#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/09/2210910.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210910_Fobs loop_ _publ_author_name 'Kopylovich, Maximilian N.' 'Luzyanin, Konstantin V.' 'Haukka, Matti' 'Pombeiro, Armando J. L.' 'Kukushkin, Vadim Yu.' _publ_section_title ; Bis[1,1-bis(propan-2-iminooxy)-1H-isoindol-3-amine-\k^3^N,N',N'']nickel(II) dinitrate ; _journal_coeditor_code BV2035 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2846 _journal_page_last m2848 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.101 _cell_angle_gamma 90.000 _cell_length_a 10.8430 _cell_length_b 9.4644 _cell_length_c 17.1009 _exptl_crystal_F_000 764.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file bv2035Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' max375be in P2(1)/n (SIR2002, purple block)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 371.69 585.36 27.39 o 4 0 0 594.58 515.59 15.23 o 6 0 0 9.50 -3.31 4.49 o 8 0 0 59.96 66.08 14.83 o 10 0 0 151.70 154.39 10.16 o 12 0 0 258.55 303.28 27.48 o 2 1 0 2302.49 2876.79 58.98 o 3 1 0 3722.89 4097.88 88.28 o 4 1 0 1634.66 1767.19 44.95 o 5 1 0 4191.25 4118.18 120.74 o 6 1 0 568.43 581.88 14.20 o 7 1 0 661.59 566.90 19.20 o 8 1 0 376.68 404.32 11.07 o 9 1 0 429.00 389.35 13.32 o 10 1 0 16.15 -0.17 3.87 o 11 1 0 19.19 2.93 4.46 o 12 1 0 5.21 -15.48 12.39 o 0 2 0 343.51 500.71 26.71 o 1 2 0 81.38 70.11 4.51 o 2 2 0 1074.78 1015.60 28.06 o 3 2 0 3862.18 4020.48 85.67 o 4 2 0 413.56 471.43 9.88 o 5 2 0 2117.68 2235.99 70.34 o 6 2 0 2963.01 2940.18 103.58 o 7 2 0 60.29 32.14 2.69 o 8 2 0 654.90 646.27 21.91 o 9 2 0 530.19 549.36 17.91 o 10 2 0 298.91 307.59 27.53 o 11 2 0 9.85 3.41 4.41 o 12 2 0 21.50 13.58 10.20 o 1 3 0 5238.63 6083.11 161.23 o 2 3 0 513.18 712.20 16.65 o 3 3 0 4728.82 5287.38 135.53 o 4 3 0 675.88 678.74 20.55 o 5 3 0 64.51 40.98 2.65 o 6 3 0 449.73 465.24 13.67 o 7 3 0 57.18 79.40 3.56 o 8 3 0 21.54 21.09 2.62 o 9 3 0 17.92 12.61 3.87 o 10 3 0 96.98 93.35 8.33 o 11 3 0 362.55 449.99 21.55 o 0 4 0 1909.82 2150.07 112.60 o 1 4 0 2185.06 2525.90 132.59 o 2 4 0 429.75 468.15 10.75 o 3 4 0 793.60 1019.78 22.75 o 4 4 0 1687.07 1680.99 43.78 o 5 4 0 64.86 73.22 2.84 o 6 4 0 736.56 739.75 21.16 o 7 4 0 697.77 756.21 21.80 o 8 4 0 197.30 198.98 6.72 o 9 4 0 