#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210759.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210759_Fobs loop_ _publ_author_name 'Bandichhor, Rakeshwar' 'Thivierge, Cliferson' 'Bhuvanesh, Nattamai S. P.' 'Burgess, Kevin' _publ_section_title ; 4,4-Difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene ; _journal_coeditor_code OM2050 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4310 _journal_page_last o4311 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.245 _cell_angle_gamma 90.000 _cell_length_a 7.6932 _cell_length_b 14.3786 _cell_length_c 11.5295 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8949 _[local]_cod_data_source_file om2050Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KB in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 9.75 8.69 12.39 o 6 0 0 4.21 -4.79 22.36 o 8 0 0 553.71 580.40 29.77 o 1 1 0 7670.60 6951.25 74.82 o 2 1 0 9.61 31.32 10.23 o 3 1 0 684.58 658.32 20.33 o 4 1 0 39.65 51.25 10.50 o 5 1 0 60.41 68.52 11.70 o 6 1 0 28.37 38.20 21.12 o 7 1 0 0.15 6.83 17.59 o 8 1 0 3.04 21.79 15.09 o 0 2 0 4013.20 3753.09 49.75 o 1 2 0 3952.76 3575.18 50.51 o 3 2 0 608.63 681.40 62.55 o 4 2 0 93.42 77.66 25.80 o 5 2 0 6.74 3.23 9.98 o 6 2 0 31.72 27.97 18.44 o 7 2 0 59.51 55.33 18.41 o 8 2 0 15.92 22.64 16.34 o 1 3 0 1321.63 1304.55 17.67 o 2 3 0 20.77 25.01 5.66 o 3 3 0 11.94 7.99 9.05 o 4 3 0 187.93 141.51 15.62 o 5 3 0 240.82 255.70 14.90 o 6 3 0 6.55 -3.64 14.37 o 7 3 0 128.31 171.48 22.36 o 8 3 0 25.45 18.16 15.55 o 2 4 0 18.20 20.38 7.11 o 3 4 0 3.95 4.05 9.81 o 4 4 0 4555.33 4291.94 148.87 o 5 4 0 45.99 49.86 14.10 o 6 4 0 12.38 6.05 14.82 o 7 4 0 22.48 7.58 21.09 o 1 5 0 3226.79 3394.10 62.90 o 2 5 0 0.16 5.47 7.70 o 3 5 0 404.51 430.51 15.42 o 4 5 0 177.24 176.28 12.33 o 5 5 0 62.58 75.89 15.69 o 6 5 0 92.12 100.17 15.43 o 7 5 0 38.98 43.71 17.32 o 0 6 0 19.39 18.50 8.18 o 1 6 0 184.40 194.61 7.83 o 2 6 0 0.26 -8.45 8.45 o 3 6 0 2.21 4.33 10.21 o 4 6 0 278.96 289.10 14.25 o 5 6 0 25.59 49.00 17.01 o 6 6 0 3.28 17.19 15.07 o 7 6 0 55.13 41.45 16.60 o 1 7 0 495.48 490.58 13.41 o 2 7 0 149.76 167.66 13.99 o 3 7 0 88.85 70.28 10.27 o 4 7 0 116.29 114.50 14.77 o 5 7 0 30.85 30.55 18.62 o 6 7 0 0.07 -12.54 15.33 o 7 7 0 17.92 7.74 18.08 o 0 8 0 70.47 50.61 10.96 o 1 8 0 264.40 