#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/07/2210700.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210700_Fobs loop_ _publ_author_name 'Coe, Benjamin J.' 'Fitzgerald, Emma C.' 'Raftery, James' _publ_section_title ; 1,2,7,8-Tetramethyl-4,5-dihydro-3a,5a-diazapyrene ditriflate ; _journal_coeditor_code LH2168 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4335 _journal_page_last o4336 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.284 _cell_angle_gamma 90.000 _cell_length_a 12.8820 _cell_length_b 8.1520 _cell_length_c 22.5850 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.7502 _[local]_cod_data_source_file lh2168IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' s2402m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 266.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3983.12 3548.40 426.15 o 2 0 0 24576.22 25153.08 753.45 o 3 0 0 0.70 14.93 3.58 o 4 0 0 106.37 104.44 6.31 o 5 0 0 16551.20 16574.55 233.12 o 6 0 0 1164.49 1467.49 47.85 o 7 0 0 5362.43 5291.99 139.26 o 8 0 0 690.99 645.49 18.60 o 9 0 0 453.09 546.14 20.36 o 10 0 0 4276.97 4347.50 111.54 o 11 0 0 96.96 56.09 9.72 o 12 0 0 755.41 685.50 24.42 o 13 0 0 6.27 0.17 15.13 o 14 0 0 214.08 221.14 31.76 o 1 1 0 675.66 748.58 33.45 o 2 1 0 6718.90 7112.38 286.08 o 3 1 0 142.36 103.85 4.09 o 4 1 0 253.33 234.14 6.12 o 5 1 0 12070.65 12181.14 297.07 o 6 1 0 5384.57 5734.65 72.68 o 7 1 0 53.27 65.77 5.38 o 8 1 0 430.96 404.66 12.11 o 9 1 0 526.97 529.58 14.40 o 10 1 0 122.25 113.62 8.14 o 11 1 0 36.28 26.76 6.34 o 12 1 0 14.01 32.77 8.54 o 13 1 0 4.95 19.74 12.39 o 14 1 0 49.18 50.05 21.95 o 15 1 0 7.82 0.83 16.96 o 16 1 0 16.15 16.79 21.12 o 0 2 0 9538.73 9767.38 440.88 o 1 2 0 13.70 2.25 2.46 o 2 2 0 1199.05 1025.02 38.01 o 3 2 0 49.52 43.17 3.13 o 4 2 0 8.78 6.34 3.01 o 5 2 0 7488.73 7684.76 184.84 o 6 2 0 643.90 564.05 19.74 o 7 2 0 802.90 713.66 15.17 o 8 2 0 612.15 563.91 12.66 o 9 2 0 1387.64 1192.70 38.68 o 10 2 0 14.53 6.19 5.11 o 11 2 0 325.86 277.04 14.76 o 12 2 0 23.06 17.33 8.91 o 13 2 0 54.34 56.27 11.98 o 14 2 0 57.77 57.78 15.18 o 15 2 0 2.81 -5.15 16.96 o 16 2 0 177.28 137.67 31.92 o 1 3 0 3412.83 3535.80 98.08 o 2 3 0 4115.94 4221.58 110.44 o 3 3 0 123.26 