#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:16:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/04/2210424.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210424_Fobs loop_ _publ_author_name 'Li, Hong-Song' 'Li, Song-Lin' 'Hou, Jian-Feng' _publ_section_title ; Diaquabis[2-(1-pyridyl)butanedioato-\kO]copper(II) ; _journal_coeditor_code XU2027 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2143 _journal_page_last m2144 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.303 _cell_angle_gamma 90.000 _cell_length_a 5.1090 _cell_length_b 19.1870 _cell_length_c 10.2900 _exptl_crystal_F_000 502.00 _reflns_d_resolution_high 0.7991 _cod_data_source_file xu2027Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 224.15 193.94 3.58 o 4 0 0 5511.10 6190.40 41.20 o 1 1 0 4239.43 4102.16 24.88 o 2 1 0 9.12 11.61 2.22 o 3 1 0 465.14 446.91 4.70 o 4 1 0 0.67 2.44 3.20 o 5 1 0 452.26 478.20 6.44 o 0 2 0 6439.38 6438.85 159.41 o 1 2 0 7557.89 7451.82 22.95 o 2 2 0 1611.64 2053.01 70.33 o 3 2 0 771.40 904.46 11.24 o 4 2 0 804.24 802.67 5.96 o 5 2 0 5.55 8.77 1.58 o 1 3 0 5662.79 5602.21 40.52 o 2 3 0 14.00 14.04 1.23 o 3 3 0 2242.64 2167.06 27.95 o 4 3 0 28.98 32.38 1.62 o 5 3 0 214.95 239.61 4.81 o 6 3 0 78.12 82.95 4.89 o 0 4 0 4679.73 4196.27 16.57 o 1 4 0 8117.19 8172.14 29.69 o 2 4 0 468.28 450.32 5.81 o 3 4 0 646.59 673.16 4.82 o 4 4 0 1066.51 1034.39 9.37 o 5 4 0 37.27 40.14 2.44 o 6 4 0 31.52 30.04 3.58 o 1 5 0 855.42 797.91 11.83 o 2 5 0 41.93 54.96 1.18 o 3 5 0 195.58 169.87 3.10 o 4 5 0 10.31 9.32 1.19 o 5 5 0 790.96 773.32 27.46 o 6 5 0 25.92 25.24 3.58 o 0 6 0 836.61 796.75 16.53 o 1 6 0 3066.93 3208.13 36.01 o 2 6 0 197.34 164.36 6.49 o 3 6 0 277.97 292.17 4.72 o 4 6 0 721.99 723.67 18.32 o 5 6 0 107.37 112.72 5.30 o 6 6 0 11.29 11.75 2.99 o 1 7 0 178.48 154.79 3.49 o 2 7 0 11.44 13.42 1.95 o 3 7 0 146.67 143.35 3.47 o 4 7 0 0.18 0.93 1.85 o 5 7 0 212.22 223.20 8.34 o 0 8 0 17.05 22.66 1.21 o 1 8 0 322.16 323.00 4.69 o 2 8 0 4839.11 5188.16 36.74 o 3 8 0 21.92 22.88 2.43 o 4 8 0 551.57 548.22 29.18 o 5 8 0 56.12 61.99 3.02 o 1 9 0 3620.82 3549.53 41.25 o 2 9 0 35.53 42.86 1.21 o 3 9 0 1737.24 1789.68 27.08 o 4 9 0 9.21 6.21 1.79 o 5 9 0 651.82 661.72 12.01 o 0 10 0 2441.72 2730.58 27.49 o 1 10 0 0.54 7.67 3.69 o 2 10 0 2040.82 2075.21 20.23 o 3 10 0 14.26 13.48 2.56 o 4 10 0 424.65 394.50 6.32 o 5 10 0 0.06 0.69 1.89 o 1 