#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:18:04 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181029 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/09/2210933.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210933_Fobs loop_ _publ_author_name 'Wang, Qing-Wei' 'Yu, Zhi-Xin' 'Meng, Qing-Long' 'Zhao, Xiao-Hong' _publ_section_title ; (4-Carboxynaphthalene-1-carboxylato)bis[4-(1H-1,3,7,8-tetraazacyclopenta[l]phenanthren-2-yl)phenol]zinc(II) 4-carboxynaphthalene-1-carboxylate dihydrate ; _journal_coeditor_code CI2188 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3012 _journal_page_last m3013 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.600 _cell_angle_gamma 90.000 _cell_length_a 17.1407 _cell_length_b 16.7285 _cell_length_c 19.5950 _exptl_crystal_F_000 2384.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file ci2188Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 632.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5717.34 4616.39 95.46 o 6 0 0 3236.83 3348.62 66.49 o 8 0 0 4728.13 5517.19 215.63 o 10 0 0 5187.89 4877.05 273.41 o 12 0 0 2734.18 2469.65 91.69 o 14 0 0 140.54 184.67 49.09 o 16 0 0 158.05 165.80 121.65 o 18 0 0 953.21 943.26 94.12 o 20 0 0 230.26 305.99 82.16 o 4 1 0 31905.96 31004.29 461.48 o 5 1 0 20317.49 19359.49 257.75 o 6 1 0 1538.56 2023.29 47.96 o 7 1 0 1257.10 1938.37 102.50 o 8 1 0 13405.12 14195.27 208.30 o 9 1 0 4600.45 5165.15 352.45 o 10 1 0 540.59 702.20 66.28 o 11 1 0 790.81 931.65 45.57 o 12 1 0 109.57 108.00 30.37 o 13 1 0 25.50 62.79 32.36 o 14 1 0 706.77 755.41 55.91 o 15 1 0 655.23 615.85 78.93 o 16 1 0 2.26 -6.79 31.80 o 17 1 0 3.31 -3.97 38.60 o 18 1 0 0.31 17.56 36.50 o 19 1 0 15.71 56.30 42.98 o 20 1 0 2.13 -45.93 45.93 o 2 2 0 4073.42 4120.08 29.55 o 3 2 0 4876.45 4380.56 41.99 o 4 2 0 400256.16 449187.72 22839.18 o 5 2 0 17765.94 17947.18 242.68 o 6 2 0 16690.45 15998.44 210.92 o 7 2 0 6986.58 7520.89 119.80 o 8 2 0 3668.19 4098.35 335.11 o 9 2 0 12866.40 12605.21 208.03 o 10 2 0 741.74 873.40 35.21 o 11 2 0 904.62 751.18 40.21 o 12 2 0 771.60 804.57 39.17 o 13 2 0 38.32 45.20 23.99 o 14 2 0 1196.26 1420.22 63.74 o 15 2 0 1244.22 1529.22 62.97 o 16 2 0 757.51 766.67 54.56 o 17 2 0 24.20 103.04 38.07 o 18 2 0 185.44 224.55 68.48 o 19 2 0 73.47 47.57 31.76 o 1 3 0 188.37 379.01 11.99 o 2 3 0 34511.99 34753.86 408.09 o 3 3 0 5042.52 5284.43 45.70 o 4 3 0 72740.73 75381.92 