#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/06/2210687.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210687_Fobs loop_ _publ_author_name 'Liang, Zu-Pei' 'Li, Jian' _publ_section_title ; N-Methylphthalimide ; _journal_coeditor_code KJ2028 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4274 _journal_page_last o4275 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.803 _cell_angle_gamma 90.000 _cell_length_a 4.0233 _cell_length_b 7.9475 _cell_length_c 12.4454 _exptl_crystal_F_000 168.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file kj2028Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 60731E in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 61.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 79.07 71.58 2.45 o 2 0 0 47.94 44.14 1.68 o 3 0 0 0.80 3.85 2.32 o 4 0 0 0.11 -0.93 3.94 o 1 1 0 1368.23 1353.78 96.74 o 2 1 0 99.93 113.07 6.58 o 3 1 0 2.54 3.47 1.21 o 4 1 0 1.17 0.42 3.81 o 0 2 0 398.39 343.27 6.53 o 1 2 0 294.42 302.28 4.32 o 2 2 0 209.08 223.82 7.68 o 3 2 0 19.97 22.64 1.74 o 4 2 0 2.72 -1.13 3.78 o 1 3 0 16.00 15.74 2.41 o 2 3 0 97.88 100.56 3.34 o 3 3 0 20.84 22.05 1.86 o 4 3 0 4.49 4.49 1.81 o 0 4 0 132.75 136.27 3.67 o 1 4 0 25.54 25.97 1.87 o 2 4 0 15.90 17.26 6.59 o 3 4 0 15.86 13.73 2.19 o 4 4 0 1.95 2.34 1.38 o 1 5 0 14.59 14.58 0.96 o 2 5 0 78.34 70.10 3.33 o 3 5 0 9.63 6.41 3.02 o 4 5 0 2.55 1.96 8.12 o 0 6 0 59.65 63.45 2.88 o 1 6 0 37.82 35.07 5.41 o 2 6 0 4.52 6.83 2.83 o 3 6 0 11.45 8.47 1.78 o 1 7 0 37.83 40.29 4.21 o 2 7 0 6.08 5.40 3.66 o 3 7 0 8.34 8.62 9.48 o 0 8 0 14.96 15.78 2.46 o 1 8 0 6.99 7.83 2.03 o 2 8 0 4.74 3.09 8.35 o 1 9 0 3.26 4.31 3.87 o -4 0 1 3.01 1.33 4.64 o -3 0 1 2.33 3.30 1.02 o -2 0 1 8.83 9.07 4.93 o -1 0 1 1049.98 1023.96 28.31 o 0 0 1 5.19 9.32 0.62 o 1 0 1 2186.92 2403.40 80.81 o 2 0 1 24.37 21.26 1.34 o 3 0 1 0.79 0.66 0.96 o 4 0 1 2.24 2.90 5.54 o -4 1 1 6.03 3.79 3.66 o -3 1 1 9.87 5.92 3.15 o -2 1 1 0.08 -0.07 0.38 o -1 1 1 579.60 536.84 9.49 o 0 1 1 1054.20 1147.95 23.87 o 1 1 1 3804.24 4149.98 411.03 o 2 1 1 426.74 442.88 5.93 o 3 1 1 33.31 43.05 2.39 o 4 1 1 3.86 4.11 3.86 o -4 2 1 2.18 -1.08 3.27 o -3 2 1 8.68 9.86 1.74 o -2 2 1 3.38 3.34 0.92 o -1 2 1 15.83 13.52 2.29 o 0 2 1 334.61 293.50 4.45 o 1 2 1 375.58 368.00 12.35 o 2 2 1 198.94 196.47 3.32 o 3 2 1 30.24 36.81 4.68 o 4 2 1 4.41 3.21 3.73 o -4 3 1 3.52 -1.34 4.61 o -3 3 1 1.73 1.48 1.14 o -2 3 1 42.39 42.73 2.17 o -1 3 1 420.33 399.56 13.38 o 0 3 1 