#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210802_Fobs loop_ _publ_author_name 'Okabe, Nobuo' 'Mizubayashi, Yu' 'Odoko, Mamiko' _publ_section_title ; (Cyclobutane-1,1-dicarboxylato-\k^2^O,O')(di-2-pyridylamine-\k^2^N,N')palladium(II) ; _journal_coeditor_code TK2079 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2747 _journal_page_last m2749 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.923 _cell_angle_beta 67.300 _cell_angle_gamma 71.211 _cell_length_a 9.1146 _cell_length_b 9.6976 _cell_length_c 10.2267 _exptl_crystal_F_000 420.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file tk2079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ca13' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9909.64 10334.94 27.74 o 3 0 0 4997.06 5166.61 19.97 o 4 0 0 0.69 2.12 0.64 o 5 0 0 676.44 679.06 6.08 o 6 0 0 1837.85 1772.48 17.64 o 7 0 0 88.56 99.38 2.99 o 8 0 0 13.02 15.71 2.02 o 9 0 0 240.50 253.40 5.10 o 10 0 0 22.55 10.57 6.53 o -10 1 0 71.19 74.21 3.63 o -9 1 0 108.19 100.58 4.12 o -8 1 0 523.68 519.84 7.89 o -7 1 0 21.69 24.64 2.23 o -6 1 0 540.88 555.16 7.82 o -5 1 0 1883.38 1852.29 21.22 o -4 1 0 510.33 520.65 4.91 o -3 1 0 3464.51 3672.72 22.65 o -2 1 0 4939.24 4926.55 24.16 o -1 1 0 368.62 342.85 2.65 o 1 1 0 3426.57 3384.74 44.57 o 2 1 0 6297.46 6782.83 21.86 o 3 1 0 3685.28 3758.70 13.05 o 4 1 0 3625.91 3930.19 14.31 o 5 1 0 8.51 6.44 0.75 o 6 1 0 1254.46 1249.06 9.65 o 7 1 0 271.88 288.53 5.11 o 8 1 0 40.17 39.61 2.59 o 9 1 0 359.11 352.69 6.41 o 10 1 0 55.80 62.49 9.95 o -10 2 0 117.26 125.12 5.42 o -9 2 0 10.76 7.81 1.88 o -8 2 0 63.69 69.08 3.08 o -7 2 0 508.77 535.28 19.58 o -6 2 0 56.96 59.28 2.79 o -5 2 0 1116.35 1104.54 14.10 o -4 2 0 2122.47 2091.69 18.42 o -3 2 0 212.05 240.60 3.87 o -2 2 0 2058.10 2046.45 13.75 o -1 2 0 1248.48 1151.51 7.73 o 0 2 0 14.22 13.33 2.26 o 1 2 0 4.21 6.56 0.85 o 2 2 0 120.43 102.22 1.96 o 3 2 0 467.82 485.86 8.51 o 4 2 0 3741.16 4018.94 40.90 o 5 2 0 4148.26 4193.38 31.25 o 6 2 0 77.56 79.80 2.54 o 7 2 0 1288.25 1256.77 24.55 o 8 2 0 480.95 518.24 17.05 o 9 2 0 122.08 121.78 10.42 o 10 2 0 441.51 427.70 16.06 o -9 3 0 107.68 114.69 4.53 o -8 3 0 174.96 183.41 6.14 o -7 3 0 1059.88 1080.83 13.61 o -6 3 0 387.17 377.62 6.58 o -5 3 0 1.38 2.44 1.67 o -4 3 0 3009.13 2881.43 25.95 o -3 3 0 392.46 348.88 5.34 o -2 3 0 108.93 116.67 2.72 o -1 3 0 