1397.97 o 5 3 0 276.02 176.75 12.60 o 6 3 0 4760.18 4171.30 55.12 o 7 3 0 55.26 49.44 11.43 o 8 3 0 5422.84 5950.05 89.28 o 9 3 0 1753.42 2042.82 124.05 o 10 3 0 43.49 87.44 30.25 o 11 3 0 5.19 -4.07 17.88 o 12 3 0 39.61 28.75 36.70 o 13 3 0 652.88 654.79 56.26 o 14 3 0 35.63 41.72 22.82 o 15 3 0 228.64 172.48 48.15 o 16 3 0 13.05 13.49 26.87 o 17 3 0 8.87 -28.46 28.46 o 18 3 0 36.69 50.74 32.02 o 19 3 0 19.46 9.23 29.53 o 1 4 0 15507.15 14107.35 154.31 o 2 4 0 454.04 409.44 9.75 o 3 4 0 5337.80 5294.07 46.92 o 4 4 0 28.47 29.31 7.76 o 5 4 0 6861.63 7434.64 79.43 o 6 4 0 10294.47 10110.43 109.42 o 7 4 0 4561.11 4173.16 59.52 o 8 4 0 50459.23 51831.36 930.65 o 9 4 0 8335.65 8294.27 114.56 o 10 4 0 4258.45 4397.68 74.18 o 11 4 0 5177.10 5063.73 94.40 o 12 4 0 502.67 466.04 26.38 o 13 4 0 3409.31 3486.32 87.81 o 14 4 0 135.82 152.69 29.99 o 15 4 0 1642.64 1586.86 56.75 o 16 4 0 58.43 82.21 27.76 o 17 4 0 107.94 101.69 35.84 o 18 4 0 51.04 95.26 36.26 o 19 4 0 325.17 217.00 49.50 o 1 5 0 2407.98 1954.28 37.57 o 2 5 0 5802.45 4810.14 44.53 o 3 5 0 11152.34 11050.74 100.18 o 4 5 0 0.77 4.18 8.18 o 5 5 0 201.96 198.15 10.25 o 6 5 0 8033.87 8101.15 84.65 o 7 5 0 154.82 319.63 21.87 o 8 5 0 12468.60 12869.73 152.02 o 9 5 0 191.84 239.49 28.15 o 10 5 0 2036.46 1962.28 41.36 o 11 5 0 11.93 32.33 16.87 o 12 5 0 5016.35 5087.77 82.50 o 13 5 0 1106.72 1168.85 41.95 o 14 5 0 134.80 167.85 25.91 o 15 5 0 1.00 17.97 24.60 o 16 5 0 63.20 75.10 36.16 o 17 5 0 33.56 34.53 25.01 o 18 5 0 33.90 -10.81 34.61 o 19 5 0 9.45 45.66 39.38 o 0 6 0 940.45 1045.72 32.24 o 1 6 0 1600.00 1340.10 37.68 o 2 6 0 94.97 105.62 10.53 o 3 6 0 11771.24 11420.40 125.56 o 4 6 0 308.55 280.99 11.94 o 5 6 0 19170.13 18807.04 208.26 o 6 6 0 1654.21 1814.70 23.03 o 7 6 0 3416.09 3311.25 50.94 o 8 6 0 765.19 938.94 30.29 o 9 6 0 4771.84 5181.19 70.83 o 10 6 0 808.41 932.11 40.05 o 11 6 0 6313.96 6229.28 97.69 o 12 6 0 4721.42 4357.99 92.63 o 13 6 0 937.69 1063.70 45.66 o 14 6 0 92.48 96.21 25.47 o 15 6 0 1519.40 1507.96 52.55 o 16 6 0 328.81 302.69 40.94 o 17 6 0 1465.31 1362.52 59.67 o 18 6 0 295.32 180.59 37.17 o 19 6 0 46.75 27.38 48.74 o 1 7 0 217.27 249.26 14.03 o 2 7 0 2744.71 2029.84 31.21 o 3 7 0 123.63 180.06 13.87 o 4 7 0 2359.74 2452.65 28.44 o 5 7 0 16.97 20.69 9.48 o 6 7 0 4.52 -1.83 9.33 o 7 7 0 257.61 255.87 24.51 o 8 7 0 453.72 609.76 33.60 o 9 7 0 851.26 746.71 41.63 o 10 7 0 586.63 475.70 