#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210932.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210932_Fobs loop_ _publ_author_name 'Zhang, Shu-Hua' _publ_section_title ; Poly[[\m~3~-2-[(2-pyridylmethylene)amino]ethanesulfonato-\k^5^N,N':O:O':O'']sodium(I)] ; _journal_coeditor_code CI2187 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3062 _journal_page_last m3064 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.198 _cell_angle_gamma 90.000 _cell_length_a 10.3001 _cell_length_b 10.1413 _cell_length_c 9.6613 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7967 _[local]_cod_data_source_file ci2187Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zsh in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 141.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2341.61 3052.31 18.50 o 2 0 0 2229.95 2575.94 106.13 o 3 0 0 1771.65 2218.99 6.91 o 4 0 0 5482.69 6942.58 202.10 o 5 0 0 1042.09 1569.17 95.74 o 6 0 0 67.39 61.37 5.75 o 7 0 0 31.27 34.30 2.89 o 8 0 0 203.79 218.34 5.05 o 9 0 0 390.46 415.58 7.50 o 10 0 0 147.00 135.87 4.68 o 11 0 0 109.96 109.02 4.44 o 12 0 0 619.40 543.73 10.39 o 1 1 0 605.04 698.48 37.93 o 2 1 0 3025.40 3228.08 215.14 o 3 1 0 2642.22 3149.69 191.87 o 4 1 0 400.14 435.05 31.18 o 5 1 0 88.75 134.76 6.88 o 6 1 0 119.15 148.88 6.47 o 7 1 0 24.83 34.61 1.88 o 8 1 0 41.21 51.30 4.02 o 9 1 0 744.83 744.67 15.12 o 10 1 0 169.96 165.77 7.70 o 11 1 0 42.96 39.11 2.00 o 12 1 0 13.64 12.97 1.41 o 0 2 0 53.86 35.90 6.10 o 1 2 0 5646.06 4711.45 253.60 o 2 2 0 58.79 68.38 5.89 o 3 2 0 382.55 316.58 10.20 o 4 2 0 129.43 112.42 6.45 o 5 2 0 1676.47 1738.25 6.96 o 6 2 0 1419.62 1525.56 27.09 o 7 2 0 243.93 258.09 9.74 o 8 2 0 12.89 10.18 0.74 o 9 2 0 339.80 336.96 29.78 o 10 2 0 45.39 39.83 2.68 o 11 2 0 0.05 1.36 0.76 o 12 2 0 0.05 0.92 0.81 o 1 3 0 831.68 739.45 17.74 o 2 3 0 419.71 436.31 20.99 o 3 3 0 11.43 7.60 0.58 o 4 3 0 21.94 22.72 1.20 o 5 3 0 270.35 299.98 4.95 o 6 3 0 780.26 808.34 16.82 o 7 3 0 1433.85 1466.80 79.88 o 8 3 0 433.15 409.19 18.78 o 9 3 0 38.51 46.77 2.24 o 10 3 0 8.07 12.52 1.88 o 11 3 0 3.27 1.76 0.79 o 12 3 0 59.10 53.26 7.76 o 0 4 0 448.67 446.99 15.86 o 1 4 0 8.38 13.28 1.17 o 2 4 0 