#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:17:28 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181027 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/07/2210745.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210745_Fobs loop_ _publ_author_name 'Wei, Lin-Heng' _publ_section_title ; A 1:1 cocrystal of pyridine and 4-hydroxybenzoic acid ; _journal_coeditor_code OB2064 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4506 _journal_page_last o4507 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.339 _cell_angle_gamma 90.000 _cell_length_a 12.1626 _cell_length_b 9.0024 _cell_length_c 11.1713 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8109 _cod_data_source_file ob2064tsup2.hkl _cod_data_source_block t #BEGIN Tags that were not found in dictionaries: _shelx_title ' t in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.01 0.22 0.22 o 2 0 0 99.49 92.62 31.43 o 3 0 0 1206.72 1129.71 342.18 o 4 0 0 760.63 785.42 232.53 o 5 0 0 205.14 184.18 59.52 o 6 0 0 126.65 106.26 33.25 o 7 0 0 0.47 0.30 0.58 o 8 0 0 112.17 101.30 33.30 o 9 0 0 143.70 123.48 30.73 o 10 0 0 294.89 264.93 78.79 o 11 0 0 365.24 319.42 87.78 o 12 0 0 2.88 4.34 1.67 o 13 0 0 1.82 4.30 2.62 o 1 1 0 23.33 14.85 3.46 o 2 1 0 0.35 0.35 0.13 o 3 1 0 618.14 606.92 92.84 o 4 1 0 795.97 780.15 134.61 o 5 1 0 131.72 125.12 22.27 o 6 1 0 117.35 106.31 18.22 o 7 1 0 290.49 274.47 48.13 o 8 1 0 176.90 157.74 31.57 o 9 1 0 52.61 43.30 6.53 o 10 1 0 50.39 43.71 7.90 o 11 1 0 116.43 95.52 14.34 o 12 1 0 7.63 8.97 1.70 o 13 1 0 19.69 16.94 2.25 o 0 2 0 27.49 24.36 1.65 o 1 2 0 347.89 320.43 20.10 o 2 2 0 9099.29 8450.07 676.58 o 3 2 0 94.61 80.21 6.94 o 4 2 0 150.06 140.59 13.08 o 5 2 0 68.84 66.86 7.93 o 6 2 0 81.59 65.83 16.70 o 7 2 0 59.85 44.22 6.20 o 8 2 0 306.82 271.35 45.99 o 9 2 0 38.21 38.99 6.81 o 10 2 0 125.99 126.96 24.08 o 11 2 0 0.53 0.81 0.98 o 12 2 0 5.72 6.74 1.52 o 13 2 0 21.58 19.53 2.66 o 1 3 0 249.47 256.52 16.96 o 2 3 0 2329.19 2286.47 125.51 o 3 3 0 319.16 291.66 23.54 o 4 3 0 29.77 26.81 1.96 o 5 3 0 8.22 7.38 0.68 o 6 3 0 16.00 13.34 1.15 o 7 3 0 0.46 0.00 0.44 o 8 3 0 67.42 65.99 6.80 o 9 3 0 411.67 461.73 11.51 o 10 3 0 6.08 2.64 2.50 o 11 3 0 12.13 17.39 2.73 o 12 3 0 0.01 -0.20 1.12 o 0 4 