.73 22.29 o -5 5 1 1152.27 1190.61 41.16 o -4 5 1 141.34 260.98 17.14 o -3 5 1 1865.00 1687.72 41.18 o -2 5 1 2928.26 2672.27 58.40 o -1 5 1 9727.86 9440.99 199.53 o 0 5 1 187.08 174.00 7.29 o 1 5 1 27105.14 26644.10 540.23 o 2 5 1 27027.42 26872.87 539.79 o 3 5 1 2199.95 1677.32 42.48 o 4 5 1 563.26 799.84 26.15 o 5 5 1 3673.38 4000.03 105.16 o 6 5 1 66.14 60.42 15.86 o 7 5 1 5047.91 5249.76 143.38 o 8 5 1 989.68 1063.91 45.01 o 9 5 1 702.68 677.19 40.72 o 10 5 1 644.83 691.31 55.29 o 11 5 1 359.33 221.56 42.86 o 12 5 1 498.63 536.99 93.86 o 13 5 1 989.23 1019.66 117.44 o -13 6 1 132.24 -33.42 90.42 o -12 6 1 291.33 169.27 66.85 o -11 6 1 1930.81 2038.56 105.89 o -10 6 1 10069.90 10748.21 375.10 o -9 6 1 1183.50 1242.26 60.44 o -8 6 1 3594.04 3658.96 106.39 o -7 6 1 3.60 42.42 17.14 o -6 6 1 815.15 902.73 37.29 o -5 6 1 500.43 513.90 24.86 o -4 6 1 2403.88 2596.89 58.78 o -3 6 1 1178.38 1064.71 27.44 o -2 6 1 733.45 744.67 18.86 o -1 6 1 5.10 9.86 3.86 o 0 6 1 32651.48 30115.41 601.56 o 1 6 1 19014.65 18655.72 431.96 o 2 6 1 2946.23 3152.01 72.12 o 3 6 1 3311.89 2939.91 67.83 o 4 6 1 117.14 251.12 19.71 o 5 6 1 1795.59 1839.76 51.46 o 6 6 1 1774.30 1842.58 57.46 o 7 6 1 581.94 627.90 31.29 o 8 6 1 205.07 178.27 27.00 o 9 6 1 686.86 632.61 42.86 o 10 6 1 3.38 -21.43 30.00 o 11 6 1 45.42 68.13 39.00 o 12 6 1 262.46 380.11 84.85 o 13 6 1 2737.65 2890.35 211.38 o -13 7 1 107.43 145.27 85.28 o -12 7 1 5075.19 5583.23 285.73 o -11 7 1 1852.58 1948.91 112.32 o -10 7 1 271.18 236.13 45.43 o -9 7 1 8786.32 9122.63 260.33 o -8 7 1 953.20 1003.44 48.01 o -7 7 1 572.17 691.32 33.00 o -6 7 1 1140.62 1037.01 40.30 o -5 7 1 747.49 680.69 25.29 o -4 7 1 1905.50 1934.73 48.46 o -3 7 1 965.03 1006.22 26.58 o -2 7 1 814.01 722.38 17.58 o -1 7 1 9537.29 9485.32 165.50 o 0 7 1 3272.56 3239.29 62.69 o 1 7 1 3804.51 3094.55 70.87 o 2 7 1 6229.65 5997.92 162.55 o 3 7 1 686.96 621.13 19.72 o 4 7 1 13978.03 14695.73 326.04 o 5 7 1 2321.30 2402.83 61.34 o 6 7 1 104.64 87.85 17.14 o 7 7 1 1173.59 1171.16 45.87 o 8 7 1 1.84 -16.71 21.43 o 9 7 1 1043.90 1001.73 62.15 o 10 7 1 1017.73 987.56 69.87 o 11 7 1 18.53 25.28 55.28 o 12 7 1 601.00 730.72 82.29 o 13 7 1 388.97 360.41 101.99 o -12 8 1 13.22 30.85 48.85 o -11 8 1 1880.51 1848.16 113.18 o -10 8 1 2278.33 2461.54 115.34 o -9 8 1 3754.24 4112.01 147.99 o -8 8 1 362.43 404.99 28.71 o -7 8 1 2716.86 2888.17 86.21 o -6 8 1 1564.94 1547.37 53.17 o -5 8 1 1765.08 1588.74 43.74 o -4 8 1 4381.30 4537.53 97.46 o -3 8 1 4129.89 4185.31 89.30 o -2 8 1 946.27 1001.49 24.87 o -1 8 1 9167.66 9140.14 168.81 o 0 8 1 20742.45 20345.37 370.97 o 1 8 1 422.27 420.90 19.29 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