#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210955.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210955_Fobs loop_ _publ_author_name 'Ershov, Mikhail A.' 'Skvortsov, Vikenty G.' 'Pilchikova, Yulia Yu.' 'Koltsova, Olga V.' 'Suponitsky, Kyrill Yu.' _publ_section_title ; Bis(malonamide-\k^2^O,O')bis(nitrato-\kO)copper(II) ; _journal_coeditor_code CV2140 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3073 _journal_page_last m3075 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.661 _cell_angle_beta 69.488 _cell_angle_gamma 73.482 _cell_length_a 6.8515 _cell_length_b 7.0698 _cell_length_c 7.4611 _exptl_crystal_F_000 199.00 _reflns_d_resolution_high 0.7324 _[local]_cod_data_source_file cv2140Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' no2 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 62.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 435.29 433.01 4.18 o 2 0 0 1819.48 1698.96 14.96 o 3 0 0 439.61 439.91 2.50 o 4 0 0 722.66 713.20 8.71 o 5 0 0 300.13 296.46 2.56 o 6 0 0 47.54 39.54 1.94 o 7 0 0 238.89 231.70 3.55 o 8 0 0 57.81 59.86 1.67 o -8 1 0 198.55 212.65 4.78 o -7 1 0 128.07 121.06 2.16 o -6 1 0 701.69 732.37 4.98 o -5 1 0 3.70 4.84 0.40 o -4 1 0 1872.40 1837.28 19.90 o -3 1 0 473.93 472.18 8.04 o -1 1 0 51.65 55.22 0.50 o 0 1 0 639.68 711.82 7.58 o 2 1 0 129.09 141.62 4.67 o 3 1 0 216.93 201.70 1.46 o 4 1 0 944.03 1002.93 11.16 o 5 1 0 460.88 476.53 3.71 o 6 1 0 2.13 2.27 0.41 o 7 1 0 106.74 110.76 2.11 o 8 1 0 158.33 161.44 2.74 o -7 2 0 68.60 71.90 3.56 o -6 2 0 173.90 177.89 2.46 o -5 2 0 65.56 64.63 2.96 o -4 2 0 182.88 189.86 1.93 o -3 2 0 564.03 601.78 4.72 o -2 2 0 62.01 67.07 2.43 o 0 2 0 16.65 13.56 0.29 o 3 2 0 1.76 1.33 0.13 o 4 2 0 600.33 571.82 14.93 o 5 2 0 156.90 135.13 3.84 o 6 2 0 25.04 25.33 1.00 o 7 2 0 1.07 0.62 0.36 o 8 2 0 92.92 92.24 2.82 o -7 3 0 1.66 1.67 0.69 o -6 3 0 9.55 8.72 0.97 o -5 3 0 200.83 199.97 2.14 o -4 3 0 59.94 55.62 1.42 o -3 3 0 335.13 332.12 4.12 o -2 3 0 1177.11 1213.59 17.52 o -1 3 0 95.74 86.09 1.44 o 0 3 0 805.91 784.80 11.16 o 1 3 0 363.01 356.47 8.60 o 2 3 0 224.94 198.12 4.77 o 3 3 0 623.71 590.66 16.43 o 4 3 0 194.04 174.56 3.76 o 5 3 0 1908.67 1834.41 15.23 o 6 3 0 126.54 116.97 2.08 o 7 3 0 188.65 193.35 2.92 o 8 3 0 96.45 101.58 4.83 o -6 4 0 75.81 75.32 2.57 o -5 4 0 88.92 83.72 8.82 o -4 4 0 32.38 28.49 1.33 o -3 4 0 115.04 106.14 7.30 o -2 4 0 37.22 34.57 0.69 o -1 4 0 1765.59 1823.24 15.72 o 0 4 0 325.87 330.00 6.63 o 1 4 0 1469.32 1430.94 23.21 o 2 4 0 818.67 828.69 25.48 o 3 4 0 437.87 425.73 10.23 o 4 4 0 445.64 509.40 24.02 o 5 4 0 351.60 313.82 3.16 o 6 4 0 209.20 191.86 2.94 o 7 