#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/08/2210884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210884_Fobs loop_ _publ_author_name 'Bortoluzzi, Adailton J.' 'Neves, Ademir' 'Terra, Geovana G.' _publ_section_title ; trans-Bis(6-amino-6-methylperhydro-1,4-diazepine)zinc(II) bis(perchlorate) ; _journal_coeditor_code BI2077 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2965 _journal_page_last m2966 _journal_volume 62 _journal_year 2006 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8330 _cell_length_b 17.0120 _cell_length_c 13.8680 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8116 _[local]_cod_data_source_file bi2077Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ; Trans-[bis-(6-amino-6-methylperhydro-1,4-diazepine)]zinc diperchlorate ; _shelx_refln_list_code 4 _shelx_f_calc_maximum 414.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 171984.59 142523.42 1148.14 o 4 0 0 8335.38 8003.49 103.91 o 6 0 0 38660.00 38184.42 282.79 o 8 0 0 19599.49 20081.85 251.44 o 10 0 0 1108.68 1223.40 42.19 o 0 2 0 65414.13 66828.79 583.98 o 2 2 0 14487.13 13935.77 101.91 o 4 2 0 1925.27 1914.71 55.87 o 6 2 0 6797.14 6682.17 126.00 o 8 2 0 4516.45 4668.11 128.85 o 10 2 0 902.62 932.62 34.92 o 0 4 0 28447.14 28960.81 140.97 o 2 4 0 106.68 74.55 8.27 o 4 4 0 1577.09 1945.64 40.91 o 6 4 0 14.21 28.22 12.12 o 8 4 0 38.35 7.98 47.89 o 10 4 0 341.98 320.42 27.65 o 0 6 0 13844.76 13433.04 120.87 o 2 6 0 921.92 820.87 24.94 o 4 6 0 553.17 663.51 20.67 o 6 6 0 12.67 16.39 36.77 o 8 6 0 9.54 12.26 20.38 o 10 6 0 21.60 -51.88 59.87 o 0 8 0 250.71 236.18 11.97 o 2 8 0 4016.52 4190.75 86.66 o 4 8 0 5124.35 5023.31 107.62 o 6 8 0 262.25 280.23 20.67 o 8 8 0 63.58 97.92 20.38 o 10 8 0 470.48 439.87 32.36 o 0 10 0 11124.82 10739.22 140.11 o 2 10 0 14311.43 14370.08 172.04 o 4 10 0 9652.33 9478.47 156.79 o 6 10 0 2959.38 2889.81 73.98 o 8 10 0 1075.94 1095.54 36.92 o 0 12 0 45187.38 43794.84 319.14 o 2 12 0 19449.30 19565.01 223.64 o 4 12 0 9083.52 9629.99 171.19 o 6 12 0 10299.36 10095.09 196.70 o 8 12 0 4182.92 4295.52 106.48 o 0 14 0 2869.06 2839.07 67.85 o 2 14 0 2077.36 2254.80 64.85 o 4 14 0 2689.36 2768.37 77.11 o 6 14 0 2518.13 2271.05 65.00 o 8 14 0 781.43 712.26 36.63 o 0 16 0 2348.44 2608.58 75.83 o 2 16 0 16.10 48.18 20.10 o 4 16 0 870.17 928.35 32.36 o 6 16 0 67.78 84.95 24.23 o 0 18 0 452.85 448.28 27.79 o 2 18 0 612.38 539.22 31.93 o 4 18 0 312.61 343.94 27.94 o 0 20 0 1951.44 1773.88 55.30 o 2 20 0 818.55 738.20 35.92 o 1 1 1 11467.33 11205.60 66.28 o 3 1 1 693.38 744.19 23.09 o 5 1 1 677.50 720.81 22.95 