261.01 17.14 o 2 8 0 139.28 147.24 10.01 o 3 8 0 160.24 177.50 12.09 o 4 8 0 3.03 10.65 19.80 o 5 8 0 235.48 230.27 19.35 o 6 8 0 1.27 4.02 18.98 o 7 8 0 81.17 79.09 14.79 o 1 9 0 12.80 10.59 8.65 o 2 9 0 16.73 6.35 10.64 o 3 9 0 124.99 106.67 14.39 o 4 9 0 0.15 -16.06 16.48 o 5 9 0 127.23 135.39 20.27 o 6 9 0 19.17 23.47 18.66 o 0 10 0 3.34 -11.36 18.34 o 1 10 0 74.70 81.10 12.75 o 2 10 0 16.75 16.54 13.15 o 3 10 0 4.76 12.48 17.39 o 4 10 0 266.33 277.08 26.55 o 5 10 0 371.10 380.50 29.49 o 6 10 0 0.00 -2.49 15.99 o 1 11 0 119.49 85.77 16.10 o 2 11 0 283.79 249.18 59.91 o 3 11 0 244.32 255.54 43.14 o 4 11 0 2.47 -13.86 15.80 o 5 11 0 247.61 247.68 41.83 o 0 12 0 190.86 180.45 25.46 o 1 12 0 629.32 617.93 61.90 o 2 12 0 133.42 127.18 20.54 o 3 12 0 256.84 252.46 43.36 o 4 12 0 18.58 23.36 14.68 o 5 12 0 79.69 74.66 14.34 o 1 13 0 29.31 30.72 15.68 o 2 13 0 77.23 91.99 28.16 o 3 13 0 3.83 -5.74 15.11 o 4 13 0 121.05 109.25 16.24 o 0 14 0 9.53 9.86 21.67 o 1 14 0 88.51 87.49 19.46 o 2 14 0 1.12 6.07 17.84 o 3 14 0 1.33 -4.83 16.32 o 1 15 0 11.42 -2.90 17.30 o 2 15 0 17.58 8.56 16.66 o 0 16 0 3.30 -1.21 13.88 o -7 0 1 318.99 306.99 28.33 o -5 0 1 0.01 -2.90 20.04 o -3 0 1 964.69 1015.26 23.77 o 1 0 1 0.08 27.59 16.42 o 3 0 1 92.63 79.01 10.83 o 5 0 1 3039.17 3148.62 67.11 o 7 0 1 21.75 32.68 24.31 o -8 1 1 0.03 -1.47 16.08 o -7 1 1 89.97 109.28 18.01 o -6 1 1 70.33 88.72 17.33 o -5 1 1 147.81 115.00 16.84 o -4 1 1 99.10 86.86 17.09 o -3 1 1 3659.95 3606.57 61.05 o -2 1 1 249.03 273.52 8.04 o -1 1 1 1180.85 1096.66 12.70 o 0 1 1 4640.46 4081.96 40.43 o 1 1 1 1142.78 955.98 18.85 o 2 1 1 0.04 11.23 5.86 o 3 1 1 22.97 28.76 8.39 o 4 1 1 390.53 340.03 12.14 o 5 1 1 173.43 166.81 14.26 o 6 1 1 322.22 372.39 20.05 o 7 1 1 8.85 -3.78 18.31 o -8 2 1 8.46 17.80 17.37 o -7 2 1 5.45 1.33 17.19 o -6 2 1 23.99 21.26 17.47 o -5 2 1 70.83 56.43 10.01 o -4 2 1 532.16 576.16 40.26 o -3 2 1 451.68 393.80 12.66 o -2 2 1 4321.92 4465.93 72.62 o -1 2 1 1.28 11.57 9.10 o 1 2 1 1715.15 1487.18 21.58 o 2 2 1 1398.79 1276.51 31.73 o 3 2 1 11.22 18.21 8.50 o 4 2 1 19.57 22.90 13.07 o 5 2 1 89.09 73.44 11.56 o 6 2 1 162.69 181.12 20.46 o 7 2 1 6.60 7.62 17.13 o -8 3 1 83.34 96.82 17.40 o -7 3 1 83.08 105.77 22.12 o -6 3 1 46.86 54.38 20.80 o -5 3 1 84.12 73.35 12.52 o -4 