42.33 o 11 7 0 119.13 146.95 27.83 o 12 7 0 3725.66 3805.40 68.00 o 13 7 0 170.40 169.96 21.83 o 14 7 0 765.42 703.91 29.52 o 15 7 0 0.07 -26.18 26.18 o 16 7 0 541.03 438.65 39.42 o 17 7 0 60.42 46.11 34.12 o 18 7 0 195.40 147.12 40.09 o 19 7 0 88.98 148.41 116.78 o 1 8 0 10037.04 9756.40 140.50 o 2 8 0 1399.51 1494.76 51.69 o 3 8 0 2274.45 2333.28 34.24 o 4 8 0 124.43 163.42 11.01 o 5 8 0 8142.53 8576.85 92.19 o 6 8 0 2921.10 2762.31 58.52 o 7 8 0 2386.52 2324.06 33.83 o 8 8 0 1492.35 1414.06 33.83 o 9 8 0 1525.41 1610.29 34.47 o 10 8 0 1421.36 1283.36 35.83 o 11 8 0 2313.04 2277.78 46.98 o 12 8 0 2148.18 2096.21 43.69 o 13 8 0 956.97 972.36 37.95 o 14 8 0 216.06 230.95 32.96 o 15 8 0 420.43 336.91 35.67 o 16 8 0 5.44 7.21 40.29 o 17 8 0 216.39 224.66 41.04 o 18 8 0 300.17 346.92 81.56 o 1 9 0 10.69 27.20 17.12 o 2 9 0 2635.99 2650.54 42.58 o 3 9 0 4108.29 4145.95 72.13 o 4 9 0 9.13 6.18 11.96 o 5 9 0 565.35 452.02 27.93 o 6 9 0 440.68 526.15 57.36 o 7 9 0 1.26 58.61 38.02 o 8 9 0 1537.61 1866.30 37.49 o 9 9 0 203.36 586.52 125.56 o 10 9 0 27.04 36.00 21.33 o 11 9 0 50.92 23.90 21.17 o 12 9 0 104.48 89.96 26.31 o 13 9 0 17.39 21.97 25.79 o 14 9 0 24.10 31.43 23.09 o 15 9 0 338.56 340.01 45.01 o 16 9 0 188.56 121.94 29.89 o 17 9 0 13.72 -11.32 33.41 o 18 9 0 22.90 -43.10 43.10 o 0 10 0 2126.67 2046.43 47.51 o 1 10 0 6.90 167.80 64.71 o 2 10 0 1020.56 858.74 59.61 o 3 10 0 3197.41 2913.74 48.97 o 4 10 0 5194.71 5535.21 77.35 o 5 10 0 944.58 924.20 30.03 o 6 10 0 3462.41 3103.06 48.20 o 7 10 0 5.07 200.97 75.27 o 8 10 0 3933.86 3828.88 53.47 o 9 10 0 159.62 154.25 17.35 o 10 10 0 2873.05 3114.14 60.53 o 11 10 0 226.17 193.89 25.13 o 12 10 0 2453.43 2537.83 65.32 o 13 10 0 401.18 393.05 43.72 o 14 10 0 2032.20 1963.26 65.10 o 15 10 0 136.70 111.49 32.94 o 16 10 0 624.34 656.64 70.95 o 17 10 0 369.24 428.33 54.16 o 1 11 0 468.16 608.80 19.37 o 2 11 0 628.67 678.88 21.20 o 3 11 0 260.45 345.62 19.07 o 4 11 0 184.86 117.31 18.47 o 5 11 0 159.57 236.69 25.02 o 6 11 0 2025.43 2035.83 39.16 o 7 11 0 1.95 -0.32 13.80 o 8 11 0 495.28 598.83 33.36 o 9 11 0 689.09 921.96 36.91 o 10 11 0 223.41 221.71 28.31 o 11 11 0 427.76 497.58 52.68 o 12 11 0 12.49 6.42 21.16 o 13 11 0 640.11 627.17 37.99 o 14 11 0 1.97 49.44 25.25 o 15 11 0 10.55 24.45 27.46 o 16 11 0 4.97 -2.20 31.43 o 17 11 0 38.30 17.05 44.86 o 0 12 0 7118.62 8132.07 304.43 o 1 12 0 605.68 1048.88 185.54 o 2 12 0 4830.84 