#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:17:28 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181027 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/07/2210750.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210750_Fobs loop_ _publ_author_name 'Teh, Jeannie Bee-Jan' 'Karthikeyan, Mari Sithambaram' 'Fun, Hoong-Kun' 'Patil, P. S.' 'Razak, Ibrahim Abdul' 'Holla, Bantwal Shivarama' 'Dharmaprakash, S. M.' _publ_section_title ; N-(4-Methoxyphenyl)thiourea ; _journal_coeditor_code OB2070 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4693 _journal_page_last o4694 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 63.779 _cell_angle_beta 72.413 _cell_angle_gamma 83.428 _cell_length_a 6.7328 _cell_length_b 8.3813 _cell_length_c 9.0571 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.7108 _cod_data_source_file ob2070Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil53_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11.74 8.94 0.17 o 2 0 0 791.94 774.40 12.26 o 3 0 0 196.80 212.24 3.86 o 4 0 0 66.20 78.46 1.34 o 5 0 0 0.73 0.94 0.12 o 6 0 0 53.58 55.00 1.41 o 7 0 0 19.86 20.21 0.72 o 8 0 0 1.82 1.87 0.28 o 9 0 0 96.45 106.00 2.73 o -9 1 0 14.83 14.99 0.69 o -8 1 0 66.19 63.46 1.74 o -7 1 0 143.41 145.24 3.44 o -6 1 0 115.93 128.12 3.02 o -5 1 0 336.94 362.08 7.96 o -4 1 0 340.00 349.16 7.06 o -3 1 0 0.15 0.37 0.16 o -2 1 0 271.63 265.89 6.90 o -1 1 0 22.21 16.33 0.32 o 0 1 0 113.78 115.83 1.34 o 1 1 0 53.21 54.05 0.78 o 2 1 0 33.18 30.65 0.87 o 3 1 0 506.15 584.23 15.72 o 4 1 0 231.13 238.82 3.83 o 5 1 0 222.12 214.01 3.49 o 6 1 0 46.12 54.46 1.39 o 7 1 0 426.48 439.18 9.70 o 8 1 0 9.90 11.72 0.57 o -8 2 0 6.04 5.97 0.43 o -7 2 0 14.91 13.66 0.59 o -6 2 0 6.61 6.69 0.37 o -5 2 0 1.88 2.10 0.34 o -4 2 0 40.20 38.33 1.03 o -3 2 0 126.87 99.82 3.24 o -2 2 0 24.32 24.65 0.46 o -1 2 0 1664.41 1527.44 23.62 o 0 2 0 770.16 763.36 9.29 o 1 2 0 1534.26 1410.63 22.99 o 2 2 0 264.96 287.61 8.95 o 3 2 0 323.01 330.00 5.10 o 4 2 0 76.68 75.90 1.21 o 5 2 0 171.60 168.68 2.83 o 6 2 0 2.97 2.09 0.08 o 7 2 0 15.77 18.70 0.40 o 8 2 0 1.10 0.98 0.23 o -8 3 0 32.62 34.65 1.16 o -7 3 0 256.59 230.51 5.31 o -5 3 0 197.82 175.81 8.66 o -4 3 0 11.40 8.39 0.34 o -3 3 0 425.70 426.32 8.12 o -2 3 0 1.90 1.18 0.14 o -1 3 0 68.29 62.79 1.02 o 0 3 0 1051.06 1024.27 22.59 o 1 3 0 