396.90 337.39 12.66 o 10 4 0 150.09 147.83 13.14 o 11 4 0 1.46 -30.77 61.18 o 1 5 0 53.35 -1.63 6.32 o 2 5 0 92.83 33.96 4.77 o 3 5 0 1950.54 1984.53 58.01 o 4 5 0 713.47 805.29 26.64 o 5 5 0 1560.98 1649.04 48.85 o 6 5 0 11.84 8.30 2.27 o 7 5 0 9.51 6.40 3.05 o 8 5 0 339.72 348.91 14.45 o 9 5 0 338.82 327.94 22.34 o 10 5 0 124.47 114.43 24.73 o 11 5 0 294.53 305.82 14.58 o 0 6 0 945.33 908.04 48.53 o 1 6 0 562.27 625.63 23.96 o 2 6 0 2290.58 2394.86 91.84 o 3 6 0 410.74 478.18 23.93 o 4 6 0 203.22 206.78 6.55 o 5 6 0 614.11 599.80 18.15 o 6 6 0 6.99 3.82 2.58 o 7 6 0 913.11 846.91 22.40 o 8 6 0 452.57 456.76 15.65 o 9 6 0 1.52 -6.06 7.45 o 10 6 0 132.12 153.20 8.55 o 1 7 0 1129.31 1190.25 35.86 o 2 7 0 4.32 10.12 38.84 o 3 7 0 848.89 772.78 53.05 o 4 7 0 95.99 91.45 3.63 o 5 7 0 379.68 411.81 14.23 o 6 7 0 458.77 447.79 14.13 o 7 7 0 94.27 98.98 7.80 o 8 7 0 179.51 171.30 7.26 o 9 7 0 114.03 121.07 10.34 o 10 7 0 10.84 10.91 8.25 o 0 8 0 1072.82 1183.01 63.94 o 1 8 0 25.87 28.23 4.54 o 2 8 0 710.59 771.19 28.83 o 3 8 0 29.62 12.84 6.20 o 4 8 0 5.64 1.00 4.55 o 5 8 0 486.98 450.49 18.71 o 6 8 0 826.90 761.11 30.79 o 7 8 0 601.75 642.55 24.51 o 8 8 0 225.97 223.36 14.31 o 1 9 0 326.95 362.45 14.38 o 2 9 0 15.35 -3.77 8.32 o 3 9 0 1186.24 613.89 32.38 o 5 9 0 76.00 61.97 9.88 o 0 10 0 2018.42 1973.55 112.15 o 1 10 0 11.17 0.37 19.95 o 2 10 0 1887.61 1882.37 85.09 o 3 10 0 533.64 541.86 31.62 o 4 10 0 129.80 105.16 11.95 o 5 10 0 32.64 20.97 10.61 o 1 11 0 491.71 468.14 18.64 o -11 0 1 73.54 50.20 7.85 o -9 0 1 580.65 509.32 46.36 o -7 0 1 279.99 265.31 23.69 o -5 0 1 6873.10 6457.51 230.74 o -3 0 1 19139.49 19683.96 1062.71 o 3 0 1 2537.88 2477.49 92.67 o 5 0 1 2102.08 1563.67 85.19 o 7 0 1 54.17 34.68 3.00 o 9 0 1 747.73 671.15 35.35 o -12 1 1 100.63 89.15 7.58 o -11 1 1 85.26 84.18 6.92 o -10 1 1 28.67 37.73 18.75 o -9 1 1 840.64 787.18 38.90 o -8 1 1 2132.10 1907.70 75.93 o -6 1 1 605.34 590.83 13.25 o -5 1 1 1493.59 1861.68 48.98 o -4 1 1 10.88 47.61 1.64 o -3 1 1 232.39 203.36 4.77 o -2 1 1 11257.28 11571.58 565.44 o -1 1 1 0.94 14.61 14.82 o 1 1 1 179.04 174.93 6.38 o 2 1 1 5854.04 5332.34 153.35 o 3 1 1 10457.98 10839.98 272.81 o 4 1 1 3.99 1.92 5.17 o 5 1 1 1436.86 1327.13 38.91 o 6 1 1 68.99 64.84 7.79 o 7 1 1 43.74 30.30 3.44 o 8 1 1 101.45 