#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210898.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210898_Fobs loop_ _publ_author_name 'Yang, Guo-Zhong' 'Yao, Li' 'Cui, Xue-Yu' _publ_section_title ; N-Benzylpyridinium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)nickel(III) ; _journal_coeditor_code BT2199 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2963 _journal_page_last m2964 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.013 _cell_angle_beta 77.688 _cell_angle_gamma 73.750 _cell_length_a 9.1539 _cell_length_b 10.8254 _cell_length_c 12.5210 _exptl_crystal_F_000 630.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bt2199Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 40330Am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 339.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 620.57 709.46 29.09 o 2 0 0 984.62 1265.98 174.69 o 3 0 0 2.80 15.54 7.62 o 4 0 0 56.80 114.38 14.16 o 5 0 0 30.01 66.21 25.80 o 6 0 0 246.88 195.89 41.58 o 7 0 0 434.49 401.98 63.27 o 8 0 0 3.98 5.42 24.65 o 9 0 0 85.48 121.78 44.87 o 10 0 0 21.29 29.09 47.66 o -10 1 0 208.59 212.66 53.74 o -9 1 0 0.37 5.09 24.32 o -8 1 0 90.69 58.83 33.36 o -7 1 0 1107.72 975.36 96.63 o -6 1 0 1971.97 1835.20 120.30 o -5 1 0 225.24 294.01 46.02 o -4 1 0 5405.01 5399.69 370.84 o -3 1 0 8016.35 9553.30 114.87 o -2 1 0 1309.52 1188.35 56.53 o -1 1 0 41.07 24.49 8.05 o 0 1 0 7.90 1.64 3.29 o 1 1 0 2764.09 3129.03 86.77 o 2 1 0 1360.04 1618.77 62.53 o 3 1 0 543.41 413.91 23.76 o 4 1 0 9839.68 10020.85 352.84 o 5 1 0 5017.99 5454.59 135.91 o 6 1 0 80.86 108.61 24.16 o 7 1 0 941.77 740.19 82.50 o 8 1 0 35.34 29.58 28.92 o 9 1 0 101.62 83.32 40.92 o 10 1 0 36.54 46.02 41.58 o -9 2 0 91.87 120.79 43.88 o -8 2 0 390.48 373.38 66.07 o -7 2 0 46.37 58.83 29.42 o -6 2 0 835.32 748.41 79.71 o -5 2 0 156.84 190.47 39.61 o -4 2 0 1.48 1.15 17.09 o -3 2 0 1675.55 1795.84 140.10 o -2 2 0 3471.38 3550.31 157.52 o -1 2 0 506.11 454.38 16.40 o 0 2 0 1483.07 1560.25 50.62 o 1 2 0 2700.62 2560.63 49.54 o 2 2 0 116.45 170.11 14.46 o 3 2 0 73.26 52.18 11.13 o 4 2 0 246.40 226.67 21.59 o 5 2 0 4631.41 4639.03 196.96 o 6 2 0 2346.98 2213.24 140.51 o 7 2 0 32.46 7.40 22.35 o 8 2 0 961.13 991.80 100.91 o 9 2 0 830.27 777.50 98.77 o 10 2 0 144.29 131.31 52.59 o -9 3 0 3.17 11.67 25.64 o -8 3 0 0.43 0.00 20.73 o -7 3 0 183.23 200.99 48.64 o -6 3 0 1584.79 1433.38 111.59 o -5 3 0 7047.49 7079.31 227.61 o -4 3 0 918.04 905.85 73.95 o -3 3 0 367.22 358.24 18.86 o -2 3 0 935.87 901.65 28.68 o -1 3 0 93.97 106.79 10.68 o 0 3 0 653.35 572.45 20.60 o 1 3 0 5636.41 5816.35 91.13 o 2 3 0 2993.74 2634.86 81.97 o 3 3 0 1786.77 1636.55 62.53 o 4 3 0 3968.08 4073.17 91.76 o 5 3 0 7.11 9.75 11.02 o 6 3 0 327.17 330.86 39.03 o 7 3 0 179.09 215.27 29.98 o 8 3 0 11.21 0.00 26.46 o 9 3 0 615.54 604.28 86.11 o 10 3 0 36.34 28.27 42.24 o -8 4 0 73.89 81.32 26.35 o -7 4 0 13.72 20.17 19.36 o -6 4 0 20.24 0.00 14.45 o -5 4 0 1551.29 1573.58 78.05 o -4 4 0 726.85 680.19 47.42 o -3 4 0 1878.84 2017.57 49.49 o -2 4 0 278.71 277.39 21.84 o -1 4 0 6660.83 7301.93 92.01 o 0 4 0 3456.88 3559.89 50.34 o 1 4 0 0.63 13.15 9.41 o 2 4 0 170.85 174.45 12.14 o 3 4 0 121.09 141.19 21.12 o 4 4 0 63.22 69.41 14.57 o 5 4 0 1873.92 2021.46 73.15 o 6 4 0 2.87 0.51 21.53 o 7 4 0 1058.23 953.78 59.61 o 8 4 0 231.01 213.64 49.14 o 9 4 0 44.15 37.96 30.57 o 10 4 0 0.13 13.48 38.62 o -8 5 0 30.18 66.59 27.21 o -7 5 0 1.08 0.00 18.32 o -6 5 0 430.84 409.52 45.67 o -5 5 0 34.45 35.14 17.14 o -4 5 0 1.17 4.27 21.86 o -3 5 0 135.01 131.22 21.94 o -2 5 0 95.81 83.60 13.31 o -1 5 0 108.41 84.71 11.81 o 0 5 0 12736.55 13937.81 118.63 o 1 5 0 5938.23 6036.42 182.58 o 2 5 0 1076.35 1219.21 106.16 o 3 5 0 710.25 764.47 29.83 o 4 5 0 241.01 233.31 24.21 o 5 5 0 446.44 459.79 36.37 o 6 5 0 6.55 16.12 15.44 o 7 5 0 32.91 22.27 15.04 o 8 5 0 11.22 33.32 18.64 o 9 5 0 293.13 328.52 64.59 o 10 5 0 76.47 104.03 46.34 o -7 6 0 26.28 28.51 23.18 o -6 6 0 330.42 364.23 48.81 o -5 6 0 99.32 99.17 24.17 o -4 6 0 25.20 23.42 16.24 o -3 6 0 729.89 652.88 76.01 o -2 6 0 32.27 36.26 11.67 o -1 6 0 398.25 353.37 26.21 o 0 6 0 384.03 366.24 32.94 o 1 6 0 0.85 4.47 11.37 o 2 6 0 47.61 36.55 13.90 o 3 6 0 2452.27 2483.80 50.58 o 4 6 0 160.44 139.27 19.35 o 5 6 0 2659.02 2592.01 84.29 o 6 6 0 420.67 420.04 38.30 o 7 6 0 312.94 319.26 36.81 o 8 6 0 47.34 49.09 21.95 o 9 6 0 2.62 37.80 32.70 o -7 7 0 190.96 177.82 57.19 o -6 7 0 1064.46 1112.10 118.65 o -5 7 0 75.57 98.28 38.78 o -4 7 0 31.42 14.13 23.01 o -3 7 0 73.00 41.25 28.92 o -2 7 0 1579.24 1534.75 127.12 o -1 7 0 2337.46 2214.51 270.18 o 0 7 0 1.63 5.05 14.38 o 1 7 0 1126.14 1065.68 60.15 o 2 7 0 9.54 14.31 13.42 o 3 7 0 5.07 9.32 13.19 o 4 7 0 269.22 244.87 45.69 o 5 7 0 31.22 50.12 25.80 o 6 7 0 272.19 198.03 44.54 o 7 7 0 35.88 50.12 30.07 o 8 7 0 424.29 433.20 68.53 o 9 7 0 295.42 297.46 59.16 o -6 8 0 