0 328.96 302.58 25.01 o 1 4 0 128.52 112.84 5.34 o 2 4 0 42.27 41.92 1.96 o 3 4 0 271.10 294.32 23.72 o 4 4 0 1.94 2.12 0.52 o 5 4 0 15.61 15.55 1.18 o 6 4 0 92.57 92.86 8.78 o 7 4 0 18.23 20.44 2.06 o 8 4 0 543.47 526.72 53.97 o 9 4 0 43.75 52.28 6.35 o 10 4 0 0.06 -0.26 1.10 o 11 4 0 10.38 11.59 2.33 o 12 4 0 0.30 -0.76 1.09 o 1 5 0 643.89 708.34 39.50 o 2 5 0 39.73 35.38 1.14 o 3 5 0 102.11 104.03 6.03 o 4 5 0 45.28 38.75 3.30 o 5 5 0 101.08 94.60 6.86 o 6 5 0 1.11 0.78 0.43 o 7 5 0 9.43 9.51 1.19 o 8 5 0 13.43 15.48 1.91 o 9 5 0 39.42 45.78 3.33 o 10 5 0 10.47 11.04 2.25 o 11 5 0 0.00 0.22 1.41 o 0 6 0 106.72 111.69 13.66 o 1 6 0 26.07 28.37 1.28 o 2 6 0 68.38 69.12 3.76 o 3 6 0 0.74 0.96 0.45 o 4 6 0 26.13 19.93 4.37 o 5 6 0 22.03 17.52 2.20 o 6 6 0 278.43 301.49 26.87 o 7 6 0 4.76 3.99 1.22 o 8 6 0 28.91 30.62 2.76 o 9 6 0 20.61 18.98 2.36 o 10 6 0 0.68 1.56 1.40 o 11 6 0 0.67 0.30 1.63 o 1 7 0 265.33 271.87 13.92 o 2 7 0 38.92 44.34 1.77 o 3 7 0 2.82 3.52 0.72 o 4 7 0 3.61 4.68 0.81 o 5 7 0 18.61 18.98 2.23 o 6 7 0 3.08 1.14 1.16 o 7 7 0 0.64 0.35 1.16 o 8 7 0 2.70 1.86 1.43 o 9 7 0 0.28 1.71 1.41 o 10 7 0 7.37 8.94 3.36 o 0 8 0 108.74 98.77 6.18 o 1 8 0 23.08 25.05 2.53 o 2 8 0 60.65 52.22 3.23 o 3 8 0 5.81 6.43 1.48 o 4 8 0 7.55 8.97 1.81 o 5 8 0 0.68 -0.15 0.71 o 6 8 0 1.50 1.94 0.97 o 7 8 0 1.18 -0.58 1.23 o 8 8 0 0.03 -0.22 1.78 o 9 8 0 0.47 1.81 1.34 o 1 9 0 3.03 2.02 1.22 o 2 9 0 4.05 5.08 1.51 o 3 9 0 0.28 0.58 0.96 o 4 9 0 0.20 0.29 0.91 o 5 9 0 2.52 0.89 1.13 o 6 9 0 0.18 1.63 1.73 o 7 9 0 2.22 4.79 2.22 o 0 10 0 0.34 -0.15 1.38 o 1 10 0 0.23 0.44 1.05 o 2 10 0 0.50 0.33 0.98 o 3 10 0 5.89 5.34 1.80 o 4 10 0 1.65 1.50 1.06 o 5 10 0 0.68 1.28 1.58 o 1 11 0 0.62 2.17 1.09 o -13 1 1 0.31 1.83 1.68 o -12 1 1 51.46 58.12 4.05 o -11 1 1 5.71 6.13 1.32 o -10 1 1 16.37 14.99 2.52 o -9 1 1 60.91 58.66 9.36 o -8 1 1 62.09 61.31 11.47 o -7 1 1 55.18 53.33 9.02 o -6 1 1 2118.35 2319.06 406.49 o -5 1 1 28.42 20.88 14.12 o -4 1 1 104.93 116.51 31.11 o -3 1 1 191.41 176.88 32.60 o -2 1 1 6699.93 6429.07 508.65 o -1 1 1 725.56 738.01 56.65 o 0 1 1 9.97 11.52 1.23 o 1 1 1 594.62 620.03 45.63 o 2 1 1 1291.53 1188.20 96.05 o 3 1 1 362.01 329.85 42.64 o 4 1 1 142.36 146.95 24.71 o 5 1 1 70.46 66.03 11.17 o 6 1 1 