#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:17:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181028 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/08/2210866.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210866_Fobs loop_ _publ_author_name 'Meijboom, Reinout' 'Janse van Rensburg, J. Marthinus' 'Senekal, Nadine D.' 'Venter, Jacobus S.' _publ_section_title ; (p-Toluenesulfonato)tris(triphenylarsine)silver(I) ; _journal_coeditor_code BG2008 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3056 _journal_page_last m3058 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 87.473 _cell_angle_beta 81.202 _cell_angle_gamma 85.870 _cell_length_a 13.1327 _cell_length_b 13.8625 _cell_length_c 14.3603 _exptl_crystal_F_000 1208.00 _reflns_d_resolution_high 0.7493 _cod_data_source_file bg2008Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6frm26_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 368.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26024.78 25663.53 320.04 o 3 0 0 9785.18 10174.06 148.47 o 4 0 0 3050.19 3059.59 77.90 o 5 0 0 363.65 416.68 16.77 o 6 0 0 940.20 855.10 45.45 o 7 0 0 3112.43 3427.67 75.51 o 8 0 0 8371.74 8085.38 153.02 o 9 0 0 835.69 820.77 90.14 o 10 0 0 2582.10 2635.66 71.16 o 11 0 0 531.65 565.13 35.71 o 12 0 0 5552.50 5492.27 124.36 o 13 0 0 360.19 378.49 35.40 o 14 0 0 712.39 640.66 45.10 o 15 0 0 1056.75 1027.55 69.03 o 16 0 0 1904.09 2052.85 97.65 o 17 0 0 1094.44 1219.49 200.81 o -17 1 0 1063.92 1144.44 234.21 o -16 1 0 3012.87 3102.38 120.92 o -15 1 0 11.13 47.57 37.83 o -14 1 0 2862.51 2832.11 158.26 o -13 1 0 7.27 6.67 23.65 o -12 1 0 367.14 393.98 33.92 o -11 1 0 1276.68 1213.52 49.71 o -10 1 0 853.73 825.30 41.94 o -9 1 0 3054.30 3000.37 73.94 o -8 1 0 2001.77 1913.71 53.47 o -7 1 0 340.79 284.07 20.70 o -6 1 0 5369.73 5270.08 101.80 o -5 1 0 1767.90 1949.83 35.68 o -4 1 0 8194.92 8439.02 113.00 o -3 1 0 1117.10 1070.11 18.62 o -2 1 0 114.60 116.99 6.09 o -1 1 0 23975.67 24011.07 391.91 o 0 1 0 5845.09 -1.66 0.83 o 1 1 0 51112.66 46191.58 835.85 o 2 1 0 15766.03 15910.67 183.63 o 3 1 0 123236.91 113556.81 1797.58 o 4 1 0 32429.81 32401.51 508.70 o 5 1 0 4533.95 5002.92 196.55 o 6 1 0 17563.97 18072.02 305.26 o 7 1 0 1393.73 1485.66 44.03 o 8 1 0 112.60 104.77 17.50 o 9 1 0 3474.14 3443.94 82.00 o 10 1 0 