11 0 1772.65 1783.30 15.41 o 2 11 0 0.02 -0.73 1.00 o 3 11 0 538.40 565.44 16.20 o 4 11 0 2.27 2.54 2.07 o 5 11 0 581.43 558.77 40.77 o 0 12 0 136.42 125.05 5.70 o 1 12 0 83.96 79.07 5.56 o 2 12 0 512.29 475.28 10.45 o 3 12 0 5.79 5.60 1.76 o 4 12 0 336.69 333.11 5.89 o 5 12 0 15.48 15.16 2.28 o 1 13 0 1850.57 1874.60 13.35 o 2 13 0 59.96 61.30 6.42 o 3 13 0 1145.94 1115.74 10.70 o 4 13 0 7.82 5.01 3.35 o 5 13 0 230.20 255.65 5.82 o 0 14 0 463.87 455.51 7.70 o 1 14 0 466.38 438.43 3.59 o 2 14 0 2061.69 2068.47 64.27 o 3 14 0 82.94 78.20 3.06 o 4 14 0 367.10 350.69 27.56 o 5 14 0 1.94 2.78 2.11 o 1 15 0 6.17 7.46 1.16 o 2 15 0 36.96 34.92 3.07 o 3 15 0 9.19 7.15 1.88 o 4 15 0 0.01 0.52 1.71 o 0 16 0 1312.45 1350.53 47.07 o 1 16 0 721.64 766.27 5.43 o 2 16 0 30.45 30.98 6.70 o 3 16 0 55.40 57.20 2.78 o 4 16 0 245.46 260.98 6.27 o 1 17 0 1444.01 1471.49 13.12 o 2 17 0 0.00 -0.28 2.07 o 3 17 0 169.98 180.94 4.73 o 4 17 0 0.88 -0.06 1.72 o 0 18 0 1957.26 2046.65 75.09 o 1 18 0 62.39 71.58 2.34 o 2 18 0 16.57 16.57 2.07 o 3 18 0 21.25 20.41 2.23 o 4 18 0 284.70 290.17 6.32 o 1 19 0 228.47 237.26 6.04 o 2 19 0 34.91 30.15 3.68 o 3 19 0 168.36 163.85 4.59 o 0 20 0 1551.94 1731.59 17.59 o 1 20 0 59.08 57.33 4.50 o 2 20 0 21.53 20.68 2.25 o 3 20 0 1.80 1.21 1.90 o 1 21 0 312.11 295.32 5.55 o 2 21 0 10.72 11.00 2.66 o 3 21 0 160.08 161.47 6.93 o 0 22 0 1163.31 1278.00 16.84 o 1 22 0 232.28 252.41 5.28 o 2 22 0 14.95 18.90 3.02 o 1 23 0 202.16 235.39 6.94 o -5 0 1 432.04 453.47 8.63 o -3 0 1 2620.26 2697.03 78.98 o -1 0 1 35.27 62.82 2.43 o 1 0 1 9936.78 10828.24 58.14 o 3 0 1 1772.24 1926.99 16.71 o 5 0 1 406.54 404.32 8.67 o -5 1 1 20.38 24.65 3.05 o -4 1 1 1753.13 1816.84 19.35 o -3 1 1 8.11 9.08 1.80 o -2 1 1 848.07 771.83 10.68 o -1 1 1 2063.83 1996.24 19.00 o 0 1 1 579.51 567.31 9.06 o 1 1 1 2728.27 2750.01 61.01 o 2 1 1 2671.60 2676.14 93.13 o 3 1 1 0.64 2.30 1.33 o 4 1 1 169.73 164.52 3.63 o 5 1 1 32.23 31.77 1.88 o -5 2 1 1038.01 1073.40 13.75 o -4 2 1 30.70 32.75 1.30 o -3 2 1 1689.24 1764.94 16.89 o -2 2 1 159.78 177.33 6.80 o -1 2 1 8198.43 8012.50 74.78 o 0 2 1 190.26 231.23 12.09 o 1 2 1 3319.72 3128.26 17.96 o 2 2 1 613.29 625.80 8.62 o 3 2 1 1041.31 992.65 12.69 o 4 2 1 46.22 40.67 5.58 o 5 2 1 114.58 121.74 3.21 o 6 2 1 25.92 24.95 3.41 o -5 3 1 204.31 206.85 10.62 o -4 3 1 1038.19 1068.86 8.83 o -3 3 1 366.66 405.19 15.68 o -2 3 1 1196.83 