183.60 8.14 o 4 3 0 4609.37 5012.39 140.58 o 5 3 0 1416.28 1474.60 31.93 o 6 3 0 588.05 659.78 11.77 o 7 3 0 1.34 1.90 4.33 o 8 3 0 401.41 351.29 14.55 o 9 3 0 3.74 11.11 5.85 o 10 3 0 10.56 3.09 6.79 o 11 3 0 260.38 259.38 18.03 o 12 3 0 581.01 684.38 27.09 o 13 3 0 4.15 10.80 9.34 o 14 3 0 1202.59 1291.65 53.31 o 15 3 0 24.64 13.47 19.45 o 0 4 0 1221.99 1368.38 35.69 o 1 4 0 65.69 77.63 5.35 o 2 4 0 304.63 340.35 11.92 o 3 4 0 435.08 431.00 20.68 o 4 4 0 87.81 102.42 7.32 o 5 4 0 86.30 112.57 8.43 o 6 4 0 437.60 334.44 11.75 o 7 4 0 2755.55 2776.29 86.45 o 8 4 0 1128.33 1098.15 29.12 o 9 4 0 1248.07 1378.81 30.02 o 10 4 0 389.41 355.39 27.14 o 11 4 0 95.88 100.79 13.88 o 12 4 0 169.38 183.95 17.33 o 13 4 0 232.48 268.20 20.06 o 14 4 0 0.63 0.55 9.11 o 15 4 0 1.94 -4.66 14.63 o 1 5 0 332.47 386.26 9.62 o 2 5 0 673.55 744.18 30.31 o 3 5 0 675.30 669.41 26.54 o 4 5 0 1205.91 1240.40 52.97 o 5 5 0 9.15 5.43 5.06 o 6 5 0 3.41 2.64 5.11 o 7 5 0 75.80 101.22 9.16 o 8 5 0 1425.77 1367.94 49.97 o 9 5 0 302.25 311.78 16.29 o 10 5 0 510.86 418.96 22.40 o 11 5 0 31.90 29.75 10.26 o 12 5 0 7.57 6.94 9.22 o 13 5 0 20.38 11.16 9.81 o 14 5 0 40.02 55.31 13.81 o 0 6 0 730.09 725.33 28.12 o 1 6 0 822.52 796.74 30.57 o 2 6 0 85.29 95.19 8.14 o 3 6 0 1.00 4.22 5.50 o 4 6 0 895.75 917.66 39.26 o 5 6 0 103.67 92.04 8.92 o 6 6 0 15.23 8.64 6.11 o 7 6 0 1773.93 1832.29 93.14 o 8 6 0 31.39 23.54 8.35 o 9 6 0 534.94 632.37 27.50 o 10 6 0 188.45 197.96 18.05 o 11 6 0 195.72 217.13 19.41 o 12 6 0 60.51 67.19 13.99 o 13 6 0 1.86 7.40 9.85 o 1 7 0 1020.81 921.01 24.43 o 2 7 0 901.80 864.16 29.65 o 3 7 0 9.86 11.16 7.51 o 4 7 0 297.62 328.57 14.37 o 5 7 0 0.55 5.35 7.25 o 6 7 0 346.44 324.24 16.77 o 7 7 0 1370.03 1344.11 45.79 o 8 7 0 9.98 7.54 9.09 o 9 7 0 140.36 147.79 16.74 o 10 7 0 1439.10 1355.84 68.24 o 11 7 0 33.74 41.46 12.71 o 12 7 0 339.11 338.27 24.76 o 0 8 0 2767.55 3049.30 95.11 o 1 8 0 10.11 14.88 8.45 o 2 8 0 274.52 317.81 17.16 o 3 8 0 195.03 200.29 14.95 o 4 8 0 836.04 732.70 24.43 o 5 8 0 40.08 33.78 11.55 o 6 8 0 612.94 594.60 26.85 o 7 8 0 43.58 59.45 13.15 o 8 8 0 277.66 253.47 20.72 o 9 8 0 8.06 3.02 9.51 o 10 8 0 45.97 50.48 14.41 o 1 9 0 162.25 147.45 14.40 o 2 9 0 54.86 56.70 