68.10 40.69 32.68 o 11 1 0 4814.41 4690.75 108.66 o 12 1 0 1923.58 2079.16 67.60 o 13 1 0 1308.81 1279.44 96.79 o 14 1 0 836.25 811.04 48.18 o 15 1 0 200.32 195.77 44.51 o 16 1 0 236.57 289.04 61.10 o 17 1 0 1733.86 1810.17 96.19 o -17 2 0 1945.76 2411.94 160.38 o -16 2 0 209.37 258.50 50.31 o -15 2 0 1456.56 1496.67 80.88 o -14 2 0 2237.37 2197.37 91.83 o -13 2 0 1042.64 995.39 71.11 o -12 2 0 958.11 971.62 47.88 o -11 2 0 55.05 41.25 21.22 o -10 2 0 2467.03 2363.01 65.67 o -9 2 0 378.81 404.37 27.04 o -8 2 0 1565.44 1597.50 40.71 o -7 2 0 518.78 578.22 33.42 o -6 2 0 560.54 633.34 27.89 o -5 2 0 2877.87 2896.23 46.29 o -4 2 0 892.42 860.16 17.95 o -3 2 0 559.89 579.50 11.85 o -2 2 0 9.82 0.67 2.99 o -1 2 0 3907.95 3934.80 39.23 o 0 2 0 12914.36 13315.76 137.80 o 1 2 0 1711.84 1687.14 20.75 o 2 2 0 503.81 518.02 9.78 o 3 2 0 37636.54 36927.04 459.69 o 4 2 0 15649.86 16587.46 227.18 o 5 2 0 48068.32 49353.80 797.53 o 6 2 0 6990.46 7131.76 257.93 o 7 2 0 5956.92 5817.78 114.52 o 8 2 0 2020.79 1958.81 54.97 o 9 2 0 650.18 719.93 34.42 o 10 2 0 377.93 378.44 38.68 o 11 2 0 288.43 267.19 49.67 o 12 2 0 2990.82 3026.02 84.42 o 13 2 0 155.78 161.05 30.03 o 14 2 0 19.67 4.12 26.48 o 15 2 0 2250.32 2199.02 79.81 o 16 2 0 37.26 29.14 40.65 o 17 2 0 160.50 146.78 48.97 o -16 3 0 401.55 293.06 74.23 o -15 3 0 211.28 226.93 44.62 o -14 3 0 179.79 169.84 58.59 o -13 3 0 609.30 611.84 49.63 o -12 3 0 6.27 23.11 28.19 o -11 3 0 944.63 1030.22 91.46 o -10 3 0 602.93 583.50 43.32 o -9 3 0 44.18 26.57 16.64 o -8 3 0 63.10 65.65 13.65 o -7 3 0 931.39 961.40 26.56 o -6 3 0 477.47 514.26 16.29 o -5 3 0 4996.00 5598.61 73.20 o -4 3 0 140.51 183.15 8.04 o -3 3 0 63.03 64.07 5.61 o -2 3 0 3553.30 3777.62 40.59 o -1 3 0 533.90 506.47 15.02 o 0 3 0 914.02 917.23 12.82 o 1 3 0 11762.44 12412.20 123.70 o 2 3 0 3030.61 3258.09 41.41 o 3 3 0 202.01 203.74 8.05 o 4 3 0 15967.24 15931.62 186.56 o 5 3 0 249.65 293.79 12.34 o 6 3 0 3009.41 3220.99 123.97 o 7 3 0 2479.78 2252.78 57.34 o 8 3 0 1978.72 2242.26 59.52 o 9 3 0 3662.07 3777.61 87.49 o 10 3 0 860.13 747.86 39.45 o 11 3 0 23.28 7.04 20.17 o 12 3 0 183.85 205.13 31.20 o 13 3 0 351.86 380.65 36.26 o 14 3 0 7.03 -17.60 25.14 o 15 3 0 478.62 401.65 41.53 o 16 3 0 125.04 183.91 38.80 o 17 3 0 61.18 72.77 63.62 o -16 4 0 3150.97 3431.35 188.22 o -15 4 0 2500.80 2393.51 