#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210766.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210766_Fobs loop_ _publ_author_name 'Dordea, Crenguta' 'B\"ohmer, Volker' 'Bolte, Michael' _publ_section_title ; 26,28-Diallyloxy-5,11,17,23-tetra-tert-butyl-25,27-bis(cyanomethoxy)calix[4]arene in the partial cone conformation ; _journal_coeditor_code SF2001 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4765 _journal_page_last o4767 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.951 _cell_angle_beta 79.257 _cell_angle_gamma 79.858 _cell_length_a 11.1136 _cell_length_b 18.7060 _cell_length_c 26.0130 _exptl_crystal_F_000 1744.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file sf2001Ibsup2.hkl _[local]_cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' boeh51 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1248.71 1292.12 2.55 o 2 0 0 3100.47 2311.50 227.96 o 3 0 0 86.37 -12.79 89.11 o 4 0 0 9998.81 8076.31 194.49 o 5 0 0 45.73 25.40 74.50 o 6 0 0 1820.87 2259.07 78.56 o 7 0 0 170.96 -77.19 79.68 o 8 0 0 6497.00 6604.31 124.60 o 9 0 0 1654.36 1480.67 85.03 o 10 0 0 0.39 141.51 98.85 o 11 0 0 22.14 41.06 96.29 o 12 0 0 79.81 116.47 69.71 o -12 1 0 210.45 267.00 72.62 o -11 1 0 3.29 -61.70 71.32 o -10 1 0 195.87 259.11 97.48 o -9 1 0 90.29 175.51 70.61 o -8 1 0 5916.48 6146.08 153.55 o -7 1 0 107.82 45.34 79.80 o -6 1 0 232.18 670.41 137.60 o -5 1 0 4427.10 5263.43 177.23 o -4 1 0 17096.65 14463.23 246.65 o -3 1 0 3906.46 2803.99 139.79 o -2 1 0 8771.95 9496.50 6.91 o -1 1 0 6041.45 6437.33 5.69 o 0 1 0 412.19 433.97 1.48 o 1 1 0 3592.44 3777.66 4.36 o 2 1 0 1763.89 1644.53 239.92 o 3 1 0 18.74 40.78 93.86 o 4 1 0 15411.82 13128.93 451.14 o 5 1 0 39.66 88.28 76.05 o 6 1 0 398.27 223.55 63.69 o 7 1 0 2747.14 2923.91 83.04 o 8 1 0 53.71 -0.29 60.37 o 9 1 0 750.14 788.54 106.80 o 10 1 0 102.15 188.26 100.75 o 11 1 0 10.83 88.41 78.32 o 12 1 0 55.37 186.25 105.38 o -12 2 0 472.40 475.56 104.19 o -11 2 0 77.22 86.21 66.93 o -10 2 0 87.50 197.23 107.57 o -9 2 0 234.42 374.52 105.26 o -8 2 0 732.18 566.22 106.08 o -7 2 0 550.99 595.53 114.99 o -6 2 0 15.08 96.42 91.79 o -5 2 0 2351.30 2363.38 119.38 o -4 2 0 12783.79 10617.64 192.66 o -3 2 0 9578.00 10166.63 7.15 o -2 2 0 45736.27 44178.27 14.90 o -1 2 0 3467.75 3105.13 3.95 o 0 2 0 5368.86 5013.16 5.02 o 1 2 0 47.34 48.82 0.49 o 2 2 0 31501.18 25552.45 589.07 o 3 2 0 1003.55 833.34 94.27 o 4 2 0 107.70 70.84 82.41 o 5 2 0 5144.25 5807.14 129.04 o 6 2 0 11.89 617.04 301.74 o 7 2 0 261.65 204.75 66.85 o 8 2 0 1367.24 1438.36 68.39 o 9 2 0 2264.74 2364.89 74.40 o 