#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/08/2210857.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210857_Fobs loop_ _publ_author_name 'Eey, Stanley Tze Chiang' 'Lai, Chian Sing' 'Tiekink, Edward R. T.' _publ_section_title ; Tris(O,O'-dicyclohexyl dithiophosphato-\k^2^S,S')bismuth(III) chloroform disolvate ; _journal_coeditor_code AT2126 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2878 _journal_page_last m2880 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.390 _cell_angle_gamma 90.000 _cell_length_a 17.4376 _cell_length_b 16.0715 _cell_length_c 20.6221 _exptl_crystal_F_000 2680.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file at2126Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_f_calc_maximum 561.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 52670.95 58425.72 1789.74 o 4 0 0 1103.22 1652.76 191.25 o 6 0 0 78820.09 78444.98 3528.73 o 8 0 0 2204.12 2316.99 253.63 o 10 0 0 51999.89 52102.31 1810.76 o 12 0 0 57062.34 55250.34 1523.62 o 14 0 0 2866.96 2903.54 435.12 o 16 0 0 14830.13 14936.70 1050.31 o 18 0 0 168.71 142.73 365.41 o 20 0 0 2760.96 2512.66 902.67 o 1 1 0 89114.62 102201.95 3047.34 o 2 1 0 31645.69 33674.43 853.85 o 3 1 0 28415.60 28721.33 755.40 o 4 1 0 42370.36 42418.64 1163.63 o 5 1 0 22351.76 20976.49 536.75 o 6 1 0 1539.29 1571.98 136.94 o 7 1 0 8816.81 8420.81 311.93 o 8 1 0 14086.68 13882.56 502.21 o 9 1 0 60524.70 62054.05 1292.78 o 10 1 0 14418.99 13142.51 325.78 o 11 1 0 37697.70 36030.85 960.39 o 12 1 0 348.45 201.01 170.18 o 13 1 0 3113.29 2988.56 287.72 o 14 1 0 1642.79 1691.56 264.91 o 15 1 0 14810.39 15071.60 627.71 o 16 1 0 1396.16 1913.34 319.95 o 17 1 0 1895.65 1834.10 324.61 o 18 1 0 1865.52 1529.29 397.13 o 19 1 0 599.18 854.73 510.02 o 20 1 0 942.25 -101.89 509.76 o 21 1 0 3112.59 2378.20 725.89 o 0 2 0 38841.87 42016.95 1818.82 o 1 2 0 10085.58 10329.89 286.78 o 2 2 0 276.90 176.51 47.05 o 3 2 0 160673.17 173862.64 4256.33 o 4 2 0 1545.84 1445.27 117.78 o 5 2 0 673.04 768.27 126.11 o 6 2 0 25999.07 25113.76 730.15 o 7 2 0 49749.95 47803.39 1299.06 o 8 2 0 27207.48 26897.13 715.99 o 9 2 0 50162.98 48476.68 1191.15 o 10 2 0 16465.62 15801.27 516.88 o 11 2 0 1633.70 1686.66 307.67 o 12 2 0 13537.46 13793.06 473.52 o 13 2 0 9277.07 9586.29 461.33 o 14 2 0 456.40 -38.86 210.86 o 15 2 0 1425.25 1525.13 269.52 o 16 2 0 4238.49 4383.82 391.81 o 17 2 0 6390.72 6545.24 580.63 o 18 2 0 673.53 595.78 376.39 o 19 2 0 10881.31 