69.72 66.51 1.90 o 1 3 1 117.16 121.42 2.38 o 2 3 1 0.78 0.50 0.54 o 3 3 1 24.34 26.54 2.09 o 4 3 1 8.54 8.89 1.93 o -4 4 1 1.43 -0.39 3.97 o -3 4 1 31.83 32.34 3.66 o -2 4 1 32.12 33.05 7.20 o -1 4 1 226.35 237.45 6.92 o 0 4 1 239.63 224.81 3.96 o 1 4 1 17.21 19.20 1.45 o 2 4 1 28.70 24.45 13.86 o 3 4 1 5.83 5.13 1.37 o 4 4 1 3.89 2.21 2.47 o -4 5 1 1.63 1.24 10.11 o -3 5 1 11.66 10.14 1.96 o -2 5 1 25.92 25.67 2.76 o -1 5 1 34.09 37.17 3.48 o 0 5 1 15.76 17.85 2.32 o 1 5 1 64.66 62.03 1.97 o 2 5 1 14.67 14.49 5.90 o 3 5 1 17.77 22.26 2.53 o 4 5 1 1.10 -2.33 6.62 o -3 6 1 1.79 3.23 2.73 o -2 6 1 63.13 59.30 8.44 o -1 6 1 52.21 58.68 3.02 o 0 6 1 16.01 15.37 1.15 o 1 6 1 16.88 17.63 3.38 o 2 6 1 43.89 41.75 5.23 o 3 6 1 0.02 -2.04 5.52 o -3 7 1 0.58 0.51 3.73 o -2 7 1 3.84 4.71 1.90 o -1 7 1 55.76 52.41 8.16 o 0 7 1 22.39 20.25 1.33 o 1 7 1 0.37 0.42 4.84 o 2 7 1 1.23 2.15 1.36 o 3 7 1 0.96 2.04 1.84 o -2 8 1 1.12 1.12 2.47 o -1 8 1 5.79 9.27 2.05 o 0 8 1 25.48 24.74 2.46 o 1 8 1 10.91 12.08 2.71 o 2 8 1 1.31 1.12 3.15 o -1 9 1 0.02 0.71 1.52 o 0 9 1 0.00 1.55 2.60 o 1 9 1 6.53 5.59 3.44 o -4 0 2 3.41 0.71 4.08 o -3 0 2 96.66 106.89 8.24 o -2 0 2 8.53 8.20 0.93 o -1 0 2 0.24 0.00 0.71 o 0 0 2 1210.30 1282.69 24.78 o 1 0 2 52.26 48.21 2.88 o 2 0 2 26.45 26.23 1.46 o 3 0 2 4.42 4.94 1.18 o 4 0 2 5.17 2.65 4.18 o -4 1 2 2.57 1.73 3.66 o -3 1 2 4.13 4.55 1.06 o -2 1 2 45.55 52.27 1.20 o -1 1 2 138.52 126.65 5.64 o 0 1 2 552.12 511.08 6.46 o 1 1 2 1000.62 1002.11 12.90 o 2 1 2 132.56 132.13 3.49 o 3 1 2 9.58 12.08 3.27 o 4 1 2 8.51 3.12 3.34 o -4 2 2 9.20 4.51 3.90 o -3 2 2 6.59 8.40 3.06 o -2 2 2 29.08 32.56 2.98 o -1 2 2 14.49 15.42 1.45 o 0 2 2 287.97 251.54 3.36 o 1 2 2 409.72 408.69 5.78 o 2 2 2 532.50 561.31 7.98 o 3 2 2 96.45 106.42 3.59 o 4 2 2 0.50 -1.73 3.52 o -4 3 2 10.03 7.82 5.05 o -3 3 2 5.45 4.93 1.31 o -2 3 2 85.88 89.98 40.97 o -1 3 2 8.11 9.59 1.43 o 0 3 2 340.71 339.59 8.29 o 1 3 2 157.09 148.58 7.37 o 2 3 2 47.02 51.71 2.74 o 3 3 2 64.52 69.96 3.32 o 4 3 2 2.16 0.96 1.51 o -4 4 2 4.07 3.25 3.17 o -3 4 2 3.99 5.24 1.61 o -2 4 2 34.40 36.62 4.63 o -1 4 2 6.07 6.48 0.79 o 0 4 2 265.06 262.36 3.76 o 1 4 2 60.35 55.73 2.67 o 2 4 2 28.50 28.02 9.15 o 3 4 2 3.85 2.05 2.66 o 4 4 2 12.93 14.26 4.46 o -4 5 2 2.62 0.59 8.13 o -3 5 2 9.80 9.32 1.75 o -2 5 2 44.94 50.94 2.68 o -1 5 2 154.87 156.70 4.07 o 0 5 2 30.55 27.71 2.17 o 1 5 2 24.82 21.12 1.96 o 2 5 2 25.49 28.80 7.52 o 3 5 2 13.59 15.39 2.28 o -3 6 2 5.28 