4 0 101.88 107.81 7.06 o 8 4 0 121.00 128.44 8.05 o -5 5 0 384.44 388.89 4.51 o -4 5 0 461.45 450.89 4.51 o -3 5 0 111.06 112.83 3.18 o -2 5 0 110.79 101.06 1.87 o -1 5 0 557.75 542.91 9.46 o 0 5 0 247.12 233.01 5.00 o 1 5 0 218.88 215.91 6.02 o 2 5 0 1.56 1.82 0.50 o 3 5 0 48.29 46.59 0.79 o 4 5 0 84.33 86.25 1.99 o 5 5 0 1.26 0.83 0.31 o 6 5 0 121.37 115.96 4.38 o 7 5 0 1.69 1.22 0.43 o 8 5 0 205.66 190.94 12.41 o -4 6 0 73.67 69.71 1.95 o -3 6 0 55.79 53.23 2.08 o -2 6 0 9.17 5.95 0.61 o -1 6 0 43.49 41.75 1.27 o 0 6 0 461.92 431.95 19.96 o 1 6 0 154.92 150.48 2.36 o 2 6 0 282.80 307.76 2.77 o 3 6 0 271.16 258.67 2.01 o 4 6 0 478.32 497.59 2.90 o 5 6 0 110.60 113.75 3.46 o 6 6 0 45.00 47.58 1.51 o 7 6 0 2.66 2.18 0.51 o 8 6 0 50.67 49.22 1.77 o -3 7 0 162.09 155.54 2.93 o -2 7 0 27.58 27.89 1.26 o -1 7 0 16.53 17.49 0.96 o 0 7 0 321.16 355.23 3.89 o 1 7 0 13.42 13.54 0.80 o 2 7 0 156.43 177.80 4.77 o 3 7 0 25.21 25.52 1.01 o 4 7 0 526.17 549.66 5.93 o 5 7 0 414.47 417.57 4.12 o 6 7 0 222.02 218.36 3.31 o 7 7 0 240.67 231.88 4.26 o -2 8 0 173.05 173.85 7.93 o -1 8 0 87.17 79.20 2.06 o 0 8 0 228.03 222.81 5.11 o 1 8 0 369.64 374.39 4.20 o 2 8 0 25.13 23.13 1.96 o 3 8 0 145.26 145.88 2.50 o 4 8 0 127.83 119.47 2.88 o 5 8 0 129.37 132.42 11.39 o 6 8 0 87.81 83.29 4.53 o 0 9 0 215.07 227.14 5.58 o 1 9 0 149.70 143.23 3.42 o 2 9 0 51.39 54.50 1.75 o 3 9 0 9.85 9.81 0.86 o 4 9 0 29.51 26.59 1.55 o 5 9 0 24.22 20.66 1.52 o -5 -9 1 110.30 106.37 5.28 o -4 -9 1 75.30 85.73 2.77 o -3 -9 1 47.13 52.23 2.16 o -2 -9 1 14.73 15.73 1.02 o -1 -9 1 498.36 531.25 6.97 o 0 -9 1 0.99 1.18 0.54 o -6 -8 1 16.54 11.70 1.99 o -5 -8 1 274.41 265.95 7.70 o -4 -8 1 82.52 84.31 2.53 o -3 -8 1 82.37 85.86 5.13 o -2 -8 1 96.50 88.14 2.75 o -1 -8 1 294.62 321.30 10.43 o 0 -8 1 473.93 499.74 9.58 o 1 -8 1 3.99 4.61 0.66 o 2 -8 1 90.39 87.21 5.99 o -7 -7 1 182.43 173.52 3.18 o -6 -7 1 66.97 59.97 2.67 o -5 -7 1 92.91 86.66 2.02 o -4 -7 1 167.32 162.63 1.99 o -3 -7 1 63.31 68.81 2.43 o -2 -7 1 53.27 59.30 3.05 o -1 -7 1 245.71 240.56 16.45 o 0 -7 1 683.03 705.23 9.79 o 1 -7 1 155.99 153.70 2.54 o 2 -7 1 57.15 55.42 1.62 o 3 -7 1 162.58 150.20 6.26 o 4 -7 1 71.20 55.68 2.89 o -7 -6 1 156.73 149.64 2.91 o -6 -6 1 436.98 437.93 23.87 o -5 -6 1 274.52 255.95 11.11 o -4 -6 1 508.61 462.08 4.06 o -3 -6 1 372.05 390.86 5.90 o -2 -6 1 23.30 24.43 0.84 o -1 -6 1 138.14 145.71 1.58 o 0 -6 1 42.24 46.82 2.26 o 1 -6 1 74.96 76.45 1.64 o 2 -6 1 16.99 16.84 0.86 o 3 -6 1 1.07 0.91 0.40 o 4 -6 1 250.54 241.53 7.62 o 5 -6 1 6.60 2.98 1.09 o -8 -5 1 2.83 1.30 0.55 o -7 -5 1 12.97 11.48 0.88 o -6 -5 1 19.30 19.55 1.02 o -5 -5 1 62.13 62.84 4.56 