84.91 124.57 57.35 o -5 8 0 4309.09 4473.69 238.29 o -4 8 0 0.81 20.87 27.61 o -3 8 0 619.47 499.76 74.28 o -2 8 0 314.06 333.45 59.66 o -1 8 0 30.35 20.90 14.92 o 0 8 0 79.22 74.16 20.44 o 1 8 0 5.49 6.33 11.49 o 2 8 0 295.86 290.66 35.00 o 3 8 0 247.87 233.42 32.83 o 4 8 0 1314.38 1228.43 100.74 o 5 8 0 274.91 241.42 50.12 o 6 8 0 1809.89 1924.93 138.87 o 7 8 0 16.11 13.97 25.64 o 8 8 0 2.13 6.90 25.14 o 9 8 0 125.13 124.24 44.21 o -5 9 0 0.03 0.00 42.40 o -4 9 0 101.75 60.15 37.63 o -3 9 0 27.61 31.72 30.57 o -2 9 0 251.19 281.68 58.67 o -1 9 0 2143.14 2441.38 204.19 o 0 9 0 1356.55 1307.21 76.23 o 1 9 0 1162.70 1068.70 69.31 o 2 9 0 399.08 411.33 46.84 o 3 9 0 182.48 185.60 31.67 o 4 9 0 0.03 14.87 16.05 o 5 9 0 100.29 97.45 36.65 o 6 9 0 10.57 22.19 27.61 o 7 9 0 390.19 394.58 69.68 o 8 9 0 7.11 50.95 30.57 o 9 9 0 153.87 256.54 60.97 o -4 10 0 79.91 92.03 49.30 o -3 10 0 0.71 12.33 35.00 o -2 10 0 21.94 32.21 30.24 o -1 10 0 15.60 30.73 20.21 o 0 10 0 516.46 470.94 50.60 o 1 10 0 151.18 143.20 29.76 o 2 10 0 13.52 29.67 23.01 o 3 10 0 520.32 488.24 51.43 o 4 10 0 339.80 329.55 43.16 o 5 10 0 615.04 660.32 89.89 o 6 10 0 116.41 87.59 39.93 o 7 10 0 49.51 65.57 34.18 o 8 10 0 4.33 25.31 29.75 o -2 11 0 23.44 23.34 38.13 o -1 11 0 994.18 1010.20 114.87 o 0 11 0 1.40 8.05 20.54 o 1 11 0 325.83 322.80 44.74 o 2 11 0 1.73 0.00 16.26 o 3 11 0 8.89 18.41 17.83 o 4 11 0 370.11 381.03 49.07 o 5 11 0 6.99 31.88 35.66 o 6 11 0 142.30 200.82 52.59 o 7 11 0 126.94 140.51 43.71 o 0 12 0 229.31 243.22 55.22 o 1 12 0 29.10 47.06 26.77 o 2 12 0 78.52 86.77 28.15 o 3 12 0 38.17 89.71 29.79 o 4 12 0 32.70 35.87 25.98 o 5 12 0 53.45 59.16 49.30 o 6 12 0 11.92 18.41 48.64 o -5 -12 1 95.83 67.22 48.64 o -4 -12 1 30.32 50.95 23.81 o -3 -12 1 66.23 83.93 29.92 o -2 -12 1 87.15 121.55 32.87 o -1 -12 1 0.48 23.61 19.73 o 0 -12 1 44.83 51.60 28.10 o -7 -11 1 48.11 81.51 34.51 o -6 -11 1 74.19 69.35 36.16 o -5 -11 1 839.43 869.36 111.92 o -4 -11 1 563.44 587.98 59.83 o -3 -11 1 135.89 160.22 34.28 o -2 -11 1 105.27 84.20 27.80 o -1 -11 1 25.94 18.32 17.75 o 0 -11 1 31.13 20.38 25.64 o 1 -11 1 49.26 40.10 24.65 o 2 -11 1 53.42 49.80 28.10 o -8 -10 1 20.24 14.46 33.20 o -7 -10 1 51.17 76.09 35.17 o -6 -10 1 75.19 112.57 42.07 o -5 -10 1 3.73 27.94 33.69 o -4 -10 1 30.60 66.67 22.99 o -3 -10 1 343.73 397.75 66.80 o -2 -10 1 431.26 424.53 64.26 o -1 -10 1 321.53 345.33 43.91 o 0 -10 1 3209.75 3453.12 431.89 o 1 -10 