#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/06/2210697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210697_Fobs loop_ _publ_author_name 'Klausmeyer, Kevin K.' 'Hung, Fernando' _publ_section_title ; [Bis(2-methyl-1-pyridyl)phenylphosphine-\k^2^N,P,N']trichlorochromium(III) acetonitrile solvate ; _journal_coeditor_code LH2165 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2415 _journal_page_last m2416 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.081 _cell_angle_gamma 90.000 _cell_length_a 11.0206 _cell_length_b 16.1145 _cell_length_c 13.0390 _exptl_crystal_F_000 1004.00 _reflns_d_resolution_high 0.7489 _[local]_cod_data_source_file lh2165Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kk11 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9471.71 9373.05 153.35 o 4 0 0 8534.51 8078.51 151.26 o 6 0 0 7949.21 7695.12 132.14 o 8 0 0 1030.03 900.59 63.15 o 10 0 0 6034.95 6084.57 182.94 o 12 0 0 19.94 29.45 43.55 o 14 0 0 333.12 495.41 103.72 o 2 1 0 9523.40 9251.04 93.21 o 3 1 0 205.66 191.12 10.05 o 4 1 0 26982.10 26280.72 273.45 o 5 1 0 2213.54 2006.96 37.94 o 6 1 0 514.98 582.37 22.55 o 7 1 0 39.81 34.61 11.96 o 8 1 0 113.32 123.85 16.87 o 9 1 0 534.90 458.73 31.83 o 10 1 0 21.78 21.13 28.50 o 11 1 0 255.43 296.81 35.78 o 12 1 0 153.10 155.55 40.06 o 13 1 0 3.01 0.52 34.16 o 14 1 0 3461.42 3814.90 178.95 o 0 2 0 40810.45 40516.82 1846.83 o 1 2 0 5.94 9.11 5.64 o 2 2 0 1202.24 1185.51 17.93 o 3 2 0 505.05 541.23 16.38 o 4 2 0 129.53 189.17 14.43 o 5 2 0 277.00 262.15 17.02 o 6 2 0 372.00 325.73 19.56 o 7 2 0 292.36 290.42 19.08 o 8 2 0 1162.34 1129.78 34.55 o 9 2 0 1829.25 1687.84 49.22 o 10 2 0 1446.10 1455.08 52.46 o 11 2 0 110.17 109.71 37.77 o 12 2 0 55.60 83.66 31.72 o 13 2 0 516.48 559.08 78.48 o 1 3 0 5461.21 5326.86 59.81 o 2 3 0 4325.29 4747.10 62.47 o 3 3 0 5176.97 5157.78 82.22 o 4 3 0 6511.52 6300.73 77.33 o 5 3 0 4613.30 4290.94 65.69 o 6 3 0 0.03 -10.22 10.22 o 7 3 0 97.56 121.91 16.22 o 8 3 0 42.16 76.91 17.05 o 9 3 0 2290.58 2265.40 56.66 o 10 3 0 524.63 547.82 36.45 o 11 3 0 1.43 -20.63 20.63 o 12 3 0 5.04 -27.89 40.33 o 13 3 0 41.19 49.17 37.56 o 0 4 0 647.82 721.96 19.81 o 1 4 0 2.43 -1.04 4.68 o 2 4 0 1188.59 1316.85 19.40 o 3 4 0 5182.74 5412.93 60.85 o 4 4 0 104.59 148.62 11.08 o 5 4 0 3.25 7.10 9.24 o 6 4 0 786.05 941.32 26.92 o 7 4 0 519.88 517.30 25.90 o 8 4 0 1872.14 1864.90 48.21 o 9 4 0 1421.93 1389.46 41.67 o 10 4 0 1136.75 1154.71 