o -4 -5 1 48.02 40.11 1.18 o -3 -5 1 5.68 4.36 0.48 o -2 -5 1 650.18 660.63 2.97 o 0 -5 1 670.79 665.27 6.25 o 1 -5 1 201.86 201.68 5.76 o 2 -5 1 325.92 329.92 6.33 o 3 -5 1 374.16 371.81 3.59 o 4 -5 1 225.77 217.51 2.97 o 5 -5 1 195.04 189.40 5.68 o 6 -5 1 16.74 13.11 1.53 o -8 -4 1 66.95 66.26 2.51 o -7 -4 1 4.74 2.84 0.53 o -6 -4 1 229.83 224.90 3.72 o -5 -4 1 269.89 256.54 5.34 o -4 -4 1 211.99 213.35 2.51 o -3 -4 1 270.90 256.81 18.69 o -2 -4 1 782.48 800.78 15.05 o -1 -4 1 751.98 725.05 6.63 o 0 -4 1 356.94 350.55 2.39 o 1 -4 1 28.16 21.57 0.79 o 2 -4 1 261.15 249.69 4.09 o 3 -4 1 307.33 300.92 5.59 o 4 -4 1 224.95 237.85 4.13 o 5 -4 1 442.56 440.64 4.28 o 6 -4 1 119.44 111.02 3.98 o -8 -3 1 239.91 242.10 5.52 o -7 -3 1 31.57 28.97 1.19 o -6 -3 1 479.44 474.16 8.75 o -5 -3 1 375.79 352.14 3.54 o -4 -3 1 710.23 716.60 6.24 o -3 -3 1 16.34 14.00 0.38 o -2 -3 1 709.15 699.01 3.10 o -1 -3 1 3798.76 3547.43 24.12 o 0 -3 1 1094.37 1131.39 3.46 o 1 -3 1 1031.08 996.70 24.02 o 2 -3 1 185.25 165.00 1.87 o 3 -3 1 531.34 535.48 4.98 o 4 -3 1 130.51 121.90 1.39 o 5 -3 1 14.91 19.07 1.65 o 6 -3 1 1.21 1.27 0.33 o -8 -2 1 117.59 118.72 5.58 o -7 -2 1 20.36 22.31 1.07 o -6 -2 1 57.19 52.24 3.73 o -5 -2 1 610.09 616.20 10.18 o -4 -2 1 679.52 621.29 16.73 o -3 -2 1 49.14 41.82 1.95 o 0 -2 1 218.34 222.81 7.76 o 1 -2 1 920.56 902.86 4.44 o 2 -2 1 301.67 357.21 4.57 o 3 -2 1 917.93 917.79 13.87 o 4 -2 1 111.86 100.65 2.11 o 5 -2 1 39.44 40.10 1.42 o 6 -2 1 37.25 33.89 1.07 o 7 -2 1 8.20 8.85 0.68 o -8 -1 1 127.46 131.29 6.12 o -7 -1 1 91.51 90.62 1.93 o -6 -1 1 3.89 2.29 0.44 o -5 -1 1 648.18 634.07 7.96 o -4 -1 1 1.29 1.21 0.26 o -3 -1 1 340.02 343.29 10.44 o -2 -1 1 1296.67 1421.85 15.55 o -1 -1 1 3.47 4.54 0.15 o 0 -1 1 853.43 858.82 21.22 o 1 -1 1 79.99 96.84 2.01 o 2 -1 1 1418.54 1379.49 21.41 o 3 -1 1 388.11 394.99 2.94 o 4 -1 1 1380.54 1409.31 30.66 o 5 -1 1 599.86 620.43 8.05 o 6 -1 1 50.41 52.46 1.98 o 7 -1 1 146.65 154.38 4.04 o 8 -1 1 101.00 104.91 2.14 o -7 0 1 30.56 33.02 1.25 o -6 0 1 53.86 55.22 1.42 o -5 0 1 71.28 68.21 1.42 o -4 0 1 1417.95 1295.05 47.55 o -3 0 1 702.53 732.35 5.94 o -2 0 1 2313.94 2139.40 26.88 o 0 0 1 1425.58 1322.62 26.02 o 1 0 1 1058.42 1111.42 7.33 o 2 0 1 1.54 1.65 0.13 o 3 0 1 473.14 441.16 11.30 o 4 0 1 512.15 518.53 4.62 o 5 0 1 315.33 327.59 3.90 o 6 0 1 248.13 243.45 12.37 o 7 0 1 64.17 68.94 4.97 o 8 0 1 124.97 130.52 2.38 o -7 1 1 110.34 113.02 5.55 o -6 1 1 79.63 78.97 3.73 o -5 1 1 217.44 211.47 2.49 o -4 1 1 186.51 177.30 3.76 o -3 1 1 204.26 169.92 4.97 o -2 1 1 282.17 282.34 4.16 o -1 1 1 2153.09 2084.61 25.70 o 1 1 1 1637.56 1562.84 17.87 o 2 1 1 884.76 