10 2 0 420.93 340.52 75.83 o 11 2 0 17.72 -8.37 75.18 o 12 2 0 121.96 173.66 102.47 o -12 3 0 134.72 210.46 73.28 o -11 3 0 8.12 -41.41 70.08 o -10 3 0 36.82 144.95 102.64 o -9 3 0 220.39 235.44 75.12 o -8 3 0 1.55 -43.55 69.54 o -7 3 0 47.90 143.94 111.49 o -6 3 0 282.39 408.86 121.64 o -5 3 0 414.73 415.04 135.28 o -4 3 0 5212.77 4508.64 4.76 o -3 3 0 1330.67 1490.56 2.74 o -2 3 0 3713.97 4113.32 4.55 o -1 3 0 15443.73 14933.76 8.66 o 0 3 0 51829.94 58148.94 576.37 o 1 3 0 8325.69 9024.62 196.97 o 2 3 0 7219.41 8744.73 573.37 o 3 3 0 3275.15 3080.91 192.21 o 4 3 0 4000.37 3232.23 118.61 o 5 3 0 2150.70 2076.15 98.29 o 6 3 0 179.41 164.43 70.86 o 7 3 0 568.34 735.28 97.54 o 8 3 0 249.71 364.03 139.97 o 9 3 0 47.13 43.25 61.66 o 10 3 0 337.93 343.16 90.37 o 11 3 0 218.29 319.96 79.09 o 12 3 0 4.48 -35.54 100.45 o -12 4 0 14.62 -53.94 100.57 o -11 4 0 203.37 139.61 98.85 o -10 4 0 206.85 329.77 106.62 o -9 4 0 914.83 899.92 77.96 o -8 4 0 34.52 -43.02 101.64 o -7 4 0 789.56 777.68 116.18 o -6 4 0 127.20 108.23 82.06 o -5 4 0 411.23 442.92 1.49 o -4 4 0 5.73 4.49 0.15 o -3 4 0 5.31 5.43 0.16 o -2 4 0 4072.31 4407.46 4.71 o -1 4 0 39750.57 39399.02 14.08 o 0 4 0 56026.58 50571.45 4176.97 o 1 4 0 2078.65 2919.88 207.84 o 2 4 0 0.11 251.02 94.29 o 3 4 0 6108.19 6389.11 422.34 o 4 4 0 763.76 857.48 103.35 o 5 4 0 350.98 276.90 80.69 o 6 4 0 95.89 136.44 63.87 o 7 4 0 298.78 305.13 64.91 o 8 4 0 0.37 90.86 73.63 o 9 4 0 76.51 157.54 60.80 o 10 4 0 753.47 770.91 188.83 o 11 4 0 9.57 54.49 109.56 o 12 4 0 14.16 -57.44 57.95 o -12 5 0 6.66 121.28 108.35 o -11 5 0 276.78 261.66 76.84 o -10 5 0 251.12 203.10 68.77 o -9 5 0 1126.50 1191.72 111.31 o -8 5 0 168.25 374.99 99.32 o -7 5 0 161.75 258.75 80.22 o -6 5 0 151.58 205.76 1.02 o -5 5 0 741.75 706.52 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-14.28 65.14 o 7 6 0 440.19 436.29 76.72 o 8 6 0 16.59 8.61 71.16 o 9 6 0 0.40 85.94 52.01 o 10 6 0 73.80 99.07 59.80 o 11 6 0 21.58 85.16 60.35 o 12 6 0 32.21 175.12 59.91 o -11 7 0 5.47 39.34 74.76 o -10 7 0 206.25 375.52 73.99 o -9 7 0 5.88 -6.35 70.73 o -8 7 0 81.85 147.08 69.95 o -7 7 0 131.71 115.27 0.76 o -6 7 0 0.98 1.22 0.08 o -5 7 0 16.90 18.97 0.30 o -4 7 0 400.91 374.72 1.37 o -3 7 0 1635.92 1697.21 2.93 o -2 7 0 980.25 1176.29 2.43 o -1 7 0 133.62 226.89 142.16 o 0 7 0 1134.27 1235.88 104.35 o 1 7 0 533.64 648.19 101.68 o 2 7 0 733.74 731.08 85.23 o 3 7 0 9361.29 8973.16 654.18 o 4 7 0 3737.63 4264.87 554.06 o 5 7 0 1437.79 1290.70 92.90 o 6 7 0 9.68 64.00 63.25 o 7 7 0 441.97 399.58 61.06 o 8 7 0 16.14 -53.96 67.93 o 9 7 0 51.76 1.55 96.09 