3 1 78.52 74.00 21.49 o -3 3 1 3.16 19.50 10.10 o -2 3 1 14.82 33.94 6.94 o 0 3 1 203.72 217.03 7.67 o 1 3 1 3171.23 2949.60 33.70 o 2 3 1 838.19 889.71 14.63 o 3 3 1 24.22 14.49 9.92 o 4 3 1 25.69 11.68 10.77 o 5 3 1 0.02 -10.98 10.98 o 6 3 1 9.91 3.82 14.93 o 7 3 1 13.78 19.55 16.69 o -8 4 1 9.98 9.29 16.04 o -7 4 1 60.27 72.56 21.70 o -6 4 1 12.22 14.69 14.87 o -5 4 1 99.36 111.14 13.46 o -4 4 1 23.75 2.57 9.98 o -3 4 1 145.03 152.73 15.52 o -2 4 1 214.99 252.64 9.30 o -1 4 1 6.86 18.70 6.96 o 0 4 1 123.62 108.62 9.68 o 1 4 1 443.63 485.87 9.74 o 2 4 1 14.65 8.26 8.00 o 3 4 1 5.27 5.81 12.97 o 4 4 1 122.47 94.14 11.35 o 5 4 1 726.37 725.60 18.69 o 6 4 1 47.85 57.62 15.70 o 7 4 1 64.18 53.73 17.90 o -7 5 1 46.84 32.83 17.17 o -6 5 1 35.03 50.32 15.36 o -5 5 1 168.25 175.63 14.50 o -4 5 1 247.43 270.74 11.50 o -3 5 1 57.51 67.10 12.83 o -2 5 1 1824.51 1966.35 28.67 o -1 5 1 1050.19 1044.57 23.01 o 0 5 1 757.68 839.05 16.43 o 1 5 1 295.85 300.58 9.02 o 2 5 1 218.52 251.44 12.10 o 3 5 1 183.80 178.46 16.73 o 4 5 1 19.33 13.76 12.49 o 5 5 1 159.25 170.18 17.31 o 6 5 1 400.07 418.70 18.43 o 7 5 1 42.41 31.88 15.22 o -7 6 1 360.40 352.74 18.64 o -6 6 1 85.52 101.48 20.60 o -5 6 1 1.90 -2.11 15.96 o -4 6 1 1105.12 981.45 28.95 o -3 6 1 1513.85 1525.68 27.80 o -2 6 1 382.66 425.31 12.78 o -1 6 1 85.61 98.03 8.67 o 0 6 1 6533.65 7228.79 88.00 o 1 6 1 3073.76 3142.97 33.36 o 2 6 1 6.59 -4.68 13.26 o 3 6 1 101.43 103.17 11.74 o 4 6 1 26.19 32.16 13.36 o 5 6 1 475.62 506.11 20.68 o 6 6 1 0.33 -4.26 15.18 o 7 6 1 7.21 16.59 15.65 o -7 7 1 232.27 213.29 17.01 o -6 7 1 16.31 31.65 17.35 o -5 7 1 151.56 169.68 19.12 o -4 7 1 5.97 3.47 10.89 o -3 7 1 322.51 338.13 19.59 o -2 7 1 463.49 522.55 18.06 o -1 7 1 565.58 612.46 24.73 o 0 7 1 81.84 60.93 9.95 o 1 7 1 1625.02 1918.78 32.08 o 2 7 1 52.76 72.04 16.31 o 3 7 1 5.27 7.91 11.98 o 4 7 1 24.75 8.03 14.97 o 5 7 1 379.10 397.97 20.20 o 6 7 1 18.54 15.16 16.64 o 7 7 1 9.73 13.02 15.51 o -7 8 1 85.62 86.35 15.75 o -6 8 1 164.41 162.46 18.19 o -5 8 1 30.80 36.50 17.62 o -4 8 1 27.49 22.24 12.35 o -3 8 1 287.46 330.21 16.31 o -2 8 1 1186.83 1203.10 27.80 o -1 8 1 0.42 -4.83 9.08 o 0 8 1 933.37 917.63 23.04 o 1 8 1 66.15 72.70 12.45 o 2 8 1 224.40 241.40 13.00 o 3 8 1 37.51 19.67 13.10 o 4 8 1 264.49 296.40 23.54 