3.57 4.52 o -2 6 2 6.87 9.03 2.08 o -1 6 2 12.39 12.61 2.11 o 0 6 2 31.73 25.95 1.84 o 1 6 2 30.44 27.97 1.48 o 2 6 2 1.74 2.51 1.24 o 3 6 2 2.61 0.12 2.56 o -3 7 2 2.50 -0.47 5.63 o -2 7 2 27.46 30.66 12.21 o -1 7 2 1.08 1.56 1.59 o 0 7 2 103.78 95.44 2.61 o 1 7 2 0.79 0.98 1.46 o 2 7 2 0.75 0.31 1.45 o 3 7 2 2.97 -0.73 7.81 o -2 8 2 22.65 23.61 12.21 o -1 8 2 14.30 11.96 3.44 o 0 8 2 8.16 6.70 2.44 o 1 8 2 17.85 16.34 9.19 o 2 8 2 4.80 6.97 4.76 o -1 9 2 5.37 6.31 5.34 o 0 9 2 2.39 5.90 4.03 o 1 9 2 5.76 6.95 3.61 o -4 0 3 2.10 -0.21 3.72 o -3 0 3 2.80 2.46 4.40 o -2 0 3 9.22 8.30 1.32 o -1 0 3 102.91 94.90 2.15 o 0 0 3 97.61 107.15 2.78 o 1 0 3 77.11 69.54 2.21 o 2 0 3 162.01 155.66 4.02 o 3 0 3 1.03 0.74 1.15 o 4 0 3 5.04 5.36 6.53 o -4 1 3 10.57 5.16 3.34 o -3 1 3 2.10 2.55 1.14 o -2 1 3 276.80 282.19 5.26 o -1 1 3 169.63 168.68 2.35 o 0 1 3 34.19 32.27 2.89 o 1 1 3 249.75 224.92 17.27 o 2 1 3 4.48 4.81 0.84 o 3 1 3 0.93 0.13 1.14 o 4 1 3 1.47 1.13 3.49 o -4 2 3 1.71 0.78 3.46 o -3 2 3 25.37 28.11 1.77 o -2 2 3 8.00 13.18 3.60 o -1 2 3 104.55 98.63 2.09 o 0 2 3 130.51 123.96 2.29 o 1 2 3 58.79 56.08 1.59 o 2 2 3 420.45 434.16 8.69 o 3 2 3 25.82 26.99 2.14 o 4 2 3 1.75 -3.53 3.50 o -4 3 3 10.00 5.23 7.35 o -3 3 3 12.71 17.01 3.82 o -2 3 3 18.78 21.39 2.40 o -1 3 3 214.50 210.32 3.04 o 0 3 3 198.49 201.66 3.11 o 1 3 3 79.92 83.80 2.14 o 2 3 3 23.19 24.22 3.96 o 3 3 3 66.40 81.10 9.76 o 4 3 3 27.74 27.13 5.67 o -4 4 3 1.03 -1.13 13.69 o -3 4 3 37.08 41.09 2.47 o -2 4 3 36.16 33.44 2.97 o -1 4 3 89.12 101.24 3.21 o 0 4 3 40.72 40.85 2.38 o 1 4 3 85.67 84.27 2.23 o 2 4 3 9.89 9.04 5.39 o 3 4 3 12.40 15.54 2.23 o 4 4 3 5.46 5.57 4.94 o -3 5 3 3.21 3.64 1.97 o -2 5 3 20.66 21.99 3.54 o -1 5 3 5.65 5.14 1.06 o 0 5 3 104.41 98.30 2.23 o 1 5 3 21.60 27.34 5.59 o 2 5 3 2.84 2.35 1.31 o 3 5 3 0.03 1.00 1.53 o -3 6 3 0.23 -2.72 4.21 o -2 6 3 2.94 2.86 3.16 o -1 6 3 82.35 75.84 3.45 o 0 6 3 10.55 10.15 4.86 o 1 6 3 78.13 70.98 5.02 o 2 6 3 15.37 17.57 2.22 o 3 6 3 2.91 1.72 2.78 o -3 7 3 0.39 0.97 2.57 o -2 7 3 2.26 5.64 9.82 o -1 7 3 59.00 55.84 3.66 o 0 7 3 4.40 5.21 1.09 o 1 7 3 10.48 9.43 2.66 o 2 7 3 3.79 4.55 3.24 o 3 7 3 4.16 3.02 6.49 o -2 8 3 9.73 11.72 10.56 o -1 8 3 14.01 12.78 2.98 o 0 8 3 16.55 14.91 1.45 o 1 8 3 9.32 8.61 2.00 o 2 8 3 8.71 8.00 4.57 o -1 9 3 4.64 6.81 1.96 o 0 9 3 0.42 2.97 1.29 o 1 9 3 14.68 16.24 8.17 o -4 0 4 2.62 0.06 4.02 o -3 0 4 16.37 23.70 5.88 o -2 0 4 2.99 5.44 1.12 o -1 0 4 621.06 