149.25 o -14 4 0 0.80 -1.87 33.80 o -13 4 0 5695.27 5715.95 354.89 o -12 4 0 102.61 109.21 31.75 o -11 4 0 733.68 718.10 95.96 o -10 4 0 37.46 44.60 18.54 o -9 4 0 163.27 156.48 20.86 o -8 4 0 5567.23 5382.19 116.35 o -7 4 0 9.56 15.94 9.99 o -6 4 0 4715.81 4942.24 91.01 o -5 4 0 454.06 370.95 11.96 o -4 4 0 11959.50 12208.73 144.91 o -3 4 0 801.22 823.19 14.76 o -2 4 0 946.77 933.18 15.61 o -1 4 0 5.81 28.67 5.77 o 0 4 0 25538.94 26447.51 248.69 o 1 4 0 2287.59 2351.55 28.16 o 2 4 0 25543.46 26181.54 326.05 o 3 4 0 270.38 195.00 8.19 o 4 4 0 8054.01 7930.07 107.21 o 5 4 0 10088.69 10184.26 136.90 o 6 4 0 792.86 850.08 34.70 o 7 4 0 4809.31 4683.81 80.59 o 8 4 0 495.53 464.97 20.85 o 9 4 0 976.86 1034.66 31.93 o 10 4 0 950.34 1003.29 32.36 o 11 4 0 40.24 67.32 15.25 o 12 4 0 552.41 632.76 41.12 o 13 4 0 826.96 677.40 44.07 o 14 4 0 1612.04 1739.45 90.49 o 15 4 0 556.80 552.50 46.27 o 16 4 0 1618.92 1666.13 89.80 o 17 4 0 58.06 -6.49 58.32 o -16 5 0 2489.68 2371.77 160.12 o -15 5 0 539.50 402.94 78.20 o -14 5 0 8253.77 7743.19 298.76 o -13 5 0 1565.61 1601.53 76.77 o -12 5 0 4968.64 5047.75 142.62 o -11 5 0 67.29 89.22 29.09 o -10 5 0 1033.23 1126.71 56.05 o -9 5 0 81.83 70.98 17.37 o -8 5 0 433.03 394.04 22.61 o -7 5 0 2831.77 2727.56 49.18 o -6 5 0 5123.29 5127.35 112.61 o -5 5 0 4228.00 3995.30 73.97 o -4 5 0 17112.96 17529.25 189.98 o -3 5 0 2218.50 2196.75 29.71 o -2 5 0 6740.04 6712.99 90.39 o -1 5 0 706.56 684.75 13.26 o 0 5 0 25467.71 26334.90 302.01 o 1 5 0 497.78 444.45 11.51 o 2 5 0 11622.20 12073.71 130.16 o 3 5 0 7565.74 7749.21 103.10 o 4 5 0 19991.52 19809.41 253.40 o 5 5 0 10655.24 11101.91 157.85 o 6 5 0 19587.63 19376.17 252.05 o 7 5 0 8.67 15.22 10.43 o 8 5 0 6175.65 6271.52 105.11 o 9 5 0 1735.52 1829.59 44.59 o 10 5 0 518.60 483.29 32.74 o 11 5 0 2.01 -5.23 13.36 o 12 5 0 100.46 88.97 26.72 o 13 5 0 934.57 1001.72 51.48 o 14 5 0 531.25 530.88 53.98 o 15 5 0 949.93 1308.48 80.40 o 16 5 0 2870.97 3389.75 129.95 o -15 6 0 3837.03 4355.85 209.02 o -14 6 0 1574.95 1576.23 119.16 o -13 6 0 4538.19 4414.83 199.35 o -12 6 0 2010.01 2144.19 128.04 o -11 6 0 1758.00 1624.28 69.77 o -10 6 0 12104.33 11829.63 265.96 o -9 6 0 1194.94 1079.75 83.77 o -8 6 0 922.23 933.07 31.81 o -7 6 0 327.41 395.24 21.91 o -6 6 0 375.25 396.45 28.73 o -5 6 0 8300.66 8199.23 149.78 o -4 6 