5.39 3.68 0.16 o 2 3 0 0.08 -0.11 0.06 o 3 3 0 41.56 32.92 0.63 o 4 3 0 0.01 0.02 0.04 o 5 3 0 13.97 14.09 0.25 o 6 3 0 59.13 57.41 0.81 o 7 3 0 19.62 20.16 0.77 o 8 3 0 40.39 39.03 1.27 o -8 4 0 0.10 -0.04 0.21 o -7 4 0 66.93 66.71 1.88 o -6 4 0 321.59 312.04 7.09 o -5 4 0 296.51 287.69 5.25 o -4 4 0 28.23 28.75 0.77 o -3 4 0 196.01 205.95 3.78 o -2 4 0 166.92 176.99 3.24 o -1 4 0 248.19 253.01 3.54 o 0 4 0 872.94 879.70 11.29 o 1 4 0 316.10 317.37 3.87 o 2 4 0 368.64 340.83 3.36 o 3 4 0 160.76 146.38 1.67 o 4 4 0 1020.52 965.66 10.23 o 5 4 0 112.59 108.93 1.31 o 6 4 0 180.48 184.49 2.76 o 7 4 0 2.65 3.50 0.34 o 8 4 0 2.98 4.93 0.43 o -8 5 0 12.23 13.22 0.71 o -7 5 0 41.99 39.29 1.32 o -6 5 0 76.24 76.16 2.10 o -5 5 0 140.22 132.95 4.70 o -4 5 0 177.07 168.11 3.25 o -3 5 0 579.30 567.01 7.82 o -2 5 0 47.38 38.42 1.35 o -1 5 0 74.61 63.27 1.13 o 0 5 0 320.59 316.88 3.77 o 1 5 0 33.10 42.60 1.11 o 2 5 0 224.79 232.81 2.70 o 3 5 0 0.77 0.84 0.08 o 4 5 0 85.73 81.41 1.17 o 5 5 0 61.25 58.82 0.92 o 6 5 0 36.11 37.30 1.25 o 7 5 0 5.03 5.41 0.46 o -7 6 0 7.07 6.65 0.51 o -6 6 0 67.20 63.15 1.88 o -5 6 0 4.09 4.20 0.41 o -4 6 0 23.87 24.57 0.78 o -3 6 0 9.14 9.22 0.31 o -2 6 0 3.83 3.08 0.16 o -1 6 0 59.98 64.41 1.05 o 0 6 0 0.55 1.11 0.14 o 1 6 0 118.86 119.13 1.50 o 2 6 0 29.75 29.26 0.51 o 3 6 0 164.04 165.05 2.69 o 4 6 0 329.59 322.77 5.36 o 5 6 0 121.17 125.25 3.27 o 6 6 0 47.81 48.51 1.58 o 7 6 0 12.01 10.99 0.66 o -6 7 0 133.25 119.19 3.18 o -5 7 0 2.61 3.58 0.43 o -4 7 0 34.48 36.22 0.86 o -3 7 0 36.14 32.46 0.71 o -2 7 0 528.29 495.78 7.17 o -1 7 0 296.53 276.80 6.33 o 0 7 0 74.36 71.19 1.16 o 1 7 0 144.51 149.00 1.69 o 2 7 0 9.79 8.62 0.32 o 3 7 0 0.39 0.39 0.12 o 4 7 0 16.93 17.60 0.62 o 5 7 0 24.32 23.24 1.01 o 6 7 0 2.77 3.02 0.41 o -6 8 0 8.51 8.23 0.63 o -5 8 0 67.51 64.29 2.03 o -4 8 0 13.07 13.83 0.51 o -3 8 0 364.16 373.87 12.60 o -2 8 0 219.69 212.23 5.19 o -1 8 0 9.07 8.81 0.32 o 0 8 0 22.60 24.00 0.58 o 1 8 0 95.11 83.68 1.52 o 2 8 0 20.03 18.43 0.64 o 3 8 0 28.32 27.52 0.75 o 4 8 0 76.49 77.86 2.34 o 5 8 0 219.50 221.15 5.49 o -4 9 0 49.56 51.60 1.60 o -3 9 0 62.35 66.81 1.94 o -2 9 0 197.17 187.17 4.57 o -1 9 0 70.32 69.06 2.49 o 0 9 0 54.49 53.07 1.07 o 1 9 0 190.39 179.37 4.38 o 2 9 0 51.75 52.31 1.59 o 3 9 0 0.70 0.47 0.34 o 4 9 0 64.97 77.66 1.64 o -3 10 0 0.51 -0.02 0.20 o -2 10 0 18.60 20.42 0.86 o -1 10 0 11.41 11.09 0.38 o 0 10 0 33.29 34.58 0.81 o 1 10 0 6.34 6.77 0.50 o 2 10 0 7.77 8.44 0.57 o -1 -10 1 2.33 2.02 0.34 o 0 -10 1 45.71 47.82 1.15 o 1 -10 1 63.26 65.08 1.28 o -3 -9 1 14.66 15.27 0.75 o -2 -9 1 93.39 89.87 2.46 o -1 -9 1 78.17 80.56 2.22 o 0 -9 1 163.99 162.06 2.79 o 1 -9 1 71.34 71.74 1.37 o 2 -9 1 32.97 37.49 1.24 o 3 -9 1 22.50 26.43 1.00 o 4 -9 1 1.99 2.11 0.34 o -5 -8 1 27.03 25.34 1.17 o -4 -8 1 28.83 27.66 0.79 o -3 -8 1 0.56 0.25 0.17 o -2 -8 1 22.56 16.78 0.73 o -1 -8 1 11.07 10.19 0.34 o 0 -8 1 2.20 2.25 0.19 o 1 -8 1 11.91 9.86 0.35 o 2 -8 1 236.37 227.08 5.42 o 3 -8 1 10.82 11.06 0.45 o 4 -8 1 61.15 63.28 1.83 o 5 -8 1 48.83 45.95 1.64 o -6 -7 1 5.65 5.85 0.57 o -5 -7 1 50.12 51.30 1.75 o -4 -7 1 33.27 37.60 1.39 o -3 -7 1 50.42 50.95 1.12 o -2 -7 1 52.29 54.11 1.69 o -1 -7 1 75.63 79.02 1.27 o 0 -7 1 462.75 430.07 6.05 o 1 -7 1 412.63 400.86 5.66 o 2 -7 1 0.69 1.10 0.17 o 3 -7 1 51.28 56.13 1.06 o 4 -7 1 11.72 15.83 1.34 o 5 -7 1 222.15 218.86 5.34 o 6 -7 1 0.05 0.30 0.22 o -6 -6 1 73.19 70.76 2.15 o -5 -6 1 34.94 33.43 1.25 o -4 -6 1 173.75 176.01 4.35 o -3 -6 1 41.66 43.06 0.94 o -2 -6 1 42.71 46.13 1.23 o -1 -6 1 30.39 26.14 0.45 o 0 -6 1 1.11 0.66 0.10 o 1 -6 1 4.15 3.78 0.16 o 2 -6 1 197.42 189.00 2.36 o 3 -6 1 59.23 54.71 1.00 o 4 -6 1 61.40 63.89 1.80 o 5 -6 1 90.58 84.16 2.31 o 6 -6 1 55.23 51.03 1.61 o 7 -6 1 13.66 14.12 0.73 o -7 -5 1 18.72 19.80 0.93 o -6 -5 1 10.98 10.18 0.62 o -5 -5 1 4.14 3.56 0.38 o -4 -5 1 6.87 6.40 0.45 o -3 -5 1 44.37 43.04 1.19 o -2 -5 1 59.98 62.80 1.50 o -1 -5 1 116.50 101.37 1.63 o 0 -5 1 164.01 147.79 2.16 o 1 -5 1 75.84 64.81 1.04 o 2 -5 1 163.03 164.62 2.64 o 3 -5 1 290.94 283.12 4.03 o 4 -5 1 289.20 276.68 5.11 o 5 -5 1 198.45 189.35 4.49 o 6 -5 1 5.76 5.70 0.43 o 7 -5 1 2.56 1.67 0.30 o 8 -5 1 1.13 1.03 0.29 o -7 -4 1 148.25 148.04 3.73 o -6 -4 1 65.91 64.26 1.86 o -5 -4 1 315.08 294.24 6.74 o -4 -4 1 83.02 80.47 2.12 o -3 -4 1 431.48 429.38 6.88 o -2 -4 1 296.88 308.34 4.06 o -1 -4 1 276.32 299.36 7.77 o 0 -4 1 270.45 264.70 3.73 o 1 -4 1 4.01 2.85 0.13 o 2 -4 1 79.95 89.81 1.79 o 3 -4 1 135.03 130.65 2.51 o 4 -4 1 43.73 43.17 1.04 o 5 -4 1 13.89 13.52 0.91 o 6 -4 1 24.85 24.40 0.87 o 7 -4 1 11.74 12.67 0.61 o 8 -4 1 22.91 22.67 0.90 o -8 -3 1 18.42 20.89 0.92 o -7 -3 1 25.32 27.26 1.01 o -6 -3 1 2.64 2.65 0.30 o -5 -3 1 34.22 36.15 1.11 o -4 -3 1 210.39 194.99 4.50 o -3 -3 1 60.98 60.84 1.18 o -2 -3 1 2.45 0.52 0.08 o -1 -3 1 1816.18 1841.07 41.15 o 0 -3 1 38.52 61.65 1.97 o 1 -3 1 73.32 67.33 1.55 o 2 -3 1 335.36 331.07 9.57 o 3 -3 1 24.97 39.79 0.90 o 4 -3 1 658.27 662.17 11.40 o 5 -3 1 600.10 590.53 12.90 o 6 -3 1 275.66 268.51 4.94 o 7 -3 1 1.45 2.18 0.26 o 8 -3 1 14.53 15.25 0.67 o -8 -2 1 9.71 10.51 0.62 o -7 -2 1 20.73 21.76 0.85 o -6 -2 1 41.11 37.46 1.14 o -5 -2 1 36.72 35.50 1.05 o -4 -2 1 30.14 32.96 0.95 o -3 -2 1 1077.49 1042.76 11.03 o -2 -2 1 428.51 468.76 11.68 o -1 -2 1 409.65 417.48 6.82 o 0 -2 1 432.99 431.66 9.63 o 1 -2 1 151.43 150.69 2.30 o 2 -2 1 18.92 25.94 0.83 o 4 -2 1 17.94 17.95 0.49 o 5 -2 1 75.66 73.07 1.73 o 6 -2 1 513.73 500.97 8.80 o 7 -2 1 57.02 54.60 1.46 o 8 -2 1 11.88 11.47 0.53 o 9 -2 1 1.66 1.18 0.26 o -8 -1 1 95.87 97.64 2.60 o -7 -1 1 37.82 42.02 1.29 o -6 -1 1 76.75 77.52 1.99 o -5 -1 1 45.33 45.41 1.23 o -4 -1 1 56.72 68.87 0.90 o -3 -1 1 11.89 9.31 0.33 o -2 -1 1 169.65 171.29 4.18 o -1 -1 1 3.22 2.65 0.19 o 1 -1 1 5.03 2.88 0.21 o 2 -1 1 146.50 154.26 6.51 o 3 -1 1 380.15 383.32 6.76 o 4 -1 1 739.08 774.25 10.46 o 5 -1 1 331.44 334.16 4.64 o 6 -1 1 96.37 97.96 2.30 o 7 -1 1 46.36 43.21 1.17 o 8 -1 1 12.83 12.45 0.53 o 9 -1 1 72.11 73.84 1.94 o -8 0 1 14.40 13.18 0.68 o -7 0 1 16.61 16.47 0.70 o -6 0 1 7.91 8.55 0.45 o -5 0 1 1.78 1.76 0.20 o -4 0 1 4.90 8.22 0.26 o -3 0 1 232.73 247.39 5.95 o -2 0 1 1537.35 1458.13 34.83 o -1 0 1 9024.05 5742.55 140.33 o 0 0 1 24.94 27.89 0.72 o 1 0 1 426.33 474.20 9.45 o 2 0 1 0.21 0.37 0.08 o 3 0 1 18.73 17.00 0.39 o 4 0 1 32.20 22.37 0.61 o 5 0 1 12.18 11.64 0.53 o 6 0 1 22.22 23.82 0.53 o 7 0 1 11.88 11.89 0.45 o 8 0 1 7.07 7.53 0.40 o 9 0 1 8.15 10.02 0.50 o -8 1 1 111.42 109.94 2.85 o -7 1 1 1.82 3.02 0.32 o -6 1 1 335.46 346.28 7.77 o -5 1 1 103.46 111.27 2.67 o -4 1 1 0.18 0.10 0.05 o -3 1 1 388.77 422.85 10.06 o -2 1 1 398.52 427.53 6.04 o -1 1 1 830.89 829.31 12.06 o 0 1 1 0.31 6.93 0.22 o 1 1 1 711.02 688.46 14.39 o 2 1 1 817.18 839.54 16.59 o 3 1 1 1053.67 1075.86 24.35 o 4 1 1 260.13 251.62 5.87 o 5 1 1 184.94 190.84 4.61 o 6 1 1 509.76 479.40 7.56 o 7 1 1 2.45 4.45 0.26 o 8 1 1 53.17 53.81 1.44 o 9 1 1 6.72 6.27 0.42 o -8 2 1 3.47 3.36 0.37 o -7 2 1 4.78 3.99 0.36 o -6 2 1 0.10 -0.02 