#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:16:04 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181023 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/03/2210377.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210377_Fobs loop_ _publ_author_name 'Yang, E.' 'Yang, Fa-Fu' _publ_section_title ; L-Phenylalaninium 4-sulfonate ; _journal_coeditor_code SJ2096 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3895 _journal_page_last o3896 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.950 _cell_angle_gamma 90.000 _cell_length_a 5.6357 _cell_length_b 9.1773 _cell_length_c 10.3076 _exptl_crystal_F_000 256.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file sj2096Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 58.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -9 0 40.31 36.71 2.96 o 1 -8 0 165.38 152.23 5.16 o 2 -8 0 31.88 31.11 2.60 o 3 -8 0 75.31 74.34 4.29 o 5 -8 0 12.70 15.62 2.44 o 1 -7 0 694.12 744.95 10.09 o 2 -7 0 157.66 154.59 5.27 o 3 -7 0 206.04 199.85 6.90 o 4 -7 0 83.07 85.25 3.26 o 5 -7 0 25.21 21.97 2.62 o 0 -6 0 1070.19 1124.96 9.70 o 1 -6 0 133.52 154.65 4.36 o 2 -6 0 4.47 3.91 1.11 o 3 -6 0 204.34 201.30 4.30 o 4 -6 0 170.15 169.20 4.43 o 5 -6 0 34.29 36.18 3.22 o 6 -6 0 48.45 51.32 4.20 o 1 -5 0 508.81 522.43 4.38 o 2 -5 0 474.29 485.01 5.53 o 3 -5 0 64.03 62.53 2.41 o 4 -5 0 377.84 397.01 16.71 o 5 -5 0 104.49 101.76 5.51 o 0 -4 0 1235.43 1350.19 11.91 o 1 -4 0 349.67 355.07 3.06 o 2 -4 0 789.29 822.10 7.57 o 3 -4 0 405.85 435.10 5.70 o 4 -4 0 268.47 265.48 5.61 o 5 -4 0 65.81 64.29 5.07 o 6 -4 0 7.54 4.80 1.60 o 1 -3 0 1371.06 1365.27 8.92 o 2 -3 0 555.06 566.39 6.77 o 3 -3 0 10.17 14.32 1.10 o 4 -3 0 338.17 345.11 3.78 o 5 -3 0 168.50 169.74 9.25 o 6 -3 0 34.14 36.28 3.80 o 1 -2 0 1687.03 1580.46 10.93 o 2 -2 0 355.15 359.37 2.90 o 3 -2 0 474.60 497.81 3.14 o 4 -2 0 161.44 173.58 3.45 o 5 -2 0 89.82 89.31 2.85 o 6 -2 0 83.53 75.87 4.65 o 7 -2 0 3.75 3.34 1.33 o 1 -1 0 2966.89 2987.12 21.41 o 2 -1 0 578.13 548.55 5.48 o 3 -1 0 90.88 91.13 1.94 o 4 -1 0 103.26 96.73 1.70 o 5 -1 0 39.83 39.83 1.57 o 6 -1 0 7.42 6.54 1.21 o 7 -1 0 93.78 104.99 6.41 o 1 0 0 200.08 173.26 4.49 o 2 0 0 484.47 525.38 4.78 o 3 0 0 127.17 121.06 1.99 o 4 0 0 254.53 276.14 11.09 o 5 0 0 189.24 177.12 3.87 o 6 0 0 8.82 8.78 1.23 o 7 0 0 18.54 21.48 3.36 o 1 1 0 2952.00 3000.21 21.26 o 2 1 0 569.80 532.52 4.56 o 3 1 0 90.67 86.59 3.43 o 4 1 0 108.65 107.13 2.79 o 5 1 0 38.27 38.29 1.68 o 6 1 0 7.91 8.88 1.03 o 7 