1 2.79 13.97 23.34 o 2 -10 1 308.24 232.38 53.90 o 3 -10 1 50.52 45.52 37.47 o 4 -10 1 13.82 24.49 40.10 o -8 -9 1 8.40 13.97 27.94 o -7 -9 1 62.21 109.45 39.11 o -6 -9 1 16.19 20.21 32.38 o -5 -9 1 245.56 245.20 54.56 o -4 -9 1 323.28 293.62 37.90 o -3 -9 1 1317.67 1125.47 98.85 o -2 -9 1 409.64 386.62 42.88 o -1 -9 1 97.11 96.10 23.81 o 0 -9 1 45.30 48.23 20.77 o 1 -9 1 2218.43 2209.24 151.85 o 2 -9 1 82.14 55.55 26.79 o 3 -9 1 458.24 375.52 69.02 o 4 -9 1 89.00 98.11 43.39 o 5 -9 1 23.60 35.99 39.28 o -9 -8 1 287.19 261.63 59.98 o -8 -8 1 291.25 281.68 59.98 o -7 -8 1 0.54 0.00 20.21 o -6 -8 1 23.70 0.00 20.71 o -5 -8 1 86.98 64.26 32.70 o -4 -8 1 653.43 656.10 52.52 o -3 -8 1 154.34 156.71 27.39 o -2 -8 1 3913.49 3564.57 353.25 o -1 -8 1 230.42 256.68 32.82 o 0 -8 1 173.37 183.33 30.07 o 1 -8 1 3.22 12.37 12.83 o 2 -8 1 2.99 0.00 18.24 o 3 -8 1 19.50 44.37 29.91 o 4 -8 1 29.82 42.56 33.69 o 5 -8 1 1348.16 1184.41 125.39 o 6 -8 1 64.62 61.13 43.06 o -9 -7 1 2.77 0.00 24.16 o -8 -7 1 1.00 12.33 27.12 o -7 -7 1 455.71 524.25 72.97 o -6 -7 1 198.55 198.20 46.02 o -5 -7 1 4463.61 4515.60 198.36 o -4 -7 1 202.41 226.79 30.35 o -3 -7 1 17.08 28.33 17.20 o -2 -7 1 1.24 0.37 12.56 o -1 -7 1 2.13 16.47 16.68 o 0 -7 1 649.28 639.74 46.94 o 1 -7 1 4525.44 4509.13 485.71 o 2 -7 1 1047.53 887.28 88.42 o 3 -7 1 89.98 119.48 37.14 o 4 -7 1 62.18 49.96 30.40 o 5 -7 1 14.66 18.73 25.80 o 6 -7 1 6.65 0.00 32.87 o 7 -7 1 57.35 81.02 50.62 o -8 -6 1 21.88 44.87 21.32 o -7 -6 1 116.60 139.43 26.63 o -6 -6 1 673.03 641.65 47.97 o -5 -6 1 1337.59 1145.80 94.99 o -4 -6 1 2783.37 2649.40 76.56 o -3 -6 1 1594.89 1494.83 66.71 o -2 -6 1 1.71 2.76 10.88 o -1 -6 1 1286.75 1102.30 55.99 o 0 -6 1 405.55 330.39 31.51 o 1 -6 1 144.63 132.44 15.02 o 2 -6 1 217.28 208.42 20.50 o 3 -6 1 1780.95 1858.38 84.14 o 4 -6 1 228.95 234.41 41.09 o 5 -6 1 812.16 731.49 63.02 o 6 -6 1 50.64 21.16 19.67 o 7 -6 1 1382.99 1429.90 93.20 o -10 -5 1 121.17 159.08 54.89 o -9 -5 1 313.73 350.21 66.23 o -8 -5 1 61.23 62.52 22.93 o -7 -5 1 1106.39 1067.28 65.30 o -6 -5 1 113.02 92.77 20.49 o -5 -5 1 575.11 532.46 40.03 o -4 -5 1 15.81 14.80 11.25 o -3 -5 1 1.63 9.00 7.84 o -2 -5 1 3344.34 3381.26 95.15 o -1 -5 1 320.94 298.55 28.68 o 0 -5 1 22558.90 24500.68 193.04 o 1 -5 1 10133.13 11165.16 165.90 o 2 -5 1 15.25 15.39 8.73 o 3 -5 1 973.61 927.28 52.82 o 4 -5 1 284.05 290.43 34.43 o 5 -5 1 34.60 18.12 24.49 o 6 -5 1 10.76 21.63 17.81 o 7 -5 