888.09 26.15 o 3 1 1 854.85 894.78 3.04 o 4 1 1 1196.09 1201.18 21.55 o 5 1 1 13.82 17.01 0.47 o 6 1 1 630.23 646.58 8.27 o 7 1 1 2.89 2.70 0.48 o 8 1 1 92.64 94.00 2.04 o -7 2 1 134.54 131.78 3.65 o -6 2 1 34.39 34.35 1.59 o -5 2 1 459.24 464.57 3.73 o -4 2 1 72.27 71.70 2.38 o -3 2 1 66.31 56.35 1.35 o -2 2 1 254.67 206.13 3.76 o -1 2 1 7.79 7.07 0.23 o 1 2 1 1669.10 1474.91 81.08 o 2 2 1 1084.95 1058.62 3.03 o 3 2 1 12.35 23.28 3.85 o 4 2 1 137.23 131.34 4.88 o 5 2 1 37.92 32.44 0.86 o 6 2 1 2.72 2.36 0.61 o 7 2 1 600.17 599.95 16.69 o 8 2 1 97.63 99.74 2.13 o -6 3 1 227.93 238.43 4.78 o -5 3 1 21.60 19.84 1.03 o -4 3 1 870.24 887.58 4.19 o -3 3 1 4.13 2.55 0.27 o -2 3 1 27.17 22.03 0.84 o -1 3 1 185.50 165.09 2.69 o 0 3 1 283.66 261.73 14.35 o 1 3 1 514.56 519.43 13.01 o 2 3 1 1.59 1.80 0.15 o 3 3 1 1916.94 1866.85 40.52 o 4 3 1 1178.01 1248.56 31.50 o 5 3 1 259.41 265.21 8.85 o 6 3 1 4.60 5.42 0.54 o 7 3 1 245.41 223.20 8.02 o 8 3 1 119.84 120.64 4.70 o 9 3 1 69.21 67.71 3.85 o -6 4 1 0.76 -0.25 0.46 o -5 4 1 27.57 24.13 1.16 o -4 4 1 213.89 203.43 6.20 o -3 4 1 300.10 303.86 7.62 o -2 4 1 175.88 179.55 2.40 o -1 4 1 751.08 749.38 13.66 o 0 4 1 1379.30 1362.11 46.09 o 1 4 1 1671.21 1648.93 41.83 o 3 4 1 980.34 969.43 5.14 o 4 4 1 1412.92 1392.18 40.84 o 5 4 1 529.79 514.77 34.21 o 6 4 1 73.61 73.54 1.73 o 7 4 1 76.61 81.96 2.77 o 8 4 1 251.02 244.05 12.19 o -5 5 1 169.69 169.36 4.01 o -4 5 1 86.61 83.82 2.09 o -3 5 1 355.44 346.28 6.22 o -2 5 1 118.94 118.17 2.15 o -1 5 1 57.22 53.68 1.39 o 0 5 1 457.07 450.88 4.43 o 1 5 1 179.81 181.31 12.71 o 2 5 1 23.49 19.99 0.46 o 3 5 1 40.63 41.30 1.39 o 4 5 1 316.49 314.21 9.85 o 5 5 1 894.36 793.55 26.86 o 6 5 1 14.38 13.31 0.84 o 7 5 1 141.43 144.62 5.06 o 8 5 1 154.88 149.89 2.82 o -4 6 1 31.16 31.17 1.42 o -3 6 1 104.59 105.65 2.35 o -2 6 1 84.63 81.48 1.95 o -1 6 1 372.04 354.78 4.17 o 0 6 1 100.18 98.89 2.38 o 1 6 1 588.30 588.95 8.81 o 2 6 1 92.93 94.04 1.96 o 3 6 1 3.36 2.58 0.27 o 4 6 1 14.49 17.11 0.55 o 5 6 1 28.02 28.88 0.89 o 6 6 1 6.97 5.21 0.63 o 7 6 1 1.72 1.12 0.42 o 8 6 1 116.90 104.65 4.88 o -3 7 1 1.99 0.97 0.65 o -2 7 1 28.03 30.92 1.52 o -1 7 1 38.96 41.88 4.17 o 0 7 1 19.57 20.61 1.02 o 1 7 1 167.35 172.68 2.70 o 2 7 1 207.16 207.79 2.83 o 3 7 1 411.84 404.08 3.76 o 4 7 1 260.03 248.45 2.89 o 5 7 1 277.29 292.08 4.42 o 6 7 1 369.01 367.07 4.13 o 7 7 1 18.03 14.29 1.21 o -2 8 1 16.43 16.74 2.09 o -1 8 1 201.96 203.23 5.89 o 0 8 1 153.41 151.68 2.84 o 1 8 1 25.89 28.98 1.28 o 2 8 1 257.30 256.61 3.41 o 3 8 1 193.44 192.42 2.90 o 4 8 1 268.61 280.96 3.43 o 5 8 1 58.80 61.99 2.22 o 6 8 1 143.68 139.34 5.49 o 7 8 1 29.30 24.52 2.77 