11074.99 811.82 o 20 2 0 597.09 823.68 408.32 o 21 2 0 886.79 1442.40 671.20 o 1 3 0 11775.96 12047.20 433.04 o 2 3 0 3737.22 3729.12 159.35 o 3 3 0 1050.76 1074.25 91.51 o 4 3 0 29658.01 30720.77 821.18 o 5 3 0 46039.48 47308.91 1243.59 o 6 3 0 176.88 313.66 96.20 o 7 3 0 13.80 28.14 145.26 o 8 3 0 48466.03 47105.07 1309.73 o 9 3 0 3058.78 3502.41 455.31 o 10 3 0 541.91 539.53 156.69 o 11 3 0 735.41 586.90 170.51 o 12 3 0 14360.60 14147.37 547.55 o 13 3 0 837.97 1076.42 202.49 o 14 3 0 18522.92 17464.21 590.45 o 15 3 0 1047.72 1739.80 351.25 o 16 3 0 61.86 -277.72 277.72 o 17 3 0 587.58 948.90 338.78 o 18 3 0 10395.40 10671.11 761.44 o 19 3 0 434.57 126.96 363.05 o 20 3 0 7089.93 7239.99 731.28 o 21 3 0 330.10 57.54 409.01 o 0 4 0 6960.18 8446.28 507.47 o 1 4 0 3715.16 4186.45 245.88 o 2 4 0 63647.58 65365.63 2031.54 o 3 4 0 54368.20 55256.98 1411.79 o 4 4 0 60882.30 63600.85 1620.84 o 5 4 0 3047.40 3199.50 240.22 o 6 4 0 39125.62 37415.26 914.46 o 7 4 0 20117.99 19906.81 621.74 o 8 4 0 323.15 418.30 123.19 o 9 4 0 28557.50 27799.15 957.53 o 10 4 0 33778.08 32743.41 1001.49 o 11 4 0 381.28 494.39 313.08 o 12 4 0 206.19 507.20 208.72 o 13 4 0 13293.60 12798.79 498.75 o 14 4 0 649.87 1097.77 250.83 o 15 4 0 12497.07 12758.59 638.56 o 16 4 0 11209.05 10687.92 712.60 o 17 4 0 301.33 322.06 318.53 o 18 4 0 3126.30 3588.10 501.43 o 19 4 0 3242.21 3323.92 914.71 o 20 4 0 3706.84 3653.27 558.92 o 21 4 0 917.93 340.90 445.81 o 1 5 0 31655.09 32008.07 1067.36 o 2 5 0 6766.05 6521.03 579.89 o 3 5 0 4156.87 4228.36 188.55 o 4 5 0 28.34 -5.80 99.72 o 5 5 0 141331.48 142287.69 3539.55 o 6 5 0 1153.36 1289.67 98.59 o 7 5 0 21090.10 19668.79 554.70 o 8 5 0 1320.84 1928.54 238.77 o 9 5 0 10209.00 10040.35 519.25 o 10 5 0 4379.29 4573.47 295.76 o 11 5 0 37702.80 38141.82 1592.93 o 12 5 0 52.03 -31.21 222.73 o 13 5 0 84.60 351.81 279.15 o 14 5 0 3994.81 4412.13 384.99 o 15 5 0 8186.61 8460.38 533.67 o 16 5 0 72.99 344.19 271.03 o 17 5 0 10474.37 10715.93 583.93 o 18 5 0 391.37 453.41 376.85 o 19 5 0 134.39 -349.55 349.55 o 20 5 0 130.77 249.00 495.18 o 21 5 0 6051.67 6136.05 820.70 o 0 6 0 108286.57 121988.84 5286.92 o 1 6 0 98.95 -17.99 110.22 o 2 6 0 17062.01 16605.13 643.38 o 3 6 0 1320.00 1489.39 351.98 o 4 6 0 88220.66 90584.88 2842.08 o 5 6 0 23.00 285.55 84.21 o 6 6 0 70517.84 68243.10 1782.11 o 7 6 0 6449.26 5722.12 217.68 o 8 6 0 1910.56 1990.79 149.31 o 9 6 0 3354.14 3339.52 227.76 o 10 6 0 46909.04 44309.26 