616.67 9.12 o 0 0 4 229.90 227.59 4.77 o 1 0 4 42.88 42.22 1.87 o 2 0 4 16.81 19.73 6.31 o 3 0 4 8.91 8.74 1.85 o 4 0 4 0.47 -1.70 4.86 o -4 1 4 0.25 -2.06 3.12 o -3 1 4 30.14 33.08 1.75 o -2 1 4 9.83 10.37 0.84 o -1 1 4 12.80 12.88 0.88 o 0 1 4 309.79 297.00 9.15 o 1 1 4 11.48 12.85 1.75 o 2 1 4 19.21 18.80 2.55 o 3 1 4 27.69 29.53 2.91 o 4 1 4 1.00 -5.09 3.39 o -4 2 4 13.83 8.37 4.11 o -3 2 4 11.91 15.91 1.79 o -2 2 4 27.31 27.56 2.00 o -1 2 4 448.71 452.54 5.90 o 0 2 4 141.16 125.19 4.62 o 1 2 4 61.55 62.90 1.84 o 2 2 4 20.92 25.66 3.00 o 3 2 4 11.64 13.77 1.86 o 4 2 4 0.99 -3.40 3.27 o -4 3 4 16.66 7.21 8.00 o -3 3 4 11.04 10.67 3.27 o -2 3 4 50.72 48.74 2.94 o -1 3 4 12.28 12.48 1.95 o 0 3 4 250.35 249.54 3.70 o 1 3 4 77.96 68.86 2.50 o 2 3 4 6.38 6.54 1.23 o 3 3 4 43.87 46.95 2.69 o 4 3 4 6.85 3.05 1.86 o -4 4 4 0.87 1.17 4.07 o -3 4 4 38.04 58.87 14.94 o -2 4 4 13.62 17.25 3.11 o -1 4 4 5.12 6.17 2.18 o 0 4 4 27.00 27.74 2.42 o 1 4 4 91.91 92.18 4.33 o 2 4 4 3.06 3.77 1.01 o 3 4 4 18.11 23.84 2.79 o 4 4 4 12.15 6.18 4.05 o -3 5 4 12.35 22.93 9.46 o -2 5 4 38.20 32.82 3.22 o -1 5 4 46.33 43.41 2.46 o 0 5 4 76.11 72.15 2.06 o 1 5 4 55.05 57.10 2.11 o 2 5 4 37.17 43.93 8.30 o 3 5 4 1.36 0.06 4.08 o -3 6 4 1.07 -2.05 4.94 o -2 6 4 2.41 1.90 1.30 o -1 6 4 54.65 45.10 2.56 o 0 6 4 20.47 20.38 1.47 o 1 6 4 19.83 20.53 1.48 o 2 6 4 16.14 17.76 4.33 o 3 6 4 2.24 0.64 6.34 o -3 7 4 1.76 7.46 3.83 o -2 7 4 11.92 20.25 9.24 o -1 7 4 12.59 15.38 4.70 o 0 7 4 52.90 46.81 2.03 o 1 7 4 5.29 5.98 1.23 o 2 7 4 0.89 0.51 4.60 o -2 8 4 3.59 2.98 7.06 o -1 8 4 0.79 5.24 4.18 o 0 8 4 11.23 12.29 2.47 o 1 8 4 5.41 7.21 2.18 o 2 8 4 1.07 -1.27 1.57 o 0 9 4 2.89 7.16 3.26 o -4 0 5 4.11 2.72 5.29 o -3 0 5 27.52 30.80 6.42 o -2 0 5 63.76 64.65 2.18 o -1 0 5 79.51 69.75 2.43 o 0 0 5 16.20 18.94 1.82 o 1 0 5 147.30 156.51 4.06 o 2 0 5 0.15 0.78 1.08 o 3 0 5 15.75 15.58 2.04 o 4 0 5 1.26 -1.29 5.23 o -4 1 5 2.28 0.24 2.95 o -3 1 5 1.75 3.85 2.08 o -2 1 5 113.88 106.70 1.99 o -1 1 5 51.08 48.04 1.40 o 0 1 5 348.85 362.86 6.47 o 1 1 5 191.45 196.02 5.16 o 2 1 5 20.22 21.65 2.10 o 3 1 5 7.30 7.35 1.69 o 4 1 5 2.36 -1.44 3.42 o -4 2 5 7.84 5.54 2.88 o -3 2 5 17.99 17.65 1.73 o -2 2 5 1.37 1.40 1.06 o -1 2 5 23.66 23.77 2.66 o 0 2 5 127.11 129.33 6.42 o 1 2 5 95.37 98.40 4.55 o 2 2 5 29.42 31.21 1.46 o 3 2 5 2.24 2.61 1.47 o 4 2 5 0.72 -4.37 4.05 o -4 3 5 6.54 4.67 4.41 o -3 3 5 29.52 26.68 3.22 o -2 3 5 65.83 74.08 2.98 o -1 3 5 60.25 62.80 2.06 