41.55 o 11 4 0 1690.11 1760.60 55.80 o 12 4 0 61.12 37.02 30.13 o 13 4 0 33.46 10.88 77.55 o 1 5 0 9857.31 10599.63 95.91 o 2 5 0 4105.12 4072.49 44.92 o 3 5 0 5660.57 5830.08 66.87 o 4 5 0 6755.13 6583.37 76.96 o 5 5 0 4023.94 3965.91 57.57 o 6 5 0 2354.03 2259.19 48.08 o 7 5 0 595.96 591.85 26.64 o 8 5 0 919.90 960.14 35.41 o 9 5 0 79.44 86.21 16.91 o 10 5 0 284.69 224.92 21.81 o 11 5 0 633.95 714.72 39.66 o 12 5 0 61.91 107.21 32.65 o 13 5 0 150.61 247.10 66.94 o 0 6 0 11742.18 11470.63 334.61 o 1 6 0 332.01 356.09 10.72 o 2 6 0 264.49 292.83 11.44 o 3 6 0 1.15 5.89 7.16 o 4 6 0 2611.67 2555.90 42.18 o 5 6 0 65.66 67.97 10.74 o 6 6 0 791.84 725.94 35.35 o 7 6 0 1209.72 1256.84 33.75 o 8 6 0 1643.30 1682.15 44.55 o 9 6 0 3332.04 3249.21 63.04 o 10 6 0 2606.60 2658.75 62.55 o 11 6 0 1084.40 1083.15 42.92 o 12 6 0 207.77 290.04 99.63 o 13 6 0 61.25 61.79 52.85 o 1 7 0 2625.23 2464.45 38.32 o 2 7 0 1280.83 1246.83 22.88 o 3 7 0 359.17 287.44 13.22 o 4 7 0 3456.40 3304.17 49.78 o 5 7 0 8016.69 7662.59 105.75 o 6 7 0 1346.47 1339.48 31.24 o 7 7 0 1019.65 986.77 29.66 o 8 7 0 63.95 55.67 14.57 o 9 7 0 59.38 74.20 16.40 o 10 7 0 179.70 217.70 24.30 o 11 7 0 334.33 369.22 33.50 o 12 7 0 124.50 34.86 39.76 o 13 7 0 108.61 29.10 43.04 o 0 8 0 32.88 71.26 10.05 o 1 8 0 523.36 523.07 14.51 o 2 8 0 6.28 32.54 7.21 o 3 8 0 5427.09 5301.39 72.97 o 4 8 0 191.85 204.86 14.92 o 5 8 0 215.19 230.37 17.42 o 6 8 0 15.77 23.26 14.62 o 7 8 0 1780.46 1866.20 48.02 o 8 8 0 2251.90 2216.54 46.04 o 9 8 0 2043.42 2043.72 52.28 o 10 8 0 576.41 621.05 34.85 o 11 8 0 525.40 540.48 45.97 o 12 8 0 433.71 447.26 84.12 o 13 8 0 658.37 588.12 97.46 o 1 9 0 3948.84 4057.60 58.43 o 2 9 0 770.21 813.77 23.09 o 3 9 0 675.37 606.44 26.43 o 4 9 0 21.62 36.62 10.39 o 5 9 0 5049.19 4975.59 77.39 o 6 9 0 3242.42 3063.75 59.54 o 7 9 0 1245.37 1234.80 40.67 o 8 9 0 309.81 307.26 29.97 o 9 9 0 110.74 132.52 40.89 o 10 9 0 9.37 32.33 22.53 o 11 9 0 627.02 615.03 48.21 o 12 9 0 366.97 329.20 75.13 o 0 10 0 4887.73 4857.16 95.07 o 1 10 0 101.64 88.57 12.94 o 2 10 0 3631.82 3453.51 57.78 o 3 10 0 175.22 150.95 18.53 o 4 10 0 1248.78 1251.22 32.83 o 5 10 0 480.16 477.25 24.41 o 6 10 0 162.75 170.71 19.94 o 7 10 0 126.30 134.98 24.42 o 8 10 0 1217.29 1314.10 55.96 o 9 10 0 119.91 165.47 28.89 o 10 10 0 48.89 60.76 25.12 o 11 10 0 887.23 951.39 100.22 o 12 10 0 67.81 56.04 34.58 o 1 11 0 7.06 15.83 10.82 o 2 11 0 54.57 59.05 10.48 o 3 11 0 8.27 