o 5 8 1 33.46 39.93 19.90 o 6 8 1 234.44 237.06 26.41 o -6 9 1 105.18 116.40 20.21 o -5 9 1 87.03 103.18 19.11 o -4 9 1 201.64 224.82 18.48 o -3 9 1 225.54 242.95 13.05 o -2 9 1 55.61 54.02 10.92 o -1 9 1 4.88 0.51 7.62 o 0 9 1 874.60 888.05 15.10 o 1 9 1 276.34 224.08 19.41 o 2 9 1 373.87 381.14 15.82 o 3 9 1 61.35 51.19 14.02 o 4 9 1 5.10 13.37 19.87 o 5 9 1 180.48 185.04 18.96 o 6 9 1 0.54 6.22 16.23 o -6 10 1 90.30 107.49 19.98 o -5 10 1 4.18 8.66 19.71 o -4 10 1 779.63 871.92 28.58 o -3 10 1 417.15 473.73 40.39 o -2 10 1 197.44 215.51 13.75 o -1 10 1 195.03 196.70 11.47 o 0 10 1 493.93 549.58 15.95 o 1 10 1 449.82 462.92 15.86 o 2 10 1 40.12 39.98 13.84 o 3 10 1 115.98 113.64 27.92 o 4 10 1 795.06 870.90 28.68 o 5 10 1 186.80 201.69 18.12 o 6 10 1 0.00 -15.78 15.78 o -6 11 1 0.52 -1.58 12.88 o -5 11 1 10.97 20.48 16.44 o -4 11 1 2.57 -2.22 16.13 o -3 11 1 173.47 148.40 18.04 o -2 11 1 209.68 196.89 22.79 o -1 11 1 294.84 320.97 31.53 o 0 11 1 412.45 449.80 20.04 o 1 11 1 118.25 111.45 31.51 o 2 11 1 452.49 433.17 92.67 o 3 11 1 0.83 -7.57 16.70 o 4 11 1 25.55 17.45 17.89 o 5 11 1 36.23 45.82 15.21 o -5 12 1 0.31 1.26 14.50 o -4 12 1 602.19 619.12 21.81 o -3 12 1 139.89 126.60 25.40 o -2 12 1 72.52 57.22 21.77 o -1 12 1 16.84 44.63 17.70 o 0 12 1 4.13 2.84 17.04 o 1 12 1 0.62 9.51 16.02 o 2 12 1 951.18 875.19 123.34 o 3 12 1 53.67 51.15 16.27 o 4 12 1 10.19 8.28 14.10 o 5 12 1 29.87 38.71 14.08 o -4 13 1 192.77 179.44 15.11 o -3 13 1 33.88 19.66 15.83 o -2 13 1 300.55 271.04 38.24 o -1 13 1 0.03 15.03 16.17 o 0 13 1 31.13 14.72 16.16 o 1 13 1 492.96 471.87 54.43 o 2 13 1 4.71 8.59 19.03 o 3 13 1 0.49 -3.89 18.11 o 4 13 1 112.38 103.33 15.35 o -4 14 1 0.78 10.16 11.39 o -3 14 1 24.23 46.77 17.08 o -2 14 1 14.55 -6.00 18.24 o -1 14 1 50.46 44.79 18.93 o 0 14 1 378.40 376.69 18.76 o 1 14 1 135.54 115.08 19.23 o 2 14 1 28.54 20.34 18.26 o 3 14 1 25.87 36.74 16.42 o -3 15 1 45.97 53.56 20.96 o -2 15 1 32.07 28.78 16.97 o -1 15 1 5.26 1.51 13.06 o 0 15 1 3.65 -0.87 17.19 o 1 15 1 0.58 -5.64 24.10 o 2 15 1 5.79 -8.07 22.46 o 0 16 1 13.98 13.14 19.07 o -8 0 2 223.58 247.23 35.61 o -6 0 2 653.72 650.85 30.08 o -4 0 2 1251.69 1286.26 38.26 o -2 0 2 46222.37 44160.61 659.50 o 0 0 2 2263.90 2055.23 37.05 o 2 0 2 2279.09 2142.12 34.42 o 4 0 2 27.30 