0 442.53 425.81 11.98 o -3 6 0 22577.04 23099.74 295.84 o -2 6 0 6590.49 7254.99 88.33 o -1 6 0 24719.27 24866.86 316.00 o 0 6 0 4279.63 4748.66 59.38 o 1 6 0 5227.97 5088.99 61.89 o 2 6 0 2606.85 2685.90 33.64 o 3 6 0 24648.91 25037.52 353.26 o 4 6 0 170.81 210.68 11.36 o 5 6 0 41411.72 42950.49 539.97 o 6 6 0 146.87 149.25 12.33 o 7 6 0 20797.63 20327.79 296.59 o 8 6 0 4382.25 4174.29 77.02 o 9 6 0 6039.70 6124.27 105.84 o 10 6 0 4148.55 4078.87 79.29 o 11 6 0 1249.86 1256.17 39.25 o 12 6 0 78.87 116.66 27.06 o 13 6 0 1.15 -2.99 30.36 o 14 6 0 18.79 37.24 35.32 o 15 6 0 1391.97 1406.56 82.34 o 16 6 0 151.98 133.02 48.07 o -15 7 0 223.69 341.97 78.60 o -14 7 0 774.02 804.82 89.47 o -13 7 0 2376.45 2256.72 136.92 o -12 7 0 1776.94 1804.48 118.36 o -11 7 0 3970.66 3976.37 173.90 o -10 7 0 140.44 152.06 73.17 o -9 7 0 13238.11 12865.81 356.02 o -8 7 0 363.75 380.11 30.02 o -7 7 0 352.92 371.65 17.63 o -6 7 0 419.98 426.52 16.07 o -5 7 0 63.82 80.61 9.70 o -4 7 0 0.05 15.72 6.48 o -3 7 0 410.28 460.25 12.34 o -2 7 0 2663.49 2453.74 39.16 o -1 7 0 7212.04 7443.38 100.57 o 0 7 0 20878.93 21536.73 251.96 o 1 7 0 8800.34 8945.17 105.46 o 2 7 0 1069.71 994.83 20.72 o 3 7 0 12947.21 13617.03 160.65 o 4 7 0 1505.70 1386.45 31.64 o 5 7 0 4298.53 4572.80 76.59 o 6 7 0 5224.13 5340.15 81.13 o 7 7 0 5198.94 5121.40 89.00 o 8 7 0 4768.10 5081.35 90.32 o 9 7 0 10252.26 10305.54 164.41 o 10 7 0 710.47 707.54 35.70 o 11 7 0 5836.75 5908.59 161.40 o 12 7 0 16.38 9.03 42.61 o 13 7 0 672.28 699.30 57.12 o 14 7 0 11.99 41.04 39.18 o 15 7 0 19.88 48.02 41.59 o 16 7 0 681.80 677.65 68.44 o -15 8 0 60.66 -18.69 61.63 o -14 8 0 188.25 256.61 69.19 o -13 8 0 493.69 455.96 72.10 o -12 8 0 388.25 460.60 68.26 o -11 8 0 83.71 152.96 50.63 o -10 8 0 2961.91 2737.34 134.14 o -9 8 0 761.73 782.95 66.41 o -8 8 0 394.96 412.98 31.07 o -7 8 0 7572.79 7459.74 120.00 o -6 8 0 372.25 354.48 16.02 o -5 8 0 707.70 672.01 31.37 o -4 8 0 2693.28 2821.25 41.79 o -3 8 0 160.18 179.59 10.76 o -2 8 0 812.52 859.92 19.87 o -1 8 0 2005.62 1835.49 31.65 o 0 8 0 30.67 39.06 6.65 o 1 8 0 9.61 24.08 7.63 o 2 8 0 11496.32 11833.24 153.49 o 3 8 0 2158.40 2338.03 46.18 o 4 8 0 802.69 809.42 23.98 o 5 8 0 3.48 12.79 9.21 o 6 8 0 1693.83 1670.53 36.08 o 7 8 0 2881.97 2767.39 85.40 o 8 8 0 3573.95 3427.64 68.19 o 9 8 0 15.04 14.12 14.38 o 