0.38 2.21 0.58 o 7 1 1 3.07 2.55 0.78 o 8 1 1 38.65 37.17 4.60 o 9 1 1 118.28 112.36 17.42 o 10 1 1 86.91 75.41 12.13 o 11 1 1 26.14 27.17 4.57 o 12 1 1 46.07 43.49 7.25 o -13 2 1 19.02 22.11 3.14 o -12 2 1 0.02 0.35 0.99 o -11 2 1 10.46 11.08 2.16 o -10 2 1 279.54 259.38 44.21 o -9 2 1 60.81 56.96 17.26 o -8 2 1 148.94 90.44 54.19 o -7 2 1 87.19 72.69 12.54 o -6 2 1 156.48 136.90 19.41 o -5 2 1 37.76 41.11 5.77 o -4 2 1 280.27 258.76 20.33 o -3 2 1 254.66 234.17 17.62 o -2 2 1 1504.88 1477.83 94.70 o -1 2 1 1.24 1.39 0.36 o 0 2 1 615.79 465.05 72.13 o 1 2 1 30579.82 21886.30 2176.68 o 2 2 1 0.23 0.48 0.18 o 3 2 1 4.74 3.50 0.73 o 4 2 1 352.93 348.86 33.76 o 5 2 1 514.28 486.21 44.64 o 6 2 1 7.67 7.53 0.75 o 7 2 1 106.75 93.60 11.44 o 8 2 1 0.29 1.00 0.65 o 9 2 1 545.87 507.88 82.70 o 10 2 1 38.92 40.61 6.93 o 11 2 1 52.50 47.51 5.36 o 12 2 1 54.63 51.63 7.19 o -13 3 1 0.03 0.20 2.12 o -12 3 1 2.27 2.95 1.62 o -11 3 1 3.90 5.86 1.79 o -10 3 1 183.12 164.78 21.10 o -9 3 1 219.24 182.64 34.91 o -8 3 1 439.67 430.05 75.10 o -7 3 1 67.65 69.49 12.22 o -6 3 1 246.97 218.16 19.54 o -5 3 1 7.92 9.93 1.47 o -4 3 1 204.64 190.55 13.83 o -3 3 1 36.93 38.06 2.43 o -2 3 1 159.48 164.71 8.29 o -1 3 1 5.41 6.08 0.50 o 0 3 1 232.52 231.18 14.98 o 1 3 1 245.37 244.83 21.80 o 2 3 1 3770.37 3941.44 280.13 o 3 3 1 249.88 238.29 17.52 o 4 3 1 488.90 469.32 35.89 o 5 3 1 8.39 8.73 0.61 o 6 3 1 642.76 568.90 50.72 o 7 3 1 25.89 24.68 5.57 o 8 3 1 1.09 0.56 0.73 o 9 3 1 48.56 42.27 6.25 o 10 3 1 3.52 3.92 1.11 o 11 3 1 0.46 -0.13 0.91 o 12 3 1 0.43 3.31 1.52 o -12 4 1 0.02 0.39 1.26 o -11 4 1 0.11 1.01 1.25 o -10 4 1 15.10 14.24 2.32 o -9 4 1 121.71 126.16 16.27 o -8 4 1 259.97 304.50 7.08 o -7 4 1 455.41 395.95 45.97 o -6 4 1 18.66 18.82 1.61 o -5 4 1 0.21 0.08 0.25 o -4 4 1 15.18 13.77 1.06 o -3 4 1 0.13 0.65 0.26 o -2 4 1 87.51 84.27 4.74 o -1 4 1 43.63 42.68 2.42 o 0 4 1 75.09 82.01 3.73 o 1 4 1 82.80 79.66 4.79 o 2 4 1 203.60 207.87 17.77 o 3 4 1 3758.93 4125.98 311.67 o 4 4 1 235.57 222.38 16.46 o 5 4 1 169.19 169.23 14.01 o 6 4 1 0.01 0.20 0.33 o 7 4 1 571.81 570.11 80.31 o 8 4 1 13.46 14.39 2.45 o 9 4 1 41.74 41.30 6.98 o 10 4 1 1.31 0.97 1.17 o 11 4 1 3.32 5.14 1.69 o -12 5 1 2.64 5.23 1.69 o -11 5 1 12.83 10.55 2.21 o -10 