o 7 1 1 1343.74 1365.65 41.91 o 9 1 1 17.97 30.65 19.24 o 0 2 1 10773.25 11487.25 69.99 o 2 2 1 17110.08 17567.06 115.74 o 4 2 1 10146.79 10123.03 121.44 o 6 2 1 3399.11 3731.78 93.65 o 8 2 1 1262.29 1322.46 46.47 o 10 2 1 357.88 350.79 26.94 o 1 3 1 102.24 98.49 4.13 o 3 3 1 29531.39 28526.78 184.59 o 5 3 1 7292.53 7380.60 118.59 o 7 3 1 231.96 273.39 19.53 o 9 3 1 771.90 769.42 31.07 o 0 4 1 1819.28 1784.86 37.34 o 2 4 1 863.78 928.92 24.52 o 4 4 1 103.49 72.69 12.12 o 6 4 1 1168.71 1055.78 35.92 o 8 4 1 827.27 820.16 27.65 o 10 4 1 140.14 152.66 27.37 o 1 5 1 16441.14 15811.85 124.72 o 3 5 1 34754.61 33584.59 216.94 o 5 5 1 15382.75 15416.45 181.88 o 7 5 1 4426.31 4464.85 120.16 o 9 5 1 3023.47 2971.20 87.09 o 0 6 1 6398.89 6064.69 82.39 o 2 6 1 0.29 16.53 20.67 o 4 6 1 2607.65 2714.92 73.98 o 6 6 1 50.07 56.73 16.25 o 8 6 1 36.23 0.00 48.04 o 10 6 1 15.73 11.97 27.79 o 1 7 1 16382.17 15814.84 145.25 o 3 7 1 13252.71 13173.19 152.94 o 5 7 1 8106.43 7970.14 139.69 o 7 7 1 4600.84 4630.34 130.14 o 9 7 1 2078.81 2053.26 56.16 o 0 8 1 525.84 618.04 16.39 o 2 8 1 1778.21 1713.16 41.34 o 4 8 1 5022.13 5015.33 107.19 o 6 8 1 983.56 951.30 28.65 o 8 8 1 161.80 171.05 20.38 o 10 8 1 221.73 215.66 27.94 o 1 9 1 6433.78 6253.13 107.19 o 3 9 1 3868.30 3713.68 90.80 o 5 9 1 1348.20 1368.93 41.19 o 7 9 1 493.71 596.66 24.52 o 9 9 1 368.81 344.23 32.36 o 0 10 1 773.41 707.27 20.38 o 2 10 1 2064.83 2007.22 49.60 o 4 10 1 1758.55 1761.34 53.45 o 6 10 1 318.71 350.36 20.67 o 8 10 1 88.78 155.22 24.52 o 1 11 1 3115.96 3191.99 90.08 o 3 11 1 214.04 197.56 16.53 o 5 11 1 49.47 -8.27 45.18 o 7 11 1 878.54 866.34 32.78 o 9 11 1 54.71 57.16 28.65 o 0 12 1 631.07 637.00 20.24 o 2 12 1 17.08 36.77 12.26 o 4 12 1 245.45 250.72 20.53 o 6 12 1 59.36 65.71 20.53 o 8 12 1 8.06 8.12 24.37 o 1 13 1 6918.16 7245.19 141.97 o 3 13 1 197.35 134.70 20.38 o 5 13 1 1162.04 1065.61 32.78 o 7 13 1 2611.87 2460.91 69.56 o 0 14 1 622.35 651.68 24.09 o 2 14 1 2287.54 2267.06 65.00 o 4 14 1 2819.73 2762.67 77.40 o 6 14 1 478.75 437.16 28.65 o 8 14 1 142.79 126.00 28.51 o 1 15 1 841.33 824.44 28.08 o 3 15 1 3429.69 3247.72 81.25 o 5 15 1 1668.86 1633.20 48.75 o 7 15 1 260.65 284.93 28.51 o 0 16 1 0.48 48.04 19.96 o 2 16 1 110.74 105.34 20.24 o 4 16 1 108.79 137.69 24.37 o 6 16 1 1.60 -24.37 65.00 o 1 17 1 1765.37 1718.86 48.04 o 3 17 1 5172.81 4979.98 109.04 o 5 17 1 1813.07 1741.95 48.32 o 0 18 1 17.70 23.95 51.88 o 2 18 1 10.71 7.98 56.16 o 4 18 1 112.28 88.80 24.23 o 1 19 1 2098.35 2084.90 63.86 o 3 19 1 960.38 1076.44 36.06 o 0 20 1 83.61 95.22 27.79 o 2 20 1 219.40 