1 0 92.25 102.02 4.07 o 1 2 0 1700.05 1618.51 13.32 o 2 2 0 349.42 357.08 5.92 o 3 2 0 483.26 500.85 8.46 o 4 2 0 160.31 176.10 5.55 o 5 2 0 90.50 90.90 3.13 o 6 2 0 88.40 88.14 2.79 o 7 2 0 3.86 1.94 0.96 o 1 3 0 1352.10 1367.25 7.91 o 2 3 0 550.24 546.69 7.77 o 4 3 0 340.86 338.65 7.73 o 5 3 0 165.65 173.31 4.31 o 6 3 0 34.17 31.42 2.31 o 1 4 0 347.29 361.70 3.04 o 2 4 0 784.55 816.91 4.13 o 3 4 0 401.68 421.00 7.70 o 4 4 0 272.00 266.36 7.12 o 5 4 0 67.88 70.44 3.00 o 6 4 0 7.65 7.67 2.01 o 1 5 0 506.03 523.69 7.53 o 2 5 0 474.58 480.53 3.54 o 3 5 0 63.46 58.50 3.17 o 4 5 0 374.22 382.84 9.54 o 5 5 0 103.69 103.88 3.67 o 6 5 0 7.76 6.56 1.00 o 0 6 0 1082.25 1104.94 10.32 o 1 6 0 129.47 143.55 2.21 o 2 6 0 4.16 3.10 0.43 o 3 6 0 198.30 196.88 5.70 o 4 6 0 172.93 172.46 6.03 o 5 6 0 33.96 35.43 2.27 o 6 6 0 45.60 46.82 2.45 o 1 7 0 697.29 738.93 8.50 o 2 7 0 157.69 151.78 4.73 o 3 7 0 205.59 180.28 6.06 o 4 7 0 81.03 88.49 4.48 o 5 7 0 26.34 21.50 1.75 o 0 8 0 909.40 962.71 11.36 o 1 8 0 162.82 146.52 3.38 o 2 8 0 30.11 28.54 2.23 o 3 8 0 73.78 77.33 4.00 o 4 8 0 3.43 3.84 0.97 o 5 8 0 12.34 13.21 1.30 o 1 9 0 201.30 215.77 5.74 o 2 9 0 40.57 42.10 2.85 o 3 9 0 14.02 12.48 1.57 o 4 9 0 26.25 26.67 1.76 o 0 10 0 38.89 33.64 2.93 o 1 10 0 134.81 130.16 3.81 o 2 10 0 110.65 111.50 5.60 o 3 10 0 121.43 118.19 5.27 o 1 11 0 6.87 8.97 1.92 o 2 11 0 40.73 37.17 2.41 o -3 -10 1 40.44 34.97 3.26 o -2 -10 1 9.41 9.59 1.75 o -1 -10 1 163.57 161.63 5.56 o -4 -9 1 11.97 14.14 2.34 o -3 -9 1 32.45 28.65 2.92 o -2 -9 1 7.15 10.85 1.70 o -1 -9 1 0.51 0.96 0.96 o 0 -9 1 160.25 158.08 4.60 o -5 -8 1 12.97 14.36 2.02 o -4 -8 1 28.08 33.93 3.29 o -3 -8 1 11.31 10.20 1.84 o -2 -8 1 198.12 183.94 6.04 o -1 -8 1 291.01 294.21 7.46 o 0 -8 1 58.42 51.17 2.47 o 5 -8 1 25.80 24.55 3.18 o -5 -7 1 143.00 147.74 7.36 o -4 -7 1 8.16 5.39 0.98 o -3 -7 1 122.61 116.78 5.24 o -2 -7 1 143.49 163.06 5.48 o -1 -7 1 93.01 104.40 3.85 o 0 -7 1 328.07 332.94 5.84 o 1 -7 1 501.61 506.91 5.71 o 4 -7 1 187.92 174.86 6.59 o 5 -7 1 49.69 42.73 3.72 o -6 -6 1 82.46 93.59 3.95 o -5 -6 1 46.22 48.76 2.68 o -4 -6 1 130.70 121.74 3.69 o -3 -6 1 242.20 247.45 4.64 o -2 -6 1 140.39 131.73 4.61 o -1 -6 1 26.09 26.11 1.92 o 0 -6 1 61.13 51.50 2.22 o 1 -6 1 156.30 163.95 3.00 o 2 -6 1 227.73 215.49 5.94 o 3 -6 1 241.79 234.72 6.62 o 4 -6 1 15.04 18.03 2.24 o 5 -6 1 42.42 40.00 3.43 o 6 -6 1 20.09 23.50 3.07 o -6 -5 1 75.72 79.12 3.60 o -5 -5 1 160.76 152.30 4.38 o -4 -5 1 11.59 12.64 1.38 o -3 -5 1 172.52 