o 0 9 1 253.14 238.36 6.73 o 1 9 1 2.06 1.52 0.55 o 2 9 1 26.07 24.98 1.24 o 3 9 1 18.58 15.59 1.01 o 4 9 1 169.21 157.20 3.65 o 5 9 1 28.42 28.14 1.70 o -4 -9 2 23.47 17.88 2.00 o -3 -9 2 28.66 28.22 1.61 o -2 -9 2 41.20 42.01 1.55 o -1 -9 2 18.79 19.26 1.12 o 0 -9 2 24.45 19.88 1.23 o -5 -8 2 112.44 101.61 2.35 o -4 -8 2 108.21 109.46 4.82 o -3 -8 2 43.30 42.66 1.78 o -2 -8 2 147.98 151.91 3.76 o -1 -8 2 131.99 127.50 2.31 o 0 -8 2 44.38 51.77 3.84 o 1 -8 2 89.86 97.42 2.66 o 2 -8 2 152.27 158.61 5.46 o -6 -7 2 39.50 38.40 1.54 o -5 -7 2 77.31 68.47 2.15 o -4 -7 2 120.47 121.43 6.07 o -3 -7 2 195.17 204.98 17.35 o -2 -7 2 300.10 302.38 4.09 o -1 -7 2 1137.16 1136.13 6.42 o 0 -7 2 20.45 17.60 0.86 o 1 -7 2 361.37 376.26 3.85 o 2 -7 2 63.48 62.28 1.68 o 3 -7 2 212.78 220.55 6.05 o 4 -7 2 66.27 60.13 3.32 o -7 -6 2 331.97 304.04 4.19 o -6 -6 2 73.21 67.64 1.91 o -5 -6 2 718.81 693.69 6.94 o -4 -6 2 5.59 4.48 0.55 o -3 -6 2 81.58 89.35 1.78 o -2 -6 2 89.55 92.79 1.91 o -1 -6 2 226.66 230.17 3.76 o 0 -6 2 257.64 260.51 7.41 o 1 -6 2 49.06 45.04 1.99 o 2 -6 2 262.32 279.32 6.34 o 3 -6 2 89.74 91.59 1.88 o 4 -6 2 34.39 31.69 2.31 o 5 -6 2 2.39 1.87 1.05 o -7 -5 2 34.72 38.32 1.51 o -6 -5 2 75.90 68.47 1.84 o -5 -5 2 172.95 167.42 2.66 o -4 -5 2 193.92 173.90 2.52 o -3 -5 2 18.49 20.39 0.66 o -2 -5 2 142.50 149.02 4.40 o -1 -5 2 632.11 657.96 4.57 o 0 -5 2 560.36 566.59 8.06 o 1 -5 2 2.83 2.62 0.26 o 2 -5 2 147.10 148.52 3.46 o 3 -5 2 272.46 285.91 2.82 o 4 -5 2 36.54 40.40 1.77 o 5 -5 2 17.48 12.97 1.48 o 6 -5 2 1.02 0.19 0.86 o -7 -4 2 16.13 17.63 1.04 o -6 -4 2 92.71 91.12 2.08 o -5 -4 2 86.16 89.28 1.95 o -4 -4 2 385.73 353.78 3.44 o -3 -4 2 6.39 5.37 0.34 o -2 -4 2 1.49 1.42 0.20 o -1 -4 2 365.70 368.89 15.15 o 0 -4 2 298.87 304.88 5.58 o 1 -4 2 252.19 222.99 1.95 o 2 -4 2 186.71 174.63 1.61 o 3 -4 2 951.58 941.69 22.63 o 4 -4 2 1539.49 1570.61 14.57 o 5 -4 2 47.05 47.20 2.31 o 6 -4 2 207.78 185.14 4.74 o -7 -3 2 77.25 72.72 1.91 o -6 -3 2 72.92 71.87 3.90 o -5 -3 2 242.80 239.57 6.72 o -4 -3 2 467.60 475.20 3.86 o -3 -3 2 569.19 556.05 12.40 o -2 -3 2 1630.50 1695.14 23.87 o -1 -3 2 247.28 242.42 7.88 o 1 -3 2 185.78 177.50 1.46 o 2 -3 2 72.52 61.92 1.00 o 3 -3 2 330.82 337.96 3.26 o 4 -3 2 346.68 360.54 12.23 o 5 -3 2 250.57 251.76 2.78 o 6 -3 2 1.22 0.82 0.27 o 7 -3 2 118.83 114.37 2.80 o -7 -2 2 36.78 33.94 1.96 o -6 -2 2 511.91 490.97 13.12 o -5 -2 2 202.39 195.63 10.02 o -4 -2 2 258.51 248.56 6.51 o -3 -2 2 866.15 913.11 34.39 o -2 -2 2 635.07 644.30 22.26 o -1 -2 2 777.74 817.91 4.14 o 0 -2 2 339.70 316.30 1.83 o 1 -2 2 312.83 304.98 6.64 o 4 -2 2 228.95 226.78 2.90 o 5 -2 2 286.21 265.63 