o 0 3 5 67.06 60.10 2.08 o 1 3 5 74.76 66.96 2.64 o 2 3 5 17.93 20.22 3.56 o 3 3 5 4.01 3.34 1.58 o 4 3 5 0.29 -1.07 2.04 o -4 4 5 0.12 -0.12 4.26 o -3 4 5 10.42 23.50 10.51 o -2 4 5 88.05 86.12 3.80 o -1 4 5 27.63 27.17 3.49 o 0 4 5 35.93 36.06 2.40 o 1 4 5 5.78 7.34 9.45 o 2 4 5 30.72 37.01 6.29 o 3 4 5 7.30 6.28 1.82 o -3 5 5 2.12 4.20 4.95 o -2 5 5 29.78 27.96 2.99 o -1 5 5 16.87 18.85 2.16 o 0 5 5 21.12 22.28 2.15 o 1 5 5 17.79 19.40 2.73 o 2 5 5 33.34 34.26 7.80 o 3 5 5 2.20 0.27 5.37 o -3 6 5 1.24 2.49 6.56 o -2 6 5 16.21 17.92 2.59 o -1 6 5 2.06 1.82 1.67 o 0 6 5 115.84 108.97 2.70 o 1 6 5 33.21 34.13 1.90 o 2 6 5 3.37 0.68 2.92 o 3 6 5 2.20 0.57 8.64 o -2 7 5 6.41 4.22 3.62 o -1 7 5 26.66 34.59 3.99 o 0 7 5 13.37 19.98 1.78 o 1 7 5 2.32 4.30 3.05 o 2 7 5 3.97 3.08 5.86 o -2 8 5 7.75 5.48 7.50 o -1 8 5 2.01 7.16 2.10 o 0 8 5 0.06 10.30 4.79 o 1 8 5 6.51 5.50 2.16 o -4 0 6 6.30 3.86 3.11 o -3 0 6 0.55 0.90 2.49 o -2 0 6 60.78 61.11 2.30 o -1 0 6 78.98 79.94 3.79 o 0 0 6 61.88 72.76 2.82 o 1 0 6 51.41 52.79 2.36 o 2 0 6 78.76 77.05 3.08 o 3 0 6 6.91 7.67 1.78 o 4 0 6 7.33 5.45 6.48 o -4 1 6 3.65 99.57 74.16 o -3 1 6 0.20 -1.16 1.66 o -2 1 6 24.91 25.65 1.21 o -1 1 6 160.72 148.64 2.86 o 0 1 6 80.92 85.87 2.26 o 1 1 6 77.60 81.52 2.11 o 2 1 6 37.72 39.69 1.72 o 3 1 6 4.92 6.25 1.25 o 4 1 6 0.74 -3.72 3.76 o -4 2 6 1.91 4.98 2.24 o -3 2 6 32.07 33.71 2.01 o -2 2 6 21.63 21.74 1.71 o -1 2 6 76.96 85.71 2.42 o 0 2 6 123.16 115.76 2.53 o 1 2 6 19.10 17.87 1.47 o 2 2 6 12.55 14.21 1.42 o 3 2 6 6.95 8.23 1.83 o 4 2 6 1.26 1.79 3.30 o -4 3 6 4.46 1.34 3.38 o -3 3 6 22.89 19.60 1.87 o -2 3 6 11.40 12.53 1.76 o -1 3 6 89.81 86.36 2.05 o 0 3 6 32.78 38.42 2.51 o 1 3 6 21.04 19.36 4.40 o 2 3 6 14.84 16.19 3.21 o 3 3 6 7.26 7.69 1.81 o 4 3 6 4.14 -0.14 2.23 o -3 4 6 22.12 19.40 5.47 o -2 4 6 6.60 5.03 1.95 o -1 4 6 44.00 41.33 3.83 o 0 4 6 30.37 29.34 1.51 o 1 4 6 40.01 39.39 7.80 o 2 4 6 16.23 19.96 1.97 o 3 4 6 9.48 10.09 2.38 o -3 5 6 0.57 -0.28 3.62 o -2 5 6 31.88 33.28 2.68 o -1 5 6 88.10 87.56 3.61 o 0 5 6 3.78 6.18 1.41 o 1 5 6 78.20 72.10 3.05 o 2 5 6 8.87 9.64 2.43 o 3 5 6 3.75 2.32 3.03 o -3 6 6 7.90 -1.67 5.16 o -2 6 6 1.79 2.42 4.00 o -1 6 6 45.94 49.76 2.74 o 0 6 6 18.44 22.62 1.73 o 1 6 6 1.82 1.47 1.23 o 2 6 6 2.33 -0.68 5.61 o 3 6 6 0.49 -0.19 1.78 o -2 7 6 1.88 0.65 4.00 o -1 7 6 13.63 14.11 2.27 o 0 7 6 9.10 11.00 1.53 o 1 7 6 19.52 23.67 3.84 o 2 7 6 1.88 -1.49 7.90 o -1 8 6 0.14 7.37 2.23 o 0 8 6 2.03 