10 8 0 5761.03 5874.84 155.27 o 11 8 0 86.51 48.20 29.68 o 12 8 0 1958.18 1858.69 84.26 o 13 8 0 3871.70 4008.89 328.25 o 14 8 0 52.50 95.90 40.43 o 15 8 0 322.73 339.74 53.34 o 16 8 0 245.28 242.53 53.70 o -14 9 0 498.92 598.44 86.02 o -13 9 0 265.71 262.18 64.28 o -12 9 0 2667.20 2508.03 140.50 o -11 9 0 4.45 -14.05 43.21 o -10 9 0 761.90 722.51 70.78 o -9 9 0 578.55 532.97 58.85 o -8 9 0 984.78 900.75 56.73 o -7 9 0 261.18 287.87 29.47 o -6 9 0 1432.32 1439.90 30.15 o -5 9 0 2562.84 2583.85 48.94 o -4 9 0 23.84 32.04 9.76 o -3 9 0 4759.36 4733.14 71.21 o -2 9 0 2371.85 2439.13 41.01 o -1 9 0 931.92 976.56 21.84 o 0 9 0 15194.80 15530.63 203.87 o 1 9 0 609.03 626.87 19.76 o 2 9 0 2024.64 1910.28 28.43 o 3 9 0 1989.81 2061.81 42.55 o 4 9 0 5.31 14.46 9.15 o 5 9 0 618.79 656.65 20.76 o 6 9 0 665.36 695.46 36.91 o 7 9 0 101.59 117.35 19.64 o 8 9 0 1282.39 1296.62 45.54 o 9 9 0 95.24 88.22 20.81 o 10 9 0 524.03 487.49 31.96 o 11 9 0 1035.63 959.53 59.43 o 12 9 0 112.82 122.58 37.29 o 13 9 0 182.97 158.96 41.47 o 14 9 0 831.66 698.86 63.38 o 15 9 0 18.19 -4.08 39.30 o -13 10 0 2443.07 2291.58 142.09 o -12 10 0 812.59 594.07 76.35 o -11 10 0 1912.92 1688.50 110.94 o -10 10 0 4407.31 4225.82 177.88 o -9 10 0 1263.09 1233.07 85.49 o -8 10 0 2392.45 2317.30 69.31 o -7 10 0 29.38 45.86 20.84 o -6 10 0 147.24 165.14 22.45 o -5 10 0 31.50 -0.55 13.23 o -4 10 0 181.16 161.54 14.32 o -3 10 0 36.52 44.68 10.35 o -2 10 0 728.82 758.45 20.69 o -1 10 0 17983.01 18196.90 237.79 o 0 10 0 124.69 177.07 11.86 o 1 10 0 11730.45 12043.83 209.57 o 2 10 0 4949.32 4907.54 81.24 o 3 10 0 8654.12 8578.79 116.84 o 4 10 0 3662.81 3755.23 69.05 o 5 10 0 1454.12 1497.93 37.48 o 6 10 0 2564.93 2580.26 54.37 o 7 10 0 851.67 813.77 38.10 o 8 10 0 63.54 92.98 20.37 o 9 10 0 118.29 126.19 48.58 o 10 10 0 887.21 927.50 43.15 o 11 10 0 1774.22 1843.44 133.67 o 12 10 0 1501.63 1434.21 76.65 o 13 10 0 864.21 848.78 64.41 o 14 10 0 727.07 662.67 64.08 o 15 10 0 22.09 85.89 43.76 o -13 11 0 4113.60 4146.03 197.36 o -12 11 0 6.90 9.68 52.75 o -11 11 0 1732.25 1709.18 114.78 o -10 11 0 79.27 59.75 36.15 o -9 11 0 5381.01 5058.46 149.08 o -8 11 0 18.27 8.80 22.89 o -7 11 0 5075.47 4807.39 109.72 o -6 11 0 1303.40 1234.26 47.58 o -5 11 0 741.74 740.08 30.53 o -4 11 0 3615.75 3656.28 70.68 o -3 11 0 1240.99 1260.82 29.56 o -2 11 