5448.27 5597.77 29.98 o 0 3 0 3829.74 3984.87 21.30 o 1 3 0 829.92 883.24 6.55 o 2 3 0 5736.71 5747.65 28.19 o 3 3 0 165.35 219.90 4.30 o 4 3 0 514.93 535.37 11.03 o 5 3 0 265.07 227.36 3.52 o 6 3 0 410.29 392.38 8.45 o 7 3 0 40.11 41.06 1.85 o 8 3 0 1060.74 1037.63 21.93 o 9 3 0 286.33 267.52 11.00 o 10 3 0 99.20 99.27 8.16 o -9 4 0 243.03 227.53 7.39 o -8 4 0 328.83 321.17 8.22 o -7 4 0 398.74 391.82 7.75 o -6 4 0 2354.28 2329.12 28.70 o -5 4 0 832.66 815.04 18.43 o -4 4 0 878.03 898.86 12.14 o -3 4 0 1132.66 1099.99 12.33 o -2 4 0 1749.97 1861.34 27.07 o -1 4 0 1131.87 1062.99 10.69 o 0 4 0 3262.58 3324.00 24.98 o 1 4 0 907.29 896.30 14.62 o 2 4 0 30.93 25.38 1.38 o 3 4 0 266.32 200.34 3.25 o 4 4 0 2007.69 2096.49 23.27 o 5 4 0 1061.42 1060.52 9.88 o 6 4 0 818.47 825.33 13.46 o 7 4 0 125.72 141.61 5.67 o 8 4 0 75.28 81.94 3.40 o 9 4 0 489.23 525.20 27.09 o 10 4 0 143.66 143.18 6.44 o -8 5 0 283.44 289.04 7.89 o -7 5 0 214.68 203.65 6.02 o -6 5 0 29.17 33.24 4.48 o -5 5 0 1543.59 1504.55 20.46 o -4 5 0 247.45 244.45 6.54 o -3 5 0 1793.06 1780.86 19.30 o -2 5 0 3259.73 3350.95 28.83 o -1 5 0 93.41 92.54 3.38 o 0 5 0 981.31 871.42 9.72 o 1 5 0 2250.51 2126.61 26.75 o 2 5 0 22.45 25.93 1.66 o 3 5 0 1528.52 1451.70 12.99 o 4 5 0 3200.67 3411.48 26.21 o 5 5 0 11.12 11.45 3.25 o 6 5 0 697.29 785.60 9.80 o 7 5 0 1565.27 1572.19 27.57 o 8 5 0 28.38 28.42 2.08 o 9 5 0 184.50 185.45 5.32 o 10 5 0 120.53 131.46 6.14 o -8 6 0 211.97 213.15 9.98 o -7 6 0 56.64 52.85 5.36 o -6 6 0 5.38 3.66 3.04 o -5 6 0 19.87 16.83 3.71 o -4 6 0 126.11 124.23 5.22 o -3 6 0 109.98 98.48 5.54 o -2 6 0 994.59 943.13 13.53 o -1 6 0 2272.08 2243.61 21.55 o 0 6 0 0.03 1.72 1.31 o 1 6 0 2582.86 2549.77 24.76 o 2 6 0 2087.35 2097.46 18.77 o 3 6 0 59.21 59.22 2.74 o 4 6 0 3220.05 3302.80 27.90 o 5 6 0 1586.99 1600.54 25.87 o 6 6 0 23.96 27.03 1.98 o 7 6 0 720.91 715.63 14.36 o 8 6 0 378.42 396.77 9.71 o 9 6 0 19.41 21.84 1.71 o 10 6 0 197.26 201.74 12.18 o -7 7 0 135.94 138.19 9.38 o -6 7 0 361.03 376.34 14.33 o -5 7 0 56.36 55.35 5.01 o -4 7 0 548.69 554.78 11.70 o -3 7 0 109.22 108.61 5.01 o -2 7 0 29.00 23.02 3.41 o -1 7 0 327.64 351.54 7.43 o 0 7 0 1785.54 1790.57 20.36 o 1 7 0 188.83 173.33 4.83 o 2 7 0 3391.70 3523.23 30.83 o 3 7 0 1500.39 1469.00 16.31 o 4 7 0 299.64 313.48 6.41 o 5 7 0 2632.46 2589.41 36.81 o 6 7 0 507.06 505.26 12.65 o 7 7 0 