1504.75 o 11 6 0 1278.49 1164.16 353.08 o 12 6 0 10232.99 10259.87 748.48 o 13 6 0 2356.97 2554.62 473.62 o 14 6 0 156.79 213.96 287.92 o 15 6 0 18.88 98.61 244.35 o 16 6 0 10066.71 10602.80 703.79 o 17 6 0 695.97 542.64 289.64 o 18 6 0 1389.66 1140.03 345.68 o 19 6 0 1511.20 390.91 501.43 o 20 6 0 1671.17 2118.93 774.12 o 1 7 0 4765.15 4800.23 732.58 o 2 7 0 19165.11 18583.25 723.49 o 3 7 0 1928.80 1993.22 239.62 o 4 7 0 6073.00 5533.42 367.43 o 5 7 0 9299.07 9108.83 581.57 o 6 7 0 3752.84 3052.22 172.95 o 7 7 0 436.30 688.57 211.17 o 8 7 0 7604.21 7271.78 314.22 o 9 7 0 6413.49 6513.90 527.92 o 10 7 0 6269.78 6710.20 767.38 o 11 7 0 9362.67 9467.08 1999.02 o 12 7 0 11009.29 10570.45 766.42 o 13 7 0 25.01 -156.63 329.83 o 14 7 0 12215.47 11850.54 858.35 o 15 7 0 4683.59 5422.70 453.27 o 16 7 0 349.96 548.23 283.62 o 17 7 0 3619.04 4488.10 604.94 o 18 7 0 3417.94 3998.56 657.61 o 19 7 0 1.79 -180.40 300.43 o 20 7 0 231.39 388.12 527.75 o 0 8 0 4585.81 4712.09 483.90 o 1 8 0 11237.12 10224.42 497.12 o 2 8 0 15073.32 15395.82 651.92 o 3 8 0 28063.73 28081.61 1066.03 o 4 8 0 99.28 37.02 162.80 o 5 8 0 43.75 -91.65 158.61 o 6 8 0 4484.13 3901.90 403.06 o 7 8 0 26371.90 22382.48 1416.32 o 8 8 0 3.92 -116.62 182.30 o 9 8 0 6916.87 6688.81 537.82 o 10 8 0 1610.36 1415.30 576.52 o 11 8 0 252.53 320.37 312.55 o 12 8 0 363.06 -316.39 317.36 o 13 8 0 19402.10 18629.21 1071.32 o 14 8 0 128.19 143.02 361.60 o 15 8 0 1942.92 2192.45 344.35 o 16 8 0 199.80 334.31 283.82 o 17 8 0 2929.99 3159.53 435.60 o 18 8 0 827.90 933.56 488.42 o 19 8 0 8774.88 9251.99 676.00 o 20 8 0 5.13 173.71 416.45 o 1 9 0 307.43 644.40 195.28 o 2 9 0 11099.38 10857.11 582.13 o 3 9 0 12838.43 13053.32 842.05 o 4 9 0 7331.10 8237.58 607.96 o 5 9 0 21807.63 22252.95 1184.48 o 6 9 0 9535.46 9546.13 566.35 o 7 9 0 278.96 -65.01 215.42 o 8 9 0 24301.00 22015.23 757.71 o 9 9 0 663.50 718.75 313.80 o 10 9 0 18154.60 15181.29 824.67 o 11 9 0 15381.46 13763.71 854.96 o 12 9 0 1713.46 2970.42 594.48 o 13 9 0 5.60 -278.02 520.38 o 14 9 0 1686.06 1549.79 453.90 o 15 9 0 9026.71 8666.91 893.79 o 16 9 0 43.79 246.67 268.15 o 17 9 0 1097.43 806.98 323.95 o 18 9 0 7652.86 8286.21 789.84 o 19 9 0 189.69 -127.72 324.68 o 0 10 0 65488.52 65010.41 3065.05 o 1 10 0 3780.38 4120.06 379.03 o 2 10 0 7633.44 8702.21 521.37 o 3 10 0 10919.19 10363.89 566.23 o 4 10 0 17572.08 16118.57 747.60 o 5 10 0 2472.32 3099.15 363.14 o 6 10 0 15499.43 14704.16 1297.87 o 7 10 0 2586.21 