8.47 6.41 o 1 8 6 7.67 6.27 1.90 o -4 0 7 4.86 -0.88 3.19 o -3 0 7 0.08 -0.76 3.88 o -2 0 7 19.55 22.75 2.08 o -1 0 7 30.08 34.22 2.43 o 0 0 7 2.10 1.50 2.00 o 1 0 7 0.29 -1.45 1.22 o 2 0 7 40.58 45.82 2.56 o 3 0 7 1.55 0.93 2.14 o 4 0 7 3.65 -0.85 4.80 o -4 1 7 12.79 4.15 2.45 o -3 1 7 18.47 13.23 4.08 o -2 1 7 41.34 43.08 1.76 o -1 1 7 11.11 11.45 1.24 o 0 1 7 131.77 136.60 3.45 o 1 1 7 30.22 32.11 1.53 o 2 1 7 2.62 3.83 1.15 o 3 1 7 9.80 8.85 1.44 o 4 1 7 0.07 -5.05 3.37 o -4 2 7 8.96 2.51 2.60 o -3 2 7 7.54 6.19 2.29 o -2 2 7 14.66 19.23 2.10 o -1 2 7 52.95 50.22 2.49 o 0 2 7 55.78 46.92 1.77 o 1 2 7 66.94 64.65 3.81 o 2 2 7 8.24 8.81 1.36 o 3 2 7 2.17 1.14 1.83 o -4 3 7 3.41 -1.90 4.19 o -3 3 7 1.06 -0.03 1.77 o -2 3 7 27.81 30.99 2.25 o -1 3 7 69.19 63.80 1.92 o 0 3 7 5.43 5.83 1.27 o 1 3 7 33.07 33.46 4.91 o 2 3 7 18.02 21.16 3.14 o 3 3 7 3.64 4.79 1.96 o -3 4 7 15.99 16.89 4.51 o -2 4 7 75.27 75.41 3.73 o -1 4 7 5.54 6.41 1.25 o 0 4 7 41.62 45.95 1.95 o 1 4 7 36.41 35.37 1.85 o 2 4 7 21.00 22.64 1.63 o 3 4 7 13.08 12.43 2.32 o -3 5 7 6.87 5.46 1.89 o -2 5 7 46.74 49.66 3.44 o -1 5 7 20.23 25.45 2.68 o 0 5 7 68.63 65.06 3.68 o 1 5 7 4.52 2.99 1.43 o 2 5 7 16.23 15.74 2.25 o 3 5 7 0.46 -0.31 1.67 o -3 6 7 5.82 5.36 5.02 o -2 6 7 17.33 21.92 7.72 o -1 6 7 29.30 31.28 2.92 o 0 6 7 40.43 45.14 2.16 o 1 6 7 7.03 5.22 6.17 o 2 6 7 6.84 2.81 5.20 o -2 7 7 0.25 3.85 2.32 o -1 7 7 1.53 0.34 1.92 o 0 7 7 5.81 5.38 2.26 o 1 7 7 11.71 11.86 2.16 o 2 7 7 0.96 -2.00 8.44 o -1 8 7 2.22 6.37 2.40 o 0 8 7 0.19 5.31 7.01 o 1 8 7 2.17 -0.27 3.20 o -4 0 8 0.38 -2.32 2.85 o -2 0 8 9.08 12.62 2.17 o -1 0 8 146.64 132.66 4.05 o 0 0 8 71.11 71.59 3.15 o 1 0 8 34.79 33.77 2.80 o 2 0 8 0.18 -1.52 1.34 o 3 0 8 11.23 6.72 2.15 o -4 1 8 3.10 0.55 1.92 o -3 1 8 2.57 2.97 3.54 o -2 1 8 14.02 18.92 2.25 o -1 1 8 24.06 22.07 1.47 o 0 1 8 43.51 41.19 1.82 o 1 1 8 43.37 42.79 2.14 o 2 1 8 10.23 11.13 1.48 o 3 1 8 4.38 -0.18 1.30 o -4 2 8 4.95 -1.53 2.06 o -3 2 8 40.96 43.49 7.08 o -2 2 8 37.68 42.34 2.81 o -1 2 8 12.60 13.97 1.53 o 0 2 8 37.19 41.54 3.31 o 1 2 8 23.46 23.84 4.50 o 2 2 8 4.06 4.66 1.32 o 3 2 8 2.40 4.71 1.99 o -3 3 8 35.53 34.08 5.67 o -2 3 8 4.36 4.29 1.66 o -1 3 8 63.86 55.31 2.05 o 0 3 8 65.28 68.30 3.16 o 1 3 8 17.12 15.46 1.71 o 2 3 8 10.92 13.14 2.27 o 3 3 8 12.82 8.47 2.13 o -3 4 8 6.02 7.45 2.70 o -2 4 8 40.14 41.18 3.10 o -1 4 8 14.05 15.76 1.63 o 0 4 8 42.26 44.67 2.75 o 1 4 8 2.33 3.51 1.63 o 2 4 8 24.96 29.59 2.60 o 