1 1.10 8.13 18.14 o 8 -5 1 9.56 13.12 21.89 o -10 -4 1 224.51 252.92 65.08 o -9 -4 1 3.08 35.00 31.22 o -8 -4 1 20.99 3.78 24.49 o -7 -4 1 369.07 411.67 41.41 o -6 -4 1 1268.66 1244.53 122.52 o -5 -4 1 305.87 321.10 31.18 o -4 -4 1 2520.52 2559.82 76.27 o -3 -4 1 500.41 580.56 32.16 o -2 -4 1 81.95 113.78 10.86 o -1 -4 1 2549.54 2439.90 67.50 o 0 -4 1 1318.21 1358.79 37.54 o 1 -4 1 2623.75 2575.12 58.66 o 2 -4 1 177.06 143.89 16.60 o 3 -4 1 4.53 14.03 8.80 o 4 -4 1 86.49 82.88 19.56 o 5 -4 1 2785.93 2756.82 144.62 o 6 -4 1 3.60 16.48 15.28 o 7 -4 1 465.15 448.93 49.74 o 8 -4 1 55.05 80.50 26.33 o -10 -3 1 631.44 733.29 105.51 o -9 -3 1 198.87 259.82 59.66 o -8 -3 1 1097.05 1012.18 101.40 o -7 -3 1 224.40 232.95 32.13 o -6 -3 1 362.62 362.82 34.92 o -5 -3 1 18.91 27.35 13.36 o -4 -3 1 217.20 232.40 23.59 o -3 -3 1 40.60 35.08 10.85 o -2 -3 1 2459.33 2456.15 44.73 o -1 -3 1 242.64 225.76 18.61 o 0 -3 1 680.05 545.81 18.03 o 1 -3 1 11782.94 13060.81 205.68 o 2 -3 1 1796.04 1815.33 63.03 o 3 -3 1 1.72 2.33 7.60 o 4 -3 1 100.76 104.03 29.75 o 5 -3 1 952.99 988.02 84.64 o 6 -3 1 1940.18 1740.04 121.94 o 7 -3 1 233.78 181.10 46.34 o 8 -3 1 488.25 513.89 78.72 o 9 -3 1 184.08 124.90 46.02 o -10 -2 1 36.87 19.06 39.61 o -9 -2 1 124.98 126.71 46.51 o -8 -2 1 38.21 25.97 31.55 o -7 -2 1 89.09 98.44 37.14 o -6 -2 1 771.72 829.05 50.20 o -5 -2 1 18531.14 17935.36 487.76 o -4 -2 1 384.74 347.83 27.71 o -3 -2 1 3522.29 3718.14 78.88 o -2 -2 1 81.32 87.29 12.00 o -1 -2 1 1968.79 2084.86 33.00 o 0 -2 1 57.62 101.58 10.98 o 1 -2 1 5207.40 5197.54 66.16 o 2 -2 1 2109.41 2324.77 82.33 o 3 -2 1 166.00 103.21 22.68 o 4 -2 1 1365.81 1354.83 85.79 o 5 -2 1 167.88 197.37 39.61 o 6 -2 1 1241.95 1210.37 99.26 o 7 -2 1 1.28 0.00 18.41 o 8 -2 1 47.57 49.63 29.58 o 9 -2 1 100.54 142.32 46.67 o -10 -1 1 106.15 59.49 45.19 o -9 -1 1 231.14 197.21 56.04 o -8 -1 1 765.24 705.02 90.39 o -7 -1 1 596.58 629.10 77.57 o -6 -1 1 4.85 25.15 20.79 o -5 -1 1 387.68 374.28 35.25 o -4 -1 1 5009.85 5514.73 211.42 o -3 -1 1 4.97 34.95 10.44 o -2 -1 1 7359.52 7480.46 630.90 o -1 -1 1 7383.05 7660.78 227.45 o 0 -1 1 7043.70 7686.39 106.00 o 1 -1 1 1310.62 1507.01 48.15 o 2 -1 1 911.78 780.95 45.52 o 3 -1 1 114.22 79.21 19.23 o 4 -1 1 1.15 9.70 15.28 o 5 -1 1 41.40 44.37 24.65 o 6 -1 1 486.06 346.43 52.42 o 7 -1 1 2949.62 2659.53 157.44 o 8 -1 1 847.77 706.34 88.58 o 9 -1 1 188.80 185.05 51.27 o 10 -1 1 12.43 18.08 33.85 o -10 0 1 29.42 