11.09 o 3 9 0 4.13 8.27 10.26 o 4 9 0 253.73 266.00 20.83 o 5 9 0 378.21 452.20 25.12 o 6 9 0 18.35 13.81 12.05 o 7 9 0 39.06 53.87 16.61 o 8 9 0 7.53 4.87 12.28 o 0 10 0 164.84 198.70 37.24 o 1 10 0 2.27 4.53 8.96 o 2 10 0 43.42 37.45 12.30 o 3 10 0 224.82 225.97 20.79 o 4 10 0 97.75 93.11 15.77 o 5 10 0 49.18 54.87 25.77 o -16 1 1 91.88 87.46 26.77 o -15 1 1 145.32 129.53 28.93 o -14 1 1 415.73 455.25 42.40 o -13 1 1 156.00 127.73 17.79 o -12 1 1 136.82 172.53 11.45 o -11 1 1 20.54 30.22 6.44 o -10 1 1 600.46 669.56 15.34 o -9 1 1 15.73 19.49 4.86 o -8 1 1 38.42 42.20 5.08 o -7 1 1 8432.47 8782.76 201.29 o -6 1 1 2939.60 3252.31 44.02 o -5 1 1 42532.13 43886.19 940.44 o -4 1 1 6446.05 6728.11 202.85 o -3 1 1 1716.55 1766.87 45.84 o -2 1 1 340.27 374.51 10.97 o -1 1 1 3898.26 4286.17 125.55 o 0 1 1 2.36 25.83 4.12 o 1 1 1 12086.03 13261.17 406.41 o 2 1 1 11116.43 11667.30 261.69 o 3 1 1 5802.22 6216.84 129.14 o 4 1 1 285.81 204.15 7.57 o 5 1 1 9929.54 10765.91 255.34 o 6 1 1 101.02 141.12 7.16 o 7 1 1 133.94 141.20 7.03 o 8 1 1 850.26 787.78 19.58 o 9 1 1 663.95 544.19 13.34 o 10 1 1 1730.56 1917.93 50.73 o 11 1 1 62.71 86.78 8.93 o 12 1 1 12.62 0.02 6.21 o 13 1 1 246.48 256.33 22.46 o 14 1 1 121.28 134.35 28.43 o 15 1 1 7.61 15.30 20.29 o 16 1 1 147.61 165.44 33.59 o -16 2 1 210.43 202.19 36.41 o -15 2 1 2.20 2.49 17.29 o -14 2 1 259.61 250.82 24.17 o -13 2 1 382.36 382.75 21.40 o -12 2 1 751.51 652.80 25.51 o -11 2 1 836.80 670.90 33.89 o -10 2 1 3488.93 3474.34 67.47 o -9 2 1 933.03 857.24 20.58 o -8 2 1 25.09 31.78 4.96 o -7 2 1 1764.09 1624.80 33.93 o -6 2 1 536.27 582.02 16.57 o -5 2 1 1985.32 2129.08 39.18 o -4 2 1 467.85 521.94 19.50 o -3 2 1 7386.82 7950.55 224.12 o -2 2 1 10160.32 11153.33 204.40 o -1 2 1 184.18 218.21 5.16 o 0 2 1 60341.57 62419.18 1569.75 o 1 2 1 11.51 21.89 2.92 o 2 2 1 558.02 576.67 15.52 o 3 2 1 2250.16 2267.04 41.09 o 4 2 1 15.93 23.72 3.58 o 5 2 1 5356.44 5773.75 158.29 o 6 2 1 631.41 683.41 18.75 o 7 2 1 2797.16 2773.02 45.59 o 8 2 1 1042.99 930.83 29.05 o 9 2 1 821.86 765.27 24.12 o 10 2 1 81.29 77.08 9.49 o 11 2 1 434.42 386.52 16.71 o 12 2 1 121.65 101.95 13.30 o 13 2 1 288.78 307.00 19.62 o 14 2 1 965.23 1004.61 62.02 o 15 2 1 24.52 