33.69 32.88 1.80 o 3 4 0 657.27 587.89 33.70 o 4 4 0 251.63 236.90 19.49 o 5 4 0 2.90 2.09 0.45 o 6 4 0 479.28 486.49 5.94 o 7 4 0 156.48 178.44 8.37 o 8 4 0 68.28 65.11 2.79 o 9 4 0 737.96 750.99 41.51 o 10 4 0 1.01 2.41 0.81 o 11 4 0 84.65 67.29 4.04 o 12 4 0 37.62 37.44 2.14 o 1 5 0 129.71 120.57 1.90 o 2 5 0 0.45 4.53 1.57 o 3 5 0 1119.64 1058.53 42.86 o 4 5 0 862.84 876.77 19.48 o 5 5 0 413.31 429.35 4.61 o 6 5 0 15.60 13.53 2.39 o 7 5 0 163.81 163.92 3.22 o 8 5 0 97.10 97.25 7.13 o 9 5 0 606.23 637.67 63.83 o 10 5 0 41.19 39.38 1.62 o 11 5 0 0.15 0.75 0.61 o 0 6 0 2442.58 2237.79 35.99 o 1 6 0 1.34 0.69 0.17 o 2 6 0 0.32 0.81 0.18 o 3 6 0 591.59 538.46 17.70 o 4 6 0 727.47 651.30 41.06 o 5 6 0 626.14 613.88 8.28 o 6 6 0 475.79 481.40 12.90 o 7 6 0 264.15 259.50 6.67 o 8 6 0 32.24 34.80 1.73 o 9 6 0 5.06 6.11 0.99 o 10 6 0 0.61 0.00 0.59 o 11 6 0 98.77 104.05 8.00 o 1 7 0 151.11 126.43 4.07 o 2 7 0 993.27 944.00 19.71 o 3 7 0 785.88 748.55 36.19 o 4 7 0 28.54 31.05 1.83 o 5 7 0 327.90 306.73 18.57 o 6 7 0 84.03 77.08 7.55 o 7 7 0 98.61 98.77 6.61 o 8 7 0 100.15 93.87 5.46 o 9 7 0 370.40 382.02 43.04 o 10 7 0 170.56 182.34 17.87 o 0 8 0 55.12 55.42 7.32 o 1 8 0 370.06 336.69 19.16 o 2 8 0 150.21 139.48 3.76 o 3 8 0 127.78 134.86 2.88 o 4 8 0 503.09 482.74 10.90 o 5 8 0 199.22 189.01 8.24 o 6 8 0 392.98 389.91 21.35 o 7 8 0 63.28 65.87 3.98 o 8 8 0 2.55 3.30 0.81 o 9 8 0 19.44 18.85 2.09 o 1 9 0 2.48 2.87 1.33 o 2 9 0 26.77 21.35 1.05 o 3 9 0 86.68 85.82 3.32 o 4 9 0 165.94 165.36 6.09 o 5 9 0 444.78 438.65 10.01 o 6 9 0 0.20 1.08 0.68 o 7 9 0 46.78 45.21 4.18 o 8 9 0 99.85 94.15 6.09 o 9 9 0 1.21 1.90 2.10 o 0 10 0 84.45 86.93 4.35 o 1 10 0 194.22 184.90 7.78 o 2 10 0 4.93 4.72 0.64 o 3 10 0 103.30 104.12 10.63 o 4 10 0 0.52 2.43 2.36 o 5 10 0 29.76 30.65 1.76 o 6 10 0 278.49 291.48 18.08 o 7 10 0 20.72 21.43 2.12 o 1 11 0 85.20 92.77 5.13 o 2 11 0 14.36 13.44 1.01 o 3 11 0 85.74 100.36 7.14 o 4 11 0 56.71 67.24 6.24 o 5 11 0 310.31 346.02 25.96 o 6 11 0 6.11 5.93 1.06 o 0 12 0 15.92 14.98 1.86 o 1 12 0 62.77 67.48 2.54 o 2 12 0 54.96 66.26 5.39 o 3 12 0 19.43 22.14 1.64 o 4 12 0 0.25 0.00 0.63 o -12 1 1 0.01 0.38 0.69 o -11 1 1 31.44 37.14 1.92 o -10 