0 98.49 97.35 11.68 o -1 11 0 2216.73 2267.05 40.84 o 0 11 0 4174.97 4219.26 84.57 o 1 11 0 3854.64 3879.55 80.05 o 2 11 0 4359.04 4309.09 82.96 o 3 11 0 11967.76 11988.12 181.56 o 4 11 0 2559.77 2524.80 45.08 o 5 11 0 13760.49 13885.06 207.35 o 6 11 0 963.33 993.83 32.96 o 7 11 0 4885.33 5008.71 107.80 o 8 11 0 60.74 73.04 22.05 o 9 11 0 1538.50 1568.40 58.98 o 10 11 0 2.29 17.38 22.82 o 11 11 0 2557.60 2692.50 102.56 o 12 11 0 643.53 617.13 70.32 o 13 11 0 1037.01 1081.06 70.69 o 14 11 0 188.73 140.97 72.83 o -12 12 0 1349.08 1392.96 83.35 o -11 12 0 1067.38 1054.97 70.73 o -10 12 0 1566.11 1651.75 83.70 o -9 12 0 1058.68 964.51 49.38 o -8 12 0 1679.96 1641.97 91.29 o -7 12 0 4512.38 4287.52 103.26 o -6 12 0 4396.87 4346.52 102.14 o -5 12 0 3122.71 3170.38 81.32 o -4 12 0 735.47 740.61 30.15 o -3 12 0 5849.30 6036.75 92.04 o -2 12 0 155.46 165.93 16.06 o -1 12 0 0.79 14.34 13.01 o 0 12 0 104.29 118.58 15.63 o 1 12 0 81.90 95.50 16.16 o 2 12 0 6751.70 6901.63 113.30 o 3 12 0 125.64 76.81 19.82 o 4 12 0 9280.58 9136.09 168.60 o 5 12 0 3385.20 3434.91 79.86 o 6 12 0 6572.08 6600.99 132.41 o 7 12 0 1419.40 1500.80 52.38 o 8 12 0 2961.08 3020.48 79.36 o 9 12 0 4184.08 4049.72 123.23 o 10 12 0 4719.42 4789.77 111.95 o 11 12 0 145.28 107.55 37.58 o 12 12 0 189.97 227.91 44.98 o 13 12 0 1676.21 1686.23 191.13 o -11 13 0 826.79 736.07 90.99 o -10 13 0 1358.87 1259.51 76.74 o -9 13 0 111.60 97.79 30.50 o -8 13 0 728.07 687.15 43.39 o -7 13 0 72.94 89.44 26.85 o -6 13 0 2748.51 2696.50 85.13 o -5 13 0 554.44 593.21 49.10 o -4 13 0 2710.57 2655.81 72.16 o -3 13 0 24.90 6.35 18.75 o -2 13 0 1397.59 1464.53 41.26 o -1 13 0 482.51 511.71 25.05 o 0 13 0 1.75 -4.25 14.25 o 1 13 0 323.32 391.83 23.76 o 2 13 0 128.18 111.24 39.50 o 3 13 0 855.84 865.46 35.46 o 4 13 0 5.73 13.36 29.89 o 5 13 0 2152.98 2276.84 72.97 o 6 13 0 3493.41 3393.56 98.82 o 7 13 0 2642.62 2680.14 88.20 o 8 13 0 4742.46 4370.78 125.77 o 9 13 0 6.55 24.91 30.09 o 10 13 0 1822.69 1812.04 81.68 o 11 13 0 43.41 22.09 42.08 o 12 13 0 764.84 764.49 90.73 o 13 13 0 182.01 150.63 47.09 o -10 14 0 4.73 50.02 43.41 o -9 14 0 222.61 243.61 35.78 o -8 14 0 121.64 118.53 31.88 o -7 14 0 129.50 126.39 29.68 o -6 14 0 13.37 10.69 23.76 o -5 14 0 117.27 139.44 25.88 o -4 14 0 770.13 684.46 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