23.44 21.28 o 16 2 1 121.50 112.57 29.60 o -15 3 1 24.52 46.91 16.21 o -14 3 1 39.54 28.60 13.57 o -13 3 1 684.11 655.08 38.95 o -12 3 1 65.42 54.12 11.64 o -11 3 1 95.56 83.72 12.54 o -10 3 1 77.15 71.42 9.52 o -9 3 1 1167.76 1225.01 51.47 o -8 3 1 442.04 442.23 13.50 o -7 3 1 465.43 454.75 13.45 o -6 3 1 674.20 684.06 21.54 o -5 3 1 1.28 3.66 4.30 o -4 3 1 81.83 94.07 5.16 o -3 3 1 614.04 658.02 19.81 o -2 3 1 1170.63 1139.48 26.24 o -1 3 1 563.09 599.01 13.56 o 0 3 1 1984.08 2024.75 51.82 o 1 3 1 410.60 364.11 10.83 o 2 3 1 2276.77 2595.26 100.93 o 3 3 1 4950.39 5403.55 174.92 o 4 3 1 230.67 269.39 10.58 o 5 3 1 539.22 440.46 12.57 o 6 3 1 801.98 677.77 12.02 o 7 3 1 756.88 750.57 21.76 o 8 3 1 156.76 144.38 9.19 o 9 3 1 153.47 195.51 12.71 o 10 3 1 11.94 6.01 6.96 o 11 3 1 59.03 52.39 9.62 o 12 3 1 80.99 77.84 12.88 o 13 3 1 51.80 46.36 11.61 o 14 3 1 43.63 66.93 13.46 o 15 3 1 43.56 50.88 24.44 o -15 4 1 240.41 261.05 38.08 o -14 4 1 26.44 14.72 9.91 o -13 4 1 1128.63 1183.95 64.37 o -12 4 1 348.18 362.36 21.63 o -11 4 1 123.24 126.58 14.74 o -10 4 1 297.82 263.23 18.26 o -9 4 1 1267.05 1292.41 48.16 o -8 4 1 1467.89 1394.78 36.96 o -7 4 1 3321.58 3389.81 102.09 o -6 4 1 2127.64 2331.44 63.10 o -5 4 1 263.33 243.83 9.92 o -4 4 1 643.83 658.08 14.40 o -3 4 1 2239.25 2105.18 110.51 o -2 4 1 80.15 90.05 5.33 o -1 4 1 578.09 475.88 10.10 o 0 4 1 23.37 36.35 4.70 o 1 4 1 1.74 0.84 3.62 o 2 4 1 1227.64 1233.02 48.01 o 3 4 1 5077.21 5532.95 151.30 o 4 4 1 84.55 99.38 7.24 o 5 4 1 34.25 44.17 5.92 o 6 4 1 386.49 375.06 12.37 o 7 4 1 1870.41 1899.79 48.24 o 8 4 1 24.79 25.39 7.74 o 9 4 1 1945.98 2056.56 95.97 o 10 4 1 24.61 28.87 8.72 o 11 4 1 17.19 9.58 9.30 o 12 4 1 301.97 319.48 20.48 o 13 4 1 404.76 402.65 23.77 o 14 4 1 1309.55 1205.30 72.33 o -14 5 1 548.70 567.32 52.38 o -13 5 1 6.96 5.54 8.74 o -12 5 1 625.03 636.66 33.86 o -11 5 1 482.65 500.67 37.36 o -10 5 1 522.35 603.34 26.36 o -9 5 1 185.69 183.30 16.37 o -8 5 1 48.86 51.78 9.08 o -7 5 1 245.33 236.62 12.05 o -6 5 1 101.27 110.29 8.81 o -5 5 1 319.96 308.67 13.44 o -4 5 1 1523.31 1726.17 64.24 o -3 5 1 21.71 25.38 5.65 o -2 5 1 3792.71 3975.03 158.49 o -1 5 1 865.56 818.01 13.62 o 0 5 1 1016.01 1107.78 31.48 