24.64 10.82 o 6 0 2 107.62 98.96 25.49 o -8 1 2 8.84 15.31 16.85 o -7 1 2 438.08 453.80 21.13 o -6 1 2 1.24 -0.94 17.02 o -5 1 2 338.12 306.46 14.58 o -4 1 2 68.86 82.43 17.31 o -3 1 2 286.02 275.30 8.88 o -2 1 2 10683.74 10274.12 85.70 o -1 1 2 9004.90 8246.38 74.20 o 0 1 2 84.88 103.47 5.85 o 1 1 2 714.67 727.01 11.30 o 2 1 2 1738.41 1732.36 21.24 o 3 1 2 728.08 728.18 14.26 o 4 1 2 88.83 81.99 8.02 o 5 1 2 393.68 383.62 14.63 o 6 1 2 7.04 7.36 17.80 o 7 1 2 63.23 57.77 17.28 o -8 2 2 12.31 7.51 18.01 o -7 2 2 31.44 43.16 19.76 o -6 2 2 21.42 28.75 17.33 o -5 2 2 162.74 139.96 17.05 o -4 2 2 22.98 0.96 16.81 o -3 2 2 2903.17 3024.91 34.40 o -2 2 2 5842.94 5755.83 97.43 o -1 2 2 1125.92 1107.17 19.16 o 1 2 2 39.70 39.72 8.61 o 2 2 2 2262.55 2202.77 28.45 o 3 2 2 511.95 515.34 22.11 o 4 2 2 95.65 89.69 9.70 o 5 2 2 21.78 15.78 11.97 o 6 2 2 103.00 57.84 19.02 o 7 2 2 536.00 542.27 21.17 o -8 3 2 15.85 6.75 17.91 o -7 3 2 37.69 51.44 22.12 o -6 3 2 238.74 221.55 34.80 o -5 3 2 161.18 133.59 13.32 o -4 3 2 5.59 11.17 14.23 o -3 3 2 1531.64 1669.30 23.40 o -2 3 2 94.28 105.02 7.79 o -1 3 2 898.10 839.20 17.36 o 0 3 2 149.72 163.66 8.06 o 1 3 2 5467.06 5374.94 52.52 o 2 3 2 413.55 453.87 13.14 o 3 3 2 180.50 193.58 14.24 o 4 3 2 34.83 40.29 9.14 o 5 3 2 26.06 23.58 13.06 o 6 3 2 210.73 205.07 16.00 o 7 3 2 8.85 -0.97 16.09 o -8 4 2 62.77 65.61 17.30 o -7 4 2 15.88 2.66 21.64 o -6 4 2 524.06 549.34 21.48 o -5 4 2 82.21 95.47 13.66 o -4 4 2 1017.34 1058.32 23.54 o -3 4 2 227.89 225.38 11.04 o -2 4 2 1136.48 1160.73 17.84 o -1 4 2 137.68 138.49 7.89 o 0 4 2 1806.60 1879.46 43.57 o 1 4 2 105.07 100.24 8.17 o 2 4 2 132.71 175.58 11.22 o 3 4 2 0.00 -8.85 18.42 o 4 4 2 100.33 105.63 11.88 o 5 4 2 65.51 61.40 13.55 o 6 4 2 45.23 28.35 15.12 o 7 4 2 85.00 79.14 17.58 o -8 5 2 6.32 5.09 14.72 o -7 5 2 201.50 216.29 22.72 o -6 5 2 3.83 0.60 19.04 o -5 5 2 161.68 151.72 14.56 o -4 5 2 94.64 94.77 10.46 o -3 5 2 0.03 -10.73 10.73 o -2 5 2 415.81 458.87 11.91 o -1 5 2 555.82 520.66 20.50 o 0 5 2 29.71 41.21 8.13 o 1 5 2 78.92 54.77 10.16 o 2 5 2 6.03 4.67 11.14 o 3 5 2 111.95 96.28 15.07 o 4 5 2 38.90 34.79 12.79 o 5 5 2 158.91 162.09 14.82 o 6 5 2 58.06 58.94 16.22 o 7 5 2 347.73 366.04 17.09 o -7 6 2 132.49 165.78 18.21 o -6 6 2 88.61 79.25 19.86 o -5 6 2 11.29 