99.15 3.24 o 9 1 1 103.13 109.68 6.06 o 10 1 1 335.02 330.60 14.84 o 11 1 1 156.75 129.97 8.79 o 12 1 1 199.82 230.61 17.45 o -11 2 1 498.85 513.39 35.13 o -10 2 1 3.03 -11.52 11.28 o -9 2 1 424.60 416.95 15.43 o -8 2 1 41.79 50.12 3.19 o -7 2 1 85.54 76.56 3.03 o -6 2 1 241.99 195.67 5.66 o -5 2 1 798.68 806.85 17.27 o -4 2 1 442.57 596.00 13.05 o -3 2 1 5842.77 6599.20 143.64 o -2 2 1 10348.49 10821.31 222.53 o -1 2 1 651.04 735.45 16.68 o 0 2 1 523.56 504.57 22.19 o 1 2 1 198.35 215.53 9.78 o 2 2 1 415.23 297.81 8.05 o 3 2 1 5704.84 6034.04 187.22 o 5 2 1 251.10 162.09 4.74 o 6 2 1 463.87 484.64 14.35 o 7 2 1 1040.95 1123.11 36.48 o 8 2 1 186.70 210.93 10.18 o 9 2 1 42.32 32.48 8.53 o 10 2 1 19.39 7.68 5.69 o 11 2 1 91.07 89.06 12.28 o 12 2 1 0.08 -0.41 11.65 o -12 3 1 43.34 15.56 6.17 o -11 3 1 40.38 38.59 8.53 o -10 3 1 8.32 -6.08 7.13 o -9 3 1 118.97 107.02 4.46 o -8 3 1 310.98 282.57 10.01 o -7 3 1 38.02 47.37 2.62 o -6 3 1 3766.05 3913.36 128.06 o -5 3 1 252.02 316.66 7.40 o -4 3 1 2929.72 3094.74 66.05 o -3 3 1 4002.30 5077.70 103.70 o -2 3 1 6779.79 7228.03 147.94 o -1 3 1 452.07 367.65 11.67 o 0 3 1 140.05 186.22 7.38 o 1 3 1 565.18 499.12 37.85 o 2 3 1 249.73 190.88 9.17 o 3 3 1 208.96 279.14 7.23 o 4 3 1 390.69 457.89 10.87 o 5 3 1 154.22 162.25 4.96 o 6 3 1 597.78 550.93 15.53 o 7 3 1 4.03 5.41 2.78 o 8 3 1 233.59 220.66 8.83 o 9 3 1 12.83 2.29 3.67 o 10 3 1 444.92 431.30 24.44 o 11 3 1 64.79 50.16 5.83 o 12 3 1 58.22 46.44 8.45 o -12 4 1 3.04 -7.15 9.08 o -11 4 1 232.33 236.25 12.25 o -10 4 1 20.40 3.52 3.53 o -9 4 1 64.40 47.41 3.15 o -8 4 1 38.66 42.33 2.49 o -7 4 1 154.13 159.17 4.38 o -6 4 1 145.04 123.78 3.05 o -5 4 1 1089.67 1104.26 24.79 o -4 4 1 122.96 115.26 5.12 o -3 4 1 994.70 1010.15 22.40 o -2 4 1 124.69 185.95 7.20 o -1 4 1 4070.06 4727.10 107.95 o 0 4 1 1923.95 2205.66 115.48 o 1 4 1 5072.80 5720.06 355.25 o 2 4 1 25.09 68.48 10.79 o 3 4 1 233.82 204.25 5.73 o 4 4 1 650.38 699.32 17.77 o 5 4 1 2262.74 2399.56 80.79 o 6 4 1 284.11 251.60 7.29 o 7 4 1 131.13 145.70 4.69 o 8 4 1 772.92 704.14 24.23 o 9 4 1 26.12 18.17 5.30 o 10 4 1 27.98 5.22 7.51 o 11 4 1 649.04 653.48 38.49 o -10 5 1 234.84 253.04 11.36 o -9 5 1 67.40 49.56 4.26 o -8 5 1 6.38 13.56 3.80 o -7 5 1 46.23 41.39 2.10 o -6 5 1 161.75 167.60 4.00 o -5 5 1 