235.04 27.94 o 0 0 2 75829.53 68709.30 619.33 o 2 0 2 12254.41 12645.52 96.21 o 4 0 2 12164.65 12386.81 130.71 o 6 0 2 16211.53 16025.51 187.72 o 8 0 2 4167.53 4442.61 125.29 o 10 0 2 127.84 151.95 26.51 o 1 1 2 10060.51 10151.54 71.41 o 3 1 2 1223.00 1729.69 45.33 o 5 1 2 6.12 38.06 11.40 o 7 1 2 786.41 853.37 26.65 o 9 1 2 39.79 19.10 22.95 o 0 2 2 4941.61 5164.14 51.31 o 2 2 2 12704.61 12861.60 104.62 o 4 2 2 13847.92 14233.24 142.82 o 6 2 2 4329.16 4169.80 99.92 o 8 2 2 1050.16 1117.07 34.64 o 10 2 2 584.23 637.57 30.79 o 1 3 2 63187.66 67475.34 860.50 o 3 3 2 140.57 256.85 7.84 o 5 3 2 333.20 273.24 15.68 o 7 3 2 4345.63 4128.89 112.60 o 9 3 2 535.27 629.02 26.94 o 0 4 2 58.91 123.44 8.27 o 2 4 2 9092.16 9031.33 100.49 o 4 4 2 6943.95 6811.59 107.90 o 6 4 2 309.51 282.37 15.68 o 8 4 2 272.19 280.80 23.38 o 10 4 2 978.14 1026.56 35.06 o 1 5 2 856.50 714.40 20.53 o 3 5 2 3732.06 4135.87 81.10 o 5 5 2 99.45 120.87 12.12 o 7 5 2 1039.64 968.12 31.64 o 9 5 2 136.61 121.73 23.52 o 0 6 2 9640.13 9805.17 108.19 o 2 6 2 3780.55 3943.30 73.98 o 4 6 2 923.69 956.86 28.51 o 6 6 2 1067.38 1137.17 36.06 o 8 6 2 1326.84 1258.04 43.47 o 10 6 2 425.33 370.46 31.50 o 1 7 2 144.84 165.91 8.27 o 3 7 2 410.20 386.42 16.39 o 5 7 2 353.21 332.97 16.25 o 7 7 2 68.03 100.49 20.10 o 9 7 2 51.89 99.35 23.80 o 0 8 2 4498.27 4093.11 82.96 o 2 8 2 5420.29 5302.40 99.21 o 4 8 2 3171.44 3337.66 90.37 o 6 8 2 1769.51 1769.89 57.02 o 8 8 2 909.11 813.46 32.21 o 1 9 2 5423.38 5219.44 99.49 o 3 9 2 742.57 788.38 24.80 o 5 9 2 1270.22 1254.76 41.05 o 7 9 2 1172.96 1105.09 36.63 o 9 9 2 148.94 192.57 28.08 o 0 10 2 5962.78 5487.70 107.33 o 2 10 2 5379.74 5246.53 111.61 o 4 10 2 3732.70 3967.11 107.19 o 6 10 2 2509.39 2672.87 73.69 o 8 10 2 919.30 886.73 36.49 o 1 11 2 0.23 32.93 12.40 o 3 11 2 46.68 20.67 37.20 o 5 11 2 72.81 24.80 49.46 o 7 11 2 120.83 147.10 20.38 o 9 11 2 6.66 -3.99 24.37 o 0 12 2 15746.75 15441.96 195.85 o 2 12 2 4340.48 4124.33 111.18 o 4 12 2 1523.09 1579.75 45.18 o 6 12 2 4223.73 4434.63 98.49 o 8 12 2 2009.64 1923.26 57.16 o 1 13 2 1455.14 1498.21 40.91 o 3 13 2 144.40 152.09 20.53 o 5 13 2 63.38 8.27 20.53 o 7 13 2 139.18 126.57 24.52 o 0 14 2 4924.72 5153.59 129.85 o 2 14 2 2799.98 2887.24 69.42 o 4 14 2 1488.21 1493.08 36.77 o 6 14 2 1180.62 1133.17 36.77 o 8 14 2 567.11 541.64 36.63 o 1 15 2 314.57 304.75 20.38 o 3 15 2 3.84 4.13 48.89 o 5 15 2 163.18 179.74 24.52 o 7 15 2 281.56 240.32 28.51 o 0 16 2 98.23 136.69 20.10 o 2 16 2 1689.63 1629.35 52.74 o 4 16 2 2029.42 1942.50 61.01 o 6 16 2 32.58 20.38 61.29 o 1 17 2 67.33 112.46 20.10 o 3 