453.77 457.29 7.79 o 8 7 0 684.40 668.69 13.17 o 9 7 0 23.96 31.14 3.61 o -6 8 0 439.19 458.77 17.43 o -5 8 0 102.66 101.65 6.65 o -4 8 0 115.56 119.95 6.43 o -3 8 0 913.19 948.38 16.68 o -2 8 0 33.83 35.28 3.73 o -1 8 0 540.37 516.40 10.02 o 0 8 0 1130.68 1117.65 15.54 o 1 8 0 13.26 14.14 2.81 o 2 8 0 122.13 119.98 4.34 o 3 8 0 1323.35 1280.67 16.80 o 4 8 0 110.95 122.21 4.96 o 5 8 0 461.39 467.18 8.89 o 6 8 0 622.94 672.56 16.04 o 7 8 0 122.90 122.89 4.61 o 8 8 0 24.22 28.55 2.31 o 9 8 0 466.42 448.11 26.85 o -5 9 0 151.22 157.05 8.71 o -4 9 0 24.89 27.69 4.67 o -3 9 0 206.48 209.76 8.64 o -2 9 0 946.26 974.48 25.35 o -1 9 0 334.57 332.58 8.97 o 0 9 0 1001.25 1030.87 17.71 o 1 9 0 1113.34 1135.32 17.95 o 2 9 0 20.55 22.85 3.01 o 3 9 0 282.77 287.17 7.77 o 4 9 0 269.17 273.17 7.64 o 5 9 0 161.44 153.80 7.25 o 6 9 0 135.95 146.81 7.70 o 7 9 0 339.92 343.99 12.44 o 8 9 0 59.73 67.64 6.80 o -3 10 0 0.51 4.14 3.93 o -2 10 0 960.49 981.30 19.68 o -1 10 0 618.84 611.54 13.83 o 0 10 0 0.86 1.49 2.24 o 1 10 0 518.32 539.23 11.78 o 2 10 0 648.24 645.05 12.82 o 3 10 0 26.77 25.67 3.93 o 4 10 0 761.82 750.31 13.62 o 5 10 0 213.57 208.13 7.73 o 6 10 0 18.61 18.74 4.51 o 7 10 0 137.44 138.82 8.98 o -1 11 0 557.17 561.93 18.13 o 0 11 0 258.68 270.26 15.39 o 1 11 0 128.66 128.45 7.84 o 2 11 0 564.20 591.88 16.09 o 3 11 0 141.78 154.70 8.49 o 4 11 0 88.48 88.00 6.31 o 5 11 0 615.80 584.01 13.18 o -4 -11 1 273.00 276.64 9.61 o -3 -11 1 0.34 1.57 2.88 o -2 -11 1 355.11 374.19 11.25 o -1 -11 1 299.53 302.46 10.39 o 0 -11 1 4.47 5.08 3.20 o -6 -10 1 377.11 350.24 17.69 o -5 -10 1 30.03 30.42 4.08 o -4 -10 1 723.51 712.86 15.59 o -3 -10 1 130.64 138.97 6.28 o -2 -10 1 101.03 106.30 5.94 o -1 -10 1 685.13 684.92 14.38 o 0 -10 1 473.44 466.01 11.97 o 1 -10 1 31.39 35.48 5.58 o 2 -10 1 746.78 736.64 18.87 o 3 -10 1 295.26 297.85 11.29 o -7 -9 1 177.56 187.98 10.36 o -6 -9 1 187.70 183.68 9.37 o -5 -9 1 224.50 231.81 7.40 o -4 -9 1 23.45 33.96 4.60 o -3 -9 1 1694.17 1669.31 23.08 o -2 -9 1 831.66 817.02 14.75 o -1 -9 1 1425.90 1441.56 24.34 o 0 -9 1 1772.42 1739.15 24.52 o 1 -9 1 143.73 147.39 6.65 o 2 -9 1 558.61 571.55 13.12 o 3 -9 1 520.66 534.75 15.37 o 4 -9 1 0.24 0.83 2.91 o -8 -8 1 275.28 292.75 11.26 o -7 -8 1 9.28 13.29 2.33 o -6 -8 1 354.03 382.80 12.89 o -5 -8 1 541.50 566.16 15.26 o -4 -8 1 3.85 5.52 2.15 o -3 -8 1 448.38 452.62 