12.97 15.44 1.76 o -4 5 1 481.29 484.17 13.85 o -3 5 1 312.73 370.27 10.53 o -2 5 1 171.65 195.37 8.37 o -1 5 1 62.45 84.82 15.96 o 0 5 1 2269.54 2323.68 86.13 o 1 5 1 895.28 970.78 51.68 o 2 5 1 2839.30 2761.24 106.78 o 3 5 1 19.70 8.79 3.89 o 4 5 1 3337.11 3549.00 112.29 o 5 5 1 546.59 560.58 17.52 o 6 5 1 286.43 274.68 10.20 o 7 5 1 64.40 62.12 5.84 o 8 5 1 579.37 559.05 19.17 o 9 5 1 10.53 10.51 9.45 o 10 5 1 616.21 697.26 61.67 o -10 6 1 213.74 251.24 11.47 o -9 6 1 124.52 126.12 6.82 o -8 6 1 687.28 634.26 23.31 o -7 6 1 10.64 -0.13 5.25 o -6 6 1 1056.30 1009.64 27.30 o -5 6 1 1184.95 1251.27 40.80 o -4 6 1 28.71 47.15 3.60 o -3 6 1 3587.43 3504.18 125.70 o -2 6 1 79.62 53.78 3.01 o -1 6 1 9.84 -5.02 13.43 o 0 6 1 1808.00 2005.35 74.68 o 1 6 1 390.51 406.67 15.25 o 3 6 1 1091.19 1058.42 40.49 o 4 6 1 64.26 49.43 2.45 o 5 6 1 31.42 24.84 2.30 o 6 6 1 343.48 359.98 9.13 o 7 6 1 979.89 1042.90 35.59 o 8 6 1 397.35 368.25 17.83 o 9 6 1 667.13 680.52 27.98 o 10 6 1 19.51 -4.35 7.93 o -10 7 1 61.26 61.66 8.66 o -9 7 1 13.70 -3.70 7.91 o -8 7 1 336.96 312.42 9.59 o -7 7 1 612.47 562.47 21.03 o -6 7 1 750.08 705.21 23.29 o -5 7 1 259.09 253.83 8.77 o -4 7 1 875.37 815.85 28.37 o -3 7 1 580.20 587.51 18.31 o -2 7 1 34.28 34.07 3.30 o -1 7 1 310.58 306.67 13.73 o 0 7 1 3387.22 3856.42 150.90 o 1 7 1 105.42 142.98 10.20 o 3 7 1 181.65 183.02 7.09 o 4 7 1 95.49 97.68 4.02 o 5 7 1 228.21 228.93 6.86 o 6 7 1 31.43 21.34 4.30 o 7 7 1 152.00 157.89 6.14 o 8 7 1 154.86 167.05 6.84 o 9 7 1 0.29 7.54 15.67 o -8 8 1 17.41 5.43 8.66 o -7 8 1 213.24 177.33 8.20 o -6 8 1 114.96 105.05 6.02 o -5 8 1 421.53 433.01 14.00 o -4 8 1 0.73 -1.10 3.53 o -3 8 1 792.99 761.06 42.69 o -2 8 1 12.28 27.48 11.95 o -1 8 1 978.31 1050.80 32.00 o 0 8 1 9.28 -0.86 4.96 o 1 8 1 325.94 340.43 20.20 o 2 8 1 16.48 20.20 6.71 o 3 8 1 454.35 270.86 16.22 o 4 8 1 6.28 0.77 2.44 o 5 8 1 156.06 128.87 5.01 o 6 8 1 167.89 182.82 10.19 o 7 8 1 322.54 346.07 15.07 o 8 8 1 223.46 182.98 11.99 o -7 9 1 2.25 -10.34 9.74 o -6 9 1 939.26 930.36 39.68 o -5 9 1 9.51 -8.60 6.97 o -4 9 1 64.74 53.29 11.93 o -3 9 1 2.12 -4.35 8.65 o -2 9 1 1304.47 1358.65 55.29 o -1 9 1 100.70 98.52 7.53 o 0 9 1 805.16 828.05 32.09 o 1 9 1 980.11 965.60 52.66 o 2 9 1 147.88 118.77 11.44 o 3 9 1 142.34 131.66 12.36 o 5 