176.94 6.05 o -2 -5 1 135.77 133.72 2.84 o -1 -5 1 147.08 157.69 4.20 o 0 -5 1 819.96 868.14 9.40 o 1 -5 1 105.75 105.69 1.90 o 2 -5 1 781.40 835.95 7.62 o 3 -5 1 701.37 718.63 7.89 o 4 -5 1 351.49 346.02 9.32 o 5 -5 1 10.80 10.34 2.03 o 6 -5 1 26.48 27.45 3.12 o -6 -4 1 30.02 30.03 2.23 o -5 -4 1 1.58 1.70 1.65 o -4 -4 1 207.05 190.85 4.26 o -3 -4 1 392.45 368.36 12.65 o -2 -4 1 332.18 351.23 4.53 o 0 -4 1 343.00 381.13 5.31 o 1 -4 1 1484.68 1616.11 9.66 o 2 -4 1 254.71 245.69 3.99 o 3 -4 1 20.59 20.51 1.03 o 4 -4 1 68.77 70.22 3.89 o 5 -4 1 173.37 170.66 6.64 o 6 -4 1 16.18 14.69 2.60 o -6 -3 1 32.52 34.83 2.24 o -5 -3 1 163.45 157.63 4.92 o -4 -3 1 218.38 223.47 5.24 o -3 -3 1 537.24 551.28 4.34 o -2 -3 1 346.47 376.08 6.70 o -1 -3 1 899.34 982.09 15.16 o 0 -3 1 1770.06 1757.86 13.94 o 1 -3 1 42.37 53.34 1.00 o 2 -3 1 1412.31 1581.86 11.42 o 3 -3 1 437.93 455.25 4.71 o 4 -3 1 491.18 494.30 8.05 o 5 -3 1 26.18 26.83 2.75 o 6 -3 1 61.06 58.50 4.28 o -7 -2 1 120.16 119.16 6.70 o -6 -2 1 132.12 128.17 4.18 o -5 -2 1 136.83 146.29 4.81 o -4 -2 1 552.38 582.11 4.00 o -3 -2 1 174.98 166.83 1.85 o -2 -2 1 121.56 109.79 2.21 o -1 -2 1 531.17 515.20 2.44 o 0 -2 1 604.06 645.65 6.15 o 1 -2 1 3389.34 3440.22 25.42 o 2 -2 1 104.97 93.42 1.16 o 3 -2 1 146.24 135.33 1.81 o 4 -2 1 157.09 162.36 3.99 o 5 -2 1 353.50 368.77 17.10 o 6 -2 1 22.09 20.69 2.65 o 7 -2 1 6.10 3.51 1.67 o -7 -1 1 50.46 46.75 4.19 o -6 -1 1 14.02 10.88 1.29 o -5 -1 1 180.65 183.64 3.20 o -4 -1 1 204.18 187.95 4.78 o -3 -1 1 146.07 137.66 2.86 o -2 -1 1 458.81 459.76 6.48 o -1 -1 1 2640.64 2621.84 24.09 o 1 -1 1 398.48 396.98 2.79 o 2 -1 1 1007.50 1032.80 7.73 o 3 -1 1 700.21 774.79 10.90 o 4 -1 1 54.21 52.30 1.49 o 5 -1 1 144.51 138.95 2.78 o 6 -1 1 26.86 25.93 1.92 o 7 -1 1 35.06 31.66 3.86 o -7 0 1 0.15 2.24 1.53 o -6 0 1 299.41 299.89 6.95 o -5 0 1 101.94 96.37 2.34 o -4 0 1 721.34 743.53 10.09 o -3 0 1 324.43 331.90 4.36 o -2 0 1 917.34 1013.69 20.40 o -1 0 1 2255.90 2214.48 11.32 o 1 0 1 2426.77 2273.21 16.83 o 2 0 1 139.83 120.08 1.72 o 3 0 1 414.02 429.21 5.18 o 4 0 1 140.70 146.69 2.92 o 5 0 1 335.66 355.25 4.98 o 6 0 1 19.72 20.20 2.10 o 7 0 1 1.76 2.07 1.02 o -7 1 1 50.24 51.66 3.03 o -6 1 1 15.22 14.44 1.29 o -5 1 1 179.43 180.02 6.61 o -4 1 1 205.14 193.79 6.01 o -3 1 1 139.05 137.12 2.62 o -2 1 1 442.98 448.47 5.22 o -1 1 1 2640.78 2603.67 19.17 o 1 1 1 407.86 399.97 2.86 o 2 1 1 1009.72 1021.15 8.90 o 3 1 1 684.13 733.09 9.39 o 4 1 1 58.57 58.37 1.77 o 5 1 1 145.36 150.44 3.24 