o 1 5 1 464.90 406.89 9.77 o 2 5 1 4366.70 4575.86 168.84 o 3 5 1 1132.52 1077.03 45.40 o 4 5 1 382.75 382.21 12.73 o 5 5 1 53.09 73.71 7.50 o 6 5 1 1495.50 1448.95 53.86 o 7 5 1 269.97 283.06 14.84 o 8 5 1 392.03 352.88 16.64 o 9 5 1 610.56 715.62 35.66 o 10 5 1 154.92 150.04 15.89 o 11 5 1 658.81 672.22 29.78 o 12 5 1 501.85 515.66 45.71 o 13 5 1 80.06 95.75 15.60 o 14 5 1 5.97 8.49 12.03 o -13 6 1 302.62 336.16 24.01 o -12 6 1 34.10 54.22 13.15 o -11 6 1 0.24 1.92 8.53 o -10 6 1 63.80 61.97 12.75 o -9 6 1 178.85 162.49 16.51 o -8 6 1 391.27 342.86 28.06 o -7 6 1 10.09 12.99 7.79 o -6 6 1 299.34 255.39 12.67 o -5 6 1 206.99 157.71 11.91 o -4 6 1 452.80 438.03 14.74 o -3 6 1 1362.79 1513.26 44.57 o -2 6 1 107.61 101.06 8.36 o -1 6 1 32.51 53.44 8.10 o 0 6 1 318.10 292.15 23.09 o 1 6 1 1603.98 1343.66 41.27 o 2 6 1 770.09 871.44 25.59 o 3 6 1 871.22 790.84 31.46 o 4 6 1 321.90 259.16 13.85 o 5 6 1 132.61 119.85 9.69 o 6 6 1 145.51 164.23 12.80 o 7 6 1 498.05 496.15 19.58 o 8 6 1 700.18 701.94 38.61 o 9 6 1 668.39 617.57 41.55 o 10 6 1 409.60 404.40 23.48 o 11 6 1 511.54 480.78 25.99 o 12 6 1 26.90 33.95 12.02 o 13 6 1 212.59 229.69 25.85 o -12 7 1 2.22 6.38 10.84 o -11 7 1 303.63 304.00 22.82 o -10 7 1 841.85 819.56 33.01 o -9 7 1 116.10 113.89 20.10 o -8 7 1 1625.50 1508.04 58.11 o -7 7 1 1249.93 1305.07 72.03 o -6 7 1 137.44 110.21 11.83 o -5 7 1 480.39 484.30 24.82 o -4 7 1 3.28 0.39 5.83 o -3 7 1 647.99 734.05 22.45 o -2 7 1 169.77 192.82 13.38 o -1 7 1 39.63 37.54 8.93 o 0 7 1 93.10 105.16 10.82 o 1 7 1 44.53 45.22 9.37 o 2 7 1 2593.08 2804.95 71.21 o 3 7 1 612.06 646.98 21.33 o 4 7 1 669.80 815.69 21.63 o 5 7 1 70.46 68.55 10.24 o 6 7 1 59.17 66.54 10.50 o 7 7 1 96.34 101.53 11.94 o 8 7 1 488.63 541.20 26.23 o 9 7 1 901.28 995.33 76.90 o 10 7 1 646.32 655.16 30.11 o 11 7 1 292.75 311.35 24.12 o 12 7 1 45.11 60.19 24.44 o -11 8 1 235.97 179.91 35.75 o -10 8 1 57.92 77.34 15.40 o -9 8 1 15.84 2.31 9.51 o -8 8 1 40.36 46.60 12.49 o -7 8 1 12.28 27.54 10.81 o -6 8 1 49.49 74.06 13.32 o -5 8 1 5.33 4.51 9.19 o -4 8 1 254.30 277.06 16.55 o -3 8 1 22.37 17.17 8.94 o -2 8 1 23.85 37.36 9.95 o -1 8 1 66.75 33.19 9.66 o 0 8 1 186.59 186.42 14.37 o 1 8 1 172.23 154.07 13.62 o 2 