0.14 o -5 2 1 0.46 0.99 0.17 o -4 2 1 42.07 35.63 0.70 o -3 2 1 232.82 243.54 3.48 o -2 2 1 651.70 660.89 15.85 o -1 2 1 2744.87 2407.97 50.69 o 0 2 1 630.34 619.79 8.00 o 1 2 1 2379.89 1974.95 49.48 o 3 2 1 453.58 451.35 7.97 o 4 2 1 30.00 21.43 0.59 o 5 2 1 18.00 12.11 0.32 o 6 2 1 0.09 0.63 0.10 o 7 2 1 0.08 0.92 0.29 o 8 2 1 6.11 8.11 0.42 o 9 2 1 96.78 105.79 2.66 o -8 3 1 66.85 66.64 1.94 o -7 3 1 164.59 162.67 3.95 o -6 3 1 115.06 113.62 2.84 o -5 3 1 106.73 101.89 2.53 o -4 3 1 93.71 93.26 1.88 o -3 3 1 9.18 7.36 0.58 o -2 3 1 13.87 11.42 0.46 o -1 3 1 261.87 264.70 3.43 o 0 3 1 95.32 100.99 1.61 o 1 3 1 36.03 37.78 0.80 o 2 3 1 27.81 26.14 0.57 o 3 3 1 330.87 351.35 5.06 o 4 3 1 9.18 5.85 0.13 o 5 3 1 34.31 31.38 0.69 o 6 3 1 71.12 65.24 1.00 o 7 3 1 11.08 13.30 0.23 o 8 3 1 132.50 132.08 1.99 o -8 4 1 0.12 0.32 0.26 o -7 4 1 120.26 116.11 2.99 o -6 4 1 274.55 262.81 6.07 o -5 4 1 4.03 3.77 0.29 o -4 4 1 11.44 12.76 0.84 o -3 4 1 125.16 123.80 2.38 o -2 4 1 269.73 262.67 7.72 o -1 4 1 457.93 489.52 7.28 o 0 4 1 601.56 593.21 7.45 o 1 4 1 27.58 15.93 0.34 o 2 4 1 55.38 59.51 0.84 o 3 4 1 809.47 756.94 8.02 o 4 4 1 281.73 276.01 3.01 o 5 4 1 58.51 56.51 0.72 o 6 4 1 27.64 26.83 0.41 o 7 4 1 0.73 0.39 0.08 o 8 4 1 0.08 0.02 0.11 o -7 5 1 6.45 8.47 0.59 o -6 5 1 132.00 129.73 3.30 o -5 5 1 248.87 251.05 4.71 o -4 5 1 490.09 478.48 8.46 o -3 5 1 5.81 8.17 0.33 o -2 5 1 134.16 117.73 2.11 o -1 5 1 153.63 143.22 2.08 o 0 5 1 50.25 61.42 0.74 o 1 5 1 486.06 507.00 4.65 o 2 5 1 0.09 0.07 0.04 o 3 5 1 12.56 10.79 0.23 o 4 5 1 253.07 236.99 2.64 o 5 5 1 0.33 0.37 0.07 o 6 5 1 9.54 9.36 0.23 o 7 5 1 29.97 29.06 0.62 o 8 5 1 51.47 52.57 1.60 o -7 6 1 6.02 7.00 0.55 o -6 6 1 106.52 106.28 2.85 o -5 6 1 2.64 1.70 0.30 o -4 6 1 1.55 1.25 0.21 o -3 6 1 12.77 14.36 0.40 o -2 6 1 6.54 6.00 0.17 o -1 6 1 7.69 11.50 0.24 o 0 6 1 25.26 24.30 0.64 o 1 6 1 141.01 142.23 1.29 o 2 6 1 173.13 169.46 1.65 o 3 6 1 1231.13 1183.94 12.55 o 4 6 1 4.25 4.40 0.17 o 5 6 1 178.94 172.21 2.02 o 6 6 1 1.76 1.45 0.14 o 7 6 1 74.62 82.25 1.43 o -6 7 1 11.31 11.94 0.71 o -5 7 1 55.19 57.18 1.78 o -4 7 1 90.84 84.04 1.61 o -3 7 1 195.53 175.31 2.66 o -2 7 1 231.15 210.55 3.05 o -1 7 1 193.53 185.49 3.99 o 0 7 1 88.91 92.02 1.23 o 1 7 1 42.11 44.37 0.64 o 2 7 1 8.91 9.01 0.24 o 3 7 1 1.26 1.46 0.11 o 4 7 1 2.30 2.39 0.17 o 5 7 1 