17 2 33.34 12.12 24.23 o 5 17 2 109.43 170.48 24.37 o 0 18 2 993.06 1023.14 31.93 o 2 18 2 1159.03 1172.52 36.35 o 4 18 2 883.73 842.97 36.35 o 1 19 2 456.50 459.68 31.93 o 3 19 2 1.30 -24.23 64.57 o 0 20 2 1074.06 1133.17 39.91 o 2 20 2 682.74 692.31 36.06 o 1 1 3 28960.47 29412.51 140.68 o 3 1 3 732.58 640.85 18.67 o 5 1 3 6902.03 6469.36 109.75 o 7 1 3 10776.31 11218.00 174.61 o 9 1 3 1588.93 1532.28 45.61 o 0 2 3 9217.03 8336.74 75.69 o 2 2 3 27526.71 26686.47 160.50 o 4 2 3 15541.90 16971.54 160.35 o 6 2 3 1161.55 1249.63 38.06 o 8 2 3 748.14 714.54 26.80 o 10 2 3 1110.16 1137.31 38.49 o 1 3 3 3905.06 3875.88 58.58 o 3 3 3 4054.67 4546.38 77.68 o 5 3 3 939.84 1003.61 30.93 o 7 3 3 688.95 639.42 23.09 o 9 3 3 997.19 1014.01 34.64 o 0 4 3 518.02 415.50 12.12 o 2 4 3 6371.63 6073.25 83.53 o 4 4 3 2693.79 2650.63 70.56 o 6 4 3 368.21 380.29 19.39 o 8 4 3 245.28 270.11 23.09 o 10 4 3 421.49 461.11 27.08 o 1 5 3 23859.11 24451.63 166.63 o 3 5 3 6241.17 6503.71 99.92 o 5 5 3 711.76 796.07 23.66 o 7 5 3 506.28 549.20 23.52 o 9 5 3 644.14 732.22 31.22 o 0 6 3 138.15 107.33 8.27 o 2 6 3 90.16 105.76 8.12 o 4 6 3 534.56 624.32 20.10 o 6 6 3 0.63 -19.81 39.77 o 8 6 3 0.00 -51.03 51.03 o 10 6 3 32.35 -46.89 66.42 o 1 7 3 15310.73 16423.33 156.36 o 3 7 3 8617.46 8758.23 130.28 o 5 7 3 2966.12 2972.20 64.85 o 7 7 3 1177.81 1187.77 39.77 o 9 7 3 514.65 469.95 27.65 o 0 8 3 1.88 16.53 8.27 o 2 8 3 5722.21 5459.05 102.91 o 4 8 3 5461.80 5649.62 118.16 o 6 8 3 202.26 209.10 20.10 o 8 8 3 108.16 115.31 23.80 o 1 9 3 400.43 463.96 16.53 o 3 9 3 6198.16 5894.65 119.45 o 5 9 3 3994.23 3709.26 106.05 o 7 9 3 311.22 254.57 24.23 o 9 9 3 426.39 395.40 31.93 o 0 10 3 188.07 190.72 12.40 o 2 10 3 2895.16 2906.49 82.53 o 4 10 3 2842.87 2827.95 65.85 o 6 10 3 162.06 175.32 20.38 o 8 10 3 105.33 124.58 24.09 o 1 11 3 3679.25 3606.20 99.21 o 3 11 3 6801.19 6967.95 140.26 o 5 11 3 5775.51 5725.74 143.68 o 7 11 3 2077.09 1945.07 61.15 o 9 11 3 642.65 587.97 36.06 o 0 12 3 31.00 86.52 16.53 o 2 12 3 9.13 45.33 12.40 o 4 12 3 46.68 70.13 16.53 o 6 12 3 1.83 16.39 53.17 o 8 12 3 1.08 -60.86 64.85 o 1 13 3 5685.20 5232.99 127.43 o 3 13 3 1941.22 2074.07 61.72 o 5 13 3 2169.89 2198.93 69.56 o 7 13 3 1856.00 1886.49 61.29 o 0 14 3 1018.00 1019.29 36.77 o 2 14 3 3530.17 3654.38 81.96 o 4 14 3 3473.28 3576.27 86.38 o 6 14 3 273.37 253.43 28.65 o 1 15 3 1595.52 1498.78 40.91 o 3 15 3 2075.25 2168.00 69.56 o 5 15 3 592.84 639.99 32.78 o 7 15 3 63.76 40.77 28.51 o 0 16 3 22.56 -20.24 48.61 o 2 16 3 165.15 203.69 20.38 o 4 16 3 245.11 294.20 24.52 o 6 16 3 0.19 20.38 65.00 