o 6 1 1 26.88 26.60 2.00 o 7 1 1 35.58 35.62 2.74 o -7 2 1 124.02 132.46 4.92 o -6 2 1 133.42 130.53 3.97 o -5 2 1 139.11 137.98 5.86 o -4 2 1 541.88 570.06 7.09 o -3 2 1 181.26 170.46 5.76 o -2 2 1 125.50 120.16 1.75 o -1 2 1 526.96 512.54 6.61 o 0 2 1 616.26 662.79 3.42 o 1 2 1 3401.43 3480.17 18.45 o 2 2 1 105.96 94.18 1.33 o 3 2 1 145.56 135.07 2.47 o 4 2 1 156.09 158.64 2.98 o 5 2 1 360.43 368.51 5.01 o 6 2 1 22.80 27.06 1.61 o 7 2 1 5.29 2.56 1.03 o -7 3 1 6.83 4.20 1.47 o -6 3 1 33.32 35.59 2.35 o -5 3 1 160.57 159.40 6.17 o -4 3 1 219.06 236.62 6.49 o -2 3 1 332.77 378.60 6.54 o -1 3 1 899.88 980.63 3.98 o 0 3 1 1765.62 1746.57 9.64 o 1 3 1 45.87 57.09 1.08 o 2 3 1 1412.42 1605.31 9.18 o 3 3 1 429.84 456.94 6.52 o 4 3 1 491.27 489.87 6.08 o 5 3 1 26.84 28.24 1.65 o 6 3 1 59.63 57.85 2.48 o -6 4 1 29.48 27.22 2.08 o -5 4 1 1.48 0.26 1.03 o -4 4 1 212.29 203.74 6.39 o -3 4 1 385.80 377.80 7.45 o -2 4 1 330.03 348.67 2.94 o -1 4 1 71.24 79.98 1.44 o 0 4 1 349.22 384.16 3.10 o 1 4 1 1488.33 1629.68 14.17 o 2 4 1 260.02 253.52 2.44 o 3 4 1 21.90 24.77 2.25 o 4 4 1 66.53 66.78 2.27 o 5 4 1 177.58 175.11 3.78 o 6 4 1 16.20 15.66 1.31 o -6 5 1 73.62 77.90 3.97 o -5 5 1 158.28 160.70 6.54 o -4 5 1 11.25 11.88 1.81 o -3 5 1 174.08 176.50 5.36 o -2 5 1 135.25 134.18 1.99 o -1 5 1 146.62 152.72 2.68 o 0 5 1 817.12 879.18 10.17 o 1 5 1 100.14 96.87 2.85 o 2 5 1 780.00 842.75 9.39 o 3 5 1 712.27 737.32 18.49 o 4 5 1 348.26 342.48 5.34 o 5 5 1 10.43 9.64 1.04 o 6 5 1 24.85 24.20 1.72 o -6 6 1 80.85 95.27 3.97 o -5 6 1 45.12 43.91 3.50 o -4 6 1 137.45 132.45 5.47 o -3 6 1 235.52 241.62 6.55 o -2 6 1 136.82 130.96 2.36 o -1 6 1 27.11 27.21 0.88 o 0 6 1 61.25 52.14 1.34 o 1 6 1 156.60 166.88 3.01 o 2 6 1 225.34 235.87 5.31 o 3 6 1 246.29 232.54 3.82 o 4 6 1 15.26 19.61 1.53 o 5 6 1 41.97 40.95 2.32 o 6 6 1 19.57 20.08 1.69 o -5 7 1 141.90 156.84 6.61 o -4 7 1 8.06 6.05 1.44 o -3 7 1 127.39 117.08 4.88 o -2 7 1 141.65 156.22 5.09 o -1 7 1 93.45 100.53 1.79 o 0 7 1 326.57 331.94 3.13 o 1 7 1 503.68 513.11 4.84 o 2 7 1 17.02 14.52 1.03 o 3 7 1 82.29 85.74 2.51 o 4 7 1 193.44 185.06 3.95 o 5 7 1 49.22 53.12 2.45 o -5 8 1 12.55 10.29 2.04 o -4 8 1 25.93 31.27 2.89 o -3 8 1 10.81 9.72 1.55 o -2 8 1 196.68 201.11 5.99 o -1 8 1 283.46 285.49 8.52 o 0 8 1 58.42 54.70 1.41 o 1 8 1 26.96 23.16 1.18 o 2 8 1 204.48 197.29 3.53 o 3 8 1 142.30 136.14 3.55 o 4 8 1 133.80 138.74 3.60 o 5 8 1 27.46 28.13 1.87 o -4 9 1 12.06 10.54 2.16 o -3 9 1 31.70 27.72 2.60 o -2 9 1 5.87 