1 1 5.72 5.84 0.91 o -9 1 1 132.23 146.13 10.46 o -8 1 1 0.15 1.01 0.40 o -7 1 1 2.13 8.41 2.46 o -6 1 1 228.92 277.13 13.70 o -5 1 1 835.61 955.69 38.55 o -4 1 1 4139.42 5038.95 185.03 o -3 1 1 122.22 143.27 10.88 o -2 1 1 2798.01 3127.73 287.18 o -1 1 1 5547.69 4975.17 90.21 o 0 1 1 15.11 40.07 4.66 o 1 1 1 690.66 643.04 100.72 o 2 1 1 17.85 18.67 3.64 o 3 1 1 3.45 10.74 1.18 o 4 1 1 4731.06 5015.17 303.25 o 5 1 1 123.53 135.80 6.26 o 6 1 1 395.13 524.91 23.91 o 7 1 1 661.08 736.19 11.75 o 8 1 1 543.63 637.28 8.92 o 9 1 1 224.27 211.37 3.88 o 10 1 1 614.72 580.43 21.41 o 11 1 1 211.13 210.99 4.42 o 12 1 1 123.34 108.02 3.39 o -12 2 1 44.02 46.66 5.32 o -11 2 1 48.86 44.55 2.11 o -10 2 1 245.72 228.35 15.32 o -9 2 1 2.02 1.63 0.53 o -8 2 1 374.07 389.10 32.99 o -7 2 1 108.29 135.75 12.43 o -6 2 1 45.44 62.71 3.09 o -5 2 1 529.19 610.29 41.07 o -4 2 1 35.81 28.27 1.93 o -3 2 1 4926.15 4936.89 364.00 o -2 2 1 7139.75 7098.78 454.13 o -1 2 1 1829.46 1877.09 82.32 o 0 2 1 6014.16 5513.06 237.41 o 1 2 1 8740.05 7592.37 705.89 o 2 2 1 19.07 15.18 2.59 o 3 2 1 1280.16 1513.27 176.47 o 4 2 1 43.35 73.35 8.05 o 5 2 1 3.70 6.42 3.80 o 6 2 1 1103.32 1166.48 70.09 o 7 2 1 134.40 147.83 4.45 o 8 2 1 212.04 231.49 4.09 o 9 2 1 314.36 335.73 9.64 o 10 2 1 440.28 437.28 23.73 o 11 2 1 154.70 134.55 7.28 o 12 2 1 9.26 9.59 1.56 o -12 3 1 195.65 182.39 10.02 o -11 3 1 755.47 681.24 45.50 o -10 3 1 1121.68 1196.79 117.46 o -9 3 1 13.35 13.30 0.94 o -8 3 1 832.62 944.74 70.90 o -7 3 1 1731.35 1945.65 133.36 o -6 3 1 598.80 628.20 75.12 o -5 3 1 425.03 444.02 37.99 o -4 3 1 83.59 106.28 9.80 o -3 3 1 225.72 207.36 15.90 o -2 3 1 28.48 48.22 3.63 o -1 3 1 1312.72 1262.99 35.99 o 0 3 1 1127.25 1162.32 38.88 o 1 3 1 11135.41 9473.06 335.32 o 2 3 1 2734.33 2694.73 265.82 o 3 3 1 1253.24 1283.08 118.88 o 4 3 1 60.17 48.32 5.25 o 5 3 1 889.50 855.96 43.64 o 6 3 1 398.24 376.05 21.56 o 7 3 1 128.77 135.28 3.30 o 8 3 1 352.26 355.86 4.54 o 9 3 1 487.20 494.37 14.21 o 10 3 1 3.80 2.40 0.76 o 11 3 1 28.47 28.38 1.78 o 12 3 1 69.77 60.88 2.66 o -12 4 1 109.35 106.14 8.90 o -11 4 1 0.00 1.52 0.67 o -10 4 1 405.09 436.02 41.36 o -9 4 1 172.02 171.96 15.85 o -8 4 1 2264.57 2422.61 320.82 