o 10 7 0 240.14 211.81 63.12 o 11 7 0 30.93 65.47 50.72 o 12 7 0 73.08 110.89 57.82 o -11 8 0 10.00 -83.78 83.78 o -10 8 0 0.35 -30.37 69.77 o -9 8 0 64.57 92.85 71.02 o -8 8 0 491.39 489.92 106.08 o -7 8 0 33.60 33.44 0.41 o -6 8 0 271.98 261.74 1.15 o -5 8 0 298.71 281.84 1.19 o -4 8 0 248.41 227.40 1.07 o -3 8 0 2320.59 2383.46 3.46 o -2 8 0 0.97 82.65 92.74 o -1 8 0 14933.82 15764.00 205.59 o 0 8 0 956.98 956.36 104.89 o 1 8 0 4701.82 4953.74 103.38 o 2 8 0 2057.01 2259.25 109.74 o 3 8 0 2856.53 2404.27 183.37 o 4 8 0 3632.66 3928.52 271.92 o 5 8 0 214.17 315.46 68.68 o 6 8 0 130.40 247.10 52.94 o 7 8 0 35.54 103.72 70.21 o 8 8 0 922.08 971.17 167.50 o 9 8 0 153.44 199.40 59.62 o 10 8 0 5.20 -65.48 65.48 o 11 8 0 22.49 67.63 74.55 o 12 8 0 31.58 -46.38 70.51 o -10 9 0 3.23 -60.29 106.39 o -9 9 0 21.77 -47.53 70.90 o -8 9 0 509.60 566.46 1.69 o -7 9 0 7.14 6.07 0.18 o -6 9 0 131.69 128.73 0.80 o -5 9 0 483.58 444.93 1.49 o -4 9 0 283.01 310.00 1.25 o -3 9 0 857.28 890.70 2.12 o -2 9 0 210.26 361.41 86.51 o -1 9 0 391.99 389.41 122.94 o 0 9 0 1.27 25.19 79.90 o 1 9 0 243.20 477.78 78.21 o 2 9 0 736.70 725.22 65.94 o 3 9 0 308.04 395.32 62.66 o 4 9 0 881.86 882.10 63.92 o 5 9 0 460.50 465.58 56.90 o 6 9 0 36.23 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6 28 4.15 5.15 0.23 o 3 6 28 32.10 33.68 0.58 o 4 6 28 26.91 28.59 0.53 o 5 6 28 185.61 161.59 1.28 o 6 6 28 6.54 8.71 0.29 o 7 6 28 41.93 38.64 0.62 o -3 7 28 27.04 -4.98 144.24 o -2 7 28 46.55 48.30 0.69 o -1 7 28 5.77 4.30 0.21 o 0 7 28 8.44 13.84 0.37 o 1 7 28 7.33 7.76 0.28 o 2 7 28 13.91 15.15 0.39 o 3 7 28 9.27 9.55 0.31 o 4 7 28 0.08 0.25 0.05 o 5 7 28 1.31 1.17 0.11 o 6 7 28 0.47 0.57 0.08 o 7 7 28 0.24 0.19 0.04 o -3 8 28 68.27 102.83 90.65 o -2 8 28 13.85 103.68 134.81 o -1 8 28 10.95 10.05 0.32 o 0 8 28 47.83 52.60 0.72 o 1 8 28 66.72 64.43 0.80 o 2 8 28 22.27 18.91 0.43 o 3 8 28 0.95 1.39 0.12 o 4 8 28 28.03 27.36 0.52 o 5 8 28 2.01 1.76 0.13 o 6 8 28 2.41 2.23 0.15 o 7 8 28 25.86 30.12 0.55 o -3 9 28 4.74 21.14 91.96 o -2 9 28 3.49 48.84 107.75 o -1 9 28 262.39 342.58 1.86 o 0 9 28 24.50 22.26 0.47 o 1 9 28 11.82 9.81 0.31 o 2 9 28 119.39 120.32 1.10 o 3 9 28 34.36 32.44 0.57 o 4 9 28 115.30 123.55 1.12 o 5 9 28 70.75 81.34 0.91 o 6 9 28 4.84 5.33 0.23 o 7 9 28 10.07 11.83 0.34 o -2 10 28 447.84 387.55 99.50 o -1 10 28 1.02 1.86 0.14 o 0 10 28 0.10 0.13 0.04 o 1 10 28 27.34 27.21 0.52 o 2 10 28 0.13 0.12 0.03 o 3 10 28 95.41 113.29 1.07 o 4 10 28 146.89 167.81 1.30 o 5 10 28 108.00 123.56 1.12 o 6 10 28 1.57 1.31 0.11 o 7 10 28 0.11 0.15 0.04 o -2 11 28 110.98 134.64 