7.47 1.86 o -1 9 1 0.50 0.65 0.43 o 0 9 1 161.22 163.77 3.91 o 1 9 1 144.15 151.43 4.58 o 2 9 1 18.11 17.45 1.76 o 3 9 1 17.79 17.17 1.90 o 4 9 1 216.48 203.80 5.85 o -3 10 1 39.79 43.40 3.43 o -2 10 1 9.17 6.62 1.40 o -1 10 1 158.69 167.12 5.82 o 0 10 1 24.87 20.50 1.65 o 1 10 1 36.92 34.92 3.12 o 2 10 1 100.85 106.73 3.80 o 3 10 1 83.67 79.79 3.63 o -2 11 1 56.16 55.25 4.00 o 0 11 1 38.14 40.21 2.39 o 1 11 1 5.47 2.72 2.19 o 2 11 1 9.88 9.19 2.04 o -2 -11 2 31.00 31.92 2.99 o -3 -10 2 18.43 18.97 2.49 o -2 -10 2 120.43 121.90 5.48 o -1 -10 2 90.08 97.83 4.46 o -4 -9 2 48.60 47.49 4.06 o -3 -9 2 52.97 55.35 3.99 o -2 -9 2 6.38 7.62 1.55 o -1 -9 2 56.47 57.66 3.32 o 0 -9 2 294.75 286.54 6.26 o -5 -8 2 80.02 80.01 5.35 o -4 -8 2 5.63 7.13 1.14 o -3 -8 2 16.35 13.39 2.00 o -2 -8 2 533.54 536.43 10.34 o -1 -8 2 214.41 218.45 6.40 o 0 -8 2 52.61 54.16 2.72 o -5 -7 2 2.94 2.65 0.99 o -4 -7 2 133.02 127.68 4.58 o -3 -7 2 84.46 79.87 2.79 o -2 -7 2 46.87 54.04 3.24 o -1 -7 2 854.55 857.96 11.14 o 0 -7 2 407.64 428.56 6.85 o 1 -7 2 70.05 61.14 2.20 o 4 -7 2 6.85 6.10 1.63 o 5 -7 2 170.45 163.30 7.22 o -6 -6 2 10.60 8.36 2.46 o -5 -6 2 35.50 42.45 2.54 o -4 -6 2 194.40 192.39 5.32 o -3 -6 2 15.36 15.01 1.22 o -2 -6 2 273.07 259.64 6.52 o -1 -6 2 240.66 249.96 5.64 o 0 -6 2 35.78 32.92 1.93 o 1 -6 2 144.32 143.20 3.15 o 2 -6 2 136.91 138.05 2.40 o 3 -6 2 48.81 53.89 3.47 o 4 -6 2 74.89 62.74 4.04 o 5 -6 2 37.72 32.89 3.24 o -6 -5 2 47.70 53.62 2.95 o -5 -5 2 112.00 113.72 3.73 o -4 -5 2 628.22 638.29 9.17 o -3 -5 2 718.79 732.85 7.34 o -2 -5 2 19.20 19.57 1.14 o -1 -5 2 71.73 69.57 2.93 o 0 -5 2 385.67 373.19 6.01 o 1 -5 2 404.17 443.38 5.79 o 2 -5 2 77.48 83.36 1.96 o 3 -5 2 523.12 497.66 9.51 o 4 -5 2 26.78 23.44 2.50 o 5 -5 2 213.98 210.42 7.61 o 6 -5 2 12.40 11.20 2.52 o -6 -4 2 14.74 15.70 1.69 o -5 -4 2 200.37 210.08 6.19 o -4 -4 2 630.78 621.49 8.34 o -3 -4 2 70.39 62.94 0.98 o -2 -4 2 10.18 8.06 0.51 o -1 -4 2 64.61 62.02 2.53 o 0 -4 2 31.23 31.71 1.60 o 2 -4 2 214.36 219.66 2.98 o 3 -4 2 105.50 101.62 2.15 o 4 -4 2 469.00 467.98 11.09 o 5 -4 2 21.14 14.96 2.26 o 6 -4 2 53.23 48.18 4.16 o -7 -3 2 129.35 131.08 4.78 o -6 -3 2 55.00 51.80 3.63 o -5 -3 2 412.63 407.44 6.65 o -4 -3 2 610.46 624.43 7.48 o -3 -3 2 1122.48 1157.78 9.71 o -2 -3 2 48.15 48.95 1.59 o -1 -3 2 922.09 1012.88 9.66 o 0 -3 2 630.00 585.58 6.88 o 1 -3 2 730.43 793.15 7.83 o 2 -3 2 371.49 355.76 6.90 o 3 -3 2 294.53 281.68 3.76 o 4 -3 2 36.20 35.53 2.22 o 5 -3 2 92.64 94.25 5.01 o 6 -3 2 