o -7 4 1 567.14 623.01 61.14 o -6 4 1 8.36 11.08 2.71 o -5 4 1 123.44 126.12 13.11 o -4 4 1 1246.57 1240.90 107.49 o -3 4 1 215.00 235.96 18.31 o -2 4 1 0.50 2.03 0.21 o -1 4 1 635.66 488.96 11.69 o 0 4 1 205.00 250.61 7.11 o 1 4 1 1.04 1.02 0.24 o 2 4 1 772.32 740.94 53.84 o 3 4 1 961.33 1025.94 121.51 o 4 4 1 673.20 622.76 55.21 o 5 4 1 330.29 329.45 24.66 o 6 4 1 35.45 41.32 1.65 o 7 4 1 5.93 5.89 0.75 o 8 4 1 78.13 82.57 2.35 o 9 4 1 134.65 127.10 8.18 o 10 4 1 228.39 242.57 10.18 o 11 4 1 571.83 533.88 32.69 o -11 5 1 43.65 47.04 5.04 o -10 5 1 96.47 91.07 9.50 o -9 5 1 441.06 478.73 63.02 o -8 5 1 0.26 0.41 0.59 o -7 5 1 69.77 75.51 5.85 o -6 5 1 1358.23 1416.21 104.27 o -5 5 1 2041.01 2157.41 157.77 o -4 5 1 46.09 57.92 6.33 o -3 5 1 360.96 375.83 26.17 o -2 5 1 1623.87 1473.89 71.65 o -1 5 1 285.60 250.47 8.05 o 0 5 1 45.49 51.93 1.74 o 1 5 1 459.83 436.87 10.88 o 2 5 1 95.21 108.89 3.85 o 3 5 1 442.66 516.14 44.07 o 4 5 1 482.31 463.68 25.00 o 5 5 1 30.80 27.56 1.43 o 6 5 1 1004.31 975.38 21.04 o 7 5 1 1827.87 1796.60 51.25 o 8 5 1 519.61 487.71 7.79 o 9 5 1 111.59 106.87 3.16 o 10 5 1 0.32 1.22 0.61 o 11 5 1 4.59 3.87 1.01 o -11 6 1 10.02 8.48 1.41 o -10 6 1 59.54 59.08 3.91 o -9 6 1 203.48 200.88 35.89 o -8 6 1 1.51 2.14 0.71 o -7 6 1 426.58 433.27 38.57 o -6 6 1 463.25 482.79 31.21 o -5 6 1 19.51 20.97 1.19 o -4 6 1 208.43 228.37 14.26 o -3 6 1 857.51 759.06 55.46 o -2 6 1 5.22 8.12 0.47 o -1 6 1 887.63 905.91 17.12 o 0 6 1 515.53 512.17 11.15 o 1 6 1 34.17 34.09 2.75 o 2 6 1 577.03 571.07 24.08 o 3 6 1 156.98 148.79 6.99 o 4 6 1 217.12 199.62 9.72 o 5 6 1 65.30 55.05 4.18 o 6 6 1 492.48 490.54 17.74 o 7 6 1 11.27 13.02 1.14 o 8 6 1 78.98 76.74 2.47 o 9 6 1 8.61 6.73 1.00 o 10 6 1 405.21 395.14 21.96 o 11 6 1 1.62 2.65 0.75 o -10 7 1 8.20 6.80 1.20 o -9 7 1 4.81 5.28 1.00 o -8 7 1 53.02 49.82 8.49 o -7 7 1 303.59 316.14 27.11 o -6 7 1 62.00 66.22 2.22 o -5 7 1 40.03 46.14 1.77 o -4 7 1 485.46 502.94 42.28 o -3 7 1 210.97 213.43 17.04 o -2 7 1 54.08 50.44 2.18 o -1 7 1 78.69 87.64 5.33 o 0 7 1 87.27 87.63 1.93 o 1 7 1 1.29 3.31 0.31 o 2 7 1 73.29 77.81 3.78 o 3 7 1 42.39 45.32 1.99 o 4 7 1 30.09 30.47 1.30 o 5 7 1 253.53 243.91 11.23 o 6 7 1 