24.63 10.59 o 4 11 0 10.75 5.98 16.06 o 5 11 0 67.04 81.18 17.52 o 6 11 0 1888.86 1841.33 58.60 o 7 11 0 1015.02 996.60 47.46 o 8 11 0 42.81 14.96 21.56 o 9 11 0 9.17 53.40 24.57 o 10 11 0 69.12 67.73 29.19 o 11 11 0 473.96 460.04 49.03 o 12 11 0 207.67 136.50 39.86 o 0 12 0 33.18 38.19 14.93 o 1 12 0 233.11 226.92 18.34 o 2 12 0 667.70 698.07 29.52 o 3 12 0 4395.73 4320.60 85.08 o 4 12 0 233.83 216.92 22.00 o 5 12 0 5.66 -10.64 15.40 o 6 12 0 1025.65 904.31 42.31 o 7 12 0 1620.46 1564.26 63.41 o 8 12 0 408.22 416.62 71.58 o 9 12 0 224.03 197.39 31.10 o 10 12 0 91.73 83.36 31.66 o 11 12 0 65.73 111.81 36.38 o 1 13 0 236.54 239.37 16.35 o 2 13 0 1692.47 1565.88 45.01 o 3 13 0 70.11 77.67 25.33 o 4 13 0 693.60 708.37 33.38 o 5 13 0 12.77 17.38 16.05 o 6 13 0 2665.78 2618.94 71.78 o 7 13 0 1126.73 1160.44 51.24 o 8 13 0 780.07 731.36 54.36 o 9 13 0 71.61 55.08 28.13 o 10 13 0 15.05 23.44 39.56 o 11 13 0 978.41 1018.13 72.44 o 0 14 0 88.97 60.03 22.51 o 1 14 0 1391.07 1421.49 40.28 o 2 14 0 705.40 737.40 32.13 o 3 14 0 8100.14 8186.83 140.46 o 4 14 0 1055.46 1065.35 41.26 o 5 14 0 3.47 -22.97 22.97 o 6 14 0 0.61 22.07 18.10 o 7 14 0 1804.73 1930.11 65.75 o 8 14 0 5.75 -19.83 26.41 o 9 14 0 44.26 39.23 27.61 o 10 14 0 34.85 50.53 31.26 o 1 15 0 1616.90 1708.61 53.31 o 2 15 0 811.41 851.84 41.86 o 3 15 0 101.47 80.15 20.18 o 4 15 0 328.56 337.35 53.00 o 5 15 0 6.19 16.09 26.99 o 6 15 0 427.63 301.72 63.56 o 7 15 0 1704.76 1781.53 90.04 o 8 15 0 97.25 49.38 66.31 o 9 15 0 18.88 26.07 29.23 o 10 15 0 1.52 26.14 37.11 o 0 16 0 1369.73 1309.36 67.91 o 1 16 0 251.23 286.35 26.09 o 2 16 0 1249.33 1227.14 71.61 o 3 16 0 1405.94 1454.64 80.12 o 4 16 0 39.31 60.74 37.44 o 5 16 0 13.52 0.16 31.36 o 6 16 0 541.94 573.76 47.71 o 7 16 0 415.08 367.08 42.03 o 8 16 0 42.35 -15.47 22.59 o 9 16 0 46.36 60.27 48.30 o 1 17 0 1026.77 1056.00 45.23 o 2 17 0 5385.76 5298.11 164.87 o 3 17 0 1.48 -1.73 28.80 o 4 17 0 537.39 491.62 73.41 o 5 17 0 74.60 42.59 34.35 o 6 17 0 261.72 166.17 31.01 o 7 17 0 349.69 323.04 39.97 o 8 17 0 146.92 92.50 39.71 o 0 18 0 67.08 74.57 29.25 o 1 18 0 6.09 28.41 18.61 o 2 18 0 72.37 159.39 43.09 o 3 18 0 271.40 329.60 60.88 o 4 18 0 6.71 37.34 37.69 o 5 18 0 37.04 25.22 33.69 o 6 18 0 247.67 210.42 56.89 o 7 18 0 43.01 30.51 34.46 o 1 19 0 870.32 897.99 63.48 o 2 19 0 427.45 408.33 38.11 o 3 19 0 84.79 51.03 38.24 o 4 19 0 76.72 29.15 34.91 o 5 19 0 424.65 358.65 69.82 o 6 19 0 30.53 57.44 