#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/07/2210732.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210732_Fobs loop_ _publ_author_name 'Meijboom, Reinout' _publ_section_title ; Di-\m-acetato-bis[(tri-p-tolylphosphine)silver(I)] ; _journal_coeditor_code NG2103 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2698 _journal_page_last m2700 _journal_volume 62 _journal_year 2006 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.456 _cell_angle_gamma 90.000 _cell_length_a 18.6210 _cell_length_b 10.2540 _cell_length_c 23.4810 _exptl_crystal_F_000 1920.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file ng2103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 490.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 240669.81 209036.14 18892.75 o 3 0 0 11220.31 10546.12 236.21 o 4 0 0 15839.03 17113.72 360.01 o 5 0 0 8314.44 8783.06 224.57 o 6 0 0 18068.17 17057.40 361.89 o 7 0 0 25983.63 24552.83 711.67 o 8 0 0 5785.92 6024.37 274.84 o 9 0 0 9153.87 9589.76 218.47 o 10 0 0 3034.74 3620.00 97.11 o 11 0 0 5481.24 5537.13 185.26 o 12 0 0 295.87 233.00 43.60 o 13 0 0 156.20 150.43 34.77 o 14 0 0 36.88 4.97 57.84 o 15 0 0 484.49 475.35 72.30 o 16 0 0 724.00 626.72 84.05 o 17 0 0 32.23 9.94 63.71 o 18 0 0 261.97 203.56 86.08 o 19 0 0 62.06 132.39 91.50 o 20 0 0 422.78 395.83 101.67 o 21 0 0 326.13 193.62 100.76 o 22 0 0 603.14 934.21 139.17 o 23 0 0 40.00 -232.71 116.35 o 0 1 0 48721.61 52925.76 1148.39 o 1 1 0 40.62 171.20 11.52 o 2 1 0 12822.14 12155.97 209.05 o 3 1 0 48406.18 46802.84 791.24 o 4 1 0 39823.40 42420.17 556.82 o 5 1 0 41996.42 44046.82 645.70 o 6 1 0 558.92 494.09 43.50 o 7 1 0 14713.14 14069.18 214.81 o 8 1 0 1663.62 1460.68 47.53 o 9 1 0 9782.08 9732.42 155.03 o 10 1 0 5878.65 5968.16 103.05 o 11 1 0 2675.59 2613.74 58.55 o 12 1 0 1525.63 1401.62 44.55 o 13 1 0 108.51 100.87 23.52 o 14 1 0 913.51 999.69 65.45 o 15 1 0 347.56 318.45 53.25 o 16 1 0 318.22 307.43 55.83 o 17 1 0 1054.60 1077.06 76.67 o 18 1 0 65.26 20.55 54.55 o 19 1 0 319.85 230.12 65.54 o 20 1 0 71.90 93.52 69.32 o 21 1 0 226.82 237.68 77.40 o 22 1 0 170.87 109.94 148.21 o 23 1 0 25.15 -53.77 82.67 o 0 2 0 26832.92 26800.98 462.19 o 1 2 0 8220.52 7815.17 106.45 o 2 2 0 11239.04 12154.70 211.57 o 3 2 0 31379.96 31479.18 535.32 o 4 2 0 261.43 154.61 14.06 o 5 2 0 29769.56 32642.50 556.02 o 6 2 0 9945.24 10016.28 180.69 o 7 2 0 19010.00 19877.69 268.14 o 8 2 0 7848.49 7469.15 124.80 o 9 2 0 103.19 76.52 25.01 o 10 2 0 8694.26 8101.21 134.77 o 11 2 0 1.81 