8.96 o -2 -8 1 649.06 633.64 10.80 o -1 -8 1 130.49 134.98 5.15 o 0 -8 1 413.82 416.54 9.18 o 1 -8 1 1449.45 1465.14 21.52 o 2 -8 1 2.80 2.78 2.29 o 3 -8 1 413.72 430.63 10.88 o 4 -8 1 349.47 373.93 10.67 o 5 -8 1 0.01 0.99 2.89 o 6 -8 1 335.85 333.98 12.06 o -9 -7 1 3.23 3.90 2.64 o -8 -7 1 230.85 225.77 5.72 o -7 -7 1 663.58 689.81 10.30 o -6 -7 1 1.98 1.07 2.41 o -5 -7 1 1052.67 1042.76 20.53 o -4 -7 1 1347.19 1367.67 17.28 o -3 -7 1 7.36 8.12 2.40 o -2 -7 1 775.30 789.19 11.44 o -1 -7 1 293.91 314.32 6.75 o 0 -7 1 2.68 -0.65 2.05 o 1 -7 1 229.44 224.09 6.10 o 2 -7 1 1089.23 1142.98 17.10 o 3 -7 1 103.68 100.84 5.02 o 4 -7 1 686.01 667.48 14.23 o 5 -7 1 454.68 456.78 20.95 o 6 -7 1 25.38 21.99 4.96 o 7 -7 1 383.90 380.91 12.80 o -9 -6 1 126.40 139.63 15.89 o -8 -6 1 29.38 31.61 1.80 o -7 -6 1 1032.90 1039.90 26.84 o -6 -6 1 1122.68 1150.93 22.90 o -5 -6 1 203.95 186.64 7.46 o -4 -6 1 1833.19 1817.20 19.52 o -3 -6 1 1940.30 1950.40 42.19 o -2 -6 1 196.98 189.15 5.34 o -1 -6 1 3192.88 3110.96 27.06 o 0 -6 1 137.19 132.93 4.22 o 1 -6 1 775.23 781.34 11.64 o 2 -6 1 274.79 275.61 6.42 o 3 -6 1 15.57 15.93 2.63 o 4 -6 1 16.61 16.50 3.29 o 5 -6 1 260.78 263.29 8.79 o 6 -6 1 79.30 70.75 5.86 o 7 -6 1 36.50 39.02 3.66 o 8 -6 1 154.07 159.25 6.53 o -10 -5 1 13.46 15.58 4.16 o -9 -5 1 716.99 710.10 40.44 o -8 -5 1 212.44 205.15 8.41 o -7 -5 1 452.53 447.23 13.59 o -6 -5 1 1576.20 1638.65 15.50 o -5 -5 1 232.38 231.58 9.52 o -4 -5 1 211.45 238.56 7.11 o -3 -5 1 2610.71 2610.92 22.28 o -2 -5 1 1.47 9.26 1.74 o -1 -5 1 806.82 764.21 8.79 o 0 -5 1 2021.47 1925.58 20.47 o 1 -5 1 1346.30 1321.59 13.60 o 2 -5 1 405.02 371.65 6.55 o 3 -5 1 1915.88 1973.88 25.45 o 4 -5 1 86.60 87.35 5.08 o 5 -5 1 569.50 557.39 12.12 o 6 -5 1 609.35 584.76 13.13 o 7 -5 1 201.26 201.84 5.98 o 8 -5 1 64.34 69.85 4.77 o -10 -4 1 0.69 2.52 2.58 o -9 -4 1 74.14 89.56 5.40 o -8 -4 1 535.33 567.65 30.98 o -7 -4 1 247.73 241.20 10.16 o -6 -4 1 936.31 954.10 20.46 o -5 -4 1 1679.36 1711.22 33.30 o -4 -4 1 3.32 6.30 2.08 o -3 -4 1 1827.48 1802.70 21.39 o -2 -4 1 1915.29 1863.08 14.86 o -1 -4 1 161.59 153.26 3.47 o 0 -4 1 4205.12 4373.57 29.10 o 1 -4 1 5295.91 5787.83 69.07 o 2 -4 1 260.18 236.33 4.43 o 3 -4 1 3061.71 3001.63 26.34 o 4 -4 1 2602.84 2630.20 26.37 o 5 -4 1 166.98 168.20 5.52 o 6 -4 1 1532.04 1546.83 23.33 o 7 -4 1 803.57 795.30 12.30 o 8 -4 1 6.66 