4847.31 62.58 o 3 12 0 418.21 489.70 25.56 o 4 12 0 1461.80 1456.40 43.56 o 5 12 0 1433.03 1553.04 55.24 o 6 12 0 1712.37 1769.83 34.33 o 7 12 0 350.05 406.39 48.46 o 8 12 0 2830.60 2934.51 100.82 o 9 12 0 19.38 8.75 15.61 o 10 12 0 2177.00 1998.04 119.42 o 11 12 0 395.57 408.67 46.24 o 12 12 0 1770.17 1714.44 58.79 o 13 12 0 69.53 68.36 23.83 o 14 12 0 264.69 244.01 26.71 o 15 12 0 484.92 394.39 38.69 o 16 12 0 28.66 -23.60 34.95 o 1 13 0 43.14 53.44 16.13 o 2 13 0 131.59 146.95 19.25 o 3 13 0 51.25 55.78 15.44 o 4 13 0 110.66 173.45 26.07 o 5 13 0 57.08 28.90 22.70 o 6 13 0 45.02 36.08 34.36 o 7 13 0 1935.39 2071.69 66.02 o 8 13 0 759.46 774.80 51.80 o 9 13 0 0.17 43.59 20.73 o 10 13 0 166.45 170.23 28.07 o 11 13 0 2.79 -5.20 21.73 o 12 13 0 6.87 2.34 26.26 o 13 13 0 145.78 162.57 36.26 o 14 13 0 110.70 47.46 32.35 o 15 13 0 0.02 -2.85 34.44 o 16 13 0 9.11 62.95 67.70 o 0 14 0 1739.01 1621.40 51.28 o 1 14 0 1434.81 1402.48 35.84 o 2 14 0 1747.35 1827.02 39.39 o 3 14 0 3468.31 3126.02 52.31 o 4 14 0 1168.32 1338.17 41.44 o 5 14 0 2539.46 2605.11 66.17 o 6 14 0 2864.58 2830.25 85.89 o 7 14 0 1251.91 1469.00 103.96 o 8 14 0 308.92 248.48 31.25 o 9 14 0 128.47 92.45 19.31 o 10 14 0 14.55 28.35 23.10 o 11 14 0 158.42 120.42 27.13 o 12 14 0 180.71 93.70 30.77 o 13 14 0 163.24 120.07 50.02 o 14 14 0 254.92 274.32 88.20 o 15 14 0 166.51 146.59 146.59 o 1 15 0 20.61 66.19 17.23 o 2 15 0 20.51 -2.12 14.73 o 3 15 0 111.80 162.91 21.12 o 4 15 0 0.38 24.87 17.29 o 5 15 0 0.26 6.11 21.87 o 6 15 0 16.68 14.73 25.06 o 7 15 0 26.16 28.07 23.64 o 8 15 0 42.28 65.57 26.12 o 9 15 0 62.98 48.41 27.49 o 10 15 0 7.39 -16.14 17.55 o 11 15 0 60.76 20.41 34.82 o 12 15 0 1.99 -34.67 60.22 o 13 15 0 44.14 37.71 113.74 o 14 15 0 174.89 125.91 79.07 o 0 16 0 321.06 325.29 52.50 o 1 16 0 4892.01 4644.16 71.06 o 2 16 0 341.06 378.88 25.28 o 3 16 0 3065.00 3175.60 58.26 o 4 16 0 64.50 55.13 15.61 o 5 16 0 753.93 695.92 39.09 o 6 16 0 33.14 27.26 17.38 o 7 16 0 760.99 733.99 82.05 o 8 16 0 162.52 171.28 38.94 o 9 16 0 924.80 882.41 165.63 o 10 16 0 296.31 213.56 37.10 o 11 16 0 243.89 247.56 121.65 o 12 16 0 224.96 257.90 79.68 o 13 16 0 25.38 231.14 140.51 o 1 17 0 14.54 20.75 17.43 o 2 17 0 134.64 174.20 19.03 o 3 17 0 5.01 2.95 17.80 o 4 17 0 770.39 828.31 30.97 o 5 17 0 0.08 -12.15 14.46 o 6 17 0 3.92 21.58 16.13 o 7 17 0 3.54 -0.77 15.82 o 8 17 0 17.12 47.71 36.50 o 9 17 0 4.86 34.49 31.77 