9 1 7.49 15.55 4.47 o 6 9 1 157.70 132.68 9.08 o -5 10 1 154.17 99.04 12.19 o -4 10 1 45.07 28.33 7.66 o -3 10 1 417.21 433.47 26.02 o -2 10 1 48.99 32.78 25.41 o -1 10 1 1416.78 1431.10 58.48 o 0 10 1 248.14 188.89 49.75 o 2 10 1 39.78 17.86 26.56 o 3 10 1 515.40 492.49 29.19 o 4 10 1 159.30 128.85 13.09 o 5 10 1 266.32 252.97 18.09 o -2 11 1 527.58 534.38 27.50 o -1 11 1 144.64 158.41 15.97 o 2 11 1 256.62 215.62 17.89 o -12 0 2 75.39 78.29 11.24 o -10 0 2 10.05 5.77 5.19 o -8 0 2 5720.27 5973.80 360.03 o -6 0 2 1347.32 1380.82 45.43 o -4 0 2 139.42 170.83 9.85 o 2 0 2 5238.40 4969.27 310.63 o 4 0 2 2960.97 2902.24 119.87 o 6 0 2 8.06 0.09 3.57 o 8 0 2 126.29 142.76 6.02 o 10 0 2 764.94 855.16 55.69 o -11 1 2 96.10 103.00 7.20 o -10 1 2 137.78 123.79 9.89 o -9 1 2 181.26 142.65 8.99 o -8 1 2 59.44 40.22 5.70 o -7 1 2 588.55 653.99 26.02 o -6 1 2 2427.90 2579.17 74.50 o -5 1 2 78.25 56.52 2.78 o -4 1 2 3.68 43.73 1.98 o -2 1 2 30.56 57.28 2.24 o 1 1 2 130.20 165.70 6.73 o 3 1 2 31.07 44.86 3.50 o 4 1 2 22.29 46.65 2.48 o 5 1 2 167.34 253.36 9.43 o 6 1 2 1063.51 1166.09 40.61 o 7 1 2 749.06 736.98 34.40 o 8 1 2 5.80 7.51 3.68 o 9 1 2 836.48 855.68 30.61 o 10 1 2 144.34 109.19 12.31 o 11 1 2 210.68 237.00 24.86 o 12 1 2 0.33 -9.74 27.97 o -12 2 2 3.64 -2.46 8.03 o -11 2 2 50.49 43.68 22.46 o -10 2 2 537.98 464.70 22.35 o -9 2 2 6.59 -5.76 7.79 o -8 2 2 238.81 231.31 5.82 o -7 2 2 855.34 796.70 25.23 o -6 2 2 2744.74 2759.39 70.74 o -5 2 2 2410.76 2354.70 57.12 o -4 2 2 4484.83 4969.69 125.12 o -3 2 2 654.85 633.67 13.08 o -2 2 2 4854.79 5417.38 106.21 o -1 2 2 2051.01 1933.65 56.50 o 0 2 2 2788.68 2891.09 86.31 o 1 2 2 9073.75 8738.41 278.38 o 2 2 2 1631.46 1327.02 49.31 o 3 2 2 0.63 -2.82 2.36 o 4 2 2 765.32 719.89 23.96 o 5 2 2 538.51 456.06 10.74 o 6 2 2 5.70 1.08 2.94 o 7 2 2 7.90 0.59 4.26 o 8 2 2 2148.71 2277.53 105.87 o 9 2 2 4.85 -11.87 9.49 o 10 2 2 82.21 64.79 5.56 o 11 2 2 5.61 2.83 5.80 o 12 2 2 93.49 75.22 9.74 o -12 3 2 53.93 40.79 9.86 o -11 3 2 305.81 301.09 26.77 o -10 3 2 162.99 136.60 8.12 o -9 3 2 173.79 151.05 9.54 o -8 3 2 82.92 76.64 2.99 o -7 3 2 1872.89 1858.41 57.79 o -6 3 2 369.11 373.93 10.88 o -5 3 2 3004.58 3361.43 76.86 o -4 3 2 394.81 461.10 11.07 o -3 3 2 381.02 373.96 7.60 o -2 3 2 606.32 792.90 20.64 o -1 3 2 