1086.69 28.21 o -1 3 1 967.75 1058.73 16.92 o 0 3 1 13869.16 12978.79 52.86 o 1 3 1 4376.04 4200.01 80.87 o 2 3 1 1256.21 1213.98 21.08 o 3 3 1 1.59 0.42 1.29 o 4 3 1 2030.64 1961.88 13.19 o 5 3 1 5.34 6.84 1.38 o 6 3 1 189.01 184.03 6.83 o -6 4 1 25.10 19.96 3.28 o -5 4 1 78.71 83.56 3.01 o -4 4 1 153.65 154.24 2.58 o -3 4 1 98.03 75.88 3.41 o -2 4 1 486.39 480.71 7.74 o -1 4 1 5.82 11.54 0.88 o 0 4 1 361.65 343.21 10.03 o 1 4 1 650.35 515.88 7.67 o 2 4 1 751.28 772.96 10.92 o 3 4 1 323.91 370.22 15.10 o 4 4 1 2.68 4.74 1.19 o 5 4 1 353.41 391.03 35.70 o -6 5 1 138.25 153.89 6.17 o -5 5 1 46.12 51.28 3.81 o -4 5 1 934.54 966.35 8.39 o -3 5 1 261.73 330.32 4.33 o -2 5 1 418.55 365.95 8.32 o 0 5 1 8479.04 8150.29 55.39 o 1 5 1 258.27 257.80 16.27 o 2 5 1 591.17 551.99 13.57 o 3 5 1 0.99 0.85 1.05 o 4 5 1 326.43 348.89 4.41 o 5 5 1 17.61 18.29 2.21 o -6 6 1 0.80 -0.59 2.43 o -5 6 1 165.71 154.20 3.93 o -4 6 1 1.17 2.28 1.51 o -3 6 1 2683.41 2856.39 39.42 o -2 6 1 104.42 102.31 4.21 o -1 6 1 222.44 179.48 3.52 o 0 6 1 129.99 161.63 3.20 o 1 6 1 9207.96 8884.69 65.84 o 2 6 1 49.69 54.94 1.27 o 3 6 1 361.94 370.93 11.63 o 4 6 1 171.20 168.65 3.88 o 5 6 1 851.68 884.88 31.87 o -6 7 1 23.60 20.62 3.28 o -5 7 1 125.25 124.07 7.50 o -4 7 1 466.88 456.37 5.94 o -3 7 1 5.10 7.76 1.15 o -2 7 1 11.72 7.83 0.66 o -1 7 1 147.91 164.36 2.92 o 0 7 1 2644.35 2621.96 8.82 o 1 7 1 450.05 498.27 12.08 o 2 7 1 520.46 473.47 8.54 o 3 7 1 37.88 46.81 1.68 o 4 7 1 662.27 678.34 27.23 o 5 7 1 0.02 -1.47 1.81 o -5 8 1 439.57 419.35 13.43 o -4 8 1 23.46 21.95 2.04 o -3 8 1 1667.23 1648.89 24.26 o -2 8 1 261.94 287.38 9.90 o -1 8 1 2963.61 3057.10 42.70 o 0 8 1 465.64 482.00 6.55 o 1 8 1 3202.34 3186.78 32.93 o 2 8 1 20.97 19.32 1.65 o 3 8 1 225.04 231.61 7.30 o 4 8 1 148.70 138.60 9.67 o 5 8 1 601.16 587.77 54.00 o -5 9 1 7.68 7.73 1.88 o -4 9 1 1118.83 1120.65 11.60 o -3 9 1 18.98 27.96 2.53 o -2 9 1 1155.83 1147.47 7.82 o -1 9 1 348.34 372.44 5.93 o 0 9 1 1085.73 1166.29 12.35 o 1 9 1 539.34 604.93 4.68 o 2 9 1 470.78 428.38 12.87 o 3 9 1 0.16 1.07 1.33 o 4 9 1 369.90 368.64 30.18 o 5 9 1 7.97 8.84 2.16 o -5 10 1 90.04 89.82 3.38 o -4 10 1 66.56 60.27 2.89 o -3 10 1 900.82 875.15 17.99 o -2 10 1 113.07 94.96 3.87 o -1 10 1 25.33 16.39 0.89 o 0 10 1 188.99 210.89 2.15 o 1 10 1 2939.66 2933.76 25.14 o 2 10 1 117.67 105.49 4.62 o 3 10 1 33.82 40.69 1.74 o 4 10 1 0.67 2.97 1.72 