19.87 20.03 0.51 o 6 7 1 33.22 32.56 1.22 o 7 7 1 31.65 32.45 1.24 o -6 8 1 25.08 24.30 1.09 o -5 8 1 63.73 60.79 1.95 o -4 8 1 35.37 38.96 0.94 o -3 8 1 114.61 105.32 1.77 o -2 8 1 0.83 1.16 0.30 o -1 8 1 4.01 2.96 0.21 o 0 8 1 4.70 2.93 0.36 o 1 8 1 4.82 4.89 0.33 o 2 8 1 109.38 109.21 1.66 o 3 8 1 120.73 121.33 1.84 o 4 8 1 345.03 354.70 5.95 o 5 8 1 63.07 64.12 1.99 o 6 8 1 27.12 27.99 1.18 o -5 9 1 99.97 106.56 4.58 o -4 9 1 65.38 68.23 1.95 o -3 9 1 159.35 160.82 4.00 o -2 9 1 8.38 8.11 0.51 o -1 9 1 170.85 160.99 3.07 o 0 9 1 279.12 256.44 4.23 o 1 9 1 22.79 23.72 0.56 o 2 9 1 4.40 5.68 0.44 o 3 9 1 41.35 44.77 1.28 o 4 9 1 12.28 13.14 0.52 o 5 9 1 25.26 26.68 1.19 o -3 10 1 26.20 23.66 0.97 o -2 10 1 167.16 168.86 4.19 o -1 10 1 7.60 8.72 0.34 o 0 10 1 28.74 30.13 0.71 o 1 10 1 39.08 35.10 1.18 o 2 10 1 12.24 14.56 0.72 o 3 10 1 47.71 51.51 1.64 o -2 -9 2 197.66 201.53 4.98 o -1 -9 2 25.50 23.21 0.93 o 0 -9 2 36.71 36.10 1.41 o 1 -9 2 10.66 12.88 1.44 o 2 -9 2 64.91 70.22 1.98 o 3 -9 2 0.42 0.91 0.27 o -4 -8 2 8.67 6.89 0.46 o -3 -8 2 2.68 3.35 0.38 o -2 -8 2 19.30 19.60 0.83 o -1 -8 2 0.83 0.99 0.14 o 0 -8 2 11.44 12.28 0.40 o 1 -8 2 7.63 9.66 0.35 o 2 -8 2 112.43 116.57 3.00 o 3 -8 2 51.43 47.07 1.46 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277.17 8.43 o 4 -5 2 198.09 193.82 3.71 o 5 -5 2 12.62 10.06 0.56 o 6 -5 2 19.29 16.89 0.75 o 7 -5 2 4.33 3.97 0.38 o -7 -4 2 45.24 46.17 1.60 o -6 -4 2 38.84 36.26 1.30 o -5 -4 2 36.47 35.19 1.24 o -4 -4 2 125.04 124.55 3.15 o -3 -4 2 179.94 181.24 3.03 o -2 -4 2 59.22 58.70 1.13 o -1 -4 2 217.22 231.33 3.79 o 0 -4 2 11.51 10.68 0.27 o 1 -4 2 4.89 6.81 0.23 o 2 -4 2 144.10 141.14 2.10 o 3 -4 2 135.30 137.42 3.03 o 4 -4 2 32.40 28.65 0.79 o 5 -4 2 11.02 12.29 1.63 o 6 -4 2 36.54 37.95 1.18 o 7 -4 2 27.72 27.70 0.97 o 8 -4 2 108.65 101.96 2.64 o -7 -3 2 16.49 16.64 0.82 o -6 -3 2 2.71 3.53 0.38 o -5 -3 2 67.01 64.31 1.84 o -4 -3 2 100.26 98.14 2.52 o -3 -3 2 53.66 49.74 1.41 o -2 -3 2 533.05 556.04 10.39 o -1 -3 2 31.45 48.59 0.74 o 0 -3 2 137.85 143.20 2.36 o 1 -3 2 94.58 95.47 1.42 o 2 -3 2 61.81 44.93 0.74 o 3 -3 2 1020.57 1024.78 17.49 o 4 -3 2 511.81 501.83 23.72 o 5 -3 2 158.81 153.04 3.56 o 6 -3 2 18.87 18.23 0.67 o 7 -3 2 0.32 0.57 0.17 o 8 -3 2 0.80 0.47 0.20 o -8 -2 2 30.45 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