2.29 o 6 -2 2 1.41 1.58 0.30 o 7 -2 2 122.15 118.24 2.93 o 8 -2 2 31.60 31.33 1.70 o -7 -1 2 9.77 9.68 0.78 o -6 -1 2 171.06 172.13 5.81 o -5 -1 2 18.65 18.29 3.52 o -4 -1 2 4.82 4.05 0.41 o -3 -1 2 222.64 272.17 6.61 o -2 -1 2 622.80 649.60 10.31 o -1 -1 2 795.21 776.09 5.23 o 0 -1 2 73.04 62.86 2.60 o 2 -1 2 554.65 560.16 6.29 o 3 -1 2 917.13 895.13 14.48 o 4 -1 2 50.57 39.03 0.69 o 5 -1 2 295.56 304.95 8.73 o 6 -1 2 99.15 101.32 1.33 o 7 -1 2 102.77 106.24 1.94 o 8 -1 2 135.33 128.49 3.33 o -7 0 2 2.03 1.91 0.46 o -6 0 2 197.36 193.20 3.20 o -5 0 2 793.66 816.95 22.62 o -4 0 2 225.63 214.80 3.94 o -3 0 2 41.65 35.84 0.65 o -2 0 2 291.31 272.96 3.75 o -1 0 2 1454.60 1351.07 5.72 o 0 0 2 420.84 437.15 5.34 o 1 0 2 379.22 355.54 10.66 o 2 0 2 134.85 133.07 0.98 o 3 0 2 3603.06 3574.44 27.52 o 4 0 2 101.67 97.05 2.42 o 5 0 2 457.75 450.51 9.33 o 6 0 2 552.79 562.16 3.10 o 7 0 2 127.76 137.38 3.65 o 8 0 2 338.93 345.43 3.79 o -7 1 2 1.10 1.99 0.49 o -6 1 2 0.87 1.26 1.06 o -5 1 2 812.83 852.63 16.88 o -4 1 2 86.21 91.25 1.79 o -3 1 2 769.14 784.59 7.42 o -2 1 2 72.56 74.23 1.75 o 0 1 2 2653.70 2540.80 13.40 o 2 1 2 3876.20 3649.60 46.33 o 3 1 2 1079.61 1080.38 68.62 o 4 1 2 1440.89 1501.56 5.51 o 5 1 2 3.07 1.60 0.25 o 6 1 2 45.30 42.32 1.18 o 7 1 2 122.26 124.76 5.79 o 8 1 2 1.48 1.00 0.43 o 9 1 2 4.87 5.11 0.96 o -6 2 2 4.07 4.55 0.92 o -5 2 2 85.78 84.56 1.68 o -4 2 2 835.56 838.83 4.10 o -3 2 2 1.75 2.67 0.29 o -2 2 2 339.82 312.24 8.95 o -1 2 2 716.84 692.98 4.40 o 0 2 2 1002.11 948.16 8.87 o 2 2 2 563.11 651.71 2.23 o 3 2 2 895.23 901.27 3.02 o 4 2 2 582.36 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297.55 308.62 12.24 o 4 -2 7 342.47 329.74 9.40 o 5 -2 7 52.24 54.85 2.04 o 6 -2 7 252.54 248.79 5.80 o 7 -2 7 37.98 34.96 1.35 o -4 -1 7 24.95 23.83 1.48 o -3 -1 7 131.27 140.99 2.55 o -2 -1 7 241.72 245.98 5.53 o -1 -1 7 30.17 33.00 0.90 o 0 -1 7 358.31 373.33 3.79 o 1 -1 7 197.13 195.93 2.70 o 2 -1 7 549.24 532.82 4.95 o 3 -1 7 154.15 154.31 2.39 o 4 -1 7 255.46 242.74 2.98 o 5 -1 7 235.01 221.70 2.94 o 6 -1 7 46.81 44.31 1.39 o 7 -1 7 60.94 52.71 1.57 o -3 0 7 80.09 83.78 2.00 o -2 0 7 205.52 222.17 9.39 o -1 0 7 2.29 1.68 0.33 o 0 0 7 20.90 20.46 0.71 o 1 0 7 27.97 25.96 1.03 o 2 0 7 24.55 21.58 0.92 o 3 0 7 42.83 43.88 1.29 o 4 0 7 3.08 2.69 0.46 o 5 0 7 824.73 836.76 10.76 o 6 0 7 32.55 29.08 1.10 o 7 0 7 161.99 165.84 4.27 o 8 0 7 11.13 8.02 0.81 o -3 1 7 68.99 72.82 2.81 o -2 1 7 66.17 70.63 2.51 o -1 1 7 383.56 390.46 9.50 o 0 1 7 2.19 1.17 0.29 o 1 1 7 705.24 759.75 31.35 o 2 1 7 129.77 129.16 5.28 o 3 1 7 28.43 29.10 1.78 o 4 1 7 1.35 3.49 2.27 o 5 1 7 53.90 55.85 2.72 o 6 