8 1 725.09 782.78 41.40 o 3 8 1 1716.58 1950.52 58.25 o 4 8 1 325.93 287.31 20.23 o 5 8 1 37.09 27.60 14.15 o 6 8 1 187.04 202.34 24.38 o 7 8 1 30.22 21.79 9.08 o 8 8 1 816.76 828.08 33.27 o 9 8 1 346.86 333.47 23.68 o 10 8 1 39.81 43.96 13.59 o -8 9 1 1.48 7.29 12.54 o -7 9 1 38.64 50.99 16.10 o -6 9 1 24.06 37.61 15.14 o -5 9 1 100.31 132.52 16.49 o -4 9 1 16.90 23.87 11.01 o -3 9 1 79.57 120.61 13.40 o -2 9 1 877.55 924.47 31.03 o -1 9 1 924.38 847.80 27.58 o 0 9 1 7.33 12.02 8.42 o 1 9 1 327.38 338.29 18.89 o 2 9 1 6.34 21.04 9.00 o 3 9 1 36.66 41.70 12.34 o 4 9 1 31.80 24.95 10.74 o 5 9 1 62.35 90.69 14.59 o 6 9 1 2.18 1.57 8.99 o 7 9 1 6.17 3.27 10.89 o -5 10 1 19.60 31.09 21.45 o -4 10 1 578.10 549.12 35.64 o -3 10 1 50.79 86.85 15.51 o -2 10 1 36.82 51.65 11.52 o -1 10 1 189.20 181.78 16.48 o 0 10 1 11.99 25.79 10.29 o 1 10 1 15.64 13.10 9.80 o 2 10 1 9.80 8.22 10.09 o 3 10 1 77.94 69.22 14.48 o 4 10 1 544.69 549.07 29.11 o 5 10 1 44.41 79.64 25.44 o -15 0 2 0.03 23.44 19.62 o -14 0 2 94.24 68.84 23.44 o -13 0 2 17.15 14.49 11.34 o -12 0 2 2416.04 2284.85 82.05 o -11 0 2 42.06 37.65 11.58 o -10 0 2 10137.76 10486.27 83.93 o -9 0 2 27.44 46.76 7.96 o -8 0 2 6.74 9.96 5.80 o -7 0 2 553.76 568.21 23.22 o -6 0 2 13122.96 14456.11 293.84 o -5 0 2 29185.30 30872.57 1374.20 o -4 0 2 26555.00 28421.69 985.46 o -3 0 2 4136.77 4662.32 117.71 o -2 0 2 21676.61 24011.37 466.58 o -1 0 2 165.59 238.72 20.45 o 0 0 2 6495.48 6442.03 52.96 o 1 0 2 1160.18 1107.14 10.91 o 2 0 2 1978.18 2047.75 26.54 o 3 0 2 3428.55 3482.62 35.48 o 4 0 2 871.84 728.86 14.24 o 5 0 2 70891.69 72809.18 1847.81 o 6 0 2 282.45 135.24 9.69 o 7 0 2 1560.56 1395.05 25.23 o 8 0 2 112.80 54.20 7.80 o 9 0 2 4.58 1.72 5.91 o 10 0 2 150.58 131.12 14.59 o 11 0 2 4636.70 4164.44 99.76 o 12 0 2 3348.46 3119.63 118.97 o 13 0 2 56.84 78.04 15.49 o 14 0 2 874.94 985.82 58.69 o -16 1 2 95.94 109.91 28.76 o -15 1 2 307.37 323.73 38.91 o -14 1 2 128.97 133.86 19.08 o -13 1 2 196.72 195.11 16.56 o -12 1 2 441.63 332.81 14.21 o -11 1 2 533.55 514.25 16.11 o -10 1 2 853.71 874.76 17.00 o -9 1 2 106.08 118.61 7.40 o -8 1 2 157.13 154.91 7.38 o -7 1 2 2822.40 2847.93 40.83 o -6 1 2 4334.35 4483.96 83.68 o -5 1 2 4337.87 4662.90 