34.21 16.20 o -4 6 2 23.87 19.05 9.58 o -3 6 2 2.39 -3.67 11.80 o -2 6 2 0.66 -9.07 9.07 o -1 6 2 457.61 491.60 15.60 o 0 6 2 168.67 187.26 10.44 o 1 6 2 153.91 134.92 11.96 o 2 6 2 1969.96 2141.31 39.05 o 3 6 2 471.28 481.69 17.24 o 4 6 2 7.93 11.81 13.17 o 5 6 2 649.23 681.96 21.24 o 6 6 2 704.60 725.27 24.17 o 7 6 2 104.14 106.42 14.76 o -7 7 2 12.18 4.93 16.57 o -6 7 2 200.09 185.51 18.86 o -5 7 2 6.88 28.40 18.28 o -4 7 2 62.14 52.82 11.14 o -3 7 2 977.90 1035.93 21.06 o -2 7 2 65.11 82.74 11.92 o -1 7 2 148.61 157.59 13.30 o 0 7 2 6.05 -8.45 10.39 o 1 7 2 336.72 368.08 16.83 o 2 7 2 268.47 291.06 12.59 o 3 7 2 4.35 3.89 13.58 o 4 7 2 113.70 109.26 19.39 o 5 7 2 48.72 64.50 16.45 o 6 7 2 394.75 410.05 28.85 o -7 8 2 284.35 288.42 18.05 o -6 8 2 310.73 285.40 22.10 o -5 8 2 41.62 27.25 18.50 o -4 8 2 237.69 271.79 13.87 o -3 8 2 215.88 232.59 11.38 o -2 8 2 780.45 859.38 14.99 o -1 8 2 427.14 416.67 12.46 o 0 8 2 1039.94 1073.36 22.58 o 1 8 2 131.52 136.56 11.72 o 2 8 2 426.52 393.18 14.38 o 3 8 2 0.05 0.15 12.72 o 4 8 2 14.47 0.82 19.45 o 5 8 2 218.83 191.32 19.65 o 6 8 2 203.06 266.10 31.66 o -7 9 2 6.55 9.68 13.76 o -6 9 2 43.25 30.98 16.91 o -5 9 2 22.40 27.37 17.37 o -4 9 2 127.53 152.23 15.38 o -3 9 2 1.11 1.32 10.23 o -2 9 2 83.28 69.86 10.94 o -1 9 2 221.60 190.02 11.43 o 0 9 2 0.66 -8.51 11.21 o 1 9 2 52.10 38.86 14.28 o 2 9 2 299.19 258.56 14.30 o 3 9 2 45.56 39.59 15.07 o 4 9 2 3.27 -9.58 18.45 o 5 9 2 47.13 41.42 16.94 o 6 9 2 17.92 23.73 18.54 o -6 10 2 86.49 76.03 20.19 o -5 10 2 81.72 114.63 19.54 o -4 10 2 38.34 49.92 14.90 o -3 10 2 70.61 81.67 14.25 o -2 10 2 30.38 18.79 9.66 o -1 10 2 80.43 66.19 9.99 o 0 10 2 1.38 9.67 10.23 o 1 10 2 103.64 118.00 16.41 o 2 10 2 158.78 151.98 24.17 o 3 10 2 460.23 483.93 25.90 o 4 10 2 116.53 161.16 19.09 o 5 10 2 264.18 288.96 30.93 o -6 11 2 0.12 -10.78 13.85 o -5 11 2 260.21 280.58 19.74 o -4 11 2 33.11 33.78 16.76 o -3 11 2 220.52 233.25 16.21 o -2 11 2 20.49 -1.18 11.38 o -1 11 2 344.33 387.52 16.02 o 0 11 2 28.84 32.43 15.71 o 1 11 2 230.53 255.95 31.14 o 2 11 2 440.81 471.78 43.29 o 3 11 2 106.12 87.04 16.73 o 4 11 2 137.19 145.72 18.06 o 5 11 2 0.02 5.03 15.32 o -5 12 2 221.95 220.88 17.44 o -4 12 2 447.34 514.77 21.18 o -3 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