o 5 10 1 780.60 735.47 41.21 o -5 11 1 27.53 24.37 2.59 o -4 11 1 1763.43 1756.39 48.40 o -3 11 1 33.38 42.60 7.76 o -2 11 1 2105.94 2197.48 11.01 o -1 11 1 23.43 24.50 3.22 o 0 11 1 2514.88 2453.68 31.97 o 1 11 1 144.91 140.50 2.88 o 2 11 1 2175.20 2184.39 23.63 o 3 11 1 0.06 0.05 1.52 o 4 11 1 214.09 224.20 5.76 o 5 11 1 6.12 6.82 2.12 o -5 12 1 262.60 271.35 29.07 o -4 12 1 237.09 218.79 11.00 o -3 12 1 1442.37 1440.95 12.38 o -2 12 1 55.59 57.48 1.86 o -1 12 1 608.36 616.15 13.03 o 0 12 1 444.36 485.57 14.00 o 1 12 1 2218.65 2168.77 22.93 o 2 12 1 33.32 28.90 1.41 o 3 12 1 26.91 35.56 5.66 o 4 12 1 84.36 85.03 3.39 o 5 12 1 321.67 297.35 29.95 o -5 13 1 70.36 56.56 3.10 o -4 13 1 128.22 128.56 7.91 o -3 13 1 80.86 82.47 2.97 o -2 13 1 126.89 131.06 3.31 o -1 13 1 19.60 27.17 2.13 o 0 13 1 1326.41 1332.60 10.53 o 1 13 1 343.59 339.90 3.15 o 2 13 1 40.82 48.78 2.49 o 3 13 1 23.36 23.33 2.17 o 4 13 1 540.23 530.75 7.68 o 5 13 1 10.00 6.97 2.17 o -5 14 1 158.66 158.39 7.63 o -4 14 1 13.58 12.62 2.05 o -3 14 1 222.39 207.55 8.04 o -2 14 1 2.73 2.87 1.66 o -1 14 1 1018.53 1052.49 15.07 o 0 14 1 43.36 50.23 5.79 o 1 14 1 924.92 896.65 10.02 o 2 14 1 22.18 23.96 2.44 o 3 14 1 445.38 466.76 8.42 o 4 14 1 188.54 163.50 4.48 o -4 15 1 261.73 269.43 16.45 o -3 15 1 25.19 22.54 2.19 o -2 15 1 269.19 261.15 4.74 o -1 15 1 171.02 164.46 3.86 o 0 15 1 1376.46 1471.76 11.62 o 1 15 1 53.58 56.84 2.57 o 2 15 1 31.35 37.36 2.29 o 3 15 1 142.97 140.29 3.96 o 4 15 1 192.91 204.48 5.04 o -4 16 1 17.97 13.95 2.11 o -3 16 1 650.29 654.89 8.22 o -2 16 1 25.27 27.33 2.17 o -1 16 1 94.79 97.06 1.95 o 0 16 1 3.64 1.54 1.59 o 1 16 1 1447.98 1437.52 9.05 o 2 16 1 105.49 110.45 3.41 o 3 16 1 293.53 298.44 9.67 o 4 16 1 34.51 33.45 2.62 o -4 17 1 169.16 153.70 4.57 o -3 17 1 2.59 2.09 1.76 o -2 17 1 69.36 71.21 3.56 o -1 17 1 0.15 3.23 1.33 o 0 17 1 365.84 376.33 3.67 o 1 17 1 116.95 114.75 2.28 o 2 17 1 623.30 625.57 12.20 o 3 17 1 7.83 7.79 1.88 o 4 17 1 209.08 196.99 10.42 o -4 18 1 0.00 2.00 1.90 o -3 18 1 154.74 159.78 6.86 o -2 18 1 215.67 208.25 4.62 o -1 18 1 69.88 69.76 4.19 o 0 18 1 9.06 15.07 1.34 o 1 18 1 234.60 239.41 3.34 o 2 18 1 9.41 8.35 2.05 o 3 18 1 127.38 119.51 3.97 o -3 19 1 0.01 0.54 1.74 o -2 19 1 408.23 414.54 6.67 o -1 19 1 26.23 27.75 2.24 o 0 19 1 421.54 413.34 6.31 o 1 19 1 34.55 38.37 2.72 o 2 19 1 385.49 391.57 9.68 o 3 19 1 12.83 13.90 2.08 