41.58 o 0 20 0 392.80 425.14 54.77 o 1 20 0 22.55 56.83 25.01 o 2 20 0 9.40 -10.05 26.93 o 3 20 0 304.41 322.33 65.07 o 4 20 0 4.68 18.34 25.97 o 5 20 0 841.84 899.43 102.46 o 1 21 0 1235.95 1229.84 91.04 o 2 21 0 781.49 651.72 80.13 o 3 21 0 6.79 10.81 29.50 o -13 0 1 545.13 576.90 111.10 o -11 0 1 2104.00 2120.11 242.38 o -9 0 1 9.39 17.72 20.20 o -7 0 1 139.12 111.44 21.93 o -5 0 1 12056.69 11593.56 201.49 o -3 0 1 5135.25 5451.40 70.55 o 3 0 1 2303.82 2019.58 65.67 o 5 0 1 20129.35 18757.01 398.10 o 7 0 1 283.73 323.82 48.35 o 9 0 1 4572.56 4540.13 106.77 o 11 0 1 475.50 535.69 63.32 o 13 0 1 77.57 111.35 53.05 o -14 1 1 0.18 -11.47 32.19 o -13 1 1 11.72 14.22 35.54 o -12 1 1 85.82 125.46 31.25 o -11 1 1 1.51 -21.25 23.95 o -10 1 1 127.92 121.27 23.40 o -9 1 1 2534.66 2557.47 63.76 o -8 1 1 396.16 387.67 24.17 o -7 1 1 16.01 15.48 11.56 o -6 1 1 4708.40 4609.91 71.67 o -5 1 1 9346.71 9180.52 101.02 o -4 1 1 8.96 9.75 8.92 o -3 1 1 1828.73 2047.58 25.08 o -2 1 1 1306.69 1223.35 18.81 o -1 1 1 535.14 408.20 43.24 o 1 1 1 56.12 90.65 7.39 o 2 1 1 5328.75 5355.13 57.84 o 3 1 1 24217.18 23477.54 333.44 o 4 1 1 781.81 702.36 23.88 o 5 1 1 341.97 357.05 18.40 o 6 1 1 157.64 122.62 14.48 o 7 1 1 327.48 301.49 20.68 o 8 1 1 1408.81 1376.75 36.84 o 9 1 1 2579.15 2529.32 66.48 o 10 1 1 187.96 233.66 35.93 o 11 1 1 275.51 284.58 36.12 o 12 1 1 52.75 61.04 31.74 o 13 1 1 1238.85 1437.14 112.62 o -14 2 1 366.42 397.49 65.60 o -13 2 1 433.86 536.26 131.10 o -12 2 1 187.93 188.86 50.04 o -11 2 1 166.69 155.38 29.56 o -10 2 1 3888.36 3864.57 86.04 o -9 2 1 69.12 80.46 19.50 o -8 2 1 1087.61 1165.66 36.02 o -7 2 1 1460.94 1447.91 47.60 o -6 2 1 4747.94 4770.55 68.45 o -5 2 1 5794.52 5693.05 70.74 o -4 2 1 9034.13 8954.60 89.02 o -3 2 1 648.65 628.57 13.54 o -2 2 1 613.97 626.55 12.76 o -1 2 1 25137.00 26480.98 314.62 o 0 2 1 290.72 261.33 8.07 o 1 2 1 3033.35 2999.78 31.52 o 2 2 1 4251.88 4265.79 45.80 o 3 2 1 0.27 8.09 8.97 o 4 2 1 1954.56 1990.97 36.78 o 5 2 1 6796.51 6111.40 81.67 o 6 2 1 1465.06 1473.39 35.63 o 7 2 1 885.32 843.47 35.18 o 8 2 1 4583.97 4615.50 82.50 o 9 2 1 408.42 444.60 30.17 o 10 2 1 149.56 134.00 22.09 o 11 2 1 531.64 545.18 47.13 o 12 2 1 521.41 590.47 74.04 o 13 2 1 332.66 377.38 61.89 o -14 3 1 212.64 356.55 64.85 o -13 3 1 5.52 72.96 37.65 o -12 3 1 2.58 11.39 19.70 o -11 3 1 125.23 133.46 24.81 o -10 3 1 50.23 28.40 17.30 o -9 3 1 762.28 793.99 37.63 o -8 3 1 282.94 263.86 23.92 o -7 3 1 931.21 934.58 29.87 o -6 3 1 5952.74 5781.69 73.40 o -5 3 1 4239.33 4296.91 55.75 o -4 3 1 4125.35 4079.25 50.07 o -3 3 1 2340.58 2503.28 33.37 o -2 3 1 739.51 808.41 14.91 o -1 3 1 5.40 -2.75 7.10 o 0 3 1 14654.10 15234.89 138.80 o 1 3 1 14779.11 15666.97 124.79 o 2 3 1 1.74 -1.86 7.07 o 3 3 1 8505.71 8116.62 103.75 o 4 3 1 3017.10 2764.20 45.65 o 5 3 1 1647.06 1605.72 36.78 o 6 3 1 766.49 760.62 29.83 o 7 3 1 813.78 758.25 30.11 o 8 3 1 3344.53 3271.79 73.63 o 9 3 1 1889.95 1757.05 51.09 o 10 3 1 1377.45 1325.55 44.46 o 11 3 1 323.11 280.33 46.74 o 12 3 1 48.69 0.41 40.44 o 13 3 1 615.38 680.03 170.26 o -14 4 1 34.36 7.42 32.25 o -13 4 1 665.30 758.10 83.25 o -12 4 1 31.21 124.34 32.13 o -11 4 1 768.16 815.64 40.36 o -10 4 1 607.71 610.17 34.09 o -9 4 1 39.12 57.44 16.85 o -8 4 1 12.70 8.85 12.94 o -7 4 1 1360.26 1366.40 37.55 o -6 4 1 100.16 79.70 13.69 o -5 4 1 282.05 228.39 14.23 o -4 4 1 77.69 68.60 9.87 o -3 4 1 1413.93 1465.02 25.16 o -2 4 1 3455.11 3522.77 47.24 o -1 4 1 8401.37 8218.85 107.50 o 0 4 1 11294.17 12214.76 106.47 o 1 4 1 2471.15 2603.99 28.32 o 2 4 1 69.16 59.81 8.25 o 3 4 1 2557.45 2703.65 38.08 o 4 4 1 138.27 162.88 12.34 o 5 4 1 5093.94 4903.88 68.38 o 6 4 1 100.22 65.62 12.31 o 7 4 1 1427.79 1390.56 48.40 o 8 4 1 3882.73 3741.67 72.51 o 9 4 1 34.75 35.64 16.98 o 10 4 1 1944.22 1936.73 52.11 o 11 4 1 6.42 19.46 17.38 o 12 4 1 453.16 442.68 67.08 o 13 4 1 365.08 378.59 64.41 o -13 5 1 18.92 1.60 48.85 o -12 5 1 470.49 489.66 48.03 o -11 5 1 23.60 58.43 19.67 o -10 5 1 87.43 74.47 18.87 o -9 5 1 2884.16 2844.15 58.02 o -8 5 1 428.25 426.17 23.61 o -7 5 1 559.54 567.17 25.75 o -6 5 1 2394.08 2237.41 44.88 o -5 5 1 2715.48 2489.91 44.51 o -4 5 1 11257.88 11106.41 124.25 o -3 5 1 364.59 444.08 16.37 o -2 5 1 136.29 153.21 12.39 o -1 5 1 131.44 140.53 9.51 o 0 5 1 4119.40 3994.96 45.97 o 1 5 1 3277.97 3262.68 35.38 o 2 5 1 276.77 296.87 12.57 o 3 5 1 5385.92 5254.35 61.66 o 4 5 1 1976.23 2027.93 36.44 o 5 5 1 312.70 327.14 17.64 o 6 5 1 12.76 -0.66 10.56 o 7 5 1 182.32 231.70 19.18 o 8 5 1 1190.98 1198.70 37.17 o 9 5 1 1991.50 1935.10 59.36 o 10 5 1 206.15 216.76 21.75 o 11 5 1 10.79 -7.48 17.29 o 12 5 1 29.29 58.17 33.18 o 13 5 1 598.88 766.96 114.89 o -13 6 1 1047.84 1074.74 129.13 o -12 6 1 163.26 247.69 49.39 o -11 6 1 2176.91 2205.44 60.56 o -10 6 1 964.87 933.35 39.11 o -9 6 1 1725.21 1669.69 43.73 o -8 6 1 388.54 419.40 23.39 o -7 6 1 1376.62 1352.28 46.21 o -6 6 