22.14 20.10 1.05 o 7 7 1 140.19 137.38 3.26 o 8 7 1 0.05 0.12 0.50 o 9 7 1 70.37 70.72 4.92 o 10 7 1 84.48 74.66 6.32 o -10 8 1 7.27 8.00 2.50 o -9 8 1 0.30 0.66 0.66 o -8 8 1 67.88 72.28 11.44 o -7 8 1 254.78 257.74 19.74 o -6 8 1 308.81 316.25 36.84 o -5 8 1 2.56 2.72 0.70 o -4 8 1 115.05 112.31 8.18 o -3 8 1 227.59 238.44 12.52 o -2 8 1 157.55 162.70 4.18 o -1 8 1 9.29 7.57 0.46 o 0 8 1 8.35 13.14 2.42 o 1 8 1 470.16 486.25 16.87 o 2 8 1 6.81 4.96 0.54 o 3 8 1 58.29 54.62 1.91 o 4 8 1 836.46 762.68 25.93 o 5 8 1 127.85 108.87 6.39 o 6 8 1 540.76 508.15 21.93 o 7 8 1 16.69 15.43 1.01 o 8 8 1 215.09 193.57 16.55 o 9 8 1 0.31 0.60 0.54 o -9 9 1 56.94 51.02 10.58 o -8 9 1 0.71 1.33 0.77 o -7 9 1 69.48 75.05 8.63 o -6 9 1 44.26 45.56 5.14 o -5 9 1 397.30 413.72 36.79 o -4 9 1 2.82 2.85 0.73 o -3 9 1 123.20 127.04 7.29 o -2 9 1 48.59 50.51 2.38 o -1 9 1 23.21 24.96 1.00 o 0 9 1 16.88 15.91 0.69 o 1 9 1 324.89 313.82 3.05 o 2 9 1 381.75 367.20 4.49 o 3 9 1 38.32 38.01 2.46 o 4 9 1 142.83 141.70 3.26 o 5 9 1 173.27 171.01 3.70 o 6 9 1 476.86 465.94 6.27 o 7 9 1 38.35 33.75 1.87 o 8 9 1 45.32 50.57 3.03 o -8 10 1 131.51 137.54 23.44 o -7 10 1 7.72 6.67 1.11 o -6 10 1 50.47 62.32 3.08 o -5 10 1 0.02 0.51 0.63 o -4 10 1 275.91 311.83 35.08 o -3 10 1 95.12 101.53 16.89 o -2 10 1 218.01 228.53 15.01 o -1 10 1 686.58 719.44 53.69 o 0 10 1 181.79 196.60 13.48 o 1 10 1 85.46 81.54 2.01 o 2 10 1 240.77 235.75 4.66 o 3 10 1 611.13 621.82 8.75 o 4 10 1 703.34 684.61 13.92 o 5 10 1 5.19 5.62 0.96 o 6 10 1 4.16 4.76 0.96 o 7 10 1 1.52 4.82 1.22 o -6 11 1 155.43 186.13 23.35 o -5 11 1 117.15 131.14 22.59 o -4 11 1 9.09 10.59 4.11 o -3 11 1 106.72 118.56 20.67 o -2 11 1 0.01 0.00 0.42 o -1 11 1 15.19 15.63 1.38 o 0 11 1 186.39 188.94 6.15 o 1 11 1 138.40 140.99 4.65 o 2 11 1 51.47 52.04 1.76 o 3 11 1 7.92 8.25 1.06 o 4 11 1 11.01 11.80 1.24 o 5 11 1 0.01 0.07 0.56 o 6 11 1 72.13 76.78 2.91 o -4 12 1 66.83 86.93 13.82 o -3 12 1 332.70 397.76 64.58 o -2 12 1 183.99 195.61 20.41 o -1 12 1 19.69 17.26 1.88 o 0 12 1 8.27 9.86 1.11 o 1 12 1 23.78 24.49 1.31 o 2 12 1 0.59 0.44 0.49 o 3 12 1 3.34 2.40 0.79 o -12 0 2 45.74 42.46 3.06 o -11 0 2 65.42 54.95 3.19 o -10 0 2 0.68 2.45 1.03 o -9 0 2 247.15 240.90 5.62 o -8 0 2 75.40 71.17 5.20 o -7 0 2 158.97 163.17 7.41 o -6 0 2 2285.57 2599.95 114.64 o -5 0 2 3348.69 3854.43 109.64 o -4 0 2 1617.24 1954.06 50.63 o -3 0 2 4394.99 5110.46 95.85 o -2 0 2 4193.29 4745.70 23.40 o -1 0 2 1019.41 947.08 25.84 o 0 0 2 1073.45 936.59 35.04 o 1 0 2 9129.49 7676.57 33.17 o 2 0 2 1170.29 861.83 5.31 o 4 0 2 1217.11 1319.81 232.45 o 5 0 2 7.62 5.53 0.47 o 6 0 2 877.53 866.85 96.56 o 7 0 2 1686.46 1740.96 88.16 o 8 0 2 408.87 472.16 7.72 o 9 0 2 69.67 60.11 3.08 o 10 0 2 121.39 114.59 4.48 o 11 0 2 39.69 35.09 2.71 o 12 0 2 13.30 13.36 2.08 o -12 1 2 44.11 37.43 2.28 o -11 1 2 14.07 15.01 1.31 o -10 1 2 71.24 61.14 2.19 o -9 1 2 1518.24 1575.23 114.23 o -8 1 2 12.02 14.81 0.69 o -7 1 2 363.76 366.32 17.55 o -6 1 2 370.28 407.51 15.95 o -5 1 2 685.51 894.63 52.90 o -4 1 2 1422.68 1869.55 89.61 o -3 1 2 0.08 10.02 5.55 o -2 1 2 1061.73 1184.44 79.19 o -1 1 2 3861.14 3651.24 47.47 o 0 1 2 427.86 424.45 16.40 o 1 1 2 10763.60 9018.09 1172.90 o 2 1 2 74.69 58.88 11.12 o 3 1 2 1431.24 1331.42 166.05 o 4 1 2 518.73 467.02 52.33 o 5 1 2 1286.34 1252.93 114.02 o 6 1 2 50.43 58.46 3.41 o 7 1 2 53.19 49.72 2.19 o 8 1 2 200.99 200.70 3.59 o 9 1 2 442.94 459.83 13.71 o 10 1 2 507.48 487.92 6.36 o 11 1 2 37.84 42.34 2.12 o 12 1 2 29.04 27.92 1.88 o -12 2 2 158.83 143.23 11.21 o -11 2 2 30.74 31.78 3.04 o -10 2 2 9.21 11.53 0.92 o -9 2 2 494.90 525.36 42.12 o -8 2 2 229.79 261.68 19.02 o -7 2 2 2.30 1.98 0.58 o -6 2 2 460.81 494.89 35.12 o -5 2 2 97.01 119.82 8.48 o -4 2 2 3107.73 3413.98 284.04 o -3 2 2 728.76 679.35 52.40 o -2 2 2 280.98 280.41 22.22 o -1 2 2 17.32 14.55 1.70 o 0 2 2 20035.85 15949.21 1039.63 o 1 2 2 455.09 413.96 20.54 o 2 2 2 3628.83 3901.19 348.98 o 3 2 2 25.07 35.85 4.16 o 4 2 2 142.97 129.16 12.07 o 5 2 2 400.85 426.45 24.11 o 6 2 2 40.16 50.52 5.70 o 7 2 2 39.96 37.59 3.84 o 8 2 2 429.16 447.32 16.39 o 9 2 2 511.78 501.41 11.25 o 10 2 2 109.15 114.32 4.79 o 11 2 2 2.36 1.27 1.31 o 12 2 2 47.03 39.78 2.23 o -12 3 2 36.81 35.25 2.03 o -11 3 2 0.15 0.48 0.67 o -10 3 2 1.06 1.03 0.88 o -9 3 2 86.79 103.67 9.83 o -8 3 2 178.79 195.84 16.20 o -7 3 2 0.24 1.01 0.39 o -6 3 2 19.11 14.70 4.02 o -5 3 2 