44.51 39.28 3.80 o -7 -2 2 28.16 23.90 3.21 o -6 -2 2 32.38 29.60 2.02 o -5 -2 2 576.13 588.28 13.97 o -4 -2 2 235.54 237.85 4.35 o -3 -2 2 283.82 287.70 4.32 o -2 -2 2 139.61 128.57 2.37 o -1 -2 2 1178.41 1145.20 7.03 o 0 -2 2 888.90 881.03 8.52 o 1 -2 2 269.47 251.85 2.96 o 2 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48.03 1.88 o -3 1 2 301.98 293.00 3.95 o -2 1 2 67.47 64.13 1.68 o -1 1 2 1351.21 1273.69 7.49 o 0 1 2 184.03 200.46 4.62 o 1 1 2 605.73 616.90 4.03 o 2 1 2 4.36 2.99 0.40 o 3 1 2 197.01 210.83 3.01 o 4 1 2 42.21 43.11 1.60 o 5 1 2 67.02 63.59 2.16 o 6 1 2 26.49 28.60 2.16 o -7 2 2 26.73 29.25 3.43 o -6 2 2 31.74 32.48 3.45 o -5 2 2 580.13 616.82 15.98 o -4 2 2 238.58 244.07 4.34 o -3 2 2 284.91 288.21 3.72 o -2 2 2 133.53 125.86 2.02 o -1 2 2 1180.26 1141.95 12.72 o 0 2 2 899.16 898.78 6.21 o 1 2 2 265.49 254.31 2.91 o 2 2 2 334.86 360.33 4.32 o 3 2 2 114.90 110.04 3.01 o 4 2 2 355.72 361.63 4.55 o 5 2 2 24.40 23.31 1.48 o 6 2 2 21.58 19.38 1.55 o -7 3 2 130.28 131.85 7.00 o -6 3 2 51.71 46.37 3.76 o -5 3 2 414.66 416.70 9.95 o -4 3 2 607.61 627.48 6.61 o -3 3 2 1116.48 1185.56 10.02 o -2 3 2 48.19 49.45 1.44 o -1 3 2 913.44 1022.61 5.54 o 0 3 2 623.96 579.82 5.81 o 1 3 2 730.70 806.14 7.65 o 2 3 2 362.25 347.82 4.19 o 3 3 2 294.59 279.53 3.66 o 4 3 2 36.76 32.38 1.55 o 5 3 2 96.47 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101.57 105.26 5.75 o -1 -6 10 0.51 0.26 0.94 o 0 -6 10 243.09 248.37 8.26 o 1 -6 10 26.35 29.85 2.93 o 2 -6 10 161.08 166.63 6.74 o -4 -5 10 12.69 11.66 2.52 o -3 -5 10 54.06 50.33 4.14 o -2 -5 10 154.06 165.34 7.04 o -1 -5 10 50.28 45.70 3.62 o 0 -5 10 116.14 111.04 5.58 o 1 -5 10 160.51 170.28 6.80 o 2 -5 10 16.48 18.35 2.44 o -4 -4 10 61.23 54.93 4.38 o -3 -4 10 174.07 173.09 7.35 o -2 -4 10 1.62 1.40 0.94 o -1 -4 10 67.60 62.34 4.13 o 0 -4 10 70.31 72.29 4.44 o 1 -4 10 27.62 27.31 3.01 o 2 -4 10 166.07 172.46 6.83 o 3 -4 10 73.98 78.81 4.82 o -5 -3 10 34.00 35.52 3.70 o -4 -3 10 67.26 65.35 4.68 o -3 -3 10 157.48 161.92 6.88 o -2 -3 10 89.36 84.78 4.84 o -1 -3 10 20.91 17.06 2.26 o 0 -3 10 68.25 71.55 4.39 o 1 -3 10 171.88 170.16 6.73 o 2 -3 10 23.08 20.96 2.70 o 3 -3 10 53.28 49.23 3.85 o -5 -2 10 50.08 47.54 4.01 o -4 -2 10 158.79 165.92 6.97 o -3 -2 10 101.69 97.31 5.13 o -2 -2 10 133.85 134.37 6.00 o -1 -2 10 205.78 213.40 7.31 o 0 -2 10 137.16 133.91 5.85 o 1 -2 10 3.67 2.59 1.36 o 2 -2 10 110.86 118.66 5.84 o 3 -2 10 65.82 68.25 4.62 o -5 -1 10 51.67 55.48 4.18 o -4 -1 10 74.84 75.96 