15.93 20.34 o 12 2 0 9461.63 9091.80 306.21 o 13 2 0 9.29 12.15 28.77 o 14 2 0 9422.39 9237.58 231.32 o 15 2 0 206.65 218.32 49.31 o 16 2 0 5248.66 5327.59 234.06 o 17 2 0 826.79 791.51 75.91 o 18 2 0 1354.15 1378.33 96.13 o 19 2 0 411.56 464.44 72.29 o 20 2 0 396.61 439.00 74.99 o 21 2 0 180.96 270.31 80.50 o 22 2 0 11.64 114.61 83.17 o 23 2 0 58.52 186.98 93.77 o 0 3 0 2108.96 2277.07 61.01 o 1 3 0 17.25 20.18 9.99 o 2 3 0 363.69 509.47 21.66 o 3 3 0 6163.97 6159.18 115.43 o 4 3 0 204.31 227.68 17.78 o 5 3 0 3423.60 3732.53 77.90 o 6 3 0 1.36 22.04 16.84 o 7 3 0 10812.32 10758.07 195.85 o 8 3 0 206.05 196.55 17.80 o 9 3 0 119.23 161.60 19.07 o 10 3 0 1.83 -10.46 18.05 o 11 3 0 564.22 587.36 31.73 o 12 3 0 132.43 154.49 39.91 o 13 3 0 302.37 356.74 35.98 o 14 3 0 1494.03 1344.40 79.77 o 15 3 0 61.03 -42.32 45.60 o 16 3 0 1304.91 1174.67 78.29 o 17 3 0 18.40 53.70 57.16 o 18 3 0 316.83 347.94 69.16 o 19 3 0 341.88 247.45 89.24 o 20 3 0 516.15 611.59 86.24 o 21 3 0 106.09 7.27 80.27 o 22 3 0 100.36 210.49 88.02 o 23 3 0 35.01 57.15 93.55 o 0 4 0 5895.54 5424.46 103.58 o 1 4 0 0.16 -8.74 10.15 o 2 4 0 11720.57 12424.50 170.45 o 3 4 0 151.29 168.99 31.40 o 4 4 0 16238.66 16828.73 297.04 o 5 4 0 411.27 473.54 27.34 o 6 4 0 11200.44 10827.62 266.21 o 7 4 0 158.93 258.72 43.62 o 8 4 0 5859.08 5696.61 117.00 o 9 4 0 725.24 760.87 34.00 o 10 4 0 1604.36 1588.75 86.40 o 11 4 0 555.79 518.14 33.29 o 12 4 0 1238.89 1344.28 90.63 o 13 4 0 220.10 187.81 36.33 o 14 4 0 1681.57 1841.66 90.45 o 15 4 0 332.29 364.94 86.76 o 16 4 0 167.45 98.76 57.15 o 17 4 0 87.20 19.38 60.63 o 18 4 0 26.08 -23.17 77.49 o 19 4 0 53.00 90.83 69.69 o 20 4 0 36.97 109.66 74.27 o 21 4 0 0.38 -104.38 77.89 o 22 4 0 0.27 98.98 86.38 o 0 5 0 9269.61 9272.00 231.98 o 1 5 0 1170.41 1251.45 30.39 o 2 5 0 3961.91 4801.42 97.28 o 3 5 0 529.29 559.08 25.56 o 4 5 0 14.23 42.50 18.89 o 5 5 0 1660.45 1804.00 68.91 o 6 5 0 2008.13 2078.96 60.12 o 7 5 0 422.50 416.82 31.13 o 8 5 0 41.11 62.47 42.68 o 9 5 0 275.98 269.37 32.59 o 10 5 0 2.03 -4.04 24.56 o 11 5 0 128.08 103.22 23.97 o 12 5 0 413.23 416.22 31.73 o 13 5 0 38.00 -14.81 35.95 o 14 5 0 44.75 -20.69 38.04 o 15 5 0 17.24 -59.66 52.15 o 16 5 0 87.35 29.05 56.95 o 17 5 0 162.99 172.79 65.70 o 18 5 0 162.74 71.84 67.98 o 19 5 0 2.06 -76.21 72.49 o 20 5 0 42.65 45.04 137.36 o 21 5 0 9.68 49.62 85.78 o 22 5 0 6.00 71.60 92.17 o 0 6 0 13172.21 12520.91 228.23 o 1 6 0 594.10 727.55 33.75 o 2 6 0 12867.08 12438.73 175.95 o 3 6 0 1.31 -4.39 20.45 o 4 6 0 9134.32 