87.42 o -1 11 28 108.60 162.55 113.50 o 0 11 28 1.17 1.13 0.11 o 1 11 28 17.79 23.21 0.48 o 2 11 28 39.98 41.22 0.64 o 3 11 28 213.31 196.13 1.41 o 4 11 28 11.29 7.45 0.27 o 5 11 28 90.36 90.54 0.96 o 6 11 28 2.78 2.27 0.15 o 7 11 28 9.44 10.25 0.32 o -2 12 28 10.23 -20.63 93.11 o -1 12 28 1.31 -21.12 98.32 o 0 12 28 0.46 -1.65 137.32 o 1 12 28 7.36 6.69 0.26 o 2 12 28 33.24 32.39 0.57 o 3 12 28 14.15 17.48 0.42 o 4 12 28 15.48 11.13 0.33 o 5 12 28 111.74 119.58 1.10 o 6 12 28 138.44 121.53 1.11 o 7 12 28 92.40 72.10 0.86 o -1 13 28 5.38 41.20 88.13 o 0 13 28 4.31 -21.25 104.79 o 1 13 28 108.14 4.63 134.48 o 2 13 28 95.02 90.30 0.96 o 3 13 28 15.32 13.23 0.36 o 4 13 28 0.16 0.13 0.04 o 5 13 28 143.85 126.27 1.13 o 6 13 28 105.87 117.74 1.09 o 0 14 28 216.95 252.61 91.06 o 1 14 28 8.26 30.60 101.03 o 2 14 28 225.47 113.52 119.21 o 3 14 28 71.61 70.13 149.29 o 4 14 28 15.98 9.20 250.80 o 5 14 28 6.24 22.01 190.64 o 6 14 28 0.09 70.08 150.65 o 1 15 28 24.12 53.49 81.77 o 2 15 28 144.41 127.44 123.83 o 3 15 28 31.47 57.97 144.89 o 4 15 28 24.73 80.28 146.44 o 5 15 28 4.35 27.36 131.07 o 3 16 28 6.67 25.51 128.46 o 0 1 29 15.32 16.12 0.40 o 1 1 29 16.47 16.13 0.40 o 2 1 29 42.67 50.01 0.71 o 3 1 29 11.30 10.87 0.33 o -1 2 29 22.13 20.64 0.45 o 0 2 29 0.29 0.63 0.08 o 1 2 29 8.24 8.72 0.29 o 2 2 29 12.96 14.60 0.38 o 3 2 29 44.07 55.03 0.74 o 4 2 29 7.27 7.30 0.27 o -1 3 29 448.09 438.77 2.10 o 0 3 29 6.95 5.90 0.24 o 1 3 29 0.21 0.21 0.05 o 2 3 29 0.51 0.47 0.07 o 3 3 29 20.28 24.39 0.49 o 4 3 29 4.87 6.27 0.25 o 5 3 29 12.90 14.41 0.38 o -1 4 29 102.48 100.02 1.01 o 0 4 29 170.14 171.54 1.32 o 1 4 29 19.21 17.43 0.42 o 2 4 29 4.49 4.73 0.22 o 3 4 29 20.34 23.65 0.48 o 4 4 29 39.11 44.59 0.67 o 5 4 29 41.78 33.69 0.58 o 6 4 29 31.51 29.71 0.54 o -2 5 29 3.44 3.90 0.20 o -1 5 29 0.02 0.01 0.01 o 0 5 29 0.18 0.20 0.04 o 1 5 29 21.09 19.39 0.44 o 2 5 29 69.81 67.18 0.83 o 3 5 29 1.26 1.39 0.12 o 4 5 29 154.72 170.02 1.31 o 5 5 29 2.90 5.43 0.23 o 6 5 29 23.48 23.72 0.49 o -2 6 29 41.46 37.19 0.61 o -1 6 29 122.31 129.47 1.14 o 0 6 29 8.77 7.37 0.27 o 1 6 29 1.96 2.51 0.16 o 2 6 29 0.01 0.00 0.01 o 3 6 29 13.59 15.16 0.39 o 4 6 29 18.78 27.46 0.52 o 5 6 29 5.58 7.40 0.27 o 6 6 29 0.23 0.26 0.05 o -2 7 29 3.70 2.79 0.17 o -1 7 29 109.98 120.65 1.11 o 0 7 29 260.43 246.88 1.58 o 1 7 29 49.06 55.10 0.74 o 2 7 29 39.25 43.17 0.66 o 3 7 29 124.11 145.92 1.21 o 4 7 29 0.27 0.16 0.04 o 5 7 29 15.56 15.27 0.39 o 6 7 29 1.20 0.98 0.10 o -2 8 29 126.40 137.71 1.18 o -1 8 29 11.21 10.99 0.33 o 0 8 29 198.63 196.01 1.41 o 1 8 29 4.97 5.16 0.23 o 2 8 29 119.82 110.82 