5.22 2.07 o 9 -4 1 119.45 124.38 5.38 o -10 -3 1 236.97 243.84 8.91 o -9 -3 1 46.95 44.86 4.18 o -8 -3 1 201.68 203.87 12.97 o -7 -3 1 10.94 14.52 2.81 o -6 -3 1 17.75 20.54 1.28 o -5 -3 1 122.68 120.71 2.28 o -4 -3 1 1437.42 1425.00 19.81 o -3 -3 1 849.99 925.61 12.38 o -2 -3 1 3172.90 3203.03 20.65 o -1 -3 1 3692.72 3632.28 21.30 o 0 -3 1 4.51 3.97 0.92 o 1 -3 1 4459.43 4725.65 27.61 o 2 -3 1 2080.34 1899.37 14.60 o 3 -3 1 178.91 166.41 3.98 o 4 -3 1 2301.82 2294.42 20.78 o 5 -3 1 2036.02 1987.96 21.77 o 6 -3 1 3.48 10.28 2.49 o 7 -3 1 640.31 652.76 13.06 o 8 -3 1 151.99 157.85 5.80 o 9 -3 1 82.99 79.51 4.94 o -10 -2 1 189.56 188.31 11.45 o -9 -2 1 181.63 178.63 10.05 o -8 -2 1 4.67 2.92 2.95 o -7 -2 1 1287.30 1273.49 24.45 o -6 -2 1 354.84 346.53 9.58 o -5 -2 1 24.17 21.15 1.78 o -4 -2 1 5.16 4.09 0.49 o -3 -2 1 828.99 871.15 11.10 o -2 -2 1 57.64 47.16 2.16 o -1 -2 1 4221.96 4281.21 35.14 o 0 -2 1 1486.72 1437.49 20.50 o 1 -2 1 36.69 44.09 2.44 o 2 -2 1 3096.12 3093.92 18.74 o 3 -2 1 3632.91 3773.79 31.97 o 4 -2 1 1988.91 2016.56 23.82 o 5 -2 1 3252.93 3387.78 22.82 o 6 -2 1 140.17 137.62 3.88 o 7 -2 1 430.11 400.26 6.36 o 8 -2 1 332.88 336.21 6.90 o 9 -2 1 66.35 74.38 4.10 o 10 -2 1 81.71 78.15 4.24 o -10 -1 1 14.47 14.99 5.33 o -9 -1 1 223.32 224.31 11.49 o -8 -1 1 269.10 273.95 11.06 o -7 -1 1 472.87 433.90 12.54 o -6 -1 1 2416.99 2529.52 38.60 o -5 -1 1 907.54 909.93 15.24 o -4 -1 1 4396.15 4896.80 46.67 o -3 -1 1 1747.79 1717.89 11.54 o -1 -1 1 7409.66 7555.42 51.95 o 0 -1 1 2402.81 2523.61 36.56 o 1 -1 1 8771.34 8801.35 72.99 o 2 -1 1 3436.16 3631.12 18.04 o 3 -1 1 2762.69 2774.07 17.15 o 4 -1 1 19.62 22.35 1.18 o 5 -1 1 277.45 255.74 3.71 o 6 -1 1 1074.86 1107.44 10.38 o 7 -1 1 269.01 277.13 5.31 o 8 -1 1 326.77 341.25 5.96 o 9 -1 1 375.76 353.16 6.68 o 10 -1 1 10.48 8.56 2.15 o -10 0 1 5.73 5.77 4.55 o -9 0 1 196.74 195.97 13.50 o -8 0 1 426.45 416.52 6.42 o -7 0 1 20.66 20.54 2.14 o -6 0 1 681.67 670.51 6.48 o -5 0 1 1468.21 1423.24 15.19 o -4 0 1 972.69 1012.85 6.44 o -3 0 1 3313.57 3663.82 24.79 o -2 0 1 35773.85 34137.88 316.47 o -1 0 1 2143.48 2380.45 11.00 o 2 0 1 173.88 166.01 2.62 o 3 0 1 1180.22 1135.83 8.26 o 4 0 1 2552.71 2520.55 13.53 o 5 0 1 363.12 388.02 5.53 o 6 0 1 100.53 100.16 2.52 o 7 0 1 664.28 649.46 7.42 o 8 0 1 1.23 2.04 1.44 o 9 0 1 142.38 148.07 4.48 o 10 0 1 233.54 222.49 5.98 