1 7 333.96 344.93 3.71 o 7 1 7 10.48 9.89 0.75 o 8 1 7 56.57 49.69 3.04 o -3 2 7 15.17 19.68 1.71 o -2 2 7 50.45 54.83 2.32 o -1 2 7 30.75 27.61 2.37 o 0 2 7 46.02 42.58 2.10 o 1 2 7 151.64 148.18 4.29 o 2 2 7 624.06 621.36 35.88 o 3 2 7 378.31 368.74 11.03 o 4 2 7 80.10 78.08 4.04 o 5 2 7 320.86 326.77 22.79 o 6 2 7 709.20 727.96 23.14 o 7 2 7 200.44 205.74 3.63 o 8 2 7 71.36 67.54 1.85 o -2 3 7 58.69 68.40 2.70 o -1 3 7 99.46 104.86 3.36 o 0 3 7 82.38 86.00 5.26 o 1 3 7 43.48 41.30 3.50 o 2 3 7 374.21 358.71 25.25 o 3 3 7 297.99 291.89 20.65 o 4 3 7 16.95 13.21 0.73 o 5 3 7 21.06 21.17 0.96 o 6 3 7 92.17 92.54 4.39 o 7 3 7 66.44 70.64 2.53 o 8 3 7 1.62 1.33 0.50 o -1 4 7 110.64 120.49 3.78 o 0 4 7 20.49 20.79 1.08 o 1 4 7 7.50 8.27 0.70 o 2 4 7 20.93 20.87 0.95 o 3 4 7 62.38 67.07 2.83 o 4 4 7 153.78 168.15 4.29 o 5 4 7 1.05 1.19 0.59 o 6 4 7 207.06 214.53 9.85 o 7 4 7 77.12 72.53 1.94 o 8 4 7 13.82 11.80 1.32 o 0 5 7 111.30 106.36 4.09 o 1 5 7 83.23 82.60 2.06 o 2 5 7 41.07 41.34 1.40 o 3 5 7 80.65 75.06 1.74 o 4 5 7 210.77 209.34 2.83 o 5 5 7 68.61 66.01 2.82 o 6 5 7 191.55 173.32 4.10 o 7 5 7 146.38 150.81 4.06 o 1 6 7 49.46 47.74 1.98 o 2 6 7 105.89 104.36 2.35 o 3 6 7 0.94 0.91 0.44 o 4 6 7 67.44 65.32 1.76 o 5 6 7 151.27 143.33 4.16 o 6 6 7 58.92 56.39 2.68 o 7 6 7 293.77 302.09 6.07 o 4 7 7 21.41 21.54 1.15 o -1 -5 8 38.70 30.53 1.97 o 0 -5 8 47.43 47.12 2.51 o 1 -5 8 92.50 93.75 3.84 o 2 -5 8 114.02 119.17 8.67 o 3 -5 8 164.13 168.99 3.03 o -2 -4 8 11.02 9.40 1.10 o -1 -4 8 217.37 220.75 5.29 o 0 -4 8 74.93 74.87 3.93 o 1 -4 8 142.32 142.30 2.67 o 2 -4 8 202.07 205.34 8.49 o 3 -4 8 183.20 180.30 3.01 o 4 -4 8 60.22 54.87 2.15 o 5 -4 8 16.76 14.17 0.98 o -2 -3 8 5.38 6.31 1.02 o -1 -3 8 32.01 31.25 2.12 o 0 -3 8 7.02 7.26 0.75 o 1 -3 8 51.45 47.93 1.92 o 3 -3 8 87.00 79.88 4.21 o 4 -3 8 135.39 129.92 6.49 o 5 -3 8 78.64 72.90 1.93 o 6 -3 8 276.21 279.77 4.55 o -2 -2 8 3.99 4.48 0.91 o -1 -2 8 14.72 14.81 1.43 o 0 -2 8 264.40 276.38 3.53 o 1 -2 8 165.34 164.16 2.72 o 2 -2 8 87.70 89.12 2.03 o 3 -2 8 3.82 5.01 1.03 o 4 -2 8 245.90 244.54 6.30 o 5 -2 8 77.59 74.30 1.86 o 6 -2 8 127.30 130.91 5.59 o -2 -1 8 160.64 165.84 4.03 o -1 -1 8 5.80 5.25 0.67 o 0 -1 8 424.21 450.19 14.08 o 1 -1 8 314.07 306.56 3.61 o 2 -1 8 459.27 461.33 5.60 o 3 -1 8 1.07 1.12 0.41 o 4 -1 8 161.24 143.30 7.33 o 5 -1 8 249.87 230.59 3.18 o 6 -1 8 30.62 25.51 1.15 o 7 -1 8 88.25 79.60 2.03 o -2 0 8 88.39 91.85 2.84 o -1 0 8 0.98 0.20 0.66 o 0 0 8 7.45 5.41 0.64 o 1 0 8 485.59 499.80 4.66 o 2 0 8 151.95 145.99 7.80 o 3 0 8 125.83 126.05 6.32 o 4 0 8 99.75 98.93 4.97 o 5 0 8 179.57 186.50 2.85 o 6 0 8 161.89 168.98 8.76 