24.80 20.97 3.64 o -4 3 2 149.25 169.67 21.49 o -3 3 2 1624.75 1823.78 236.79 o -2 3 2 698.01 824.45 81.49 o -1 3 2 236.72 272.61 21.82 o 0 3 2 1121.67 1182.92 90.05 o 1 3 2 435.91 417.41 20.87 o 2 3 2 451.96 513.85 40.47 o 3 3 2 695.99 734.28 53.17 o 4 3 2 1171.13 1265.25 141.94 o 5 3 2 121.08 108.63 10.51 o 6 3 2 2.62 5.33 2.02 o 7 3 2 4.63 6.17 0.71 o 8 3 2 3.66 3.21 0.67 o 9 3 2 0.00 1.12 0.90 o 10 3 2 80.95 78.01 2.90 o 11 3 2 10.83 9.38 1.26 o -12 4 2 108.30 99.42 3.94 o -11 4 2 31.40 34.69 1.57 o -10 4 2 37.34 38.47 1.70 o -9 4 2 224.01 229.80 22.02 o -8 4 2 85.23 84.56 6.11 o -7 4 2 3.54 3.46 0.68 o -6 4 2 65.60 76.10 9.53 o -5 4 2 322.31 364.62 40.38 o -4 4 2 431.85 439.40 54.84 o -3 4 2 3129.46 3250.99 402.80 o -2 4 2 832.15 850.76 55.43 o -1 4 2 9.29 7.53 0.47 o 0 4 2 3479.07 3522.50 231.66 o 1 4 2 224.70 252.96 8.68 o 2 4 2 463.77 564.25 57.11 o 3 4 2 2137.50 2184.37 163.28 o 4 4 2 181.46 183.08 22.36 o 5 4 2 1562.78 1521.97 143.19 o 6 4 2 1.72 2.54 0.53 o 7 4 2 0.02 0.76 0.46 o 8 4 2 256.94 253.88 6.73 o 9 4 2 110.95 107.33 2.84 o 10 4 2 1.79 3.18 0.87 o 11 4 2 75.06 75.44 5.58 o -11 5 2 1.96 2.83 0.74 o -10 5 2 18.51 24.60 5.12 o -9 5 2 357.60 374.82 30.04 o -8 5 2 16.24 15.46 2.51 o -7 5 2 0.63 9.40 5.79 o -6 5 2 101.79 123.86 17.04 o -5 5 2 369.47 379.04 42.38 o -4 5 2 10.97 9.52 1.75 o -3 5 2 616.99 668.64 75.65 o -2 5 2 2248.64 2228.31 96.59 o -1 5 2 1055.78 1062.11 48.88 o 0 5 2 185.12 219.58 16.51 o 1 5 2 503.53 492.66 14.47 o 2 5 2 658.87 814.61 71.73 o 3 5 2 259.28 230.61 11.71 o 4 5 2 106.08 97.09 7.35 o 5 5 2 443.32 421.70 37.44 o 6 5 2 85.73 80.33 6.11 o 7 5 2 527.21 501.28 38.67 o 8 5 2 83.42 70.02 3.80 o 9 5 2 47.08 46.78 2.00 o 10 5 2 362.61 354.42 12.80 o 11 5 2 82.99 88.45 6.82 o -11 6 2 162.10 162.01 11.52 o -10 6 2 282.04 317.69 29.03 o -9 6 2 792.85 854.43 160.66 o -8 6 2 440.01 482.78 80.76 o -7 6 2 12.73 14.09 2.16 o -6 6 2 766.27 850.26 127.74 o -5 6 2 101.56 103.37 14.41 o -4 6 2 477.67 568.38 92.05 o -3 6 2 491.63 483.93 61.93 o -2 6 2 45.80 49.48 3.35 o -1 6 2 38.47 34.76 2.33 o 0 6 2 201.37 206.70 13.92 o 1 6 2 572.70 555.67 31.39 o 2 6 2 1064.61 1083.32 98.28 o 3 6 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