o 10 17 0 5.74 19.53 28.28 o 11 17 0 30.63 -4.87 95.50 o 12 17 0 82.09 166.66 130.77 o 0 18 0 1.26 25.02 27.83 o 1 18 0 1166.36 1335.60 62.55 o 2 18 0 86.98 91.22 23.71 o 3 18 0 2139.62 2096.63 49.42 o 4 18 0 133.74 89.44 17.76 o 5 18 0 2230.13 2055.41 211.15 o 6 18 0 9.25 3.34 29.83 o 7 18 0 536.69 545.25 72.08 o 8 18 0 40.31 64.88 84.55 o 9 18 0 480.07 634.59 174.57 o 10 18 0 0.29 78.97 56.08 o 11 18 0 186.67 209.85 76.64 o 1 19 0 20.40 23.31 19.62 o 2 19 0 2.05 -10.11 19.59 o 3 19 0 7.83 36.27 29.92 o 4 19 0 26.62 0.48 33.49 o 5 19 0 7.47 -0.44 27.65 o 6 19 0 17.49 24.92 40.63 o 7 19 0 8.41 92.56 47.43 o 8 19 0 268.35 243.17 44.89 o 9 19 0 52.59 23.64 52.65 o 0 20 0 383.01 237.50 41.49 o 1 20 0 582.52 686.82 167.05 o 2 20 0 56.34 47.52 27.61 o 3 20 0 133.96 119.88 38.93 o 4 20 0 48.46 60.99 40.40 o 5 20 0 136.15 136.68 31.34 o 6 20 0 1.95 67.48 45.85 o 7 20 0 654.69 595.25 55.11 o 2 21 0 5.06 33.57 41.07 o 3 21 0 4.00 -9.32 27.82 o 4 21 0 8.21 34.94 26.10 o 5 21 0 5.11 -8.99 65.39 o -19 0 1 660.62 769.30 76.32 o -17 0 1 325.43 469.57 71.48 o -15 0 1 557.48 623.70 89.31 o -13 0 1 2837.46 2872.65 138.40 o -11 0 1 2434.90 2243.63 101.80 o -9 0 1 8180.06 8285.26 150.32 o -7 0 1 6920.39 7087.45 249.38 o -5 0 1 18824.11 20869.24 403.90 o -3 0 1 59489.09 59401.98 1513.77 o 3 0 1 41352.88 39420.57 869.49 o 5 0 1 6925.80 5891.31 99.78 o 7 0 1 7770.52 7989.81 174.87 o 9 0 1 745.64 931.22 74.51 o 11 0 1 893.65 850.64 100.97 o 13 0 1 1724.62 1938.27 115.57 o 15 0 1 2010.69 2110.35 156.93 o 17 0 1 154.79 123.22 46.86 o 19 0 1 101.68 121.02 90.93 o -20 1 1 3.98 -26.33 37.77 o -19 1 1 117.96 91.92 50.89 o -18 1 1 11.16 -29.01 47.50 o -17 1 1 15.60 23.79 36.61 o -16 1 1 218.80 212.80 46.36 o -15 1 1 373.88 382.80 56.25 o -14 1 1 48.86 9.38 30.44 o -13 1 1 1515.76 1631.67 71.12 o -12 1 1 58.43 44.32 24.48 o -11 1 1 3.32 -22.05 22.05 o -10 1 1 54.02 67.22 22.76 o -9 1 1 568.79 1242.19 310.26 o -8 1 1 342.86 1405.29 348.81 o -7 1 1 10857.47 11067.10 175.06 o -6 1 1 67.31 44.78 15.29 o -5 1 1 40640.09 40226.68 674.96 o -4 1 1 9620.71 11770.08 141.62 o -3 1 1 183.70 118.18 16.91 o 2 1 1 11316.32 10143.67 236.48 o 3 1 1 2989.30 2587.48 42.14 o 4 1 1 17438.44 15929.02 211.04 o 5 1 1 44.92 18.09 12.05 o 6 1 1 2061.97 2074.32 31.48 o 8 1 1 35.74 29.44 15.14 o 9 1 1 797.38 1141.56 118.75 o 10 1 1 72.04 51.06 20.70 o 11 1 1 438.03 390.51 27.38 o 12 1 1 0.41 14.14 27.59 o 13 1 1 355.75 