3 4 8 2.95 1.01 3.27 o -3 5 8 1.07 -1.21 2.53 o -2 5 8 6.40 8.43 2.29 o -1 5 8 100.13 96.87 6.51 o 0 5 8 2.16 1.30 1.30 o 1 5 8 17.05 17.45 1.94 o 2 5 8 0.61 -1.88 6.94 o 3 5 8 1.42 -0.92 2.15 o -2 6 8 5.70 4.77 2.63 o -1 6 8 10.82 10.58 4.32 o 0 6 8 17.35 19.03 1.83 o 1 6 8 14.26 19.14 2.00 o 2 6 8 1.51 -1.07 1.45 o -2 7 8 0.34 -1.90 5.39 o -1 7 8 2.97 4.89 2.61 o 0 7 8 18.59 20.95 6.80 o 1 7 8 4.74 3.68 1.72 o -3 0 9 9.88 4.64 4.20 o -2 0 9 8.13 9.15 3.60 o -1 0 9 29.24 26.53 5.69 o 0 0 9 0.78 1.12 2.61 o 1 0 9 14.36 17.48 2.78 o 2 0 9 42.22 39.92 3.16 o 3 0 9 0.00 -2.70 1.80 o -3 1 9 21.31 9.83 3.17 o -2 1 9 46.23 47.59 2.07 o -1 1 9 29.48 29.23 3.21 o 0 1 9 43.44 48.97 4.79 o 1 1 9 57.24 59.50 2.63 o 2 1 9 0.21 -0.77 1.84 o 3 1 9 0.75 -0.24 1.27 o -3 2 9 22.90 8.55 6.62 o -2 2 9 84.23 89.25 4.22 o -1 2 9 21.14 22.41 2.66 o 0 2 9 50.63 54.41 2.92 o 1 2 9 10.62 11.04 1.76 o 2 2 9 8.10 7.53 1.58 o 3 2 9 3.29 3.04 1.93 o -3 3 9 2.17 0.27 2.24 o -2 3 9 80.17 86.90 4.37 o -1 3 9 2.28 3.00 1.21 o 0 3 9 22.73 23.44 1.74 o 1 3 9 35.11 36.29 2.15 o 2 3 9 12.47 11.35 2.94 o 3 3 9 1.51 -0.69 1.86 o -3 4 9 4.26 1.32 4.20 o -2 4 9 0.26 -1.60 1.63 o -1 4 9 116.20 107.53 3.20 o 0 4 9 7.46 8.99 1.61 o 1 4 9 8.68 7.58 1.55 o 2 4 9 0.41 -0.21 1.33 o 3 4 9 2.06 -1.03 1.98 o -2 5 9 3.24 2.77 2.51 o -1 5 9 0.72 0.95 2.03 o 0 5 9 34.44 32.87 2.01 o 1 5 9 5.32 4.82 1.66 o 2 5 9 0.21 0.11 1.57 o -2 6 9 5.00 2.90 3.49 o -1 6 9 4.60 9.76 2.27 o 0 6 9 22.84 21.77 2.36 o 1 6 9 2.44 3.24 2.06 o 2 6 9 3.00 0.76 1.79 o -1 7 9 0.64 3.46 1.89 o 0 7 9 5.81 7.92 2.84 o 1 7 9 14.31 16.44 2.20 o -3 0 10 10.07 6.56 4.80 o -2 0 10 68.92 74.47 3.52 o -1 0 10 13.90 17.04 2.71 o 0 0 10 15.01 15.98 4.81 o 1 0 10 13.09 11.25 2.65 o 2 0 10 7.14 6.15 2.39 o 3 0 10 1.48 1.94 2.27 o -3 1 10 14.42 1.71 3.98 o -2 1 10 65.19 73.60 5.47 o -1 1 10 38.93 42.40 2.12 o 0 1 10 47.52 45.65 2.30 o 1 1 10 5.53 4.70 1.63 o 2 1 10 12.56 9.63 1.77 o 3 1 10 7.67 4.35 1.48 o -3 2 10 3.28 0.59 3.10 o -2 2 10 2.33 2.22 2.07 o -1 2 10 116.36 110.15 3.92 o 0 2 10 11.93 11.00 1.74 o 1 2 10 20.78 19.17 2.05 o 2 2 10 15.05 10.39 1.76 o 3 2 10 0.01 -2.61 1.74 o -3 3 10 0.90 0.43 6.49 o -2 3 10 3.01 3.16 2.40 o -1 3 10 17.70 17.00 2.82 o 0 3 10 53.79 55.84 2.47 o 1 3 10 18.46 23.91 2.24 o 2 3 10 1.08 0.93 1.25 o 3 3 10 1.74 1.94 2.27 o -3 4 10 0.68 3.33 6.29 o -2 4 10 4.85 5.06 3.59 o -1 4 10 18.67 19.36 3.89 o 0 4 10 46.14 48.65 2.36 o 1 4 10 5.38 5.68 1.57 o 2 4 10 1.38 0.27 1.28 o -2 5 10 9.42 9.46 4.12 o -1 5 10 10.37 8.95 3.68 o 0 5 10 11.25 14.11 2.89 o 1 5 10 4.38 4.67 1.56 o 2 5 10 2.14 0.70 1.49 o -1 6 10 1.89 4.19 1.93 o 0 6 10 8.50 6.48 2.11 o 1 6 10 14.53 19.16 2.82 o -3 0 11 0.73 -4.97 3.32 o -2 0 11 3.52 4.60 1.96 o -1 0 11 161.45 140.72 6.39 o 0 0 11 98.88 116.05 5.44 o 1 0 11 15.73 20.84 3.05 o 2 0 11 0.02 -1.89 1.98 o 3 0 11 6.79 1.88 2.71 o -3 1 11 0.77 -3.62 2.80 o -2 1 11 26.41 25.61 2.53 o -1 1 11 32.27 32.53 2.03 o 0 1 11 7.55 7.62 1.63 o 1 1 11 48.80 53.52 3.06 o 2 1 11 5.86 6.68 1.63 o -3 2 11 2.88 -1.58 3.04 o -2 2 11 3.29 -0.18 1.88 o -1 2 11 19.07 20.08 1.96 o 0 2 11 35.72 35.11 3.53 o 1 2 11 8.91 9.35 1.82 o 2 2 11 14.99 10.50 3.62 o -2 3 11 0.11 -0.80 1.85 o -1 3 11 11.27 12.99 2.48 o 0 3 11 5.92 6.19 1.68 o 1 3 11 19.67 19.14 2.91 o 2 3 11 4.68 3.34 1.41 o -2 4 11 0.06 -2.56 6.07 o -1 4 11 7.33 6.69 2.23 o 0 4 11 7.86 8.67 1.71 o 1 4 11 3.33 2.46 1.56 o 2 4 11 0.10 -3.11 2.08 o -2 5 11 1.93 -0.90 3.35 o -1 5 11 3.43 4.53 2.29 o 0 5 11 9.76 11.39 1.99 o 1 5 11 13.07 18.64 2.27 o -1 6 11 4.29 6.26 2.40 o 0 6 11 9.14 8.44 2.24 o -2 0 12 0.21 0.91 1.90 o -1 0 12 0.63 1.38 1.77 o 0 0 12 14.85 15.30 3.25 o 1 0 12 27.49 26.88 3.06 o 2 0 12 19.68 19.51 3.31 o -2 1 12 3.33 6.03 2.73 o -1 1 12 10.28 10.52 1.54 o 0 1 12 55.66 54.17 2.84 o 1 1 12 4.20 6.15 3.72 o 2 1 12 14.61 6.11 1.82 o -2 2 12 2.54 -0.79 2.53 o -1 2 12 7.86 6.03 2.47 o 0 2 12 11.72 14.32 4.39 o 1 2 12 17.36 14.60 4.01 o 2 2 12 0.94 0.66 1.66 o -2 3 12 2.65 2.44 4.44 o -1 3 12 5.15 5.36 1.66 o 0 3 12 20.51 20.88 2.54 o 1 3 12 2.99 2.85 1.66 o 2 3 12 3.68 1.11 1.43 o -2 4 12 1.09 0.60 4.31 o -1 4 12 2.14 5.04 3.09 o 0 4 12 6.41 8.25 1.96 o 1 4 12 7.67 8.99 1.90 o -1 5 12 1.13 4.91 2.06 o 0 5 12 3.54 1.12 1.68 o 1 5 12 0.27 -0.43 2.38 o -2 0 13 0.16 -2.78 1.85 o -1 0 13 3.61 2.61 1.97 o 0 0 13 1.84 0.86 2.71 o 1 0 13 6.83 6.25 2.70 o 2 0 13 2.73 -0.38 2.35 o -2 1 13 2.89 0.03 1.86 o -1 1 13 2.16 1.90 1.42 o 0 1 13 4.28 4.07 4.45 o 1 1 13 6.33 5.71 2.18 o 2 1 13 0.56 -1.64 1.99 o -2 2 13 0.64 1.40 1.96 o -1 2 13 2.11 3.19 1.34 o 0 2 13 3.16 3.81 1.71 o 1 2 13 17.60 17.77 6.96 o -1 3 13 2.02 2.11 1.66 o 0 3 13 5.30 6.63 2.04 o 1 3 13 3.29 2.04 2.37 o -1 4 13 0.09 4.26 4.87 o 0 4 13 3.69 3.20 1.67 o -1 0 14 2.12 5.48 2.08 o 0 0 14 0.02 -3.14 2.09 o 1 0 14 1.40 1.53 2.64 o -1 1 14 1.72 4.23 1.70 o 0 1 14 2.05 -1.87 3.24 o 1 1 14 0.88 0.15 1.66 o -1 2 14 3.27 2.51 1.61 o 0 2 14 0.70 1.89 1.81 o 0 3 14 0.18 -0.03 5.08 o