1.06 o 3 8 29 70.03 74.21 0.87 o 4 8 29 2.39 1.37 0.12 o 5 8 29 59.46 61.54 0.78 o 6 8 29 0.05 0.02 0.02 o -2 9 29 94.83 87.44 160.94 o -1 9 29 33.43 43.36 0.66 o 0 9 29 104.62 107.19 1.04 o 1 9 29 64.20 53.99 0.73 o 2 9 29 117.43 118.28 1.09 o 3 9 29 447.06 459.79 2.15 o 4 9 29 15.25 16.06 0.40 o 5 9 29 0.20 0.28 0.05 o 6 9 29 1.60 1.97 0.14 o -1 10 29 0.21 0.25 0.05 o 0 10 29 37.91 50.80 0.71 o 1 10 29 14.44 16.33 0.40 o 2 10 29 65.41 77.66 0.89 o 3 10 29 11.54 11.16 0.33 o 4 10 29 23.27 23.28 0.48 o 5 10 29 26.36 27.74 0.53 o 6 10 29 0.49 0.59 0.08 o -1 11 29 48.95 37.47 0.61 o 0 11 29 2.33 2.56 0.16 o 1 11 29 8.47 9.17 0.30 o 2 11 29 0.46 0.53 0.07 o 3 11 29 45.63 44.90 0.67 o 4 11 29 113.60 134.99 1.17 o 5 11 29 179.84 189.13 1.38 o 6 11 29 4.31 4.82 0.22 o 0 12 29 4.83 5.33 0.23 o 1 12 29 96.37 88.57 0.95 o 2 12 29 91.50 77.33 0.89 o 3 12 29 24.20 20.88 0.46 o 4 12 29 51.20 50.61 0.71 o 5 12 29 105.05 114.87 1.08 o 6 12 29 23.29 30.71 0.55 o 0 13 29 45.54 23.80 118.51 o 1 13 29 6.36 6.23 0.25 o 2 13 29 0.93 0.81 0.09 o 3 13 29 140.42 170.63 1.31 o 4 13 29 16.91 12.49 0.35 o 5 13 29 142.81 137.29 1.18 o 1 14 29 54.11 56.60 128.59 o 2 14 29 64.17 62.20 0.79 o 3 14 29 9.43 12.56 0.35 o 4 14 29 200.07 224.51 1.50 o 1 3 30 54.05 63.50 0.79 o 2 3 30 0.77 0.64 0.08 o 3 3 30 123.35 115.36 1.08 o 0 4 30 4.02 4.58 0.21 o 1 4 30 246.20 243.86 1.57 o 2 4 30 6.98 5.92 0.24 o 3 4 30 98.01 116.28 1.08 o 4 4 30 21.61 22.55 0.47 o 0 5 30 23.65 21.26 0.46 o 1 5 30 23.14 23.34 0.48 o 2 5 30 6.36 7.76 0.28 o 3 5 30 102.49 112.08 1.07 o 4 5 30 22.30 18.00 0.42 o 0 6 30 52.74 56.94 0.75 o 1 6 30 3.80 3.96 0.20 o 2 6 30 107.52 105.37 1.03 o 3 6 30 1.83 2.18 0.15 o 4 6 30 81.52 95.25 0.98 o 5 6 30 1.02 1.95 0.14 o 0 7 30 37.95 34.31 0.58 o 1 7 30 153.13 159.78 1.27 o 2 7 30 4.23 4.27 0.21 o 3 7 30 0.44 0.47 0.07 o 4 7 30 1.65 1.41 0.12 o 5 7 30 28.90 29.61 0.54 o 0 8 30 106.87 92.24 0.97 o 1 8 30 54.66 49.49 0.70 o 2 8 30 2.14 1.87 0.14 o 3 8 30 23.47 25.07 0.50 o 4 8 30 14.04 19.30 0.44 o 5 8 30 77.62 73.19 0.86 o 0 9 30 1.93 1.70 0.13 o 1 9 30 51.93 46.49 0.68 o 2 9 30 58.99 64.35 0.80 o 3 9 30 81.77 86.72 0.94 o 4 9 30 21.95 15.33 0.39 o 5 9 30 14.95 10.94 0.33 o 0 10 30 282.90 295.37 1.72 o 1 10 30 0.44 0.50 0.07 o 2 10 30 45.47 47.95 0.69 o 3 10 30 13.74 14.77 0.38 o 4 10 30 36.98 43.59 0.66 o 5 10 30 38.47 52.44 0.72 o 1 11 30 75.04 83.06 0.92 o 2 11 30 0.24 0.19 0.04 o 3 11 30 45.77 38.61 0.62 o 4 11 30 40.74 38.85 0.62 o 5 11 30 50.20 44.09 0.66 o 1 12 30 47.38 44.85 0.67 o 2 12 30 1.58 1.44 0.12 o 3 12 30 21.58 19.38 0.44 o 4 12 30 60.73 68.28 0.83 o