5 1 27.52 35.42 3.06 o -9 5 1 1.39 1.37 0.88 o -8 5 1 265.19 276.14 30.38 o -7 5 1 135.22 132.28 13.32 o -6 5 1 193.47 193.83 17.77 o -5 5 1 21.35 23.45 1.30 o -4 5 1 20.62 23.03 2.21 o -3 5 1 0.52 0.58 0.31 o -2 5 1 240.91 260.50 15.73 o -1 5 1 791.74 821.78 48.19 o 0 5 1 534.04 577.72 33.15 o 1 5 1 108.83 107.75 6.88 o 2 5 1 52.69 55.91 5.84 o 3 5 1 196.94 186.18 13.04 o 4 5 1 232.50 208.93 22.80 o 5 5 1 8.20 8.82 0.78 o 6 5 1 8.98 8.10 0.82 o 7 5 1 5.74 3.31 2.11 o 8 5 1 30.15 31.17 2.26 o 9 5 1 0.34 0.55 1.20 o 10 5 1 1.98 3.87 1.65 o 11 5 1 18.77 31.59 3.76 o -11 6 1 9.20 9.68 2.26 o -10 6 1 1.92 4.35 1.75 o -9 6 1 1.95 3.22 1.13 o -8 6 1 24.18 21.58 4.38 o -7 6 1 360.52 385.93 33.86 o -6 6 1 0.66 0.64 0.55 o -5 6 1 0.07 0.16 0.43 o -4 6 1 0.04 0.38 0.39 o -3 6 1 113.73 121.34 7.80 o -2 6 1 55.59 51.86 2.80 o -1 6 1 128.89 136.95 10.22 o 0 6 1 77.76 79.22 4.13 o 1 6 1 60.30 61.41 3.96 o 2 6 1 8.27 9.08 1.00 o 3 6 1 40.24 34.59 6.90 o 4 6 1 0.25 0.31 0.46 o 5 6 1 136.88 143.93 11.89 o 6 6 1 21.00 24.73 2.50 o 7 6 1 12.87 15.34 2.29 o 8 6 1 0.96 1.91 1.61 o 9 6 1 2.81 2.47 1.46 o 10 6 1 2.88 7.61 2.92 o -10 7 1 1.58 1.53 2.32 o -9 7 1 0.01 1.24 1.10 o -8 7 1 0.90 1.09 0.78 o -7 7 1 20.72 16.13 5.29 o -6 7 1 15.11 13.46 1.39 o -5 7 1 52.88 56.69 6.77 o -4 7 1 302.40 343.77 26.30 o -3 7 1 0.14 0.40 0.44 o -2 7 1 1.54 2.22 0.69 o -1 7 1 55.24 52.18 3.35 o 0 7 1 3.52 2.73 0.70 o 1 7 1 37.93 37.24 1.76 o 2 7 1 43.67 45.76 3.30 o 3 7 1 0.10 -0.28 0.48 o 4 7 1 13.92 9.33 3.03 o 5 7 1 22.49 20.60 4.09 o 6 7 1 25.13 22.82 2.69 o 7 7 1 12.22 12.12 2.30 o 8 7 1 5.97 9.05 2.11 o 9 7 1 4.82 7.56 2.72 o -9 8 1 1.73 1.88 1.58 o -8 8 1 1.91 2.22 1.78 o -7 8 1 45.07 44.66 5.88 o -6 8 1 0.38 -0.29 0.80 o -5 8 1 100.82 98.15 6.37 o -4 8 1 3.28 2.58 1.10 o -3 8 1 3.64 4.98 1.14 o -2 8 1 14.26 17.55 1.76 o -1 8 1 11.89 10.82 1.44 o 0 8 1 16.38 17.02 1.70 o 1 8 1 5.69 6.10 1.18 o 2 8 1 3.02 2.68 0.84 o 3 8 1 5.69 5.91 1.05 o 4 8 1 0.00 0.11 0.65 o 5 8 1 0.01 0.24 0.80 o 6 8 1 1.50 1.17 1.36 o 7 8 1 0.04 0.05 1.14 o 8 8 1 0.26 0.67 1.25 o -8 9 1 2.17 4.40 2.03 o -7 9 1 3.18 4.15 1.59 o -6 9 1 3.09 4.15 2.47 o -5 9 1 1.70 1.78 1.12 o -4 9 1 0.96 1.41 1.16 o -3 9 1 0.86 0.92 0.98 o -2 9 1 4.35 5.26 1.47 o -1 9 1 0.00 0.21 0.80 o 