195.09 o -4 1 2 1156.12 1180.78 38.22 o -3 1 2 169.11 157.17 4.62 o -2 1 2 36.19 19.11 2.30 o -1 1 2 6209.05 6527.74 145.68 o 0 1 2 1440.23 1606.47 39.01 o 1 1 2 4987.23 5453.78 98.92 o 2 1 2 55.02 41.69 2.75 o 3 1 2 6487.58 6593.58 122.12 o 4 1 2 2492.39 2592.62 59.23 o 5 1 2 7131.37 7433.17 169.19 o 6 1 2 1219.31 1423.72 32.26 o 7 1 2 606.33 560.43 11.79 o 8 1 2 8.16 7.08 4.14 o 9 1 2 15.32 13.86 5.00 o 10 1 2 682.61 749.93 27.47 o 11 1 2 327.74 348.94 14.21 o 12 1 2 0.40 1.83 6.85 o 13 1 2 8.50 9.35 11.07 o 14 1 2 98.35 111.52 17.74 o 15 1 2 266.27 302.45 39.91 o 16 1 2 106.39 76.65 26.94 o -16 2 2 55.95 73.33 26.44 o -15 2 2 14.89 22.97 13.26 o -14 2 2 299.66 371.84 27.44 o -13 2 2 210.99 245.30 22.57 o -12 2 2 2379.25 2183.86 67.54 o -11 2 2 509.43 463.53 17.86 o -10 2 2 1186.34 1297.10 27.96 o -9 2 2 258.35 306.92 12.02 o -8 2 2 682.89 661.92 13.43 o -7 2 2 25.84 47.35 5.05 o -6 2 2 66.08 22.97 4.45 o -5 2 2 77.14 59.77 5.13 o -4 2 2 105.98 100.27 5.01 o -3 2 2 66.14 127.89 4.62 o -2 2 2 27.02 30.38 2.58 o -1 2 2 867.72 874.24 24.04 o 0 2 2 42474.91 44715.66 885.90 o 1 2 2 10652.49 11403.98 227.77 o 2 2 2 1409.83 1321.04 42.19 o 3 2 2 2841.06 2676.69 80.87 o 4 2 2 3916.61 3455.23 78.32 o 5 2 2 670.94 770.74 23.39 o 6 2 2 194.91 210.93 7.76 o 7 2 2 715.13 664.12 12.79 o 8 2 2 124.71 89.40 6.51 o 9 2 2 11.24 10.42 5.69 o 10 2 2 626.49 622.74 19.76 o 11 2 2 760.05 744.26 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132.81 154.63 24.51 o -6 1 28 100.77 98.98 20.72 o -5 1 28 62.54 69.69 19.62 o -4 1 28 67.35 52.28 17.52 o -3 1 28 7.19 5.05 11.88 o -2 1 28 3.27 -1.45 12.76 o -1 1 28 116.55 121.86 21.70 o 0 1 28 68.19 46.89 24.28 o 1 1 28 2.19 12.97 19.12 o -9 2 28 36.60 64.18 26.27 o -8 2 28 1.75 -6.82 16.29 o -7 2 28 108.99 142.45 22.73 o -6 2 28 272.90 270.25 28.98 o -5 2 28 28.11 25.88 16.48 o -4 2 28 0.15 -1.79 12.82 o -3 2 28 214.53 164.65 24.39 o -2 2 28 742.01 779.60 42.38 o 0 2 28 2.26 5.99 20.45 o 1 2 28 243.42 286.49 41.73 o -7 3 28 93.89 88.12 27.43 o -6 3 28 426.73 469.22 46.56 o -5 3 28 56.66 29.43 25.94 o -4 3 28 165.12 172.26 36.75 o -3 3 28 80.23 59.36 27.60 o -2 3 28 540.68 658.10 57.03 o -1 3 28 326.36 344.51 45.56 o -3 1 29 23.47 27.10 22.95 o