o -10 1 1 150.58 119.98 62.68 o -9 1 1 0.15 0.85 1.02 o -8 1 1 189.49 190.63 4.58 o -7 1 1 790.24 811.52 8.82 o -6 1 1 53.01 57.71 2.32 o -5 1 1 1606.99 1607.22 22.75 o -4 1 1 3953.10 3955.24 41.83 o -3 1 1 64.29 51.90 2.29 o -2 1 1 11944.39 11830.97 128.89 o -1 1 1 17732.32 16135.35 95.38 o 2 1 1 1362.89 1437.21 4.76 o 3 1 1 2752.72 3009.26 10.46 o 4 1 1 3604.65 3597.69 19.52 o 5 1 1 1306.54 1331.08 7.49 o 6 1 1 209.67 202.70 3.29 o 7 1 1 803.88 788.30 8.19 o 8 1 1 5.72 6.77 1.27 o 9 1 1 40.39 37.69 3.37 o 10 1 1 153.79 165.91 9.72 o 11 1 1 94.48 92.95 8.57 o -9 2 1 61.21 59.68 3.20 o -8 2 1 10.07 10.26 2.06 o -7 2 1 777.06 779.13 9.76 o -6 2 1 544.53 542.15 6.88 o -5 2 1 425.52 388.08 13.67 o -4 2 1 1357.80 1307.39 13.74 o -3 2 1 626.54 629.62 7.29 o -2 2 1 4553.42 4931.18 67.99 o -1 2 1 2524.39 2407.95 23.34 o 0 2 1 456.83 503.97 3.54 o 1 2 1 70.11 77.94 1.07 o 2 2 1 6370.24 6716.01 26.52 o 3 2 1 3123.81 3349.93 19.66 o 4 2 1 1497.89 1550.54 10.19 o 5 2 1 2465.21 2541.70 35.43 o 6 2 1 179.24 176.42 3.82 o 7 2 1 168.72 170.44 4.88 o 8 2 1 1346.81 1293.14 26.55 o 9 2 1 228.28 220.38 9.39 o 10 2 1 97.57 95.50 7.33 o 11 2 1 256.70 255.29 12.77 o -9 3 1 239.87 242.55 7.34 o -8 3 1 4.02 4.83 1.69 o -7 3 1 232.84 235.04 5.40 o -6 3 1 1000.34 1017.65 11.34 o -5 3 1 82.18 67.53 3.69 o -4 3 1 193.84 200.56 4.87 o -3 3 1 2240.79 2148.13 22.24 o -2 3 1 335.82 318.84 6.57 o -1 3 1 1.28 5.29 1.14 o 0 3 1 6192.88 6238.75 28.45 o 1 3 1 1722.85 1735.75 9.65 o 2 3 1 2225.04 2303.96 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6 11 0.99 2.39 1.39 o 2 6 11 370.88 378.09 5.98 o 3 6 11 321.32 334.62 4.57 o 4 6 11 14.76 14.32 1.06 o 5 6 11 911.86 868.39 21.89 o 6 6 11 456.71 446.91 15.55 o 7 6 11 9.96 7.39 4.37 o 8 6 11 290.45 271.68 13.82 o 0 7 11 299.69 297.30 7.52 o 1 7 11 107.73 109.25 4.96 o 2 7 11 88.68 87.32 3.68 o 3 7 11 536.97 502.56 9.42 o 4 7 11 245.56 234.36 10.36 o 5 7 11 17.15 18.97 4.84 o 6 7 11 443.38 460.07 16.48 o 7 7 11 179.08 170.39 10.73 o 8 7 11 52.41 61.89 8.03 o 0 8 11 74.78 80.25 5.11 o 1 8 11 413.60 412.77 9.67 o 2 8 11 166.30 154.99 4.94 o 3 8 11 181.65 175.25 5.02 o 4 8 11 522.97 485.59 16.09 o 5 8 11 60.19 44.28 6.38 o 6 8 11 177.79 169.73 10.50 o 7 8 11 308.63 308.98 18.52 o 8 8 11 50.59 58.02 8.03 o 9 8 11 193.75 186.89 12.95 o 2 9 11 387.50 369.94 15.65 o 3 9 11 21.43 23.81 5.09 o 4 9 11 219.83 