0 9 1 20.92 19.45 2.57 o 1 9 1 0.88 1.62 1.02 o 2 9 1 33.78 31.49 3.09 o 3 9 1 1.18 1.75 1.03 o 4 9 1 27.64 24.94 2.87 o 5 9 1 0.05 1.33 1.53 o 6 9 1 2.66 2.22 1.58 o 7 9 1 4.02 4.84 2.37 o -6 10 1 0.78 1.07 1.04 o -5 10 1 0.45 2.07 1.27 o -4 10 1 0.18 0.70 1.03 o -3 10 1 15.67 19.82 2.85 o -2 10 1 13.91 15.58 2.64 o -1 10 1 1.56 1.41 1.36 o 0 10 1 0.08 -0.66 0.89 o 1 10 1 8.92 8.83 1.93 o 2 10 1 2.26 2.56 1.24 o 3 10 1 0.04 1.54 1.13 o 4 10 1 0.30 1.88 1.68 o 5 10 1 3.59 3.51 2.03 o -2 11 1 0.11 0.87 0.96 o -1 11 1 0.85 1.92 1.10 o 0 11 1 0.53 -0.16 0.94 o 1 11 1 0.05 1.25 0.97 o -14 0 2 0.00 1.19 1.73 o -13 0 2 13.27 7.96 2.87 o -12 0 2 11.82 14.08 3.56 o -11 0 2 0.16 0.79 1.48 o -10 0 2 19.64 24.16 3.61 o -9 0 2 192.27 202.19 8.05 o -8 0 2 132.29 194.48 7.36 o -7 0 2 14.50 12.55 2.17 o -6 0 2 32.70 28.76 2.47 o -5 0 2 2179.31 2852.99 21.40 o -4 0 2 326.72 264.91 53.36 o -3 0 2 67.17 52.48 15.24 o 0 0 2 1.23 3.54 1.22 o 1 0 2 3845.48 3333.34 214.62 o 2 0 2 1951.20 1904.89 468.70 o 3 0 2 21.90 21.07 5.63 o 4 0 2 152.19 166.48 47.95 o 5 0 2 285.88 293.92 84.02 o 6 0 2 528.76 548.55 153.55 o 7 0 2 129.55 119.07 41.23 o 8 0 2 158.46 157.70 40.72 o 9 0 2 1.30 0.92 1.04 o 10 0 2 760.53 742.58 232.41 o 11 0 2 15.85 12.96 2.39 o 12 0 2 10.56 9.66 2.40 o -14 1 2 4.13 5.40 1.83 o -13 1 2 1.35 1.75 1.41 o -12 1 2 2.61 4.08 1.64 o -11 1 2 12.24 16.94 2.46 o -10 1 2 0.61 2.18 1.06 o -9 1 2 83.32 92.62 3.93 o -8 1 2 505.80 562.38 46.50 o -7 1 2 73.36 90.02 3.32 o -6 1 2 3.10 5.18 0.99 o -5 1 2 3846.55 4995.28 140.72 o -4 1 2 339.78 350.24 41.76 o -3 1 2 890.40 872.82 181.98 o -2 1 2 184.57 179.47 15.62 o -1 1 2 5366.56 5015.04 456.40 o 0 1 2 447.93 468.49 39.44 o 1 1 2 613.85 623.82 57.87 o 2 1 2 1150.14 1100.68 88.20 o 3 1 2 1550.40 1640.16 181.23 o 4 1 2 381.72 340.96 45.13 o 5 1 2 0.70 1.74 0.55 o 6 1 2 7.22 6.52 1.06 o 7 1 2 289.77 278.68 45.02 o 8 1 2 0.01 0.18 0.57 o 9 1 2 115.15 103.62 15.88 o 10 1 2 38.82 40.85 4.89 o 11 1 2 44.86 42.39 7.10 o 12 1 2 0.07 1.05 0.75 o -13 2 2 0.25 2.54 1.51 o -12 2 2 6.48 6.47 1.84 o -11 2 2 62.81 67.20 3.95 o -10 2 2 36.65 37.68 2.88 o -9 2 2 70.01 74.27 3.62 o -8 2 2 5.73 5.85 1.61 o -7 2 2 289.61 289.85 54.51 o -6 2 2 141.35 101.29 19.16 o -5 2 2 54.82 58.41 4.78 o -4 2 2 346.20 