9321.11 153.89 o 5 6 0 876.63 853.69 37.73 o 6 6 0 1192.14 1143.40 43.70 o 7 6 0 1260.89 1038.27 51.00 o 8 6 0 2248.85 2255.19 103.10 o 9 6 0 2.05 10.65 35.74 o 10 6 0 1993.11 2015.28 69.30 o 11 6 0 9.10 23.25 30.11 o 12 6 0 1611.94 1620.94 59.47 o 13 6 0 108.27 92.06 40.79 o 14 6 0 209.27 289.41 56.34 o 15 6 0 227.09 168.76 58.42 o 16 6 0 15.29 -80.85 58.87 o 17 6 0 0.15 67.53 64.25 o 18 6 0 22.65 95.54 73.67 o 19 6 0 49.17 -82.68 76.49 o 20 6 0 22.69 -2.91 79.23 o 21 6 0 23.09 27.02 96.81 o 0 7 0 11098.28 10983.92 206.69 o 1 7 0 419.46 432.67 31.97 o 2 7 0 6526.44 5969.44 96.18 o 3 7 0 139.20 123.02 24.49 o 4 7 0 1196.52 1380.38 48.31 o 5 7 0 826.09 984.06 51.38 o 6 7 0 401.92 351.73 44.87 o 7 7 0 560.38 626.23 36.94 o 8 7 0 19.27 93.19 32.12 o 9 7 0 441.45 416.51 43.62 o 10 7 0 579.63 636.65 47.50 o 11 7 0 1597.63 1647.72 62.03 o 12 7 0 190.99 202.29 38.66 o 13 7 0 824.71 973.57 61.67 o 14 7 0 231.08 321.74 60.98 o 15 7 0 47.29 29.39 72.18 o 16 7 0 58.32 36.62 65.01 o 17 7 0 5.44 -46.36 67.23 o 18 7 0 56.62 82.20 76.25 o 19 7 0 69.17 -43.92 82.74 o 20 7 0 29.33 -53.46 91.42 o 0 8 0 346.84 452.15 38.43 o 1 8 0 1074.92 1080.44 43.23 o 2 8 0 793.08 854.14 43.77 o 3 8 0 2600.22 2536.71 90.82 o 4 8 0 171.81 105.22 30.19 o 5 8 0 929.51 1020.59 47.27 o 6 8 0 194.32 205.34 32.31 o 7 8 0 1038.14 1139.12 51.89 o 8 8 0 1888.83 2030.98 66.04 o 9 8 0 1450.98 1714.45 74.48 o 10 8 0 3075.39 3218.11 91.47 o 11 8 0 658.33 873.12 55.84 o 12 8 0 3050.42 3050.15 122.19 o 13 8 0 28.64 -19.05 48.43 o 14 8 0 1735.94 1769.43 89.25 o 15 8 0 127.85 286.48 102.12 o 16 8 0 294.29 206.50 108.22 o 0 9 0 1578.48 1791.83 132.17 o 1 9 0 46.35 -54.72 96.70 o 2 9 0 2592.72 2598.42 106.97 o 3 9 0 2187.33 2161.43 97.17 o 4 9 0 2.56 -99.53 49.77 o 5 9 0 4101.88 4245.61 275.52 o 6 9 0 486.91 342.47 55.87 o 7 9 0 2613.87 2471.98 108.86 o 8 9 0 1247.51 1228.93 65.15 o 9 9 0 570.19 698.99 57.59 o 10 9 0 997.96 1033.35 66.24 o 11 9 0 1.04 5.73 51.40 o 12 9 0 1358.42 1416.43 96.15 o 13 9 0 79.80 155.42 72.09 o 14 9 0 670.25 660.46 89.94 o 15 9 0 64.57 25.08 124.26 o 16 9 0 175.10 -41.34 130.36 o 17 9 0 318.63 580.63 149.56 o 0 10 0 1710.48 1689.04 140.53 o 1 10 0 24.68 40.31 55.18 o 2 10 0 2962.17 2849.93 118.86 o 3 10 0 549.88 601.42 135.56 o 4 10 0 1681.59 1603.05 98.24 o 5 10 0 2430.90 2293.92 168.77 o 6 10 0 367.40 410.61 68.84 o 7 10 0 1282.19 1249.07 154.20 o 8 10 0 57.53 8.41 62.20 o 9 10 0 640.75 580.75 76.82 o 10 10 0 21.70 29.25 65.83 o 11 10 0 40.66 72.20 72.18 o 12 10 0 41.93 -94.66 97.15 