o 7 0 8 15.25 12.35 0.90 o -2 1 8 159.59 170.06 4.11 o 0 1 8 4.43 4.03 0.62 o 1 1 8 1.13 0.83 0.40 o 2 1 8 129.72 129.32 4.50 o 3 1 8 8.22 5.95 0.65 o 4 1 8 1.15 1.37 0.43 o 5 1 8 139.67 141.32 7.13 o 6 1 8 138.25 148.75 3.61 o 7 1 8 70.94 62.15 3.54 o -1 2 8 70.90 75.15 2.58 o 0 2 8 94.13 93.78 3.09 o 1 2 8 81.15 75.60 2.82 o 2 2 8 291.69 290.06 5.31 o 3 2 8 262.12 270.95 18.21 o 4 2 8 41.62 36.56 2.30 o 5 2 8 531.15 545.70 23.69 o 6 2 8 138.19 136.84 7.00 o 7 2 8 283.44 282.44 10.26 o -1 3 8 198.76 220.06 4.59 o 0 3 8 26.57 26.35 4.05 o 1 3 8 319.47 331.26 6.36 o 2 3 8 30.55 28.69 1.87 o 3 3 8 192.27 181.83 4.39 o 4 3 8 20.11 17.57 1.50 o 5 3 8 65.62 68.31 3.68 o 6 3 8 264.13 274.67 19.72 o 7 3 8 94.01 100.11 8.29 o 0 4 8 46.74 42.19 1.56 o 1 4 8 48.98 47.95 2.96 o 2 4 8 85.11 80.59 3.14 o 3 4 8 59.89 58.80 2.81 o 4 4 8 36.31 27.56 1.88 o 5 4 8 28.26 21.79 1.72 o 6 4 8 51.04 46.85 2.36 o 7 4 8 1.02 0.32 0.64 o 2 5 8 102.90 85.38 3.25 o 3 5 8 20.29 19.45 1.72 o 4 5 8 60.55 56.82 2.81 o 5 5 8 52.52 51.32 2.59 o 6 5 8 66.62 66.72 3.01 o 4 6 8 134.67 125.19 4.21 o 1 -4 9 207.69 210.97 8.30 o 2 -4 9 38.83 39.46 1.54 o 3 -4 9 18.13 15.99 1.05 o 0 -3 9 30.93 31.74 2.14 o 1 -3 9 91.19 91.05 2.24 o 2 -3 9 76.27 75.29 2.03 o 3 -3 9 105.18 103.63 2.74 o 4 -3 9 45.27 39.94 1.55 o -1 -2 9 32.22 27.53 2.00 o 0 -2 9 1.98 3.35 0.93 o 1 -2 9 63.27 63.85 1.92 o 2 -2 9 39.54 39.16 1.45 o 3 -2 9 20.45 19.13 1.26 o 4 -2 9 75.44 73.76 1.98 o 5 -2 9 146.84 137.12 2.61 o -1 -1 9 78.13 74.97 3.10 o 0 -1 9 67.39 71.34 3.00 o 1 -1 9 168.14 174.58 6.89 o 2 -1 9 11.61 12.80 0.90 o 3 -1 9 152.90 138.11 2.59 o 4 -1 9 60.11 55.03 3.49 o 5 -1 9 148.58 130.54 2.49 o 6 -1 9 343.29 338.10 10.12 o -1 0 9 118.12 138.27 4.31 o 0 0 9 268.82 278.44 5.60 o 1 0 9 171.72 164.76 3.78 o 2 0 9 241.70 232.42 5.52 o 3 0 9 31.31 30.28 3.50 o 4 0 9 157.34 147.27 2.63 o 5 0 9 1.92 2.04 0.52 o 6 0 9 66.94 63.86 1.82 o 0 1 9 54.11 49.67 2.34 o 1 1 9 1.73 1.07 0.47 o 2 1 9 43.69 45.20 2.02 o 3 1 9 2.05 1.03 0.46 o 4 1 9 163.56 152.01 6.64 o 5 1 9 67.52 62.60 2.50 o 6 1 9 10.77 9.90 0.85 o 0 2 9 29.91 27.86 1.92 o 1 2 9 258.96 238.79 5.12 o 2 2 9 8.32 6.23 1.07 o 3 2 9 77.58 74.34 2.85 o 4 2 9 83.56 81.97 3.85 o 5 2 9 181.30 197.92 14.92 o 6 2 9 18.25 17.50 1.31 o 1 3 9 92.58 92.66 3.51 o 3 3 9 4.27 3.56 0.98 o 4 3 9 156.37 152.06 4.26 o 6 3 9 235.98 213.78 4.94 o 3 4 9 6.81 5.81 1.16 o 4 4 9 2.51 0.86 0.68 o 5 4 9 157.41 142.85 4.25 o 2 -1 10 38.49 38.80 3.08 o 3 -1 10 179.70 176.67 9.16 o 4 -1 10 147.03 136.70 2.75 o 2 0 10 5.22 4.10 0.66 o 3 0 10 31.17 29.76 1.64 o 4 0 10 136.86 129.82 3.63 o 3 1 10 51.40 47.08 4.48 o 4 1 10 61.43 59.50 2.28 o