o 1 17 3 728.08 802.49 28.36 o 3 17 3 1039.67 1158.26 36.63 o 5 17 3 303.28 381.57 28.36 o 0 18 3 0.01 -60.29 60.29 o 2 18 3 69.67 20.24 64.71 o 4 18 3 133.98 142.11 28.36 o 1 19 3 1689.82 1811.65 56.16 o 3 19 3 574.41 629.30 32.21 o 0 20 3 20.54 39.91 27.94 o 2 20 3 266.12 291.92 31.93 o 0 0 4 12332.77 11712.32 94.22 o 2 0 4 4038.99 4234.79 65.99 o 4 0 4 169.30 122.15 11.12 o 6 0 4 225.76 187.01 14.97 o 8 0 4 7.12 26.51 18.96 o 10 0 4 24.71 -11.40 71.98 o 1 1 4 3198.41 3843.39 59.01 o 3 1 4 3079.61 3070.83 63.57 o 5 1 4 4.72 -14.97 26.23 o 7 1 4 86.07 98.78 18.96 o 9 1 4 129.57 136.69 22.81 o 0 2 4 30.98 40.77 7.41 o 2 2 4 9401.83 9461.79 101.63 o 4 2 4 11831.80 11871.39 140.11 o 6 2 4 973.79 1100.68 34.21 o 8 2 4 89.07 117.74 18.96 o 10 2 4 411.57 449.71 30.79 o 1 3 4 381.80 508.57 15.25 o 3 3 4 9.66 11.55 22.95 o 5 3 4 1520.13 1617.52 45.75 o 7 3 4 563.91 571.43 22.95 o 9 3 4 111.63 88.37 23.09 o 0 4 4 8686.49 8065.78 94.93 o 2 4 4 17765.39 17009.02 148.24 o 4 4 4 13194.03 13363.62 154.37 o 6 4 4 2964.13 3133.12 69.56 o 8 4 4 1421.41 1503.63 42.48 o 10 4 4 1470.08 1474.27 46.32 o 1 5 4 652.66 887.72 27.79 o 3 5 4 1550.44 1549.81 39.48 o 5 5 4 908.43 812.46 23.38 o 7 5 4 13.99 -23.23 46.61 o 9 5 4 0.03 19.39 23.23 o 0 6 4 57767.82 56442.64 280.80 o 2 6 4 19026.45 19067.55 171.90 o 4 6 4 6600.90 6712.10 118.73 o 6 6 4 9185.82 8947.23 160.78 o 8 6 4 5204.64 5267.77 148.67 o 10 6 4 893.04 858.50 35.06 o 1 7 4 1861.20 1986.41 44.90 o 3 7 4 170.86 145.10 12.12 o 5 7 4 232.39 283.22 19.96 o 7 7 4 896.68 846.67 27.65 o 9 7 4 10.52 19.53 23.52 o 0 8 4 10568.64 10467.97 136.12 o 2 8 4 6627.65 6257.69 114.46 o 4 8 4 4367.90 4061.47 101.20 o 6 8 4 3638.93 3727.65 79.82 o 8 8 4 1557.33 1644.60 47.61 o 1 9 4 1142.06 1132.89 41.19 o 3 9 4 272.54 282.37 16.39 o 5 9 4 162.79 190.43 20.24 o 7 9 4 655.28 715.54 27.79 o 9 9 4 1.08 -71.41 71.41 o 0 10 4 305.79 236.33 16.53 o 2 10 4 1423.72 1333.73 45.33 o 4 10 4 1764.13 1737.11 44.90 o 6 10 4 417.62 481.21 24.23 o 8 10 4 106.76 163.78 23.95 o 1 11 4 108.98 103.48 16.53 o 3 11 4 270.68 296.34 20.53 o 5 11 4 179.58 207.96 20.38 o 7 11 4 39.64 32.36 20.24 o 0 12 4 772.52 893.28 28.94 o 2 12 4 18.63 45.33 16.53 o 4 12 4 66.62 36.92 49.32 o 6 12 4 232.87 240.60 24.52 o 8 12 4 201.60 168.76 28.08 o 1 13 4 18.93 4.13 41.19 o 3 13 4 796.90 758.44 24.80 o 5 13 4 1.28 32.78 20.53 o 7 13 4 213.32 251.44 28.36 o 0 14 4 3552.92 3981.36 119.30 o 2 14 4 1918.33 1934.24 53.45 o 4 14 4 682.09 633.01 28.79 o 6 14 4 655.63 694.16 32.64 o 1 15 4 105.67 131.28 20.53 o 3 15 4 619.93 566.73 28.79 o 5 15 4 31.29 0.00 24.52 