o -3 20 1 84.51 81.22 3.53 o -2 20 1 3.04 4.05 1.75 o -1 20 1 432.50 434.49 18.63 o 0 20 1 19.35 20.07 1.54 o 1 20 1 302.75 335.62 5.78 o 2 20 1 8.04 4.76 1.88 o 3 20 1 295.72 332.88 6.66 o -3 21 1 31.81 32.41 2.75 o -2 21 1 79.60 86.72 3.46 o -1 21 1 0.14 3.47 2.89 o 0 21 1 155.89 163.91 5.35 o 1 21 1 4.43 7.68 3.61 o 2 21 1 192.10 201.76 5.97 o -2 22 1 4.13 3.00 1.86 o -1 22 1 150.63 150.47 5.40 o 0 22 1 12.32 12.91 1.82 o 1 22 1 401.86 409.03 8.75 o 2 22 1 0.40 1.90 1.90 o -1 23 1 4.90 5.28 1.94 o 0 23 1 271.07 285.00 8.14 o 1 23 1 60.85 66.10 3.30 o -4 0 2 1954.08 1911.52 68.64 o -2 0 2 858.02 822.75 19.11 o 0 0 2 134.62 129.27 1.71 o 2 0 2 2208.48 2071.82 16.41 o 4 0 2 54.06 52.52 3.32 o -5 1 2 428.96 452.78 8.21 o -4 1 2 4.96 6.64 0.99 o -3 1 2 1303.69 1300.04 23.85 o -2 1 2 459.28 540.58 7.90 o 0 1 2 4900.52 4495.26 41.01 o 1 1 2 729.76 688.25 16.61 o 2 1 2 8.34 25.75 11.52 o 3 1 2 656.74 696.50 16.18 o 4 1 2 154.35 153.72 3.59 o 5 1 2 115.90 124.40 6.09 o -5 2 2 15.26 17.27 2.69 o -4 2 2 1917.70 1878.74 13.57 o -3 2 2 0.20 2.67 0.75 o -2 2 2 414.10 408.01 14.52 o -1 2 2 511.69 509.88 3.89 o 0 2 2 1843.29 1906.72 29.71 o 1 2 2 124.61 120.85 1.49 o 2 2 2 4482.27 4478.78 104.88 o 3 2 2 20.63 22.36 1.80 o 4 2 2 169.17 187.19 7.65 o 5 2 2 11.47 12.02 1.69 o -5 3 2 478.91 452.58 8.47 o -4 3 2 79.38 84.58 5.57 o -3 3 2 3196.31 3159.50 27.51 o -2 3 2 938.56 1038.08 20.45 o -1 3 2 1490.01 1302.43 103.01 o 0 3 2 3054.09 3253.23 31.02 o 1 3 2 6475.85 6308.80 94.57 o 2 3 2 1305.35 1506.50 24.74 o 3 3 2 701.18 684.03 5.53 o 4 3 2 14.24 16.69 1.61 o 5 3 2 568.45 589.80 17.74 o -5 4 2 504.01 496.86 30.68 o -4 4 2 1638.00 1570.01 19.70 o -3 4 2 91.98 94.25 3.09 o -2 4 2 655.42 652.19 10.39 o -1 4 2 6.04 8.09 4.21 o 0 4 2 169.95 176.35 2.76 o 1 4 2 1325.05 1263.46 18.47 o 2 4 2 3405.21 3240.02 12.72 o 3 4 2 483.91 502.47 7.67 o 4 4 2 45.79 44.36 2.01 o 5 4 2 102.97 102.02 2.61 o -6 5 2 11.98 11.46 2.89 o -5 5 2 342.30 341.43 13.82 o -4 5 2 33.20 25.70 1.97 o -3 5 2 2459.77 2504.60 19.79 o -2 5 2 1071.82 1215.60 10.09 o -1 5 2 2903.66 2852.52 40.94 o 0 5 2 162.74 173.03 8.58 o 1 5 2 6776.93 6935.79 154.52 o 2 5 2 184.83 228.60 10.12 o 3 5 2 1319.90 1271.03 11.56 o 4 5 2 235.12 240.52 7.46 o 5 5 2 430.17 446.51 17.07 o -6 6 2 138.22 133.90 5.81 o -5 6 2 164.01 164.99 5.20 o -4 6 2 945.73 918.07 8.33 o -3 6 2 315.84 302.82 4.19 o -2 6 2 3436.52 3504.33 16.99 