219.20 11.22 o 5 9 11 276.42 273.58 16.60 o 6 9 11 8.49 14.31 5.50 o 7 9 11 164.23 155.40 14.95 o 8 9 11 149.23 136.84 10.92 o 3 10 11 124.88 118.10 8.84 o 4 10 11 11.68 11.08 4.80 o 5 10 11 202.83 199.47 12.17 o 6 10 11 508.81 503.88 19.63 o 7 10 11 5.89 8.16 5.50 o 2 0 12 165.50 163.89 4.93 o 3 0 12 4.51 3.82 2.44 o 4 0 12 233.66 223.81 6.94 o 5 0 12 201.44 210.40 6.61 o 1 1 12 4.76 2.77 2.02 o 2 1 12 45.20 51.24 5.37 o 3 1 12 160.40 159.30 5.59 o 4 1 12 2.83 4.00 1.69 o 5 1 12 253.18 265.71 6.96 o 6 1 12 297.04 295.16 14.19 o 0 2 12 114.85 113.39 5.67 o 1 2 12 37.90 41.40 3.58 o 2 2 12 72.22 78.69 4.10 o 3 2 12 367.40 354.56 7.30 o 4 2 12 17.63 17.25 1.97 o 5 2 12 64.84 66.01 2.77 o 6 2 12 186.85 188.89 10.71 o 7 2 12 28.53 29.60 9.00 o 0 3 12 66.84 67.07 4.52 o 1 3 12 165.72 172.38 6.51 o 2 3 12 12.03 7.44 1.62 o 3 3 12 205.22 199.29 4.25 o 4 3 12 155.92 159.54 4.11 o 5 3 12 24.49 24.14 3.52 o 6 3 12 103.37 110.59 6.15 o 7 3 12 127.36 132.58 10.09 o 8 3 12 70.97 72.95 8.92 o 0 4 12 4.64 7.05 2.12 o 1 4 12 76.88 73.56 3.36 o 2 4 12 206.76 218.19 4.91 o 3 4 12 74.01 74.45 2.73 o 4 4 12 171.19 170.29 3.98 o 5 4 12 593.22 609.39 18.47 o 6 4 12 5.57 8.28 4.59 o 7 4 12 457.78 482.69 18.41 o 8 4 12 433.49 424.24 18.45 o 0 5 12 96.13 92.76 3.76 o 1 5 12 0.21 0.16 1.07 o 2 5 12 245.79 239.58 5.19 o 3 5 12 340.37 345.77 5.66 o 4 5 12 19.42 14.01 4.33 o 5 5 12 573.71 607.54 22.20 o 6 5 12 364.28 374.62 14.58 o 7 5 12 8.18 6.76 4.55 o 1 6 12 175.46 190.78 4.78 o 2 6 12 175.94 158.74 4.36 o 3 6 12 630.17 609.72 17.42 o 4 6 12 126.34 112.78 7.97 o 5 6 12 96.17 83.08 7.54 o 6 6 12 278.22 259.51 16.33 o 7 6 12 159.66 162.52 11.06 o 1 7 12 265.21 253.72 6.39 o 2 7 12 10.29 8.57 1.72 o 3 7 12 69.23 64.18 6.43 o 4 7 12 430.82 416.97 14.64 o 5 7 12 28.07 26.86 5.48 o 6 7 12 179.52 173.09 14.01 o 7 7 12 321.68 300.45 14.46 o 2 8 12 163.93 157.07 11.33 o 3 8 12 5.99 4.28 3.44 o 4 8 12 182.65 183.94 10.22 o 5 8 12 203.35 196.77 11.04 o 6 8 12 6.71 9.08 4.92 o 7 8 12 230.97 226.04 13.24 o 4 9 12 78.59 76.25 7.93 o 5 9 12 232.02 227.81 16.06 o 6 9 12 90.75 95.46 9.17 o 3 3 13 26.73 34.40 3.85 o 3 4 13 69.30 66.67 8.49 o 4 4 13 1.82 1.73 4.28 o 5 4 13 314.07 319.79 17.30 o 6 4 13 187.79 202.36 11.80 o 3 5 13 497.87 498.03 15.67 o 4 5 13 173.07 169.75 9.78 o 5 5 13 145.22 145.96 9.66 o 4 6 13 220.50 232.18 11.43 o 5 6 13 16.42 18.93 5.23 o