2640.00 374.85 o 8 10 0 1575.44 1663.40 236.60 o 9 10 0 6716.31 6164.14 558.24 o 10 10 0 18997.40 17269.79 2270.72 o 11 10 0 5280.70 4855.37 1318.08 o 12 10 0 12723.48 11745.70 848.78 o 13 10 0 52.53 -302.87 302.87 o 14 10 0 2113.15 2382.78 502.61 o 15 10 0 858.30 1099.26 445.26 o 16 10 0 7017.56 6972.77 626.01 o 17 10 0 163.47 681.54 316.79 o 18 10 0 1193.21 1728.58 398.03 o 19 10 0 3244.52 3171.58 481.82 o 1 11 0 65053.32 63672.38 2157.69 o 2 11 0 42.04 -47.97 206.72 o 3 11 0 3596.60 3552.32 377.89 o 4 11 0 125.09 544.38 250.97 o 5 11 0 18751.74 19199.21 879.18 o 6 11 0 3236.01 3322.16 404.10 o 7 11 0 13667.36 14237.71 769.48 o 8 11 0 6982.79 7875.49 1027.86 o 9 11 0 8700.91 8361.38 652.58 o 10 11 0 4204.02 4036.60 506.41 o 11 11 0 14271.74 13576.08 1180.55 o 12 11 0 1629.21 1648.75 426.58 o 13 11 0 186.97 -106.99 366.06 o 14 11 0 1826.67 2175.00 497.12 o 15 11 0 2699.17 2867.66 437.07 o 16 11 0 223.83 953.73 512.18 o 17 11 0 3399.67 3705.94 447.08 o 18 11 0 45.06 448.12 540.12 o 0 12 0 29665.43 30376.52 1700.93 o 1 12 0 696.90 531.03 253.05 o 2 12 0 5130.01 4971.18 462.70 o 3 12 0 21072.18 20874.26 1608.87 o 4 12 0 7629.57 7631.65 773.00 o 5 12 0 985.13 1464.72 343.43 o 6 12 0 3695.25 3892.43 474.91 o 7 12 0 2259.55 977.14 340.48 o 8 12 0 300.21 53.34 289.10 o 9 12 0 6146.15 5838.68 577.50 o 10 12 0 5707.46 5978.28 599.76 o 11 12 0 910.99 881.57 366.76 o 12 12 0 5581.02 4437.02 599.61 o 13 12 0 734.17 304.59 527.68 o 14 12 0 190.54 131.29 402.67 o 15 12 0 2280.20 2726.64 871.53 o 16 12 0 2793.06 3156.27 485.43 o 17 12 0 1003.32 724.06 393.79 o 1 13 0 1046.04 922.49 334.57 o 2 13 0 11786.17 11432.12 686.82 o 3 13 0 991.84 978.77 309.54 o 4 13 0 13873.91 14102.99 792.87 o 5 13 0 99.78 -254.01 254.01 o 6 13 0 2202.87 2038.78 369.49 o 7 13 0 524.16 37.65 272.37 o 8 13 0 12554.54 13161.86 829.51 o 9 13 0 103.09 110.97 297.68 o 10 13 0 936.48 1403.53 396.44 o 11 13 0 1777.00 1920.98 528.24 o 12 13 0 2595.22 2566.91 738.75 o 13 13 0 845.39 403.24 491.19 o 14 13 0 5730.33 4524.91 677.62 o 15 13 0 256.65 305.24 366.56 o 16 13 0 196.60 322.76 472.23 o 17 13 0 80.05 -216.49 373.64 o 0 14 0 4751.99 3875.66 643.32 o 1 14 0 4795.96 4543.41 486.26 o 2 14 0 509.73 151.19 272.71 o 3 14 0 13281.11 12779.57 768.65 o 4 14 0 558.43 554.59 308.77 o 5 14 0 575.36 504.29 449.65 o 6 14 0 5455.27 4833.72 521.28 o 7 14 0 3211.86 3588.57 475.67 o 8 14 0 623.40 292.45 322.62 o 9 14 0 6452.05 7078.17 672.67 o 10 14 0 915.56 