o -1 6 2 8.64 11.76 2.58 o 0 6 2 3283.36 3590.23 33.16 o 1 6 2 3556.24 3405.04 15.20 o 2 6 2 3686.91 3679.53 26.76 o 3 6 2 156.36 153.37 3.50 o 4 6 2 690.36 725.60 27.20 o 5 6 2 28.15 33.61 3.91 o -6 7 2 41.73 40.70 3.91 o -5 7 2 29.30 29.91 2.38 o -4 7 2 294.20 288.74 5.09 o -3 7 2 1291.75 1216.36 9.03 o -2 7 2 39.50 43.42 3.79 o -1 7 2 370.22 321.91 2.67 o 0 7 2 1960.67 2059.51 28.58 o 1 7 2 2964.63 3028.71 66.52 o 2 7 2 132.81 159.23 4.26 o 3 7 2 63.37 57.71 2.33 o 4 7 2 49.20 43.68 3.68 o 5 7 2 498.08 503.04 43.38 o -5 8 2 67.50 63.91 4.22 o -4 8 2 229.60 222.88 9.83 o -3 8 2 375.17 342.31 8.52 o -2 8 2 2073.07 2077.68 12.36 o -1 8 2 448.71 481.53 4.22 o 0 8 2 7049.72 7156.01 102.35 o 1 8 2 74.71 59.39 4.66 o 2 8 2 272.35 256.02 6.69 o 3 8 2 360.94 350.07 5.03 o 4 8 2 799.41 826.50 19.49 o 5 8 2 13.13 11.51 2.20 o -5 9 2 28.50 27.81 2.25 o -4 9 2 0.13 -1.43 1.51 o -3 9 2 1507.04 1481.37 20.45 o -2 9 2 31.48 33.68 1.43 o -1 9 2 179.41 144.36 3.78 o 0 9 2 674.23 779.24 18.25 o 1 9 2 2760.82 2829.08 43.17 o 2 9 2 33.24 27.66 1.23 o 3 9 2 3.69 6.88 1.15 o 4 9 2 89.87 94.80 8.29 o 5 9 2 323.52 378.79 9.68 o -5 10 2 10.54 10.26 1.94 o -4 10 2 3.47 3.41 2.28 o -3 10 2 103.23 105.27 3.02 o -2 10 2 731.43 715.75 5.55 o -1 10 2 268.22 242.57 2.61 o 0 10 2 1910.90 1914.28 11.12 o 1 10 2 112.77 127.45 4.55 o 2 10 2 174.56 161.91 3.66 o 3 10 2 68.59 62.81 2.84 o 4 10 2 469.00 512.65 21.01 o 5 10 2 0.03 1.84 2.00 o -5 11 2 74.20 83.05 4.07 o -4 11 2 57.60 70.09 8.24 o -3 11 2 1456.72 1411.11 15.74 o -2 11 2 11.42 9.46 1.66 o -1 11 2 587.75 583.01 3.54 o 0 11 2 123.87 131.05 1.88 o 1 11 2 2103.34 2067.82 23.89 o 2 11 2 303.39 309.77 10.66 o 3 11 2 296.55 292.04 10.36 o 4 11 2 0.02 0.53 1.76 o 5 11 2 233.57 236.63 25.33 o -5 12 2 156.16 135.64 4.11 o -4 12 2 127.77 127.28 3.71 o -3 12 2 626.86 598.76 11.75 o -2 12 2 661.63 651.20 10.08 o -1 12 2 912.31 917.62 12.02 o 0 12 2 949.81 951.69 7.61 o 1 12 2 149.17 141.65 2.46 o 2 12 2 163.45 162.60 4.17 o 3 12 2 1080.21 1046.94 14.21 o 4 12 2 272.16 269.33 5.49 o 5 12 2 1.71 2.78 2.03 o -5 13 2 68.47 69.56 3.26 o -4 13 2 4.10 5.96 1.90 o -3 13 2 860.23 843.82 36.88 o -2 13 2 93.83 91.62 5.04 o -1 13 2 56.02 55.24 1.37 o 0 13 2 17.40 15.89 1.78 o 1 13 2 1292.99 1313.02 19.54 o 2 13 2 24.60 23.50 1.37 o 3 13 2 29.23 37.05 6.11 o 4 13 2 28.92 26.07 2.38 o -5 14 2 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