382.53 32.24 o -3 2 2 15.63 20.05 1.86 o -2 2 2 65.26 65.12 5.47 o -1 2 2 288.15 226.41 25.10 o 0 2 2 11318.55 10479.17 796.04 o 1 2 2 162.11 191.32 13.59 o 2 2 2 89.31 90.08 7.41 o 3 2 2 32.35 47.81 3.96 o 4 2 2 533.18 520.48 47.96 o 5 2 2 57.93 52.27 5.89 o 6 2 2 11.02 10.29 1.37 o 7 2 2 2.64 2.13 0.71 o 8 2 2 323.11 309.32 52.18 o 9 2 2 5.90 5.40 1.10 o 10 2 2 2.84 4.50 1.15 o 11 2 2 2.11 3.14 1.02 o -13 3 2 7.87 9.41 2.24 o -12 3 2 6.80 10.82 2.77 o -11 3 2 45.42 44.08 4.15 o -10 3 2 4.80 3.55 1.13 o -9 3 2 45.30 44.65 6.17 o -8 3 2 19.58 19.66 2.60 o -7 3 2 10.17 8.29 0.85 o -6 3 2 151.42 140.81 18.78 o -5 3 2 422.49 415.48 44.29 o -4 3 2 567.14 578.04 51.23 o -3 3 2 59.02 77.10 7.99 o -2 3 2 780.04 764.88 48.65 o -1 3 2 13.81 15.38 1.45 o 0 3 2 484.93 502.65 35.01 o 1 3 2 2538.27 2747.54 210.86 o 2 3 2 15.90 16.19 2.21 o 3 3 2 0.30 -0.05 0.19 o 4 3 2 13.49 14.85 1.03 o 5 3 2 2.74 1.82 0.37 o 6 3 2 12.07 11.46 0.88 o 7 3 2 20.42 19.18 2.15 o 8 3 2 0.29 0.07 0.64 o 9 3 2 6.00 8.16 1.30 o 10 3 2 1.47 1.73 0.88 o 11 3 2 1.25 1.21 0.97 o -13 4 2 20.29 25.88 3.33 o -12 4 2 13.17 14.73 2.61 o -11 4 2 0.21 -0.46 0.83 o -10 4 2 76.61 80.26 6.04 o -9 4 2 82.77 83.10 6.98 o -8 4 2 116.65 120.39 6.25 o -7 4 2 212.37 190.99 18.71 o -6 4 2 107.59 113.31 11.45 o -5 4 2 12.70 9.50 0.93 o -4 4 2 78.13 82.68 5.09 o -3 4 2 4.64 5.50 0.58 o -2 4 2 320.64 376.68 21.01 o -1 4 2 430.45 430.56 25.87 o 0 4 2 235.41 242.51 18.91 o 1 4 2 108.14 135.01 9.11 o 2 4 2 2404.30 2329.84 158.96 o 3 4 2 3.28 3.73 0.45 o 4 4 2 29.17 26.75 2.38 o 5 4 2 0.04 -0.18 0.29 o 6 4 2 10.70 7.69 1.27 o 7 4 2 2.99 1.73 0.68 o 8 4 2 7.64 9.10 1.85 o 9 4 2 0.28 -0.26 0.66 o 10 4 2 14.49 16.20 2.65 o 11 4 2 1.31 4.21 1.62 o -12 5 2 1.68 0.92 1.26 o -11 5 2 4.61 7.91 1.89 o -10 5 2 0.07 -0.22 0.79 o -9 5 2 248.49 258.87 19.33 o -8 5 2 65.91 64.70 4.65 o -7 5 2 113.36 116.89 13.12 o -6 5 2 175.93 175.31 17.69 o -5 5 2 31.16 33.63 3.36 o -4 5 2 28.47 28.85 2.02 o -3 5 2 107.68 108.09 8.74 o -2 5 2 16.19 15.72 1.27 o -1 5 2 0.89 1.75 0.39 o 0 5 2 108.77 116.27 6.16 o 1 5 2 525.49 560.32 45.69 o 2 5 2 27.41 30.31 2.24 o 3 5 2 520.41 531.80 37.84 o 4 5 2 29.45 23.65 3.16 o 5 5 2 137.92 121.67 11.35 o 6 5 2 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