1297.98 409.90 o 11 14 0 927.97 873.34 400.72 o 12 14 0 23.22 -294.82 362.60 o 13 14 0 5116.58 4356.81 958.81 o 14 14 0 592.45 641.18 447.70 o 15 14 0 3801.21 4107.27 788.94 o 16 14 0 1052.80 427.38 737.70 o 1 15 0 9933.65 8603.91 819.59 o 2 15 0 2256.01 2456.25 400.58 o 3 15 0 1416.88 1143.91 340.20 o 4 15 0 4610.60 5391.52 550.34 o 5 15 0 9941.14 9606.27 1018.31 o 6 15 0 9.12 111.55 295.80 o 7 15 0 2947.80 3115.87 482.82 o 8 15 0 4734.21 5191.48 607.17 o 9 15 0 2825.03 2812.77 480.11 o 10 15 0 329.19 463.23 384.92 o 11 15 0 3923.81 4377.59 607.86 o 12 15 0 558.65 1173.42 465.67 o 13 15 0 88.58 -15.85 427.35 o 14 15 0 2560.47 3429.87 522.27 o 15 15 0 5679.35 5885.30 845.76 o 0 16 0 10330.01 10814.11 1066.59 o 1 16 0 1714.17 1812.80 487.26 o 2 16 0 324.37 115.14 295.30 o 3 16 0 17.77 326.05 307.61 o 4 16 0 5476.36 5078.28 751.67 o 5 16 0 58.86 -214.15 311.80 o 6 16 0 19176.20 18175.61 2270.16 o 7 16 0 13.60 432.56 340.09 o 8 16 0 42.78 142.60 418.22 o 9 16 0 437.22 793.25 391.56 o 10 16 0 4476.18 4453.20 619.39 o 11 16 0 36.98 -320.19 320.19 o 12 16 0 2808.16 3579.29 967.23 o 13 16 0 503.21 1173.04 504.25 o 14 16 0 825.06 837.88 548.12 o 1 17 0 2168.58 1737.87 408.11 o 2 17 0 4215.79 3644.92 510.67 o 3 17 0 312.24 359.87 341.83 o 4 17 0 855.43 599.63 422.71 o 5 17 0 4819.62 5208.30 1041.89 o 6 17 0 68.76 43.29 329.79 o 7 17 0 4358.42 5030.87 613.51 o 8 17 0 1015.60 1103.01 433.76 o 9 17 0 1877.77 1828.61 483.30 o 10 17 0 280.48 16.04 510.84 o 11 17 0 2822.59 2255.08 558.64 o 12 17 0 873.63 942.21 565.85 o 0 18 0 917.84 864.50 517.58 o 1 18 0 2783.19 3557.74 529.61 o 2 18 0 249.78 -244.14 336.26 o 3 18 0 3343.44 3429.60 520.48 o 4 18 0 24.99 -116.41 339.06 o 5 18 0 768.78 1193.48 409.22 o 6 18 0 1671.03 1466.55 462.26 o 7 18 0 3420.13 3419.44 558.02 o 8 18 0 580.59 259.04 378.18 o 9 18 0 1693.14 1659.63 501.26 o 10 18 0 275.95 1312.95 489.33 o 11 18 0 473.32 16.18 428.18 o 1 19 0 64.78 162.13 362.36 o 2 19 0 3887.82 4579.54 584.22 o 3 19 0 43.54 359.55 467.05 o 4 19 0 849.58 777.99 532.73 o 5 19 0 1303.18 1324.22 439.90 o 6 19 0 804.03 567.32 410.02 o 7 19 0 343.61 425.14 399.69 o 8 19 0 2758.96 2611.58 719.11 o 9 19 0 29.52 220.18 402.87 o 0 20 0 161.56 1565.08 616.38 o 1 20 0 1778.18 1780.70 470.77 o 2 20 0 42.48 581.75 399.35 o 3 20 0 664.01 1650.70 460.42 o 4 20 0 4669.57 4143.33 600.29 o 5 20 0 26.31 -373.84 373.84 o 6 20 0 842.75 1003.74 1063.78 o -21 0 1 164.12 -726.40 726.40 o -19 0 1 2124.34 1753.70 