1944.75 2053.36 56.98 o 0 3 2 406.37 589.03 17.38 o 1 3 2 486.25 530.60 14.38 o 2 3 2 272.29 323.09 8.74 o 3 3 2 2610.53 2647.44 80.85 o 4 3 2 605.74 594.51 18.18 o 5 3 2 1713.29 1743.84 60.54 o 6 3 2 263.21 229.80 6.74 o 7 3 2 1259.83 1266.30 44.39 o 8 3 2 20.99 29.24 3.82 o 9 3 2 152.56 132.03 6.73 o 10 3 2 10.48 1.08 4.27 o 11 3 2 82.75 87.69 8.56 o 12 3 2 1.09 -9.37 7.50 o -12 4 2 81.95 116.74 11.44 o -11 4 2 11.91 -21.38 19.17 o -10 4 2 7.46 2.80 4.91 o -9 4 2 9.69 4.22 3.55 o -8 4 2 17.81 21.82 2.30 o -7 4 2 638.71 599.62 14.22 o -6 4 2 356.89 335.73 7.07 o -5 4 2 22.27 4.46 1.80 o -4 4 2 4845.34 5010.07 118.06 o -3 4 2 6.54 31.51 8.12 o -2 4 2 6501.62 7507.11 179.76 o -1 4 2 1055.49 1252.86 38.67 o 0 4 2 2681.36 2839.03 145.27 o 1 4 2 72.75 81.68 41.36 o 2 4 2 5695.18 5720.28 145.87 o 3 4 2 52.30 89.40 5.43 o 4 4 2 174.09 130.88 3.95 o 5 4 2 206.40 272.62 9.77 o 6 4 2 168.81 152.78 5.22 o 7 4 2 67.62 37.88 3.68 o 8 4 2 324.69 312.46 9.84 o 9 4 2 188.65 179.34 7.32 o 10 4 2 447.80 483.13 23.76 o 11 4 2 8.39 -4.11 6.64 o -11 5 2 39.50 26.02 7.95 o -10 5 2 0.25 -6.65 7.03 o -9 5 2 54.43 43.88 6.12 o -8 5 2 11.30 3.32 3.38 o -7 5 2 6.05 7.31 3.71 o -6 5 2 0.18 0.43 1.63 o -5 5 2 356.70 402.03 9.44 o -4 5 2 1335.68 1391.61 45.76 o -3 5 2 572.08 500.27 11.65 o -2 5 2 288.29 410.95 9.76 o -1 5 2 3205.50 3478.69 84.23 o 0 5 2 2669.07 2858.02 124.80 o 1 5 2 1139.00 1264.67 78.96 o 2 5 2 244.34 305.24 17.49 o 3 5 2 23.52 0.43 1.95 o 4 5 2 7.86 -2.07 2.52 o 5 5 2 3328.71 3467.77 117.52 o 6 5 2 3.89 0.70 4.70 o 7 5 2 1521.45 1551.76 53.89 o 8 5 2 114.99 93.72 6.45 o 9 5 2 915.93 947.35 35.69 o 10 5 2 8.62 -23.00 20.49 o 11 5 2 186.86 185.38 14.02 o -10 6 2 21.19 3.75 5.79 o -9 6 2 33.49 33.55 5.86 o -8 6 2 211.03 198.92 5.34 o -7 6 2 433.61 405.00 9.33 o -6 6 2 239.02 237.70 6.18 o -5 6 2 0.35 2.20 4.40 o -4 6 2 578.20 503.51 15.75 o -3 6 2 348.30 396.13 14.64 o -2 6 2 307.43 441.17 10.58 o -1 6 2 741.63 706.25 18.42 o 0 6 2 1192.94 1294.24 38.77 o 2 6 2 3232.79 3311.06 259.44 o 3 6 2 281.68 344.81 10.02 o 4 6 2 1254.24 1221.89 37.09 o 5 6 2 0.26 0.84 3.32 o 6 6 2 171.25 172.28 4.83 o 7 6 2 8.16 11.61 4.25 o 8 6 2 712.34 649.20 33.03 o 9 6 2 21.60 0.60 4.86 o 10 6 2 352.40 411.75 16.68 o -9 7 2 72.66 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