339.45 41.72 o 14 1 1 45.83 80.14 26.80 o 15 1 1 829.37 819.94 71.67 o 16 1 1 13.19 -26.34 29.38 o 17 1 1 49.26 70.52 53.04 o 18 1 1 0.12 -31.94 38.79 o 19 1 1 206.66 234.79 52.32 o -20 2 1 0.92 -12.30 33.86 o -19 2 1 230.38 208.12 43.86 o -18 2 1 131.63 124.15 46.53 o -17 2 1 513.11 601.41 59.57 o -16 2 1 407.63 295.97 48.21 o -15 2 1 587.41 393.14 41.79 o -14 2 1 2.16 -23.07 25.77 o -13 2 1 1608.63 1586.54 64.69 o -12 2 1 2708.55 2790.83 75.95 o -11 2 1 467.31 434.24 25.11 o -10 2 1 1757.49 1650.84 65.41 o -9 2 1 268.68 800.55 350.24 o -8 2 1 12979.22 14153.96 219.44 o -7 2 1 4953.36 4798.22 184.63 o -6 2 1 854.62 716.90 24.95 o -5 2 1 2511.66 2746.53 51.45 o -4 2 1 208050.19 227422.97 7208.66 o -3 2 1 22657.23 22627.28 226.57 o -2 2 1 3222.90 3380.22 23.57 o 1 2 1 22712.33 10177.90 6052.96 o 2 2 1 4746.20 4528.69 52.66 o 3 2 1 4461.57 5483.02 50.30 o 4 2 1 67261.67 72052.89 1480.54 o 5 2 1 19463.49 20215.10 251.57 o 6 2 1 1781.68 2216.72 56.73 o 7 2 1 16894.75 16091.14 215.97 o 8 2 1 124.23 439.74 194.45 o 9 2 1 3788.85 3788.08 65.99 o 10 2 1 142.03 200.53 33.95 o 11 2 1 1754.81 1808.77 58.39 o 12 2 1 24.93 4.61 38.54 o 13 2 1 76.70 85.75 32.77 o 14 2 1 5.89 33.55 45.83 o 15 2 1 640.87 727.45 122.38 o 16 2 1 202.60 173.73 38.37 o 17 2 1 139.10 153.84 49.48 o 18 2 1 150.20 133.97 39.02 o 19 2 1 92.22 69.33 33.73 o -20 3 1 5.50 3.96 30.83 o -19 3 1 4.28 -4.06 33.61 o -18 3 1 0.81 20.52 32.25 o -17 3 1 161.26 167.18 40.08 o -16 3 1 224.12 189.86 38.43 o -15 3 1 221.48 200.78 26.54 o -14 3 1 153.90 55.09 30.99 o -13 3 1 1.14 21.99 28.35 o -12 3 1 534.86 563.53 46.26 o -11 3 1 453.62 390.42 30.22 o -10 3 1 2314.04 2694.76 80.51 o -9 3 1 16872.50 17498.64 265.05 o -8 3 1 2656.99 2910.25 156.47 o -7 3 1 1063.68 914.02 48.97 o -6 3 1 4032.04 3537.48 45.89 o -5 3 1 10842.40 10350.93 114.26 o -4 3 1 7.19 4.52 7.73 o -3 3 1 11542.92 10326.29 93.97 o -2 3 1 14066.36 14285.93 125.31 o 1 3 1 31615.80 29043.12 363.88 o 2 3 1 12765.12 12323.59 103.06 o 3 3 1 28003.34 28812.93 325.14 o 4 3 1 10773.49 12297.22 124.74 o 5 3 1 6759.87 7745.37 85.21 o 6 3 1 40.97 44.63 8.81 o 7 3 1 4496.51 3929.74 308.63 o 8 3 1 8945.71 8766.14 112.10 o 9 3 1 93.24 109.64 28.27 o 10 3 1 5460.73 5426.47 92.98 o 11 3 1 1195.56 1266.78 51.27 o 12 3 1 88.67 144.61 33.34 o 13 3 1 173.16 158.95 30.49 o 14 3 1 6.64 58.38 29.48 o 15 3 1 106.93 126.50 34.67 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