o 7 15 4 126.51 122.15 28.51 o 0 16 4 3232.64 3236.18 85.81 o 2 16 4 4396.94 4168.37 98.21 o 4 16 4 3280.19 3218.93 90.08 o 6 16 4 942.54 964.12 36.63 o 1 17 4 355.66 313.73 24.52 o 3 17 4 65.99 -8.12 61.29 o 5 17 4 0.22 -69.13 69.13 o 0 18 4 3437.01 3570.14 97.07 o 2 18 4 2166.46 2149.75 65.00 o 4 18 4 1271.27 1270.58 40.62 o 1 19 4 39.51 36.35 24.23 o 3 19 4 40.23 20.24 24.23 o 0 20 4 1261.24 1238.51 44.04 o 2 20 4 836.80 800.78 40.20 o 1 1 5 10520.89 9505.13 99.49 o 3 1 5 6957.57 7260.87 104.34 o 5 1 5 3797.59 3914.66 93.79 o 7 1 5 2037.87 2188.95 60.58 o 9 1 5 1275.88 1314.63 41.62 o 0 2 5 13290.78 13267.12 118.45 o 2 2 5 109.80 41.05 7.41 o 4 2 5 214.97 371.74 14.97 o 6 2 5 2895.34 2942.55 64.57 o 8 2 5 625.83 672.92 26.65 o 10 2 5 96.74 130.56 26.94 o 1 3 5 3971.43 3923.49 67.85 o 3 3 5 13198.84 12592.35 140.54 o 5 3 5 5147.67 5048.11 106.33 o 7 3 5 828.71 859.64 26.80 o 9 3 5 746.93 788.09 34.64 o 0 4 5 8086.09 8063.07 100.20 o 2 4 5 77.41 68.99 7.70 o 4 4 5 287.72 307.45 15.39 o 6 4 5 1564.54 1434.36 42.19 o 8 4 5 889.38 871.90 30.79 o 10 4 5 0.82 -65.42 65.42 o 1 5 5 6388.31 6968.10 101.91 o 3 5 5 618.81 600.51 19.53 o 5 5 5 1816.55 1822.20 50.46 o 7 5 5 2210.25 2087.46 65.57 o 9 5 5 171.59 154.37 27.08 o 0 6 5 5441.57 5777.62 96.36 o 2 6 5 91.42 137.98 11.83 o 4 6 5 996.37 953.15 31.22 o 6 6 5 53.29 11.69 46.75 o 8 6 5 61.50 65.85 23.23 o 1 7 5 10041.30 10387.01 137.12 o 3 7 5 358.38 399.96 15.82 o 5 7 5 1387.05 1322.75 39.34 o 7 7 5 2596.00 2331.20 70.70 o 9 7 5 179.58 125.01 27.37 o 0 8 5 708.87 829.71 24.52 o 2 8 5 256.53 299.04 16.11 o 4 8 5 1762.51 1697.62 51.88 o 6 8 5 1867.10 1788.28 51.46 o 8 8 5 271.50 196.84 27.51 o 1 9 5 2906.50 2752.97 81.82 o 3 9 5 5441.53 5693.24 121.44 o 5 9 5 1760.64 1768.75 48.18 o 7 9 5 316.58 238.32 23.80 o 9 9 5 627.97 625.60 35.35 o 0 10 5 1199.11 1013.73 32.93 o 2 10 5 74.31 61.43 16.39 o 4 10 5 8.84 28.36 16.25 o 6 10 5 337.34 343.94 23.95 o 8 10 5 31.94 31.79 63.43 o 1 11 5 5009.56 4939.64 115.31 o 3 11 5 6374.07 6678.60 143.11 o 5 11 5 2321.28 2421.86 68.70 o 7 11 5 802.68 758.87 31.93 o 0 12 5 182.29 165.49 16.53 o 2 12 5 1.92 -41.19 41.19 o 4 12 5 174.25 163.49 20.38 o 6 12 5 139.54 161.92 24.23 o 8 12 5 23.42 40.05 23.95 o 1 13 5 2365.68 2479.44 65.99 o 3 13 5 1314.78 1532.28 49.32 o 5 13 5 1200.26 1240.79 36.77 o 7 13 5 1123.17 1200.88 40.34 o 0 14 5 586.78 552.33 24.80 o 2 14 5 106.05 32.93 49.32 o 4 14 5 59.32 86.09 20.53 o 6 14 5 436.66 348.65 28.36 o 1 15 5 1370.84 1314.34 41.05 o 3 15 5 2588.72 2490.99 78.11 o 5 15 5 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