o 13 10 0 12.20 -213.95 107.77 o 14 10 0 92.80 104.60 111.83 o 0 11 0 702.14 463.38 99.41 o 1 11 0 69.23 0.01 59.86 o 2 11 0 347.28 350.84 74.29 o 3 11 0 99.06 67.44 64.66 o 4 11 0 210.30 259.37 66.51 o 5 11 0 550.78 423.79 74.21 o 6 11 0 243.63 205.63 77.49 o 7 11 0 303.94 262.97 74.83 o 8 11 0 29.97 -5.58 74.71 o 9 11 0 533.67 570.17 86.75 o 10 11 0 2.20 -78.14 91.95 o 11 11 0 182.58 140.75 114.32 o 12 11 0 36.24 65.97 120.65 o 13 11 0 7.88 53.77 121.78 o 0 12 0 6.64 4.52 98.96 o 1 12 0 5.03 -123.14 71.17 o 2 12 0 0.25 -77.42 75.57 o 3 12 0 20.20 15.46 72.01 o 4 12 0 8.18 34.10 77.73 o 5 12 0 0.35 -14.84 79.33 o 6 12 0 1.36 45.28 80.95 o 7 12 0 31.45 -58.74 80.71 o 8 12 0 16.94 -84.21 82.93 o 9 12 0 39.53 59.81 88.19 o 10 12 0 41.78 89.75 239.60 o 11 12 0 101.47 260.04 139.85 o 0 13 0 4.71 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70.63 o -12 2 1 490.42 562.40 46.53 o -11 2 1 2548.81 2305.57 61.21 o -10 2 1 335.41 503.61 31.96 o -9 2 1 4365.72 4670.65 97.21 o -8 2 1 464.64 623.46 31.53 o -7 2 1 112.86 257.74 17.68 o -6 2 1 2230.19 2221.23 60.65 o -5 2 1 3867.51 4223.01 82.65 o -4 2 1 4292.16 5113.42 95.87 o -3 2 1 4912.24 4433.80 83.68 o -2 2 1 4718.29 5455.19 120.97 o -1 2 1 3041.83 2655.52 40.71 o 0 2 1 25675.82 27730.55 365.07 o 1 2 1 194.16 89.11 9.08 o 2 2 1 45465.71 45529.76 769.20 o 3 2 1 20797.61 19810.79 339.92 o 4 2 1 15131.17 15997.16 292.65 o 5 2 1 3961.67 4200.85 71.52 o 6 2 1 3702.32 3519.82 64.93 o 7 2 1 3877.88 3910.06 62.63 o 8 2 1 266.30 318.05 17.40 o 9 2 1 3347.76 3476.53 67.91 o 10 2 1 1627.44 1576.98 44.88 o 11 2 1 3693.57 3410.22 70.35 o 12 2 1 2569.17 2642.35 62.22 o 13 2 1 162.58 116.64 40.04 o 14 2 1 1645.41 1707.81 82.90 o 15 2 1 725.33 704.54 64.57 o 16 2 1 1946.02 1969.34 99.85 o 17 2 1 6.71 -18.88 54.24 o 18 2 1 248.50 207.28 61.66 o 19 2 1 17.13 -31.42 61.23 o 20 2 1 3.77 -10.11 68.37 o 21 2 1 3.46 -29.79 78.10 o 22 2 1 0.52 -56.87 84.54 o 23 2 1 102.66 -67.20 125.05 o -23 3 1 31.83 -44.30 100.38 o -22 3 1 28.18 121.80 90.24 o -21 3 1 58.16 114.43 84.98 o -20 3 1 289.10 247.79 73.76 o -19 3 1 13.93 38.94 62.89 o -18 3 1 2197.79 2239.79 109.35 o -17 3 1 50.71 21.91 56.29 o -16 3 1 7080.54 6739.66 428.02 o -15 3 1 113.07 143.40 49.20 o -14 3 1 7299.47 7198.06 173.71 o -13 3 1 665.69 713.93 37.98 o -12 3 1 7855.66 7897.45 137.76 o -11 3 1 1640.08 1492.55 47.66 o -10 3 1 9243.04 9363.18 154.45 o -9 3 1 3765.75 3739.90 65.16 o -8 3 1 13925.13 13348.15 208.44 o -7 3 1 2766.72 2288.47 58.29 o -6 3 1 589.43 604.15 29.77 o -5 3 1 29275.54 31000.29 531.06 o -4 3 1 275.91 496.99 41.53 o -3 3 1 39736.49 38910.31 661.36 o -2 3 1 5430.08 6427.96 102.63 o -1 3 1 12375.19 12590.60 155.08 o 0 3 1 367.99 324.53 11.75 o 1 3 1 125.98 337.65 14.05 o 2 3 1 563.87 752.47 24.16 o 3 3 1 5676.37 5660.44 107.60 o 4 3 1 11273.97 11601.55 248.12 o 5 3 1 4669.81 5007.41 104.68 o 6 3 1 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27.82 95.83 o 4 2 28 261.31 388.29 112.71 o -15 3 28 0.01 67.27 101.38 o -14 3 28 4.29 -23.16 100.81 o -13 3 28 25.55 61.95 160.18 o -12 3 28 36.73 30.21 93.40 o -11 3 28 87.57 119.34 98.09 o -10 3 28 20.67 68.73 87.14 o -9 3 28 154.24 138.79 122.57 o -8 3 28 153.61 173.94 88.98 o -7 3 28 28.56 165.93 88.82 o -6 3 28 32.49 -5.90 60.60 o -5 3 28 104.43 160.84 76.20 o -4 3 28 18.29 88.88 86.04 o -3 3 28 9.86 107.52 95.43 o -2 3 28 44.28 129.95 94.61 o -1 3 28 0.10 46.48 190.57 o 0 3 28 72.98 -0.39 98.03 o 1 3 28 7.09 107.23 101.91 o 2 3 28 33.48 -15.40 99.08 o 3 3 28 13.85 139.43 99.71 o -14 4 28 362.26 396.05 142.79 o -13 4 28 12.83 -15.50 132.51 o -12 4 28 524.42 388.67 111.72 o -11 4 28 7.48 -34.09 93.08 o -10 4 28 246.33 269.70 96.47 o -9 4 28 42.92 19.58 90.82 o -8 4 28 437.94 364.20 96.41 o -7 4 28 15.48 48.46 77.27 o -6 4 28 131.01 141.68 67.28 o -5 4 28 64.07 125.54 77.65 o -4 4 28 162.80 114.16 160.63 o -3 4 28 40.04 -113.86 97.34 o -2 4 28 75.40 -20.23 96.47 o -1 4 28 44.29 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45.02 93.44 o -10 2 29 234.85 226.55 139.51 o -9 2 29 25.58 85.32 89.43 o -8 2 29 56.32 43.87 131.26 o -7 2 29 8.21 -5.61 99.86 o -6 2 29 7.98 -58.32 74.11 o -5 2 29 14.51 -27.03 134.09 o -4 2 29 6.09 -98.79 87.99 o -3 2 29 20.26 105.18 94.21 o -2 2 29 2.18 39.01 132.62 o -1 2 29 0.46 6.53 91.79 o 0 2 29 50.92 18.66 99.48 o 1 2 29 5.17 81.15 109.10 o 2 2 29 6.84 -117.48 145.72 o -13 3 29 262.13 183.28 127.65 o -12 3 29 78.74 56.65 99.85 o -11 3 29 108.26 209.78 103.39 o -10 3 29 30.19 56.93 101.18 o -9 3 29 80.33 -4.17 92.70 o -8 3 29 11.97 110.02 123.58 o -7 3 29 13.14 9.12 93.33 o -6 3 29 5.58 -58.43 74.09 o -5 3 29 25.23 -29.68 95.67 o -4 3 29 31.60 -9.12 116.35 o -3 3 29 5.34 -56.77 92.60 o -2 3 29 2.82 -207.26 103.63 o -1 3 29 52.97 -177.65 93.26 o 0 3 29 124.86 13.98 115.68 o 1 3 29 31.49 -151.02 108.55 o -11 4 29 6.33 -45.06 100.39 o -10 4 29 0.09 -41.95 114.66 o -9 4 29 6.51 50.52 98.55 o -8 4 29 33.15 66.60 98.88 o -7 4 29 45.10 -82.37 99.96 o -6 4 29 50.45 59.56 95.35 o -5 4 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