3.01 o -3 -1 10 66.29 63.35 2.61 o -2 -1 10 256.78 261.23 4.91 o -1 -1 10 12.12 9.45 1.55 o 0 -1 10 53.74 45.07 2.17 o 1 -1 10 139.06 140.73 6.01 o 2 -1 10 1.73 1.80 0.91 o 3 -1 10 125.95 122.01 4.29 o -5 0 10 39.28 40.07 4.15 o -4 0 10 147.49 152.59 5.92 o -3 0 10 51.06 52.61 2.91 o -2 0 10 23.30 20.74 1.67 o -1 0 10 65.26 69.46 2.75 o 0 0 10 171.15 176.09 6.73 o 1 0 10 32.54 34.07 2.97 o 2 0 10 91.16 91.32 3.64 o 3 0 10 14.99 13.61 1.72 o -5 1 10 48.76 57.06 7.92 o -4 1 10 75.49 71.91 3.07 o -3 1 10 69.16 66.75 2.78 o -2 1 10 255.68 251.09 5.20 o -1 1 10 12.41 8.26 1.02 o 0 1 10 52.45 45.08 4.00 o 1 1 10 139.81 146.45 4.45 o 2 1 10 1.77 3.04 1.96 o 3 1 10 123.77 126.83 9.21 o -5 2 10 50.59 58.36 2.93 o -4 2 10 154.39 155.66 4.43 o -3 2 10 103.38 108.87 3.62 o -2 2 10 137.03 140.04 4.04 o -1 2 10 208.74 218.34 4.18 o 0 2 10 140.83 143.10 4.33 o 1 2 10 4.14 2.71 1.22 o 2 2 10 107.55 107.68 4.08 o 3 2 10 65.27 68.80 4.37 o -5 3 10 31.86 30.02 3.27 o -4 3 10 67.62 65.21 4.46 o -3 3 10 157.78 166.12 6.59 o -2 3 10 90.57 90.81 3.38 o -1 3 10 20.92 21.77 1.96 o 0 3 10 65.51 68.19 3.12 o 1 3 10 171.89 171.50 5.00 o 2 3 10 23.08 24.71 2.16 o 3 3 10 52.87 54.50 3.26 o -4 4 10 62.90 70.98 4.80 o -3 4 10 173.84 179.97 4.77 o -2 4 10 1.88 2.28 0.79 o -1 4 10 65.99 67.04 2.48 o 0 4 10 70.97 70.26 3.20 o 1 4 10 29.21 31.75 2.37 o 2 4 10 168.25 172.54 5.32 o 3 4 10 71.80 72.20 3.71 o -4 5 10 13.26 10.78 2.27 o -3 5 10 51.76 52.72 2.73 o -2 5 10 155.31 166.55 4.22 o -1 5 10 49.91 46.43 2.47 o 0 5 10 113.61 115.83 4.08 o 1 5 10 159.33 163.15 5.82 o 2 5 10 16.46 18.01 2.13 o -3 6 10 141.56 145.98 7.08 o -2 6 10 99.58 99.83 3.04 o -1 6 10 0.24 2.00 0.93 o 0 6 10 239.30 245.71 6.00 o 1 6 10 27.70 26.87 2.25 o 2 6 10 161.16 162.10 5.40 o -3 7 10 46.42 53.55 4.63 o -2 7 10 114.58 121.90 4.36 o -1 7 10 60.83 56.00 2.43 o 0 7 10 43.34 45.42 2.26 o 1 7 10 79.51 79.89 4.77 o -2 -6 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8.43 o 3 -1 11 80.36 86.53 5.60 o -5 0 11 24.14 21.79 1.96 o -4 0 11 0.02 0.81 0.56 o -3 0 11 4.24 3.49 0.84 o -2 0 11 246.10 255.24 5.33 o -1 0 11 42.80 40.36 3.42 o 0 0 11 6.14 4.93 2.07 o 1 0 11 167.03 163.33 6.97 o 2 0 11 34.05 38.55 2.79 o 3 0 11 174.35 185.61 5.64 o -5 1 11 8.66 9.00 1.42 o -4 1 11 22.24 22.57 1.88 o -3 1 11 152.67 152.27 4.37 o -2 1 11 3.71 2.75 1.30 o -1 1 11 78.24 68.05 2.92 o 0 1 11 23.82 22.53 2.75 o 1 1 11 124.38 127.75 4.55 o 2 1 11 227.70 230.76 6.10 o 3 1 11 76.98 82.38 3.88 o -4 2 11 47.82 43.51 2.66 o -3 2 11 32.82 