1 956.56 832.27 27.68 o -5 6 1 4367.68 4347.78 76.70 o -4 6 1 8.72 2.36 7.69 o -3 6 1 765.13 758.17 15.62 o -2 6 1 2890.13 2970.00 43.55 o -1 6 1 2807.11 2655.22 39.14 o 0 6 1 3.11 7.85 7.06 o 1 6 1 8766.41 9679.58 108.38 o 2 6 1 217.85 243.93 11.95 o 3 6 1 111.28 100.35 8.95 o 4 6 1 1592.20 1748.23 33.02 o 5 6 1 7960.26 7982.62 99.21 o 6 6 1 337.33 369.57 19.83 o 7 6 1 197.13 194.53 19.12 o 8 6 1 748.66 834.70 32.02 o 9 6 1 805.74 847.85 34.70 o 10 6 1 1042.63 1158.48 55.77 o 11 6 1 110.94 102.41 21.92 o 12 6 1 126.82 275.74 80.13 o 13 6 1 27.52 47.84 40.42 o -12 7 1 27.04 27.35 25.64 o -11 7 1 7.96 8.81 20.81 o -10 7 1 60.84 64.23 18.10 o -9 7 1 2383.89 2342.89 47.54 o -8 7 1 2195.27 2173.99 45.21 o -7 7 1 717.17 660.97 23.34 o -6 7 1 5064.87 4899.13 78.42 o -5 7 1 1769.90 1670.16 37.43 o -4 7 1 2416.35 2207.61 36.39 o -3 7 1 1878.05 1697.95 25.11 o -2 7 1 3224.77 3306.30 52.71 o -1 7 1 3326.67 3393.03 52.08 o 0 7 1 5587.58 5575.58 62.94 o 1 7 1 8926.49 9118.76 97.59 o 2 7 1 27.95 18.28 7.37 o 3 7 1 1326.17 1214.60 24.30 o 4 7 1 4836.77 4618.75 55.56 o 5 7 1 6493.76 6329.66 74.87 o 6 7 1 1245.22 1242.27 31.94 o 7 7 1 1123.29 1140.76 33.45 o 8 7 1 877.52 927.74 32.75 o 9 7 1 35.57 13.27 14.87 o 10 7 1 885.01 936.89 44.41 o 11 7 1 375.96 370.90 36.52 o 12 7 1 242.17 256.39 51.87 o 13 7 1 211.99 162.48 56.94 o -13 8 1 296.31 282.41 72.25 o -12 8 1 141.81 153.03 51.33 o -11 8 1 451.68 419.30 39.14 o -10 8 1 3777.59 3867.27 84.19 o -9 8 1 1277.38 1301.42 45.02 o -8 8 1 2532.41 2583.99 59.16 o -7 8 1 534.21 527.03 30.68 o -6 8 1 5293.04 5165.49 81.67 o -5 8 1 1275.72 1254.02 32.33 o -4 8 1 5605.68 5206.40 73.96 o -3 8 1 170.18 150.52 15.30 o -2 8 1 5597.13 5902.85 89.99 o -1 8 1 763.30 758.40 18.04 o 0 8 1 164.05 179.60 10.85 o 1 8 1 60.07 54.35 7.87 o 2 8 1 934.53 918.48 19.57 o 3 8 1 2429.85 2379.66 48.85 o 4 8 1 0.39 -6.85 9.80 o 5 8 1 591.45 553.27 24.97 o 6 8 1 872.94 865.68 26.26 o 7 8 1 9.17 2.04 11.90 o 8 8 1 3654.60 3588.91 120.79 o 9 8 1 844.25 846.37 33.72 o 10 8 1 460.45 488.73 43.88 o 11 8 1 194.93 162.39 31.69 o 12 8 1 1125.29 1195.59 94.79 o -12 9 1 365.18 415.59 77.70 o -11 9 1 1044.88 1159.99 69.96 o -10 9 1 1.62 12.02 30.67 o -9 9 1 3.49 -17.60 17.90 o -8 9 1 5850.68 5582.01 107.32 o -7 9 1 54.69 55.60 15.78 o -6 9 1 5204.62 5028.41 80.43 o -5 9 1 247.29 243.03 16.43 o -4 9 1 2241.07 2271.35 41.53 o -3 9 1 1608.52 1679.16 47.15 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