864.50 o -17 0 1 11404.53 10101.50 802.52 o -15 0 1 6767.48 7563.32 854.96 o -13 0 1 15514.03 13859.59 776.33 o -11 0 1 18715.42 19568.71 630.31 o -9 0 1 6377.29 5815.13 380.60 o -7 0 1 12296.36 11997.24 564.44 o -5 0 1 668.94 945.35 325.03 o -3 0 1 4919.90 5509.74 192.32 o -1 0 1 181803.19 182642.50 4458.63 o 1 0 1 14425.25 15557.89 513.09 o 3 0 1 824.84 1193.03 113.79 o 5 0 1 30637.54 32215.87 1074.99 o 7 0 1 4013.57 4751.88 315.55 o 9 0 1 3474.28 3956.22 343.68 o 11 0 1 46945.77 45989.05 1662.67 o 13 0 1 3834.42 3988.12 462.62 o 15 0 1 9358.14 8628.74 693.27 o 17 0 1 705.61 394.29 385.63 o 19 0 1 5870.21 6171.63 1144.06 o 21 0 1 1584.63 1023.93 972.28 o -22 1 1 1154.89 254.91 676.94 o -21 1 1 1298.98 2166.34 682.21 o -20 1 1 23.33 -465.39 465.39 o -19 1 1 2691.00 2868.08 475.17 o -18 1 1 7301.93 6618.07 605.99 o -17 1 1 854.91 640.31 254.12 o -16 1 1 8714.29 8148.88 493.17 o -15 1 1 3978.13 3466.63 346.64 o -14 1 1 193.03 335.32 245.13 o -13 1 1 153.74 272.02 181.81 o -12 1 1 36653.41 34480.11 974.74 o -11 1 1 9265.17 8718.44 366.58 o -10 1 1 468.46 773.57 142.36 o -9 1 1 22868.74 21388.09 518.95 o -8 1 1 8106.53 7781.98 279.62 o -7 1 1 9212.44 9605.92 382.40 o -6 1 1 2642.78 2741.08 212.59 o -5 1 1 10769.57 10376.64 473.78 o -4 1 1 12008.37 12458.11 383.58 o -3 1 1 40704.50 42042.25 1547.68 o -2 1 1 9131.73 8329.01 499.05 o -1 1 1 1953.27 1845.92 127.78 o 0 1 1 91302.12 101787.63 1927.29 o 1 1 1 84825.85 91407.49 1735.22 o 2 1 1 2694.96 2882.21 111.95 o 3 1 1 221432.28 237265.28 5784.11 o 4 1 1 8262.76 8325.00 259.09 o 5 1 1 2333.81 2471.33 130.60 o 6 1 1 429.27 648.68 162.61 o 7 1 1 6629.94 6437.60 236.64 o 8 1 1 33443.39 34572.70 781.76 o 9 1 1 5230.69 5216.46 273.73 o 10 1 1 18112.97 17610.01 561.19 o 11 1 1 145.57 108.45 146.39 o 12 1 1 8802.88 8836.31 421.71 o 13 1 1 5787.64 5671.82 374.07 o 14 1 1 3948.29 4049.23 348.22 o 15 1 1 3550.11 3478.66 342.29 o 16 1 1 4163.65 5400.38 745.29 o 17 1 1 2317.38 2132.55 329.42 o 18 1 1 2029.22 2609.95 594.79 o 19 1 1 239.88 -238.69 347.84 o 20 1 1 5144.60 4224.54 759.57 o 21 1 1 193.91 631.07 621.43 o -21 2 1 345.50 934.80 626.87 o -20 2 1 7966.38 8997.14 753.86 o -19 2 1 906.91 950.91 396.48 o -18 2 1 5332.71 5498.97 655.45 o -17 2 1 2361.60 3066.85 440.29 o -16 2 1 1417.09 1353.56 397.05 o -15 2 1 1063.06 700.20 237.34 o -14 2 1 8968.39 8923.37 465.36 o -13 2 1 295.58 50.00 184.89 o -12 2 1 229.83 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