34.06 2.25 o -2 2 11 191.47 193.02 6.28 o -1 2 11 149.91 155.72 4.49 o 0 2 11 32.56 30.69 2.27 o 1 2 11 152.69 147.55 9.10 o 2 2 11 44.50 46.62 3.74 o 3 2 11 54.92 55.20 3.42 o -4 3 11 22.21 23.81 1.95 o -3 3 11 159.18 159.93 4.64 o -2 3 11 1.14 0.94 0.87 o -1 3 11 48.95 47.94 2.24 o 0 3 11 158.08 146.51 4.93 o 1 3 11 36.23 33.71 2.62 o 2 3 11 175.84 196.42 11.34 o -4 4 11 76.78 76.04 5.11 o -3 4 11 24.85 26.83 2.05 o -2 4 11 89.68 95.38 4.77 o -1 4 11 57.88 58.62 2.47 o 0 4 11 9.49 7.09 1.51 o 1 4 11 150.93 160.01 5.19 o 2 4 11 17.08 14.76 2.00 o -3 5 11 146.36 158.45 7.29 o -2 5 11 20.13 20.43 1.85 o -1 5 11 122.81 126.96 3.71 o 0 5 11 144.03 150.33 4.45 o 1 5 11 17.91 20.18 2.09 o -2 6 11 155.38 155.63 3.95 o -1 6 11 13.74 12.56 1.30 o 0 6 11 10.72 9.51 1.34 o -2 -5 12 10.07 8.64 2.68 o -1 -5 12 181.90 192.85 8.09 o -3 -4 12 93.78 94.82 6.07 o -2 -4 12 56.75 51.19 4.44 o -1 -4 12 13.50 10.89 2.52 o 0 -4 12 40.08 46.80 4.07 o 1 -4 12 120.10 119.31 6.38 o -3 -3 12 113.35 122.92 6.59 o -2 -3 12 231.53 244.80 9.16 o -1 -3 12 21.57 17.61 2.66 o 0 -3 12 24.58 23.59 3.35 o 1 -3 12 91.82 94.89 5.76 o -3 -2 12 92.19 95.50 5.76 o -2 -2 12 101.85 106.06 5.88 o -1 -2 12 44.24 43.50 3.92 o 0 -2 12 158.09 169.99 7.48 o 1 -2 12 24.84 32.30 3.68 o -4 -1 12 56.99 54.50 4.31 o -3 -1 12 58.58 56.93 4.35 o -2 -1 12 142.73 140.77 6.70 o -1 -1 12 82.70 87.25 5.35 o 0 -1 12 19.48 19.58 2.81 o 1 -1 12 96.09 91.84 5.60 o 2 -1 12 57.94 51.80 4.34 o -4 0 12 0.28 2.09 1.55 o -3 0 12 64.04 60.16 4.41 o -2 0 12 125.22 136.45 6.58 o -1 0 12 69.69 80.62 5.18 o 0 0 12 211.74 207.13 8.17 o 1 0 12 2.63 4.20 1.50 o 2 0 12 29.56 24.30 3.12 o -4 1 12 56.93 53.86 2.86 o -3 1 12 58.28 61.11 3.46 o -2 1 12 144.10 145.77 4.42 o -1 1 12 83.01 96.19 5.86 o 0 1 12 19.67 19.25 3.43 o 1 1 12 92.35 91.16 4.12 o 2 1 12 58.79 54.92 5.15 o -3 2 12 94.14 101.46 9.93 o -2 2 12 100.54 104.09 3.86 o -1 2 12 43.35 43.50 2.55 o 0 2 12 159.83 167.30 4.14 o 1 2 12 25.16 28.81 2.48 o -3 3 12 112.50 121.43 4.30 o -2 3 12 231.06 238.77 7.52 o -1 3 12 22.55 24.34 2.04 o 0 3 12 24.70 25.71 1.81 o 1 3 12 87.76 83.80 4.17 o -3 4 12 92.09 97.77 4.53 o -2 4 12 56.01 55.34 3.47 o -1 4 12 14.01 14.22 1.40 o 0 4 12 39.91 41.61 2.28 o 1 4 12 121.06 123.65 4.82 o -2 5 12 9.81 6.94 1.46 o -1 5 12 178.66 195.57 4.66 o 0 5 12 3.79 2.34 1.95 o -2 -2 13 11.44 14.62 3.01 o -1 -2 13 171.35 178.84 8.04 o 0 -2 13 29.74 26.80 3.45 o -2 -1 13 77.34 70.59 5.10 o -1 -1 13 34.97 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