46.02 44.70 o -9 0 1 85.98 66.39 41.25 o -8 0 1 167.54 173.87 53.58 o -7 0 1 1976.06 1868.39 132.95 o -6 0 1 2347.69 1895.51 122.43 o -5 0 1 20.28 58.71 25.06 o -4 0 1 232.19 206.57 27.12 o -3 0 1 56.23 115.02 31.06 o -2 0 1 9.94 20.05 7.32 o -1 0 1 141.46 182.99 12.41 o 0 0 1 7241.97 7078.71 65.19 o 1 0 1 7742.42 8721.24 118.16 o 2 0 1 2668.72 2960.27 84.14 o 3 0 1 662.36 780.70 32.38 o 4 0 1 1575.07 1448.34 94.50 o 5 0 1 1273.40 1389.09 77.65 o 6 0 1 41.38 44.87 25.14 o 7 0 1 67.15 45.52 27.28 o 8 0 1 279.77 231.89 56.04 o 9 0 1 89.17 126.38 46.51 o 10 0 1 19.23 20.87 38.78 o -9 1 1 22.35 39.44 26.95 o -8 1 1 43.29 60.81 30.40 o -7 1 1 383.85 374.37 61.63 o -6 1 1 4.16 35.33 23.34 o -5 1 1 721.20 800.74 52.92 o -4 1 1 587.40 602.36 31.10 o -3 1 1 718.51 630.04 28.51 o -2 1 1 732.23 653.79 47.17 o -1 1 1 1869.03 1556.19 37.35 o 0 1 1 121.81 179.97 8.03 o 1 1 1 522.50 667.67 20.09 o 2 1 1 867.82 865.71 28.06 o 3 1 1 697.63 741.96 30.36 o 4 1 1 1789.23 1753.33 156.21 o 5 1 1 468.08 423.62 28.33 o 6 1 1 2349.43 2336.08 71.55 o 7 1 1 1.59 6.90 21.53 o 8 1 1 29.09 6.24 26.62 o 9 1 1 2.02 11.50 32.70 o 10 1 1 2.58 0.00 39.77 o -9 2 1 555.52 543.80 85.62 o -8 2 1 58.92 49.30 31.88 o -7 2 1 146.00 98.60 36.16 o -6 2 1 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22.84 o 0 -1 14 123.27 225.48 51.60 o 1 -1 14 256.15 396.23 69.52 o 2 -1 14 173.41 198.69 49.30 o 3 -1 14 73.50 86.11 31.06 o -1 0 14 156.80 158.26 43.71 o 0 0 14 2.90 3.62 17.26 o 1 0 14 16.78 62.61 30.90 o 2 0 14 100.63 164.67 41.41 o 3 0 14 210.92 240.92 53.74 o 4 0 14 0.34 17.42 22.19 o -1 1 14 0.42 0.00 35.83 o 0 1 14 84.95 72.97 33.20 o 1 1 14 499.62 521.62 82.17 o 2 1 14 289.93 324.74 62.12 o 3 1 14 32.12 37.96 24.82 o 4 1 14 6.36 26.46 27.94 o -1 2 14 56.05 102.88 46.18 o 0 2 14 0.52 22.68 22.51 o 1 2 14 0.05 46.51 24.49 o 2 2 14 11.52 43.71 26.95 o 3 2 14 326.94 368.29 66.89 o 4 2 14 99.81 117.67 36.32 o 5 2 14 177.25 224.00 53.25 o 0 3 14 1132.51 998.86 121.94 o 1 3 14 169.36 222.85 54.89 o 2 3 14 34.66 52.59 28.27 o 3 3 14 6.95 0.99 17.26 o 4 3 14 0.92 21.86 23.50 o 5 3 14 22.78 28.27 24.98 o 0 4 14 9.20 16.60 34.51 o 1 4 14 128.78 165.82 42.40 o 2 4 14 263.40 218.74 52.92 o 3 4 14 1.68 17.26 18.57 o 4 4 14 69.23 117.01 36.98 o 5 4 14 190.13 177.98 46.18 o 1 5 14 147.04 160.73 60.31 o 2 5 14 49.53 47.17 30.07 o 3 5 14 40.09 72.15 31.22 o 4 5 14 37.00 78.55 29.42 o 5 5 14 367.94 306.99 60.81 o 3 6 14 13.68 59.82 25.14 o